#------------------------------------------------------------------------------
#$Date: 2016-02-20 00:18:51 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176760 $
#$URL: svn://www.crystallography.net/cod/cif/2/01/92/2019203.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2019203
loop_
_publ_author_name
'Wegner, Wojciech'
'Jaroń, Tomasz'
'Grochala, Wojciech'
_publ_section_title
;
 MYb(BH₄)₄ (M = K, Na) from laboratory X-ray powder data
;
_journal_coeditor_code           CU3040
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1289
_journal_page_last               1291
_journal_paper_doi               10.1107/S0108270113027145
_journal_volume                  69
_journal_year                    2013
_chemical_formula_iupac          'K Yb (B H4)4'
_chemical_formula_moiety         'B4 H16 Yb, K'
_chemical_formula_sum            'B4 H16 K Yb'
_chemical_formula_weight         271.5
_chemical_name_systematic
;
Potassium ytterbium tetraborohydride
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.4341(13)
_cell_length_b                   12.445(2)
_cell_length_c                   9.6449(15)
_cell_measurement_temperature    293
_cell_volume                     1012.4(3)
_computing_cell_refinement
'JANA2006 (Petříček et al., 2006)'
_computing_data_collection       'DIFFRACplus (Bruker, 2006)'
_computing_data_reduction        'DIFFRACplus (Bruker, 2006)'
_computing_molecular_graphics    'VESTA (Momma & Izumi, 2011)'
_computing_publication_material  'publCIF (Westrip, 2010)'
_computing_structure_refinement
'JANA2006 (Petříček et al., 2006)'
_computing_structure_solution
'JANA2006 (Petříček et al., 2006)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device_type  'Bruker D8 Discover'
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5418
_exptl_absorpt_coefficient_mu    19.984
_exptl_crystal_density_diffrn    1.7808
_exptl_crystal_F_000             80
_pd_char_colour                  green
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110.009
_pd_meas_2theta_range_min        10.000
_pd_meas_number_of_points        4889
_pd_meas_scan_method             cont
_pd_proc_2theta_range_inc        0.02
_pd_proc_2theta_range_max        110.009
_pd_proc_2theta_range_min        10
_pd_proc_ls_background_function  '30 Legendre polynomials'
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function     pseudo-Voigt
_pd_proc_ls_prof_R_factor        0.0052
_pd_proc_ls_prof_wR_expected     0.0055
_pd_proc_ls_prof_wR_factor       0.0073
_pd_spec_mounting                'quartz capillary'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_pd_spec_size_axial              18
_pd_spec_size_equat              0.3
_refine_diff_density_max         0.18
_refine_diff_density_min         -0.24
_refine_ls_goodness_of_fit_all   1.32
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_constraints    7
_refine_ls_number_parameters     71
_refine_ls_number_restraints     23
_refine_ls_R_factor_all          0.0204
_refine_ls_R_factor_gt           0.0204
_refine_ls_shift/su_max          0.0441
_refine_ls_shift/su_mean         0.0054
_refine_ls_weighting_details     'w = 1/[σ²(I)+0.0016I²]'
