#------------------------------------------------------------------------------
#$Date: 2016-03-21 01:21:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178377 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/21/4002192.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4002192
loop_
_publ_author_name
'Rai, Binod K.'
'Oswald, Iain W. H.'
'Wang, Jiakui K.'
'McCandless, Gregory T.'
'Chan, Julia Y.'
'Morosan, E.'
_publ_section_title
;
 Superconductivity in Single Crystals of Lu3T4Ge13--x(T= Co, Rh, Os) and
 Y3T4Ge13--x(T= Ir, Rh, Os)
;
_journal_issue                   7
_journal_name_full               'Chemistry of Materials'
_journal_page_first              2488
_journal_paper_doi               10.1021/cm504658h
_journal_volume                  27
_journal_year                    2015
_chemical_formula_sum            'Ge13 Lu3 Rh4'
_chemical_formula_weight         1880.22
_space_group_crystal_system      cubic
_space_group_IT_number           223
_space_group_name_Hall           '-P 4n 2 3'
_space_group_name_H-M_alt        'P m -3 n'
_symmetry_space_group_name_Hall  '-P 4n 2 3'
_symmetry_space_group_name_H-M   'P m -3 n'
_audit_creation_method           SHELXL-2014
_audit_update_record
;
2014-10-31 # Formatted by publCIF
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   8.8659(7)
_cell_length_b                   8.8659(5)
_cell_length_c                   8.8659(5)
_cell_measurement_reflns_used    913
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      30.46
_cell_measurement_theta_min      3.25
_cell_volume                     696.90(8)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    CrystalMaker
_computing_publication_material  'publCIF (Westrip, 2010)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS Direct Methods (Sheldrick, 2013)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker Kappa D8 Quest CMOS'
_diffrn_measurement_method       'φ scan'
_diffrn_radiation_monochromator  'HELIOS optics'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0510
_diffrn_reflns_av_unetI/netI     0.0317
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            2019
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.465
_diffrn_reflns_theta_min         3.250
_diffrn_source                   'I\mS microfocus'
_exptl_absorpt_coefficient_mu    53.121
_exptl_absorpt_correction_T_max  0.7461
_exptl_absorpt_correction_T_min  0.2725
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS(2014)
_exptl_crystal_colour            Silver
_exptl_crystal_density_diffrn    8.960
_exptl_crystal_description       Fragment
_exptl_crystal_F_000             1618
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.04
_refine_diff_density_max         2.611
_refine_diff_density_min         -1.821
_refine_diff_density_rms         0.352
_refine_ls_extinction_coef       0.00068(13)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.130
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     16
_refine_ls_number_reflns         211
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.130
_refine_ls_R_factor_all          0.0378
_refine_ls_R_factor_gt           0.0289
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0119P)²+21.2274P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0571
_refine_ls_wR_factor_ref         0.0590
_reflns_Friedel_coverage         0.000
_reflns_number_gt                188
_reflns_number_total             211
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            Lu3Rh4Ge13_CIF.cif
_cod_data_source_block           shelx
_cod_depositor_comments
'Adding full bibliography for 4002190--4002195.cif.'
