#------------------------------------------------------------------------------
#$Date: 2016-02-20 05:06:23 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176774 $
#$URL: svn://www.crystallography.net/cod/cif/2/20/33/2203351.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2203351
loop_
_publ_author_name
'Aris, Damian R.'
'Barker, James'
'Errington, William'
'Wallbridge, Malcolm G. H.'
_publ_section_title
;
 Bis(N,N'-diphenylacetamidinato)ethylindium(III)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m302
_journal_page_last               m303
_journal_paper_doi               10.1107/S1600536804002867
_journal_volume                  60
_journal_year                    2004
_chemical_formula_iupac          '[In (C2 H5) (C14 H13 N2)2]'
_chemical_formula_moiety         'C30 H31 In N4'
_chemical_formula_sum            'C30 H31 In N4'
_chemical_formula_weight         562.41
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                107.11(5)
_cell_angle_beta                 94.83(5)
_cell_angle_gamma                111.92(4)
_cell_formula_units_Z            2
_cell_length_a                   10.056(4)
_cell_length_b                   12.014(7)
_cell_length_c                   12.842(8)
_cell_measurement_reflns_used    18
_cell_measurement_temperature    240(2)
_cell_measurement_theta_max      11
_cell_measurement_theta_min      10
_cell_volume                     1342.3(15)
_computing_cell_refinement       'Siemens P3R3 software'
_computing_data_collection       'Siemens P3R3 software'
_computing_data_reduction        'SHELXTL-Plus (Sheldrick, 1994)'
_computing_molecular_graphics    'SHELXTL/PC (Sheldick, 1994)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS90 (Sheldrick, 1990)'
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Siemens P3/R3'
_diffrn_measurement_method       ω-2θ
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.076
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            4504
_diffrn_reflns_theta_full        24.1
_diffrn_reflns_theta_max         24.1
_diffrn_reflns_theta_min         2.1
_diffrn_standards_decay_%        6
_diffrn_standards_interval_count 200
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.905
_exptl_absorpt_correction_T_max  0.792
_exptl_absorpt_correction_T_min  0.731
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details   '(Alcock, 1970)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.392
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             576
_exptl_crystal_size_max          0.37
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.27
_refine_diff_density_max         1.15
_refine_diff_density_min         -1.23
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.05
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     319
_refine_ls_number_reflns         4232
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.05
_refine_ls_R_factor_gt           0.048
_refine_ls_shift/su_max          <0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[σ²(Fo²)+(0.0878P)²+0.2286P] where P = (Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.124
_reflns_number_gt                3640
_reflns_number_total             4232
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            tk6150.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Gaussian' changed to 'gaussian'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Gaussian' changed to
'gaussian' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               2203351
_cod_database_fobs_code          2203351
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_type_symbol
In1 0.12291(4) 0.15701(3) 0.33165(3) 0.03694(15) Uani d . 1 In
N1 0.1313(5) 0.0015(4) 0.1834(3) 0.0417(10) Uani d . 1 N