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0235
_refine_ls_wR_factor_gt          0.0235
_cod_data_source_file            cu3040.cif
_cod_data_source_block           I
_cod_database_code               2019203
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,z+1/2
3 -x,y,-z+1/2
4 x,-y,-z
5 -x,-y,-z
6 x,y,-z+1/2
7 x,-y,z+1/2
8 -x,y,z
9 x+1/2,y+1/2,z
10 -x+1/2,-y+1/2,z+1/2
11 -x+1/2,y+1/2,-z+1/2
12 x+1/2,-y+1/2,-z
13 -x+1/2,-y+1/2,-z
14 x+1/2,y+1/2,-z+1/2
15 x+1/2,-y+1/2,z+1/2
16 -x+1/2,y+1/2,z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_symmetry_multiplicity
K K1 0 0 0.5 0.085(3) Uiso d 1 4
Yb Yb1 0.5 0.13129(17) 0.75 0.0544(10) Uiso d 1 4
B B1 0.5 0.2416(13) 0.9453(18) 0.117(9) Uiso d 1 8
H H1 0.5 0.299(3) 0.039(4) 0.140(11) Uiso d 1 8
H H2 0.5 0.1541(17) 0.984(5) 0.140(11) Uiso d 1 8
H H3 0.61134(15) 0.257(3) 0.879(2) 0.140(11) Uiso d 1 16
B B2 0.7189(19) 0.0223(13) 0.75 0.117(9) Uiso d 1 8
H H4 0.834(5) -0.028(5) 0.75 0.140(11) Uiso d 1 8
H H5 0.750(9) 0.1122(19) 0.75 0.140(11) Uiso d 1 8
H H6 0.646(3) 0.002(4) 0.84734(13) 0.140(11) Uiso d 1 16
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B 0.0090 0.0039 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
H 0.0000 0.0000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
K 0.3868 1.0657 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
Yb -7.2108 4.4329 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
H1 B1 H2 1_556 . 108.45(3) n
H1 B1 H3 1_556 . 110.11(2) n
H1 B1 H3 1_556 8_655 110.11(2) n
H2 B1 H3 . . 110(2) n
H2 B1 H3 . 8_655 110(2) n
H3 B1 H3 . 8_655 108.18(3) n
H4 B2 H5 . . 110(5) n
H4 B2 H6 . . 109(3) n
H4 B2 H6 . 6_556 109(3) n
H5 B2 H6 . . 110(3) n
H5 B2 H6 . 6_556 110(3) n
H6 B2 H6 . 6_556 110.86(3) n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
B1 H1 1_556 1.15(4) n
B1 H2 . 1.15(3) n
B1 H3 . 1.152(16) n
B1 H3 8_655 1.152(16) n
B2 H4 . 1.16(5) n
B2 H5 . 1.15(3) n
B2 H6 . 1.150(19) n
B2 H6 6_556 1.150(19) n
loop_
_pd_proc_2theta_corrected
_pd_proc_ls_weight
_pd_proc_intensity_net
_pd_calc_intensity_net
9.9864 459.42 211062.00 210305.00
10.0069 458.35 210084.00 209912.00
10.0273 458.39 210126.00 209525.00
10.0478 457.71 209503.00 209138.00
10.0682 456.95 208802.00 208756.00
10.0887 456.07 208003.00 208375.00
10.1092 455.69 207650.00 207995.00
10.1296 455.52 207501.00 207620.00
10.1501 455.26 207264.00 207244.00
10.1705 455.62 207589.00 206872.00
10.1910 454.14 206240.00 206499.00
10.2115 453.45 205616.00 206128.00
10.2319 453.55 205710.00 205760.00
10.2524 453.04 205247.00 205391.00
10.2728 452.98 205191.00 205025.00
10.2933 452.40 204666.00 204658.00
10.3138 452.69 204932.00 204292.00
10.3342 452.14 204426.00 203928.00
10.3547 450.51 202960.00 203563.00
10.3751 450.66 203091.00 203201.00
10.3956 449.48 202033.00 202837.00
10.4161 450.55 202991.00 202474.00
10.4365 449.16 201747.00 202112.00
10.4570 448.45 201107.00 201750.00
10.4774 448.72 201347.00 201389.00
10.4979 448.69 201321.00 201027.00
10.5184 448.00 200702.00 200665.00
10.5388 447.10 199901.00 200305.00
10.5593 445.94 198863.00 199943.00
10.5797 447.33 200104.00 199583.00