_cod_original_cell_volume        696.90(17)
_cod_database_code               4002192
#BEGIN Tags that were not found in dictionaries:
_publcif_datablock.id            {ff9adc97-e1f9-4016-8756-d3a9d9d0c165}
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2014-3
#END Tags that were not found in dictionaries
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'z, x, y'
'z, -x, -y'
'-z, -x, y'
'-z, x, -y'
'y, z, x'
'-y, z, -x'
'y, -z, -x'
'-y, -z, x'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'y+1/2, -x+1/2, z+1/2'
'-y+1/2, x+1/2, z+1/2'
'x+1/2, z+1/2, -y+1/2'
'-x+1/2, z+1/2, y+1/2'
'-x+1/2, -z+1/2, -y+1/2'
'x+1/2, -z+1/2, y+1/2'
'z+1/2, y+1/2, -x+1/2'
'z+1/2, -y+1/2, x+1/2'
'-z+1/2, y+1/2, x+1/2'
'-z+1/2, -y+1/2, -x+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-z, -x, -y'
'-z, x, y'
'z, x, -y'
'z, -x, y'
'-y, -z, -x'
'y, -z, x'
'-y, z, x'
'y, z, -x'
'-y-1/2, -x-1/2, z-1/2'
'y-1/2, x-1/2, z-1/2'
'-y-1/2, x-1/2, -z-1/2'
'y-1/2, -x-1/2, -z-1/2'
'-x-1/2, -z-1/2, y-1/2'
'x-1/2, -z-1/2, -y-1/2'
'x-1/2, z-1/2, y-1/2'
'-x-1/2, z-1/2, -y-1/2'
'-z-1/2, -y-1/2, x-1/2'
'-z-1/2, y-1/2, -x-1/2'
'z-1/2, -y-1/2, -x-1/2'
'z-1/2, y-1/2, x-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Lu1 Lu 0.2500 0.5000 0.0000 0.0075(3) Uani 1 8 d S T P
Rh1 Rh 0.2500 0.2500 0.2500 0.0037(3) Uani 1 6 d S T P
Ge1 Ge 0.0000 0.0000 0.0000 0.0215(9) Uani 1 24 d S T P
Ge2A Ge 0.0000 0.2669(6) 0.1323(5) 0.0149(6) Uani 0.366(5) 2 d S T P
Ge2B Ge 0.0000 0.3338(4) 0.1553(3) 0.0149(6) Uani 0.634(5) 2 d S T P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge2B Lu1 Ge2B 123.17(4) . 17
Ge2B Lu1 Ge2B 54.70(10) . 26
Ge2B Lu1 Ge2B 177.38(12) 17 26
Ge2B Lu1 Ge2B 95.47(7) . 42_666
Ge2B Lu1 Ge2B 54.70(10) 17 42_666
Ge2B Lu1 Ge2B 123.17(4) 26 42_666
Ge2B Lu1 Ge2B 177.38(12) . 18_554
Ge2B Lu1 Ge2B 58.91(12) 17 18_554
Ge2B Lu1 Ge2B 123.17(4) 26 18_554
Ge2B Lu1 Ge2B 84.59(7) 42_666 18_554
Ge2B Lu1 Ge2B 84.59(7) . 25_565
Ge2B Lu1 Ge2B 123.17(4) 17 25_565
Ge2B Lu1 Ge2B 58.91(12) 26 25_565
Ge2B Lu1 Ge2B 177.38(12) 42_666 25_565
Ge2B Lu1 Ge2B 95.47(7) 18_554 25_565
Ge2B Lu1 Ge2B 123.17(4) . 41_665
Ge2B Lu1 Ge2B 84.59(7) 17 41_665
Ge2B Lu1 Ge2B 95.47(7) 26 41_665
Ge2B Lu1 Ge2B 58.91(12) 42_666 41_665
Ge2B Lu1 Ge2B 54.70(10) 18_554 41_665
Ge2B Lu1 Ge2B 123.17(4) 25_565 41_665
Ge2B Lu1 Ge2B 58.91(12) . 2_565
Ge2B Lu1 Ge2B 95.47(7) 17 2_565
Ge2B Lu1 Ge2B 84.59(7) 26 2_565
Ge2B Lu1 Ge2B 123.17(4) 42_666 2_565
Ge2B Lu1 Ge2B 123.17(4) 18_554 2_565
Ge2B Lu1 Ge2B 54.70(10) 25_565 2_565
Ge2B Lu1 Ge2B 177.38(12) 41_665 2_565
Ge2B Lu1 Rh1 88.69(6) . 26
Ge2B Lu1 Rh1 132.27(3) 17 26
Ge2B Lu1 Rh1 47.73(3) 26 26
Ge2B Lu1 Rh1 91.31(6) 42_666 26
Ge2B Lu1 Rh1 88.69(6) 18_554 26
Ge2B Lu1 Rh1 91.31(6) 25_565 26
Ge2B Lu1 Rh1 47.73(3) 41_665 26
Ge2B Lu1 Rh1 132.27(3) 2_565 26
Ge2B Lu1 Rh1 91.31(6) . 27_565
Ge2B Lu1 Rh1 47.73(3) 17 27_565
Ge2B Lu1 Rh1 132.27(3) 26 27_565
Ge2B Lu1 Rh1 88.69(6) 42_666 27_565
Ge2B Lu1 Rh1 91.31(6) 18_554 27_565
Ge2B Lu1 Rh1 88.69(6) 25_565 27_565
Ge2B Lu1 Rh1 132.27(3) 41_665 27_565
Ge2B Lu1 Rh1 47.73(3) 2_565 27_565
Rh1 Lu1 Rh1 180.0 26 27_565
Ge2B Lu1 Rh1 47.73(3) . .
