data_3000046
loop_
_publ_author_name
'Stephanie Hurst'
_publ_section_title
;
 
;
_journal_name_full               'To be published in Tetrahedron Letters'
_diffrn_ambient_temperature      150
_cell_measurement_temperature    150
_chemical_formula_sum            'C43 H44 B2 Cl2 F8 P2'
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_cell_length_a                   22.860(2)
_cell_length_b                   11.7003(8)
_cell_length_c                   15.6988(11)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     4198.9(6)
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_refine_ls_R_factor_all          0.0326
_refine_ls_R_factor_gt           0.0298
_refine_ls_wR_factor_gt          0.0735
_refine_ls_wR_factor_ref         0.0748
_refine_ls_goodness_of_fit_ref   1.037
_cod_hold_until_date             2015-10-11
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
? ? ? ?