N2 0.3051(4) 0.1979(4) 0.2382(3) 0.0404(9) Uani d . 1 N
N3 0.0604(5) 0.3194(4) 0.3226(4) 0.0417(9) Uani d . 1 N
N4 -0.1098(5) 0.1197(4) 0.2709(4) 0.0418(10) Uani d . 1 N
C1 0.0576(5) -0.1319(5) 0.1198(4) 0.0407(11) Uani d . 1 C
C2 0.0503(6) -0.2185(5) 0.1722(5) 0.0517(13) Uani d . 1 C
H2 0.0992 -0.1887 0.2472 0.062 Uiso calc R 1 H
C3 -0.0285(8) -0.3491(6) 0.1153(6) 0.0664(17) Uani d . 1 C
H3 -0.0321 -0.4074 0.1515 0.08 Uiso calc R 1 H
C4 -0.1017(7) -0.3935(6) 0.0052(6) 0.0678(18) Uani d . 1 C
H4 -0.1557 -0.4819 -0.0335 0.081 Uiso calc R 1 H
C5 -0.0950(7) -0.3073(6) -0.0474(5) 0.0625(16) Uani d . 1 C
H5 -0.1455 -0.3371 -0.122 0.075 Uiso calc R 1 H
C6 -0.0140(6) -0.1765(5) 0.0092(5) 0.0516(13) Uani d . 1 C
H6 -0.0079 -0.1183 -0.0277 0.062 Uiso calc R 1 H
C7 0.2542(5) 0.0804(5) 0.1657(4) 0.0384(11) Uani d . 1 C
C8 0.3277(6) 0.0363(5) 0.0746(5) 0.0483(13) Uani d . 1 C
H8A 0.2862 0.0414 0.006 0.072 Uiso calc R 1 H
H8B 0.312 -0.0516 0.0627 0.072 Uiso calc R 1 H
H8C 0.4323 0.0908 0.0962 0.072 Uiso calc R 1 H
C9 0.4351(5) 0.3033(5) 0.2430(4) 0.0410(11) Uani d . 1 C
C10 0.4667(6) 0.3394(5) 0.1516(5) 0.0497(13) Uani d . 1 C
H10 0.4046 0.289 0.0806 0.06 Uiso calc R 1 H
C11 0.5897(7) 0.4498(6) 0.1647(5) 0.0578(15) Uani d . 1 C
H11 0.6119 0.4723 0.102 0.069 Uiso calc R 1 H
C12 0.6793(6) 0.5264(5) 0.2681(6) 0.0572(15) Uani d . 1 C
H12 0.7606 0.6023 0.2764 0.069 Uiso calc R 1 H
C13 0.6495(6) 0.4917(5) 0.3604(5) 0.0526(14) Uani d . 1 C
H13 0.711 0.5435 0.4313 0.063 Uiso calc R 1 H
C14 0.5287(6) 0.3804(5) 0.3474(4) 0.0438(12) Uani d . 1 C
H14 0.5094 0.3564 0.4098 0.053 Uiso calc R 1 H
C15 -0.2522(6) 0.0191(5) 0.2433(4) 0.0412(11) Uani d . 1 C
C16 -0.2677(7) -0.1050(5) 0.1908(5) 0.0526(14) Uani d . 1 C
H16 -0.1861 -0.1195 0.1713 0.063 Uiso calc R 1 H
C17 -0.4043(8) -0.2089(6) 0.1666(5) 0.0630(16) Uani d . 1 C
H17 -0.4138 -0.293 0.1318 0.076 Uiso calc R 1 H
C18 -0.5247(7) -0.1882(7) 0.1939(5) 0.0670(18) Uani d . 1 C
H18 -0.6169 -0.2578 0.1755 0.08 Uiso calc R 1 H
C19 -0.5100(7) -0.0663(7) 0.2478(6) 0.0641(16) Uani d . 1 C
H19 -0.5922 -0.0525 0.2671 0.077 Uiso calc R 1 H
C20 -0.3743(6) 0.0372(6) 0.2742(5) 0.0504(13) Uani d . 1 C
H20 -0.3647 0.1203 0.3132 0.061 Uiso calc R 1 H
C21 -0.0809(6) 0.2392(5) 0.2766(4) 0.0428(12) Uani d . 1 C
C22 -0.1887(6) 0.2766(6) 0.2218(5) 0.0528(14) Uani d . 1 C
H22A -0.1362 0.3427 0.1929 0.079 Uiso calc R 1 H
H22B -0.2388 0.3089 0.2764 0.079 Uiso calc R 1 H
H22C -0.2602 0.2021 0.161 0.079 Uiso calc R 1 H
C23 0.1225(6) 0.4534(4) 0.3489(4) 0.0402(11) Uani d . 1 C
C24 0.2687(6) 0.5140(5) 0.3427(4) 0.0474(12) Uani d . 1 C
H24 0.3199 0.464 0.3159 0.057 Uiso calc R 1 H
C25 0.3398(6) 0.6456(5) 0.3751(5) 0.0525(13) Uani d . 1 C
H25 0.438 0.684 0.3696 0.063 Uiso calc R 1 H
C26 0.2668(7) 0.7215(5) 0.4157(5) 0.0568(15) Uani d . 1 C
H26 0.3156 0.8113 0.4395 0.068 Uiso calc R 1 H
C27 0.1224(8) 0.6636(6) 0.4206(5) 0.0610(16) Uani d . 1 C
H27 0.0718 0.7147 0.4459 0.073 Uiso calc R 1 H
C28 0.0485(7) 0.5299(5) 0.3886(5) 0.0503(13) Uani d . 1 C
H28 -0.0499 0.492 0.3939 0.06 Uiso calc R 1 H
C29 0.1903(7) 0.1478(6) 0.4917(4) 0.0538(14) Uani d . 1 C
H29A 0.2563 0.2343 0.5426 0.065 Uiso calc R 1 H
H29B 0.1035 0.1178 0.5228 0.065 Uiso calc R 1 H
C30 0.2663(10) 0.0614(8) 0.4864(6) 0.087(2) Uani d . 1 C
H30A 0.1965 -0.0269 0.4475 0.13 Uiso calc R 1 H
H30B 0.3073 0.0717 0.5616 0.13 Uiso calc R 1 H
H30C 0.3447 0.0832 0.4468 0.13 Uiso calc R 1 H
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
In In -0.7276 1.31 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_publ_flag
C29 In1 N4 120.3(2) y
C29 In1 N2 113.2(2) y
N4 In1 N2 126.51(16) y
C29 In1 N1 114.18(19) y
N4 In1 N1 96.12(16) y
N2 In1 N1 58.22(15) y
C29 In1 N3 119.96(19) y
N4 In1 N3 58.75(15) y
N2 In1 N3 96.83(15) y
N1 In1 N3 125.80(15) y
C7 N1 C1 123.8(4) ?