Ge2B Lu1 Rh1 88.69(6) 17 .
Ge2B Lu1 Rh1 88.69(6) 26 .
Ge2B Lu1 Rh1 47.73(3) 42_666 .
Ge2B Lu1 Rh1 132.27(3) 18_554 .
Ge2B Lu1 Rh1 132.27(3) 25_565 .
Ge2B Lu1 Rh1 91.31(6) 41_665 .
Ge2B Lu1 Rh1 91.31(6) 2_565 .
Rh1 Lu1 Rh1 90.0 26 .
Rh1 Lu1 Rh1 90.0 27_565 .
Ge2B Lu1 Rh1 132.27(3) . 4_565
Ge2B Lu1 Rh1 91.31(6) 17 4_565
Ge2B Lu1 Rh1 91.31(6) 26 4_565
Ge2B Lu1 Rh1 132.27(3) 42_666 4_565
Ge2B Lu1 Rh1 47.73(3) 18_554 4_565
Ge2B Lu1 Rh1 47.73(3) 25_565 4_565
Ge2B Lu1 Rh1 88.69(6) 41_665 4_565
Ge2B Lu1 Rh1 88.69(6) 2_565 4_565
Rh1 Lu1 Rh1 90.0 26 4_565
Rh1 Lu1 Rh1 90.0 27_565 4_565
Rh1 Lu1 Rh1 180.0 . 4_565
Ge2A Rh1 Ge2A 140.48(18) . 45_666
Ge2A Rh1 Ge2A 139.8(2) . 42_666
Ge2A Rh1 Ge2A 72.4(2) 45_666 42_666
Ge2A Rh1 Ge2A 94.0(3) . 14
Ge2A Rh1 Ge2A 72.4(2) 45_666 14
Ge2A Rh1 Ge2A 72.4(2) 42_666 14
Ge2A Rh1 Ge2A 72.4(2) . 9
Ge2A Rh1 Ge2A 139.8(2) 45_666 9
Ge2A Rh1 Ge2A 94.0(3) 42_666 9
Ge2A Rh1 Ge2A 140.48(18) 14 9
Ge2A Rh1 Ge2A 72.4(2) . 5
Ge2A Rh1 Ge2A 94.0(3) 45_666 5
Ge2A Rh1 Ge2A 140.48(18) 42_666 5
Ge2A Rh1 Ge2A 139.8(2) 14 5
Ge2A Rh1 Ge2A 72.4(2) 9 5
Ge2A Rh1 Ge2B 134.66(8) . 45_666
Ge2A Rh1 Ge2B 14.57(9) 45_666 45_666
Ge2A Rh1 Ge2B 82.89(18) 42_666 45_666
Ge2A Rh1 Ge2B 84.92(15) 14 45_666
Ge2A Rh1 Ge2B 131.16(11) 9 45_666
Ge2A Rh1 Ge2B 79.58(19) 5 45_666
Ge2A Rh1 Ge2B 131.16(11) . 42_666
Ge2A Rh1 Ge2B 84.92(15) 45_666 42_666
Ge2A Rh1 Ge2B 14.57(9) 42_666 42_666
Ge2A Rh1 Ge2B 82.89(18) 14 42_666
Ge2A Rh1 Ge2B 79.58(19) 9 42_666
Ge2A Rh1 Ge2B 134.66(8) 5 42_666
Ge2B Rh1 Ge2B 93.80(11) 45_666 42_666
Ge2A Rh1 Ge2B 79.58(19) . 14
Ge2A Rh1 Ge2B 82.89(18) 45_666 14
Ge2A Rh1 Ge2B 84.92(15) 42_666 14
Ge2A Rh1 Ge2B 14.57(9) 14 14
Ge2A Rh1 Ge2B 134.66(8) 9 14
