#------------------------------------------------------------------------------
#$Date: 2016-03-21 07:12:46 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178553 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/61/4066163.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4066163
loop_
_publ_author_name
'Takao, Toshiro'
'Moriya, Makoto'
'Kajigaya, Mana'
'Suzuki, Hiroharu'
_publ_section_title
;
 Direct Arylation of a Cluster-Bound Alkyne Ligand with Benzene†
;
_journal_issue                   21
_journal_name_full               Organometallics
_journal_page_first              4770
_journal_paper_doi               10.1021/om100329r
_journal_volume                  29
_journal_year                    2010
_chemical_formula_sum            'C40 H54 Ru3'
_chemical_formula_weight         838.04
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 103.33(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.418(11)
_cell_length_b                   18.059(7)
_cell_length_c                   11.485(6)
_cell_measurement_reflns_used    13472
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      25.02
_cell_measurement_theta_min      3.30
_cell_volume                     3515(3)
_computing_cell_refinement       'PROCESS-AUTO (T.Higashi, 1998)'
_computing_data_collection       'PROCESS-AUTO (T.Higashi, 1998)'
_computing_data_reduction        'PROCESS-AUTO (T.Higashi, 1998)'
_computing_molecular_graphics    'ORTEX (P.McArdle, 1995)'
_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      153(2)
_diffrn_detector_area_resol_mean 100
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID Imaging Plate'
_diffrn_measurement_method       'oscillation photograph'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku Rotating Anode ultraX18'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0806
_diffrn_reflns_av_sigmaI/netI    0.0483
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            13472
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         3.30
_exptl_absorpt_coefficient_mu    1.299
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.9017
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'ABSCOR (T.Higashi, 2001)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.583
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       unknown
_exptl_crystal_F_000             1704
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.100
_refine_diff_density_max         0.910
_refine_diff_density_min         -0.693
_refine_diff_density_rms         0.138
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     213
_refine_ls_number_reflns         3193
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.030
_refine_ls_R_factor_all          0.0531
_refine_ls_R_factor_gt           0.0420
_refine_ls_shift/su_max          0.065
_refine_ls_shift/su_mean         0.003
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0679P)²+15.8109P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1106
_refine_ls_wR_factor_ref         0.1176
_reflns_number_gt                2685
_reflns_number_total             3197
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om100329r_si_001.cif
_cod_data_source_block           7
_cod_depositor_comments
;
The following automatic conversions were performed:
'_atom_site_symetry_multiplicity' tag replaced with
'_atom_site_symmetry_multiplicity'.

Automatic conversion script
Id: cif_correct_tags 1440 2010-10-19 06:21:57Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      C2/m
_cod_database_code               4066163
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
'-x, -y, -z'
'-x, y, -z'
'-x+1/2, -y+1/2, -z'
'-x+1/2, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ru1 Ru 0.76976(2) 0.42580(2) 0.72092(3) 0.01810(16) Uani 1 1 d .
Ru2 Ru 0.66540(3) 0.5000 0.81871(5) 0.01846(17) Uani 1 2 d S
C1 C 0.6837(4) 0.5000 0.6566(6) 0.0197(14) Uani 1 2 d S
H1 H 0.647(5) 0.5000 0.576(9) 0.03(2) Uiso 1 2 d S
C4 C 0.9345(5) 0.5000 0.8559(8) 0.0295(17) Uani 1 2 d S
H4A H 0.954(4) 0.5000 0.786(7) 0.007(16) Uiso 1 2 d S
H4B H 0.959(4) 0.461(4) 0.914(7) 0.05(2) Uiso 1 1 d .
C2 C 0.8461(4) 0.5000 0.8061(6) 0.0206(15) Uani 1 2 d S
C3 C 0.7867(4) 0.5000 0.8781(6) 0.0207(15) Uani 1 2 d S
C5 C 0.8188(4) 0.5000 1.0091(7) 0.0246(16) Uani 1 2 d S
C6 C 0.8352(3) 0.4339(3) 1.0726(5) 0.0313(13) Uani 1 1 d .
H6 H 0.822(4) 0.389(4) 1.023(6) 0.043(19) Uiso 1 1 d .
C7 C 0.8679(4) 0.4338(4) 1.1951(6) 0.0407(16) Uani 1 1 d .
H7 H 0.8786 0.3881 1.2367 0.07(3) Uiso 1 1 calc R
C8 C 0.8848(5) 0.5000 1.2566(7) 0.037(2) Uani 1 2 d S
H8 H 0.9079 0.5000 1.3401 0.10(5) Uiso 1 2 calc SR
C9 C 0.7653(4) 0.3016(3) 0.7292(5) 0.0289(12) Uani 1 1 d .
C10 C 0.7177(4) 0.3249(3) 0.6170(5) 0.0283(12) Uani 1 1 d .
C11 C 0.7668(4) 0.3625(3) 0.5527(5) 0.0353(14) Uani 1 1 d .
C12 C 0.8449(4) 0.3612(3) 0.6225(7) 0.0406(16) Uani 1 1 d .
C13 C 0.8444(4) 0.3234(3) 0.7320(6) 0.0390(15) Uani 1 1 d .
C14 C 0.7387(5) 0.2559(4) 0.8219(6) 0.0463(17) Uani 1 1 d .
H14A H 0.7668 0.2720 0.9020 0.042(19) Uiso 1 1 calc R
H14B H 0.7502 0.2036 0.8110 0.022(14) Uiso 1 1 calc R
H14C H 0.6818 0.2624 0.8134 2(2) Uiso 1 1 calc R
C15 C 0.6323(4) 0.3067(4) 0.5674(7) 0.0486(18) Uani 1 1 d .