10.6002 446.50 199362.00 199222.00
10.6207 444.84 197884.00 198861.00
10.6411 445.72 198669.00 198501.00
10.6616 445.47 198444.00 198140.00
10.6820 444.25 197355.00 197781.00
10.7025 444.53 197609.00 197420.00
10.7230 444.21 197325.00 197059.00
10.7434 443.12 196355.00 196700.00
10.7639 443.06 196302.00 196340.00
10.7843 441.79 195174.00 195981.00
10.8048 442.20 195541.00 195621.00
10.8253 441.63 195037.00 195261.00
10.8457 442.08 195435.00 194903.00
10.8662 441.35 194789.00 194543.00
10.8866 441.47 194897.00 194185.00
10.9071 439.58 193229.00 193826.00
10.9276 439.60 193247.00 193467.00
10.9480 438.85 192590.00 193110.00
10.9685 438.58 192355.00 192751.00
10.9889 438.89 192629.00 192394.00
11.0094 437.21 191150.00 192036.00
11.0299 437.81 191679.00 191679.00
11.0503 437.38 191303.00 191323.00
11.0708 436.53 190559.00 190966.00
11.0913 437.85 191708.00 190610.00
11.1117 435.13 189341.00 190256.00
11.1322 435.61 189757.00 189900.00
11.1526 434.81 189060.00 189547.00
11.1731 434.38 188686.00 189192.00
11.1936 433.92 188283.00 188838.00
11.2140 433.98 188340.00 188486.00
11.2345 433.18 187643.00 188133.00
11.2549 433.40 187835.00 187783.00
11.2754 432.98 187468.00 187489.00
11.2959 433.43 187860.00 187139.00
11.3163 432.57 187119.00 186822.00
11.3368 431.69 186360.00 186475.00
11.3572 431.38 186092.00 186130.00
11.3777 431.73 186388.00 185785.00
11.3982 431.14 185879.00 185440.00
11.4186 431.10 185848.00 185098.00
11.4391 429.97 184871.00 184756.00
11.4595 429.87 184787.00 184416.00
11.4800 428.35 183482.00 184075.00
11.5005 428.69 183773.00 183735.00
11.5209 428.21 183365.00 183398.00
11.5414 428.23 183377.00 183060.00
11.5618 428.32 183460.00 182726.00
11.5823 427.72 182947.00 182390.00
11.6028 426.95 182289.00 182056.00
11.6232 426.32 181748.00 181725.00
11.6437 426.28 181717.00 181393.00
11.6641 425.98 181455.00 181064.00
11.6846 426.27 181705.00 180734.00
11.7051 424.53 180223.00 180407.00
11.7255 424.73 180392.00 180082.00
11.7460 424.04 179809.00 179756.00
11.7664 423.50 179350.00 179434.00
11.7869 423.38 179249.00 179112.00
11.8074 423.68 179507.00 178792.00
11.8278 422.73 178699.00 178474.00
11.8483 422.31 178342.00 178157.00
11.8687 421.45 177616.00 177843.00
11.8892 421.01 177249.00 177530.00
11.9097 421.77 177894.00 177219.00
11.9301 420.75 177032.00 176911.00
11.9506 420.33 176679.00 176604.00
11.9710 421.39 177570.00 176301.00
11.9915 420.08 176465.00 175999.00
12.0120 419.31 175820.00 175699.00
12.0324 418.68 175293.00 175404.00
12.0529 418.61 175230.00 175111.00
12.0733 418.68 175292.00 174823.00
12.0938 418.44 175095.00 174538.00
12.1143 416.91 173811.00 174256.00
12.1347 417.61 174395.00 173981.00
12.1552 416.82 173736.00 173710.00
12.1756 416.70 173642.00 173447.00
12.1961 415.57 172695.00 173189.00
12.2166 416.37 173362.00 172940.00
12.2370 416.07 173116.00 172701.00
12.2575 415.89 172964.00 172473.00
12.2779 415.32 172489.00 172260.00
12.2984 415.56 172690.00 172063.00
12.3189 414.78 172040.00 171888.00
12.3393 414.63 171918.00 171739.00
12.3598 414.25 171600.00 171625.00
12.3802 414.32 171661.00 171554.00
12.4007 413.15 170691.00 171541.00