Ge2A Rh1 Ge2B 131.16(11) 5 14
Ge2B Rh1 Ge2B 93.80(11) 45_666 14
Ge2B Rh1 Ge2B 93.80(11) 42_666 14
Ge2A Rh1 Ge2B 84.92(15) . 9
Ge2A Rh1 Ge2B 131.16(11) 45_666 9
Ge2A Rh1 Ge2B 79.58(19) 42_666 9
Ge2A Rh1 Ge2B 134.66(8) 14 9
Ge2A Rh1 Ge2B 14.57(9) 9 9
Ge2A Rh1 Ge2B 82.89(18) 5 9
Ge2B Rh1 Ge2B 126.44(10) 45_666 9
Ge2B Rh1 Ge2B 65.20(15) 42_666 9
Ge2B Rh1 Ge2B 133.86(10) 14 9
Ge2A Rh1 Ge2B 82.89(18) . 5
Ge2A Rh1 Ge2B 79.58(19) 45_666 5
Ge2A Rh1 Ge2B 134.66(8) 42_666 5
Ge2A Rh1 Ge2B 131.16(11) 14 5
Ge2A Rh1 Ge2B 84.92(15) 9 5
Ge2A Rh1 Ge2B 14.57(9) 5 5
Ge2B Rh1 Ge2B 65.20(15) 45_666 5
Ge2B Rh1 Ge2B 133.86(10) 42_666 5
Ge2B Rh1 Ge2B 126.44(10) 14 5
Ge2B Rh1 Ge2B 93.80(11) 9 5
Ge2A Rh1 Ge2B 14.57(9) . .
Ge2A Rh1 Ge2B 134.66(8) 45_666 .
Ge2A Rh1 Ge2B 131.15(11) 42_666 .
Ge2A Rh1 Ge2B 79.58(19) 14 .
Ge2A Rh1 Ge2B 82.89(18) 9 .
Ge2A Rh1 Ge2B 84.92(15) 5 .
Ge2B Rh1 Ge2B 133.86(10) 45_666 .
Ge2B Rh1 Ge2B 126.44(10) 42_666 .
Ge2B Rh1 Ge2B 65.20(15) 14 .
Ge2B Rh1 Ge2B 93.80(11) 9 .
Ge2B Rh1 Ge2B 93.80(11) 5 .
Ge2A Ge1 Ge2A 113.45(6) . 33
Ge2A Ge1 Ge2A 66.55(6) . 9
Ge2A Ge1 Ge2A 180.00(17) 33 9
Ge2A Ge1 Ge2A 113.45(6) . 29
Ge2A Ge1 Ge2A 66.55(6) 33 29
Ge2A Ge1 Ge2A 113.45(6) 9 29
Ge2A Ge1 Ge2A 66.55(6) . 5
Ge2A Ge1 Ge2A 113.45(6) 33 5
Ge2A Ge1 Ge2A 66.55(6) 9 5
Ge2A Ge1 Ge2A 180.0 29 5
Ge2A Ge1 Ge2A 180.0 . 25
Ge2A Ge1 Ge2A 66.55(6) 33 25
Ge2A Ge1 Ge2A 113.45(6) 9 25
Ge2A Ge1 Ge2A 66.55(6) 29 25
Ge2A Ge1 Ge2A 113.45(6) 5 25
Ge2A Ge1 Ge2A 113.45(6) . 34
Ge2A Ge1 Ge2A 127.25(19) 33 34
Ge2A Ge1 Ge2A 52.75(19) 9 34
Ge2A Ge1 Ge2A 113.45(6) 29 34
Ge2A Ge1 Ge2A 66.55(6) 5 34
Ge2A Ge1 Ge2A 66.55(6) 25 34
Ge2A Ge1 Ge2A 113.45(6) . 6
Ge2A Ge1 Ge2A 113.45(6) 33 6
