data_3000052
loop_
_publ_author_name
'Janeta, Mateusz'
'John, Lukasz'
'Ejfler, Jolanta'
'Lis, Tadeusz'
'Szafert, Slawomir'
_publ_section_title
;
 A New Family of Imino-Functionalized Polyoctahedral Oligomeric
 Silsesquioxanes: Synthesis, Structural Investigations and Properties
;
_journal_name_full
'To be published in Chemistry - A European Journal'
_diffrn_ambient_temperature      80(2)
_cell_measurement_temperature    80(2)
_chemical_formula_sum            'C84 H90 Cl12 N16 O28 Si8'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_length_a                   9.578(4)
_cell_length_b                   16.150(7)
_cell_length_c                   18.867(7)
_cell_angle_alpha                108.08(4)
_cell_angle_beta                 98.79(3)
_cell_angle_gamma                92.53(3)
_cell_volume                     2729(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_refine_ls_R_factor_all          0.0957
_refine_ls_R_factor_gt           0.0665
_refine_ls_wR_factor_gt          0.1684
_refine_ls_wR_factor_ref         0.1889
_refine_ls_goodness_of_fit_ref   1.027
_cod_hold_until_date             2016-04-29
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
? ? ? ?