12.4212 414.69 171968.00 171607.00
12.4416 414.49 171800.00 171783.00
12.4621 416.35 173348.00 172116.00
12.4825 414.48 171798.00 172674.00
12.5030 416.96 173852.00 173557.00
12.5235 418.10 174808.00 174880.00
12.5439 420.58 176885.00 176761.00
12.5644 424.15 179904.00 179315.00
12.5848 428.77 183842.00 182539.00
12.6053 432.18 186778.00 186319.00
12.6258 436.03 190126.00 190201.00
12.6462 440.41 193963.00 193319.00
12.6667 441.17 194634.00 194597.00
12.6871 441.15 194612.00 193347.00
12.7076 436.23 190295.00 189877.00
12.7281 430.98 185743.00 185254.00
12.7485 425.30 180883.00 180595.00
12.7690 420.11 176490.00 176504.00
12.7894 415.80 172886.00 173226.00
12.8099 412.51 170165.00 170688.00
12.8304 410.53 168537.00 168763.00
12.8508 408.13 166573.00 167315.00
12.8713 407.16 165781.00 166195.00
12.8917 405.98 164824.00 165313.00
12.9122 405.01 164029.00 164584.00
12.9327 404.14 163326.00 163959.00
12.9531 403.11 162498.00 163407.00
12.9736 402.57 162061.00 162900.00
12.9940 401.41 161132.00 162431.00
13.0145 401.14 160912.00 161987.00
13.0350 401.55 161245.00 161565.00
13.0554 401.17 160933.00 161163.00
13.0759 399.21 159372.00 160774.00
13.0963 400.45 160359.00 160400.00
13.1168 399.23 159386.00 160036.00
13.1373 399.09 159274.00 159682.00
13.1577 398.77 159015.00 159337.00
13.1782 397.61 158098.00 158999.00
13.1987 397.39 157922.00 158667.00
13.2191 396.88 157514.00 158342.00
13.2396 397.27 157823.00 158020.00
13.2600 396.27 157029.00 157704.00
13.2805 395.49 156416.00 157391.00
13.3010 395.21 156189.00 157081.00
13.3214 396.35 157094.00 156775.00
13.3419 394.67 155767.00 156471.00
13.3623 393.80 155078.00 156170.00
13.3828 394.77 155842.00 155870.00
13.4033 393.44 154792.00 155572.00
13.4237 394.35 155509.00 155277.00
13.4442 393.40 154764.00 154983.00
13.4646 393.39 154756.00 154691.00
13.4851 391.95 153628.00 154399.00
13.5056 392.27 153880.00 154109.00
13.5260 392.05 153707.00 153821.00
13.5465 391.37 153172.00 153533.00
13.5669 391.52 153284.00 153247.00
13.5874 390.73 152669.00 152961.00
13.6079 390.68 152634.00 152676.00
13.6283 389.10 151397.00 152393.00
13.6488 388.93 151266.00 152110.00
13.6692 389.23 151500.00 151829.00
13.6897 389.15 151441.00 151548.00
13.7102 388.42 150874.00 151267.00
13.7306 388.44 150889.00 150989.00
13.7511 387.99 150537.00 150711.00
13.7715 387.37 150057.00 150435.00
13.7920 387.48 150138.00 150158.00
13.8125 386.69 149531.00 149884.00
13.8329 386.31 149238.00 149612.00
13.8534 385.64 148717.00 149340.00
13.8738 386.35 149267.00 149072.00
13.8943 386.60 149457.00 148805.00
13.9148 385.43 148560.00 148541.00
13.9352 384.88 148134.00 148282.00
13.9557 384.47 147819.00 148027.00
13.9761 385.13 148323.00 147780.00
13.9966 384.56 147883.00 147541.00
14.0171 384.74 148029.00 147316.00
14.0375 385.01 148236.00 147110.00
14.0580 384.00 147456.00 146928.00
14.0784 384.52 147857.00 146726.00
14.0989 384.44 147791.00 146596.00
14.1194 383.67 147200.00 146547.00
14.1398 384.21 147621.00 146550.00
14.1603 384.96 148192.00 146593.00
14.1807 384.69 147984.00 146641.00
14.2012 383.54 147101.00 146630.00
14.2217 383.94 147410.00 146711.00