Ge2A Ge1 Ge2A 66.55(6) 9 6
Ge2A Ge1 Ge2A 52.75(19) 29 6
Ge2A Ge1 Ge2A 127.25(19) 5 6
Ge2A Ge1 Ge2A 66.55(6) 25 6
Ge2A Ge1 Ge2A 66.55(6) 34 6
Ge2A Ge1 Ge2A 66.55(6) . 30
Ge2A Ge1 Ge2A 66.55(6) 33 30
Ge2A Ge1 Ge2A 113.45(6) 9 30
Ge2A Ge1 Ge2A 127.25(19) 29 30
Ge2A Ge1 Ge2A 52.75(19) 5 30
Ge2A Ge1 Ge2A 113.45(6) 25 30
Ge2A Ge1 Ge2A 113.45(6) 34 30
Ge2A Ge1 Ge2A 180.00(19) 6 30
Ge2A Ge1 Ge2A 66.55(6) . 10
Ge2A Ge1 Ge2A 52.75(19) 33 10
Ge2A Ge1 Ge2A 127.25(19) 9 10
Ge2A Ge1 Ge2A 66.55(6) 29 10
Ge2A Ge1 Ge2A 113.45(6) 5 10
Ge2A Ge1 Ge2A 113.45(6) 25 10
Ge2A Ge1 Ge2A 180.0(2) 34 10
Ge2A Ge1 Ge2A 113.45(6) 6 10
Ge2A Ge1 Ge2A 66.55(6) 30 10
Ge2A Ge1 Ge2A 127.25(19) . 2
Ge2A Ge1 Ge2A 66.55(6) 33 2
Ge2A Ge1 Ge2A 113.45(6) 9 2
Ge2A Ge1 Ge2A 113.45(6) 29 2
Ge2A Ge1 Ge2A 66.55(6) 5 2
Ge2A Ge1 Ge2A 52.75(19) 25 2
Ge2A Ge1 Ge2A 66.55(6) 34 2
Ge2A Ge1 Ge2A 113.45(6) 6 2
Ge2A Ge1 Ge2A 66.55(6) 30 2
Ge2A Ge1 Ge2A 113.45(6) 10 2
Ge2A Ge1 Ge2A 52.75(19) . 26
Ge2A Ge1 Ge2A 113.45(6) 33 26
Ge2A Ge1 Ge2A 66.55(6) 9 26
Ge2A Ge1 Ge2A 66.55(6) 29 26
Ge2A Ge1 Ge2A 113.45(6) 5 26
Ge2A Ge1 Ge2A 127.25(19) 25 26
Ge2A Ge1 Ge2A 113.45(6) 34 26
Ge2A Ge1 Ge2A 66.55(6) 6 26
Ge2A Ge1 Ge2A 113.45(6) 30 26
Ge2A Ge1 Ge2A 66.55(6) 10 26
Ge2A Ge1 Ge2A 180.0 2 26
Ge2B Ge2A Ge2A 108.9(5) . 26
Ge2B Ge2A Rh1 85.4(3) . .
Ge2A Ge2A Rh1 115.15(9) 26 .
Ge2B Ge2A Rh1 85.4(3) . 28
Ge2A Ge2A Rh1 115.15(9) 26 28
Rh1 Ge2A Rh1 129.14(18) . 28
Ge2B Ge2A Ge2B 95.8(6) . 26
Ge2A Ge2A Ge2B 13.09(9) 26 26
Rh1 Ge2A Ge2B 115.33(9) . 26
Rh1 Ge2A Ge2B 115.33(9) 28 26
Ge2B Ge2A Ge1 172.6(6) . .
Ge2A Ge2A Ge1 63.63(9) 26 .
Rh1 Ge2A Ge1 97.70(14) . .
Rh1 Ge2A Ge1 97.70(14) 28 .
Ge2B Ge2A Ge1 76.72(11) 26 .
