data_3000053
loop_
_publ_author_name
'Janeta, Mateusz'
'John, Lukasz'
'Ejfler, Jolanta'
'Lis, Tadeusz'
'Szafert, Slawomir'
_publ_section_title
;
 A New Family of Imino-Functionalized Polyoctahedral Oligomeric
 Silsesquioxanes: Synthesis, Structural Investigations and Properties
;
_journal_name_full
'To be published in Chemistry - A European Journal'
_diffrn_ambient_temperature      100(2)
_cell_measurement_temperature    100(2)
_chemical_formula_sum            'C80 H96 N8 O12 Si8'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_length_a                   9.982(3)
_cell_length_b                   13.141(4)
_cell_length_c                   16.763(5)
_cell_angle_alpha                82.27(3)
_cell_angle_beta                 82.12(3)
_cell_angle_gamma                77.37(3)
_cell_volume                     2112.9(11)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_refine_ls_R_factor_all          0.1169
_refine_ls_R_factor_gt           0.0628
_refine_ls_wR_factor_gt          0.1128
_refine_ls_wR_factor_ref         0.1337
_refine_ls_goodness_of_fit_ref   1.006
_cod_hold_until_date             2016-04-29
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
? ? ? ?