C7 N1 In1 93.9(3) ?
C1 N1 In1 142.3(3) ?
C7 N2 C9 126.3(4) ?
C7 N2 In1 95.3(3) ?
C9 N2 In1 138.4(3) ?
C21 N3 C23 126.0(4) ?
C21 N3 In1 92.8(3) ?
C23 N3 In1 141.1(3) ?
C21 N4 C15 125.1(4) ?
C21 N4 In1 95.7(3) ?
C15 N4 In1 138.9(3) ?
C2 C1 C6 119.4(5) ?
C2 C1 N1 118.7(5) ?
C6 C1 N1 121.8(5) ?
C1 C2 C3 120.6(6) ?
C1 C2 H2 119.7 ?
C3 C2 H2 119.7 ?
C4 C3 C2 120.0(6) ?
C4 C3 H3 120 ?
C2 C3 H3 120 ?
C5 C4 C3 119.6(6) ?
C5 C4 H4 120.2 ?
C3 C4 H4 120.2 ?
C4 C5 C6 120.4(6) ?
C4 C5 H5 119.8 ?
C6 C5 H5 119.8 ?
C1 C6 C5 120.0(6) ?
C1 C6 H6 120 ?
C5 C6 H6 120 ?
N2 C7 N1 112.6(4) y
N2 C7 C8 124.6(5) ?
N1 C7 C8 122.8(5) ?
C7 C8 H8A 109.5 ?
C7 C8 H8B 109.5 ?
H8A C8 H8B 109.5 ?
C7 C8 H8C 109.5 ?
H8A C8 H8C 109.5 ?
H8B C8 H8C 109.5 ?
C10 C9 C14 118.7(5) ?
C10 C9 N2 123.4(5) ?
C14 C9 N2 117.7(5) ?
C11 C10 C9 120.1(5) ?
C11 C10 H10 119.9 ?
C9 C10 H10 119.9 ?
C12 C11 C10 120.8(6) ?
C12 C11 H11 119.6 ?
C10 C11 H11 119.6 ?
C11 C12 C13 119.9(5) ?
C11 C12 H12 120.1 ?
C13 C12 H12 120.1 ?
C14 C13 C12 119.6(5) ?
C14 C13 H13 120.2 ?
C12 C13 H13 120.2 ?
C13 C14 C9 120.9(5) ?
C13 C14 H14 119.5 ?
C9 C14 H14 119.5 ?
C16 C15 C20 118.3(5) ?
C16 C15 N4 117.8(5) ?
C20 C15 N4 123.6(5) ?
C15 C16 C17 120.4(6) ?
C15 C16 H16 119.8 ?
C17 C16 H16 119.8 ?
C18 C17 C16 120.1(6) ?
C18 C17 H17 120 ?
C16 C17 H17 120 ?
C19 C18 C17 120.0(6) ?
C19 C18 H18 120 ?
C17 C18 H18 120 ?
C18 C19 C20 120.3(6) ?
C18 C19 H19 119.9 ?
C20 C19 H19 119.9 ?
C19 C20 C15 120.8(6) ?
C19 C20 H20 119.6 ?
C15 C20 H20 119.6 ?
N4 C21 N3 112.4(4) y
N4 C21 C22 123.8(5) ?
N3 C21 C22 123.2(5) ?
C21 C22 H22A 109.5 ?
C21 C22 H22B 109.5 ?
