Crystallography Open Database

Information card for entry 8107307

Preview

Coordinates	8107307.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H32 N4 O8 Pb2
Calculated formula	C48 H32 N4 O8 Pb2
Title of publication	The crystal structure of tetrakis(6-phenylpyridine-2-carboxylate-κ 2 N,O)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 2 O:O′)-bis(μ2-6-phenylpyridine-2-carboxylate-κ 3N,O:O)tetralead(II) C48H32N4O8Pb2
Authors of publication	Li-Hua, Wang; Hao-Wen, Tai; Qiu-Shi, Li; Yu-Pei, Xia; Xi-Shi, Tai
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2022
Journal volume	237
Journal issue	6
Pages of publication	1113 - 1116
a	9.2712 ± 0.0008 Å
b	14.5959 ± 0.0013 Å
c	16.6178 ± 0.0013 Å
α	76.089 ± 0.007°
β	77.068 ± 0.007°
γ	74.717 ± 0.007°
Cell volume	2074.5 ± 0.3 Å³
Cell temperature	249.99 ± 0.1 K
Ambient diffraction temperature	249.99 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0774
Residual factor for significantly intense reflections	0.0563
Weighted residual factors for significantly intense reflections	0.1536
Weighted residual factors for all reflections included in the refinement	0.1783
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
284399 (current)	2023-06-08	cif/ Adding structures of 8107307 via cif-deposit CGI script.	8107307.cif