14.2421 383.37 146975.00 146377.00
14.2626 381.73 145718.00 145994.00
14.2830 380.85 145048.00 145408.00
14.3035 379.81 144253.00 144808.00
14.3240 380.12 144493.00 144247.00
14.3444 378.83 143510.00 143748.00
14.3649 378.57 143317.00 143304.00
14.3853 378.30 143113.00 142912.00
14.4058 378.03 142907.00 142556.00
14.4263 376.64 141857.00 142229.00
14.4467 376.06 141420.00 141923.00
14.4672 375.06 140668.00 141631.00
14.4876 375.83 141248.00 141350.00
14.5081 374.98 140612.00 141075.00
14.5286 375.16 140742.00 140806.00
14.5490 375.03 140650.00 140542.00
14.5695 374.02 139895.00 140281.00
14.5899 373.95 139841.00 140024.00
14.6104 374.10 139949.00 139769.00
14.6309 373.21 139289.00 139517.00
14.6513 373.04 139159.00 139269.00
14.6718 372.01 138390.00 139023.00
14.6922 371.61 138098.00 138781.00
14.7127 372.60 138830.00 138541.00
14.7332 371.44 137968.00 138304.00
14.7536 370.81 137497.00 138072.00
14.7741 371.40 137938.00 137841.00
14.7945 370.59 137338.00 137615.00
14.8150 370.78 137478.00 137392.00
14.8355 370.00 136897.00 137173.00
14.8559 369.83 136773.00 136959.00
14.8764 370.00 136900.00 136749.00
14.8968 370.72 137431.00 136545.00
14.9173 368.85 136050.00 136346.00
14.9378 369.88 136811.00 136152.00
14.9582 368.92 136102.00 135967.00
14.9787 369.59 136597.00 135788.00
14.9991 367.84 135308.00 135618.00
15.0196 368.18 135557.00 135456.00
15.0401 368.77 135992.00 135305.00
15.0605 368.50 135793.00 135167.00
15.0810 368.09 135491.00 135040.00
15.1014 368.57 135846.00 134930.00
15.1219 367.86 135324.00 134836.00
15.1424 367.55 135094.00 134762.00
15.1628 368.06 135466.00 134712.00
15.1833 367.72 135218.00 134688.00
15.2037 366.52 134339.00 134696.00
15.2242 366.84 134569.00 134743.00
15.2447 367.62 135143.00 134835.00
15.2651 367.66 135175.00 134983.00
15.2856 368.33 135664.00 135201.00
15.3061 368.55 135833.00 135504.00
15.3265 369.08 136217.00 135913.00
15.3470 370.12 136991.00 136460.00
15.3674 371.36 137908.00 137179.00
15.3879 371.52 138024.00 138134.00
15.4084 374.47 140231.00 139404.00
15.4288 377.21 142289.00 141099.00
15.4493 379.45 143983.00 143415.00
15.4697 383.05 146724.00 146582.00
15.4902 389.23 151498.00 151133.00
15.5107 396.30 157055.00 157136.00
15.5311 405.82 164690.00 165216.00
15.5516 419.09 175638.00 175627.00
15.5720 434.56 188839.00 188433.00
15.5925 450.89 203297.00 203301.00
15.6130 467.49 218549.00 218706.00
15.6334 480.28 230668.00 231685.00
15.6539 486.18 236372.00 238565.00
15.6743 485.31 235523.00 236779.00
15.6948 475.18 225797.00 226868.00
15.7153 458.33 210071.00 211838.00
15.7357 442.01 195369.00 195399.00
15.7562 425.74 181253.00 180126.00
15.7766 409.51 167701.00 167453.00
15.7971 398.52 158814.00 157468.00
15.8176 388.42 150871.00 149924.00
15.8380 382.38 146211.00 144361.00
15.8585 375.89 141291.00 140245.00
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103.7145 90.57 8203.00 8046.07
103.7350 90.80 8244.00 8051.16
103.7555 90.02 8104.00 8057.07
103.7759 90.22 8139.00 8063.74
103.7964 89.39 7990.00 8071.15
103.8168 90.45 8181.00 8079.26
103.8373 90.48 8187.00 8087.97
103.8578 89.27 7970.00 8096.93
103.8782 90.28 8150.00 8105.86