Ge2B Ge2A Ge2A 129.7(5) . 30
Ge2A Ge2A Ge2A 114.31(11) 26 30
Rh1 Ge2A Ge2A 98.1(2) . 30
Rh1 Ge2A Ge2A 53.81(10) 28 30
Ge2B Ge2A Ge2A 125.86(11) 26 30
Ge1 Ge2A Ge2A 56.73(3) . 30
Ge2B Ge2A Ge2A 129.7(5) . 5
Ge2A Ge2A Ge2A 114.31(11) 26 5
Rh1 Ge2A Ge2A 53.81(10) . 5
Rh1 Ge2A Ge2A 98.1(2) 28 5
Ge2B Ge2A Ge2A 125.86(11) 26 5
Ge1 Ge2A Ge2A 56.73(3) . 5
Ge2A Ge2A Ge2A 47.8(2) 30 5
Ge2B Ge2A Ge2A 121.4(2) . 10
Ge2A Ge2A Ge2A 66.12(11) 26 10
Rh1 Ge2A Ge2A 152.2(2) . 10
Rh1 Ge2A Ge2A 53.81(10) 28 10
Ge2B Ge2A Ge2A 72.48(11) 26 10
Ge1 Ge2A Ge2A 56.73(3) . 10
Ge2A Ge2A Ge2A 60.000(1) 30 10
Ge2A Ge2A Ge2A 99.27(16) 5 10
Ge2B Ge2A Ge2A 121.4(2) . 9
Ge2A Ge2A Ge2A 66.12(11) 26 9
Rh1 Ge2A Ge2A 53.81(10) . 9
Rh1 Ge2A Ge2A 152.2(2) 28 9
Ge2B Ge2A Ge2A 72.48(11) 26 9
Ge1 Ge2A Ge2A 56.73(3) . 9
Ge2A Ge2A Ge2A 99.27(16) 30 9
Ge2A Ge2A Ge2A 60.000(1) 5 9
Ge2A Ge2A Ge2A 109.469(2) 10 9
Ge2B Ge2A Lu1 61.0(3) . .
Ge2A Ge2A Lu1 68.83(8) 26 .
Rh1 Ge2A Lu1 64.93(6) . .
Rh1 Ge2A Lu1 143.9(2) 28 .
Ge2B Ge2A Lu1 60.28(8) 26 .
Ge1 Ge2A Lu1 114.16(12) . .
Ge2A Ge2A Lu1 160.73(15) 30 .
Ge2A Ge2A Lu1 113.06(8) 5 .
Ge2A Ge2A Lu1 132.26(19) 10 .
Ge2A Ge2A Lu1 63.81(12) 9 .
Ge2B Ge2A Lu1 61.0(3) . 25_565
Ge2A Ge2A Lu1 68.83(8) 26 25_565
Rh1 Ge2A Lu1 143.9(2) . 25_565
Rh1 Ge2A Lu1 64.93(6) 28 25_565
Ge2B Ge2A Lu1 60.28(8) 26 25_565
Ge1 Ge2A Lu1 114.16(12) . 25_565
Ge2A Ge2A Lu1 113.06(8) 30 25_565
Ge2A Ge2A Lu1 160.73(15) 5 25_565
Ge2A Ge2A Lu1 63.81(12) 10 25_565
Ge2A Ge2A Lu1 132.26(19) 9 25_565
Lu1 Ge2A Lu1 86.01(12) . 25_565
Ge2A Ge2B Rh1 80.0(2) . .
Ge2A Ge2B Rh1 80.0(2) . 28
Rh1 Ge2B Rh1 126.33(10) . 28
Ge2A Ge2B Ge2A 58.0(5) . 26
Rh1 Ge2B Ge2A 105.17(6) . 26
Rh1 Ge2B Ge2A 105.17(6) 28 26
Ge2A Ge2B Ge2B 136.4(3) . 14
Rh1 Ge2B Ge2B 57.40(8) . 14
Rh1 Ge2B Ge2B 116.34(12) 28 14
Ge2A Ge2B Ge2B 137.38(11) 26 14
Ge2A Ge2B Ge2B 136.4(3) . 13_455
Rh1 Ge2B Ge2B 116.34(12) . 13_455
Rh1 Ge2B Ge2B 57.40(8) 28 13_455
Ge2A Ge2B Ge2B 137.38(11) 26 13_455
Ge2B Ge2B Ge2B 66.81(9) 14 13_455
Ge2A Ge2B Ge2B 71.1(5) . 26
Rh1 Ge2B Ge2B 109.76(6) . 26
Rh1 Ge2B Ge2B 109.76(6) 28 26
Ge2A Ge2B Ge2B 13.09(9) 26 26
Ge2B Ge2B Ge2B 128.87(9) 14 26
Ge2B Ge2B Ge2B 128.87(9) 13_455 26
Ge2A Ge2B Lu1 108.4(4) . .
Rh1 Ge2B Lu1 69.045(16) . .
Rh1 Ge2B Lu1 164.24(9) 28 .
Ge2A Ge2B Lu1 70.36(10) 26 .
Ge2B Ge2B Lu1 67.07(8) 14 .
Ge2B Ge2B Lu1 115.14(7) 13_455 .