H22A C22 H22B 109.5 ?
C21 C22 H22C 109.5 ?
H22A C22 H22C 109.5 ?
H22B C22 H22C 109.5 ?
C24 C23 C28 118.2(5) ?
C24 C23 N3 118.4(4) ?
C28 C23 N3 123.2(5) ?
C25 C24 C23 121.5(5) ?
C25 C24 H24 119.2 ?
C23 C24 H24 119.2 ?
C24 C25 C26 120.2(6) ?
C24 C25 H25 119.9 ?
C26 C25 H25 119.9 ?
C27 C26 C25 119.1(5) ?
C27 C26 H26 120.5 ?
C25 C26 H26 120.5 ?
C26 C27 C28 121.5(6) ?
C26 C27 H27 119.3 ?
C28 C27 H27 119.3 ?
C23 C28 C27 119.5(5) ?
C23 C28 H28 120.3 ?
C27 C28 H28 120.3 ?
C30 C29 In1 113.6(4) ?
C30 C29 H29A 108.9 ?
In1 C29 H29A 108.9 ?
C30 C29 H29B 108.9 ?
In1 C29 H29B 108.9 ?
H29A C29 H29B 107.7 ?
C29 C30 H30A 109.5 ?
C29 C30 H30B 109.5 ?
H30A C30 H30B 109.5 ?
C29 C30 H30C 109.5 ?
H30A C30 H30C 109.5 ?
H30B C30 H30C 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
In1 C29 2.157(5) y
In1 N4 2.234(4) y
In1 N2 2.255(4) y
In1 N1 2.274(4) y
In1 N3 2.292(4) y
N1 C7 1.333(6) y
N1 C1 1.424(6) ?
N2 C7 1.315(6) y
N2 C9 1.422(6) ?
N3 C21 1.341(7) y
N3 C23 1.411(6) ?
N4 C21 1.331(6) y
N4 C15 1.417(7) ?
C1 C2 1.380(7) ?
C1 C6 1.384(8) ?
C2 C3 1.387(8) ?
C2 H2 0.94 ?
C3 C4 1.383(10) ?
C3 H3 0.94 ?
C4 C5 1.379(10) ?
C4 H4 0.94 ?
C5 C6 1.390(8) ?
C5 H5 0.94 ?
C6 H6 0.94 ?
C7 C8 1.507(7) ?
C8 H8A 0.97 ?
C8 H8B 0.97 ?
C8 H8C 0.97 ?
C9 C10 1.388(7) ?
C9 C14 1.395(7) ?
C10 C11 1.388(8) ?
C10 H10 0.94 ?
C11 C12 1.371(9) ?
C11 H11 0.94 ?
C12 C13 1.388(9) ?
C12 H12 0.94 ?
C13 C14 1.383(8) ?
C13 H13 0.94 ?
C14 H14 0.94 ?
C15 C16 1.385(8) ?
C15 C20 1.393(7) ?
C16 C17 1.401(9) ?
C16 H16 0.94 ?
C17 C18 1.377(9) ?
C17 H17 0.94 ?
C18 C19 1.368(10) ?
C18 H18 0.94 ?
C19 C20 1.390(8) ?
C19 H19 0.94 ?
C20 H20 0.94 ?
C21 C22 1.515(7) ?
C22 H22A 0.97 ?
C22 H22B 0.97 ?
C22 H22C 0.97 ?
C23 C24 1.397(7) ?
C23 C28 1.399(7) ?
C24 C25 1.379(8) ?
C24 H24 0.94 ?
C25 C26 1.388(8) ?
C25 H25 0.94 ?
C26 C27 1.373(9) ?
C26 H26 0.94 ?
C27 C28 1.404(8) ?
C27 H27 0.94 ?
C28 H28 0.94 ?
C29 C30 1.492(9) ?
C29 H29A 0.98 ?
C29 H29B 0.98 ?
C30 H30A 0.97 ?
C30 H30B 0.97 ?