103.8987 89.13 7945.00 8114.54
103.9192 89.50 8011.00 8122.60
103.9396 89.59 8026.00 8129.71
103.9601 89.06 7932.00 8135.67
103.9805 90.32 8158.00 8140.26
104.0010 90.68 8223.00 8143.44
104.0215 90.63 8213.00 8145.06
104.0419 89.84 8071.00 8145.49
104.0624 89.83 8070.00 8144.76
104.0828 90.69 8225.00 8143.05
104.1033 90.59 8207.00 8140.54
104.1238 89.86 8075.00 8137.46
104.1442 90.01 8101.00 8134.03
104.1647 90.00 8100.00 8130.37
104.1851 90.22 8139.00 8126.77
104.2056 90.17 8130.00 8123.30
104.2261 89.47 8005.00 8120.09
104.2465 89.69 8045.00 8117.21
104.2670 89.90 8082.00 8114.63
104.2874 89.83 8069.00 8112.36
104.3079 90.47 8185.00 8110.32
104.3284 89.78 8061.00 8108.62
104.3488 89.89 8081.00 8106.90
104.3693 89.40 7992.00 8105.27
104.3897 90.48 8186.00 8103.73
104.4102 89.66 8039.00 8102.27
104.4307 90.10 8118.00 8100.92
104.4511 89.44 7999.00 8099.65
104.4716 89.84 8072.00 8098.43
104.4920 90.36 8165.00 8097.22
104.5125 89.83 8069.00 8095.93
104.5330 90.10 8118.00 8094.60
104.5534 89.17 7951.00 8092.88
104.5739 89.96 8092.00 8090.53
104.5943 89.33 7979.00 8088.14
104.6148 90.06 8110.00 8085.50
104.6353 90.42 8176.00 8082.60
104.6557 89.83 8069.00 8079.57
104.6762 89.43 7997.00 8076.50
104.6966 90.58 8204.00 8073.82
104.7171 89.91 8084.00 8071.07
104.7376 89.81 8065.00 8068.64
104.7580 89.36 7986.00 8066.53
104.7785 90.24 8144.00 8064.74
104.7989 89.81 8065.00 8063.22
104.8194 89.82 8068.00 8061.86
104.8399 89.34 7981.00 8060.57
104.8603 89.26 7968.00 8059.24
104.8808 88.79 7883.00 8057.79
104.9012 90.01 8102.00 8056.21
104.9217 89.58 8025.00 8047.80
104.9422 89.30 7974.00 8045.86
104.9626 89.16 7949.00 8043.75
104.9831 90.43 8178.00 8041.58
105.0035 91.05 8290.00 8039.42
105.0240 90.06 8111.00 8037.35
105.0445 90.51 8192.00 8035.36
105.0649 89.50 8011.00 8033.80
105.0854 89.53 8016.00 8032.38
105.1058 90.03 8105.00 8031.07
105.1263 89.20 7957.00 8030.05
105.1468 89.63 8034.00 8029.10
105.1672 89.69 8044.00 8028.04
105.1877 90.14 8125.00 8026.79
105.2081 89.67 8041.00 8025.15
105.2286 90.42 8175.00 8023.15
105.2491 89.10 7939.00 8020.69
105.2695 89.14 7946.00 8017.82
105.2900 88.42 7818.00 8011.41
105.3104 89.68 8042.00 8008.11
105.3309 90.32 8157.00 8004.61
105.3514 89.88 8079.00 8001.22
105.3718 89.33 7980.00 7997.73
105.3923 88.52 7835.00 7994.78
105.4127 90.08 8114.00 7992.20
105.4332 89.53 8016.00 7990.21
105.4537 88.94 7911.00 7988.60
105.4741 89.60 8028.00 7987.43
105.4946 89.92 8085.00 7986.80
105.5150 90.15 8127.00 7986.71
105.5355 90.12 8121.00 7986.90
105.5560 89.33 7979.00 7987.45
105.5764 90.00 8100.00 7988.23
105.5969 89.29 7972.00 7989.27
105.6173 89.10 7938.00 7990.47
105.6378 88.45 7823.00 7991.80
105.6583 88.70 7868.00 7993.22
105.6787 89.91 8084.00 7994.69
105.6992 89.84 8072.00 7996.23
105.7196 89.68 8042.00 7997.74
105.7401 89.65 8037.00 7999.03
105.7606 90.14 8126.00 8000.37
105.7810 89.38 7988.00 8001.61
105.8015 90.27 8149.00 8002.76
105.8219 88.92 7907.00 8003.90
105.8424 89.66 8039.00 8004.97
105.8629 89.88 8078.00 8006.09
105.8833 89.39 7991.00 8007.44
105.9038 88.77 7880.00 8008.85
105.9242 90.30 8154.00 8010.42
105.9447 88.98 7918.00 8012.23
