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Information card for entry 8107365
Preview
| Coordinates | 8107365.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C76 H65 Cl2 N13 Ni3 O9 |
|---|---|
| Calculated formula | C76 H65 Cl2 N13 Ni3 O9 |
| Title of publication | Crystal structure of bis(μ2-5-chloro-2-oxido-N-(1-oxido-2-oxo-2-phenylethylidene)-benzohydrazonato-κ5 N,O,O′:N′,O′′)-oktakis(pyridine-κ1 N)trinickel(II) – methanol – pyridine (1/1/1) C76H65N13Cl2Ni3O9 |
| Authors of publication | Zhongyuan, Zhou; Liguo, Yang; Kun, Zou; Jiaqi, Fu; Xinyu, Ji |
| Journal of publication | Zeitschrift für Kristallographie - New Crystal Structures |
| Year of publication | 2023 |
| Journal volume | 238 |
| Journal issue | 1 |
| Pages of publication | 105 - 108 |
| a | 15.937 ± 0.004 Å |
| b | 16.805 ± 0.004 Å |
| c | 27.463 ± 0.007 Å |
| α | 90° |
| β | 94.613 ± 0.003° |
| γ | 90° |
| Cell volume | 7331 ± 3 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0787 |
| Residual factor for significantly intense reflections | 0.049 |
| Weighted residual factors for significantly intense reflections | 0.1385 |
| Weighted residual factors for all reflections included in the refinement | 0.1596 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.997 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284470 (current) | 2023-06-15 | cif/ Adding structures of 8107365 via cif-deposit CGI script. |
8107365.cif |
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Users of the data should acknowledge the original authors of the
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