#------------------------------------------------------------------------------
#$Date: 2017-01-27 16:16:14 +0200 (Fri, 27 Jan 2017) $
#$Revision: 191028 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/03/08/4030873.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4030873
loop_
_publ_author_name
'Flacke, F.'
'Jacobs, H.'
_publ_section_title
;
 [Li(NH3)4][Sn(SnPh3)3].C6H6, crystal structure of a stannide with
 trigonal pyramidal tin skeleton
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              495
_journal_page_last               501
_journal_volume                  34
_journal_year                    1997
_chemical_formula_sum            'C60 H63 Li N4 Sn4'
_chemical_formula_weight         1321.97
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                78.84(1)
_cell_angle_beta                 89.58(1)
_cell_angle_gamma                73.37(2)
_cell_formula_units_Z            2
_cell_length_a                   12.305(3)
_cell_length_b                   12.421(3)
_cell_length_c                   20.448(2)
_cell_volume                     2934.1(11)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.861
_exptl_crystal_density_diffrn    1.496
_refine_ls_number_parameters     575
_refine_ls_number_reflns         4082
_refine_ls_R_factor_gt           0.066
_refine_ls_wR_factor_gt          0.155
_cod_data_source_file            EJSSIC-1997-34-495-501.cif
_cod_data_source_block           stannide
_cod_depositor_comments
;
 Changing atom parameters to '?' to indicate that atomic coordinates
 for this entry are unknown.

 Antanas Vaitkus,
 2017-01-27

Atomic coordinates exclusively deposited to CCDC entry 179-100185
;
_cod_original_cell_volume        2934.09
_cod_original_formula_sum        'C60 H63 Li1 N4 Sn4'
_cod_database_code               4030873
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 x,y,z
2 -x,-y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
? ? ? ? ? ?