105.9652 89.15 7947.00 8014.32
105.9856 89.59 8026.00 8016.59
106.0061 88.82 7889.00 8019.18
106.0266 89.54 8017.00 8021.96
106.0470 90.22 8140.00 8025.23
106.0675 90.13 8123.00 8028.82
106.0879 90.18 8132.00 8032.69
106.1084 90.18 8133.00 8036.88
106.1289 89.69 8044.00 8041.51
106.1493 90.22 8140.00 8046.39
106.1698 89.78 8061.00 8051.42
106.1902 90.93 8269.00 8056.49
106.2107 90.07 8113.00 8061.93
106.2312 90.36 8165.00 8067.53
106.2516 90.51 8192.00 8073.18
106.2721 89.55 8019.00 8078.95
106.2925 89.78 8061.00 8084.50
106.3130 90.82 8248.00 8089.84
106.3335 89.59 8026.00 8094.85
106.3539 89.78 8060.00 8099.42
106.3744 89.53 8015.00 8103.57
106.3948 90.04 8108.00 8107.20
106.4153 89.97 8095.00 8110.59
106.4358 90.21 8138.00 8113.51
106.4562 90.60 8209.00 8116.04
106.4767 90.59 8207.00 8117.87
106.4971 90.91 8265.00 8119.86
106.5176 90.34 8162.00 8121.58
106.5381 89.82 8067.00 8123.01
106.5585 90.67 8221.00 8124.15
106.5790 90.61 8210.00 8125.23
106.5994 90.76 8237.00 8126.20
106.6199 89.73 8051.00 8127.13
106.6404 89.97 8095.00 8128.05
106.6608 90.77 8240.00 8129.00
106.6813 90.50 8190.00 8129.83
106.7017 90.86 8255.00 8130.90
106.7222 90.59 8206.00 8132.05
106.7427 90.07 8112.00 8133.30
106.7631 89.03 7926.00 8134.65
106.7836 89.79 8062.00 8136.13
106.8040 90.24 8143.00 8137.83
106.8245 89.50 8010.00 8139.67
106.8450 89.87 8077.00 8141.51
106.8654 90.13 8124.00 8143.73
106.8859 89.46 8003.00 8146.15
106.9063 90.31 8155.00 8148.73
106.9268 90.37 8166.00 8151.52
106.9473 89.87 8077.00 8154.42
106.9677 90.29 8152.00 8157.16
106.9882 90.58 8205.00 8160.30
107.0086 90.61 8211.00 8163.63
107.0291 90.66 8220.00 8166.95
107.0496 90.59 8206.00 8170.33
107.0700 90.49 8189.00 8173.59
107.0905 89.98 8096.00 8176.91
107.1109 90.06 8111.00 8180.27
107.1314 89.54 8017.00 8183.37
107.1519 89.29 7973.00 8186.12
107.1723 90.28 8150.00 8188.61
107.1928 90.55 8199.00 8190.98
107.2132 90.92 8267.00 8193.00
107.2337 90.45 8182.00 8195.02
107.2542 90.32 8158.00 8196.89
107.2746 90.62 8212.00 8198.77
107.2951 91.10 8299.00 8200.83
107.3155 90.68 8223.00 8203.06
107.3360 89.82 8067.00 8205.42
107.3565 90.47 8184.00 8208.18
107.3769 91.03 8287.00 8211.22
107.3974 90.91 8265.00 8214.42
107.4178 90.19 8134.00 8217.75
107.4383 89.86 8075.00 8221.26
107.4588 89.84 8071.00 8224.58
107.4792 89.98 8096.00 8227.72
107.4997 90.35 8163.00 8230.70
107.5201 90.53 8195.00 8233.21
107.5406 90.13 8124.00 8235.34
107.5611 90.28 8150.00 8237.03
107.5815 90.72 8231.00 8238.31
107.6020 90.32 8157.00 8239.12
107.6224 90.86 8256.00 8239.60
107.6429 91.20 8318.00 8239.77
107.6634 90.75 8235.00 8239.73
107.6838 91.32 8339.00 8239.61
107.7043 90.47 8184.00 8239.54
107.7247 90.48 8187.00 8239.58
107.7452 91.50 8373.00 8239.79
107.7657 90.73 8232.00 8239.99
107.7861 90.38 8168.00 8240.50
107.8066 90.64 8216.00 8241.09
107.8270 90.45 8181.00 8241.71
107.8475 89.89 8081.00 8242.12
107.8680 91.13 8305.00 8242.25
107.8884 91.15 8309.00 8242.00
107.9089 90.87 8257.00 8241.25
107.9293 90.46 8183.00 8240.00
107.9498 90.07 8113.00 8238.18
107.9703 89.88 8079.00 8235.78
107.9907 90.52 8194.00 8232.88
108.0112 89.69 8045.00 8229.48