Ge2B Ge2B Lu1 62.65(5) 26 .
Ge2A Ge2B Lu1 108.4(4) . 25_565
Rh1 Ge2B Lu1 164.24(9) . 25_565
Rh1 Ge2B Lu1 69.045(16) 28 25_565
Ge2A Ge2B Lu1 70.36(10) 26 25_565
Ge2B Ge2B Lu1 115.14(7) 14 25_565
Ge2B Ge2B Lu1 67.07(8) 13_455 25_565
Ge2B Ge2B Lu1 62.65(5) 26 25_565
Lu1 Ge2B Lu1 95.41(7) . 25_565
Ge2A Ge2B Lu1 95.3(5) . 5
Rh1 Ge2B Lu1 66.47(5) . 5
Rh1 Ge2B Lu1 66.47(5) 28 5
Ge2A Ge2B Lu1 153.25(10) 26 5
Ge2B Ge2B Lu1 61.33(9) 14 5
Ge2B Ge2B Lu1 61.33(8) 13_455 5
Ge2B Ge2B Lu1 166.34(6) 26 5
Lu1 Ge2B Lu1 124.23(6) . 5
Lu1 Ge2B Lu1 124.23(6) 25_565 5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Lu1 Ge2B 2.9966(16) .
Lu1 Ge2B 2.9966(16) 17
Lu1 Ge2B 2.9966(16) 26
Lu1 Ge2B 2.9966(16) 42_666
Lu1 Ge2B 2.9966(16) 18_554
Lu1 Ge2B 2.9966(16) 25_565
Lu1 Ge2B 2.9966(16) 41_665
Lu1 Ge2B 2.9966(16) 2_565
Lu1 Rh1 3.13457(18) 26
Lu1 Rh1 3.13457(18) 27_565
Lu1 Rh1 3.13457(18) .
Lu1 Rh1 3.13457(18) 4_565
Rh1 Ge2A 2.4543(19) .
Rh1 Ge2A 2.4543(19) 45_666
Rh1 Ge2A 2.4543(19) 42_666
Rh1 Ge2A 2.4543(19) 14
Rh1 Ge2A 2.4543(19) 9
Rh1 Ge2A 2.4543(19) 5
Rh1 Ge2B 2.4839(11) 45_666
Rh1 Ge2B 2.4839(11) 42_666
Rh1 Ge2B 2.4839(11) 14
Rh1 Ge2B 2.4839(11) 9
Rh1 Ge2B 2.4839(11) 5
Rh1 Ge2B 2.4839(11) .
Ge1 Ge2A 2.641(6) .
Ge1 Ge2A 2.641(6) 33
Ge1 Ge2A 2.641(6) 9
Ge1 Ge2A 2.641(6) 29
Ge1 Ge2A 2.641(6) 5
Ge1 Ge2A 2.641(6) 25
Ge1 Ge2A 2.641(6) 34
Ge1 Ge2A 2.641(6) 6
Ge1 Ge2A 2.641(6) 30
Ge1 Ge2A 2.641(6) 10
Ge1 Ge2A 2.641(6) 2
Ge1 Ge2A 2.641(6) 26
Ge2A Ge2B 0.627(4) .
Ge2A Ge2A 2.347(9) 26
Ge2A Rh1 2.4543(19) 28
Ge2A Ge2B 2.618(4) 26
Ge2A Ge2A 2.898(7) 30
Ge2A Ge2A 2.898(7) 5
Ge2A Ge2A 2.898(7) 10
Ge2A Ge2A 2.898(7) 9
Ge2A Lu1 3.250(4) 25_565
Ge2B Rh1 2.4839(11) 28
Ge2B Ge2A 2.618(4) 26
Ge2B Ge2B 2.677(5) 14
Ge2B Ge2B 2.677(5) 13_455
Ge2B Ge2B 2.753(5) 26
Ge2B Lu1 2.9966(16) 25_565
Ge2B Lu1 3.145(2) 5
#BEGIN Loops that were not found in dictionaries:
loop_
_publcif_info_datablock.id
_publcif_info_datablock.publ_exptl
_publcif_info_datablock.publ_geom
_publcif_info_datablock.structure
{ff9adc97-e1f9-4016-8756-d3a9d9d0c165} y y y
#END Loops that were not found in dictionaries