C30 H30C 0.97 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C29 In1 N1 C7 -103.9(3)
N4 In1 N1 C7 129.0(3)
N2 In1 N1 C7 -0.6(3)
N3 In1 N1 C7 73.5(3)
C29 In1 N1 C1 73.6(6)
N4 In1 N1 C1 -53.5(5)
N2 In1 N1 C1 176.9(6)
N3 In1 N1 C1 -109.1(5)
C29 In1 N2 C7 105.6(3)
N4 In1 N2 C7 -71.8(3)
N1 In1 N2 C7 0.6(3)
N3 In1 N2 C7 -127.6(3)
C29 In1 N2 C9 -74.0(5)
N4 In1 N2 C9 108.6(5)
N1 In1 N2 C9 -179.0(6)
N3 In1 N2 C9 52.7(5)
C29 In1 N3 C21 -112.9(3)
N4 In1 N3 C21 -3.5(3)
N2 In1 N3 C21 125.4(3)
N1 In1 N3 C21 70.0(3)
C29 In1 N3 C23 66.9(6)
N4 In1 N3 C23 176.2(6)
N2 In1 N3 C23 -54.8(5)
N1 In1 N3 C23 -110.3(5)
C29 In1 N4 C21 112.4(3)
N2 In1 N4 C21 -70.4(3)
N1 In1 N4 C21 -125.0(3)
N3 In1 N4 C21 3.6(3)
C29 In1 N4 C15 -61.4(5)
N2 In1 N4 C15 115.9(5)
N1 In1 N4 C15 61.3(5)
N3 In1 N4 C15 -170.1(6)
C7 N1 C1 C2 114.7(6)
In1 N1 C1 C2 -62.2(7)
C7 N1 C1 C6 -69.2(7)
In1 N1 C1 C6 113.8(6)
C6 C1 C2 C3 -0.3(9)
N1 C1 C2 C3 175.8(5)
C1 C2 C3 C4 -0.6(10)
C2 C3 C4 C5 0.4(10)
C3 C4 C5 C6 0.6(10)
C2 C1 C6 C5 1.4(8)
N1 C1 C6 C5 -174.6(5)
C4 C5 C6 C1 -1.6(9)
C9 N2 C7 N1 178.7(4)
In1 N2 C7 N1 -1.0(4)
C9 N2 C7 C8 0.9(8)
In1 N2 C7 C8 -178.8(4)
C1 N1 C7 N2 -177.2(4)
In1 N1 C7 N2 1.0(4)
C1 N1 C7 C8 0.7(7)
In1 N1 C7 C8 178.9(4)
C7 N2 C9 C10 51.3(7)
In1 N2 C9 C10 -129.2(5)
C7 N2 C9 C14 -134.6(5)
In1 N2 C9 C14 45.0(7)
C14 C9 C10 C11 0.4(8)
N2 C9 C10 C11 174.5(5)
C9 C10 C11 C12 -1.9(9)
C10 C11 C12 C13 1.9(9)
C11 C12 C13 C14 -0.6(8)
C12 C13 C14 C9 -0.8(8)
C10 C9 C14 C13 0.9(7)
N2 C9 C14 C13 -173.6(4)
C21 N4 C15 C16 150.4(5)
In1 N4 C15 C16 -37.3(7)
C21 N4 C15 C20 -35.1(8)
In1 N4 C15 C20 137.3(5)
C20 C15 C16 C17 1.9(8)
N4 C15 C16 C17 176.7(5)
C15 C16 C17 C18 0.7(9)
C16 C17 C18 C19 -2.0(10)
C17 C18 C19 C20 0.7(10)
C18 C19 C20 C15 2.0(9)
C16 C15 C20 C19 -3.2(8)
N4 C15 C20 C19 -177.8(5)
C15 N4 C21 N3 169.3(4)
In1 N4 C21 N3 -5.7(5)
C15 N4 C21 C22 -19.4(8)
In1 N4 C21 C22 165.6(4)
C23 N3 C21 N4 -174.3(4)
In1 N3 C21 N4 5.5(4)
C23 N3 C21 C22 14.3(8)
In1 N3 C21 C22 -165.9(5)
C21 N3 C23 C24 -148.5(5)
In1 N3 C23 C24 31.8(8)
C21 N3 C23 C28 36.4(8)
In1 N3 C23 C28 -143.4(5)
C28 C23 C24 C25 0.3(8)
N3 C23 C24 C25 -175.1(5)
C23 C24 C25 C26 0.5(9)
C24 C25 C26 C27 -1.5(9)
C25 C26 C27 C28 1.9(9)
C24 C23 C28 C27 0.1(8)
N3 C23 C28 C27 175.3(5)
C26 C27 C28 C23 -1.2(9)
N4 In1 C29 C30 127.0(5)
N2 In1 C29 C30 -50.6(6)
N1 In1 C29 C30 13.6(6)
N3 In1 C29 C30 -163.9(5)