108.0316 90.42 8175.00 8225.72
108.0521 89.97 8095.00 8221.63
108.0726 89.86 8075.00 8217.36
108.0930 91.11 8301.00 8213.03
108.1135 91.06 8292.00 8208.77
108.1340 90.20 8136.00 8204.47
108.1544 90.69 8225.00 8200.43
108.1749 90.68 8222.00 8196.59
108.1953 90.95 8272.00 8192.98
108.2158 91.69 8407.00 8189.50
108.2363 90.06 8110.00 8185.99
108.2567 90.01 8102.00 8182.80
108.2772 89.92 8086.00 8179.92
108.2976 90.78 8241.00 8177.29
108.3181 91.10 8300.00 8174.62
108.3386 90.71 8229.00 8172.15
108.3590 90.54 8197.00 8169.66
108.3795 90.49 8189.00 8167.39
108.3999 90.22 8139.00 8164.91
108.4204 90.29 8153.00 8162.79
108.4409 90.29 8153.00 8160.93
108.4613 91.22 8321.00 8159.21
108.4818 90.15 8127.00 8157.73
108.5022 89.36 7986.00 8156.59
108.5227 91.16 8311.00 8155.82
108.5432 90.23 8141.00 8155.33
108.5636 89.72 8049.00 8155.21
108.5841 90.91 8264.00 8155.52
108.6045 90.96 8273.00 8156.23
108.6250 90.87 8257.00 8157.28
108.6455 90.80 8244.00 8158.88
108.6659 90.80 8244.00 8161.07
108.6864 90.31 8156.00 8163.81
108.7068 90.13 8123.00 8167.01
108.7273 91.52 8376.00 8170.78
108.7478 90.88 8260.00 8175.00
108.7682 90.30 8154.00 8179.75
108.7887 90.61 8211.00 8184.88
108.8091 90.79 8243.00 8190.41
108.8296 91.10 8299.00 8196.29
108.8501 91.49 8370.00 8202.50
108.8705 90.83 8250.00 8208.82
108.8910 91.01 8283.00 8215.07
108.9114 92.26 8512.00 8221.63
108.9319 90.99 8279.00 8228.11
108.9524 90.98 8278.00 8234.68
108.9728 90.93 8269.00 8241.22
108.9933 91.14 8306.00 8247.78
109.0137 90.90 8263.00 8254.37
109.0342 91.92 8449.00 8261.05
109.0547 90.72 8231.00 8267.82
109.0751 92.02 8468.00 8274.67
109.0956 91.30 8335.00 8281.65
109.1160 90.82 8249.00 8288.70
109.1365 91.36 8346.00 8295.85
109.1570 90.74 8234.00 8303.04
109.1774 91.24 8324.00 8310.07
109.1979 90.83 8250.00 8317.24
109.2183 90.83 8251.00 8324.19
109.2388 90.71 8229.00 8330.98
109.2593 90.93 8268.00 8337.48
109.2797 90.75 8236.00 8343.46
109.3002 90.13 8123.00 8349.14
109.3206 91.21 8320.00 8354.24
109.3411 91.23 8323.00 8358.85
109.3616 91.18 8313.00 8362.90
109.3820 91.85 8436.00 8366.38
109.4025 91.08 8296.00 8369.37
109.4229 91.44 8362.00 8371.92
109.4434 91.74 8416.00 8374.09
109.4639 91.56 8384.00 8375.94
109.4843 91.87 8441.00 8377.50
109.5048 91.64 8398.00 8378.82
109.5252 91.72 8413.00 8379.90
109.5457 91.12 8302.00 8380.73
109.5662 92.00 8464.00 8381.00
109.5866 90.61 8210.00 8381.40
109.6071 90.50 8190.00 8381.49
109.6275 91.04 8289.00 8381.07
109.6480 91.02 8284.00 8380.20
109.6685 90.56 8201.00 8378.77
109.6889 91.94 8453.00 8376.76
109.7094 91.26 8329.00 8374.07
109.7298 90.38 8169.00 8370.66
109.7503 91.47 8367.00 8366.41
109.7708 91.14 8306.00 8361.33
109.7912 90.75 8235.00 8355.30
109.8117 92.11 8484.00 8348.21
109.8321 90.95 8272.00 8340.24
109.8526 91.10 8299.00 8330.90
109.8731 91.01 8283.00 8320.27
109.8935 91.62 8395.00 8308.31
109.9140 91.92 8449.00 8294.69
109.9344 91.96 8456.00 8279.40
109.9549 91.14 8307.00 8261.98
109.9754 91.32 8339.00 8242.46
109.9958 91.03 8286.00 8220.71
loop_
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loop_
_pd_proc_wavelength
1.5406
1.54439