H15A H 0.6044 0.3512 0.5311 0.06(2) Uiso 1 1 calc R
H15B H 0.6087 0.2893 0.6321 0.13(5) Uiso 1 1 calc R
H15C H 0.6279 0.2679 0.5066 0.10(4) Uiso 1 1 calc R
C16 C 0.7402(7) 0.3915(4) 0.4269(7) 0.069(3) Uani 1 1 d .
H16A H 0.7733 0.3703 0.3770 0.12(4) Uiso 1 1 calc R
H16B H 0.7449 0.4456 0.4275 0.13(5) Uiso 1 1 calc R
H16C H 0.6850 0.3776 0.3944 0.20(8) Uiso 1 1 calc R
C17 C 0.9162(6) 0.3890(5) 0.5841(12) 0.082(4) Uani 1 1 d .
H17A H 0.9033 0.4355 0.5399 0.13(5) Uiso 1 1 calc R
H17B H 0.9330 0.3522 0.5325 0.12(4) Uiso 1 1 calc R
H17C H 0.9590 0.3976 0.6548 0.20(8) Uiso 1 1 calc R
C18 C 0.9144(5) 0.3032(4) 0.8296(10) 0.076(3) Uani 1 1 d .
H18A H 0.9036 0.3151 0.9075 0.07(3) Uiso 1 1 calc R
H18B H 0.9606 0.3312 0.8193 0.10(4) Uiso 1 1 calc R
H18C H 0.9249 0.2501 0.8258 0.10(3) Uiso 1 1 calc R
C19 C 0.6075(3) 0.4808(2) 0.9764(5) 0.020(2) Uiso 0.50 1 d PG
C20 C 0.5916(3) 0.5547(2) 0.9326(5) 0.026(2) Uiso 0.50 1 d PG
C21 C 0.5476(3) 0.5504(3) 0.8112(5) 0.022(2) Uiso 0.50 1 d PG
C22 C 0.5364(3) 0.4738(3) 0.7800(5) 0.031(3) Uiso 0.50 1 d PG
C23 C 0.5734(3) 0.4308(3) 0.8821(5) 0.028(2) Uiso 0.50 1 d PG
C24 C 0.6528(5) 0.4592(3) 1.1013(7) 0.047(3) Uiso 0.50 1 d PG
C25 C 0.6169(5) 0.6254(4) 1.0029(6) 0.049(3) Uiso 0.50 1 d PG
C26 C 0.5179(5) 0.6157(4) 0.7297(7) 0.046(3) Uiso 0.50 1 d PG
C27 C 0.4927(5) 0.4435(4) 0.6594(7) 0.057(4) Uiso 0.50 1 d PG
C28 C 0.5761(5) 0.3468(4) 0.8891(7) 0.062(4) Uiso 0.50 1 d PG
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C2 Ru1 C1 95.1(2) . .
C2 Ru1 C3 40.4(3) . .
C1 Ru1 C3 81.1(2) . .
C2 Ru1 C11 130.7(3) . .
C1 Ru1 C11 99.0(3) . .
C3 Ru1 C11 170.8(2) . .
C2 Ru1 C12 101.4(3) . .
C1 Ru1 C12 129.1(3) . .
C3 Ru1 C12 138.0(3) . .
C11 Ru1 C12 36.7(3) . .
C2 Ru1 C13 102.4(2) . .
C1 Ru1 C13 159.7(2) . .
C3 Ru1 C13 119.1(2) . .
C11 Ru1 C13 61.7(2) . .
C12 Ru1 C13 37.2(3) . .
C2 Ru1 C9 132.9(2) . .
C1 Ru1 C9 130.4(2) . .
C3 Ru1 C9 124.70(18) . .
C11 Ru1 C9 62.1(2) . .
C12 Ru1 C9 62.1(2) . .
C13 Ru1 C9 37.0(2) . .
C2 Ru1 C10 162.2(2) . .
C1 Ru1 C10 99.7(2) . .
C3 Ru1 C10 152.2(2) . .
C11 Ru1 C10 37.0(2) . .
C12 Ru1 C10 61.5(2) . .
C13 Ru1 C10 61.4(2) . .
C9 Ru1 C10 37.0(2) . .
C2 Ru1 Ru1 47.40(14) . 2_565
C1 Ru1 Ru1 48.44(14) . 2_565
C3 Ru1 Ru1 52.73(11) . 2_565
C11 Ru1 Ru1 120.74(15) . 2_565
C12 Ru1 Ru1 121.32(15) . 2_565
C13 Ru1 Ru1 145.39(17) . 2_565
C9 Ru1 Ru1 176.53(15) . 2_565
C10 Ru1 Ru1 144.05(15) . 2_565
C2 Ru1 Ru2 84.2(2) . .
C1 Ru1 Ru2 46.3(2) . .
C3 Ru1 Ru2 48.42(19) . .
C11 Ru1 Ru2 136.80(19) . .
C12 Ru1 Ru2 173.5(2) . .
C13 Ru1 Ru2 145.12(19) . .
C9 Ru1 Ru2 116.37(15) . .
C10 Ru1 Ru2 113.23(16) . .
Ru1 Ru1 Ru2 60.28(2) 2_565 .
C1 Ru2 C3 86.3(3) . .
C1 Ru2 C21 108.3(2) . 2_565
C3 Ru2 C21 151.14(17) . 2_565
C1 Ru2 C21 108.3(2) . .
C3 Ru2 C21 151.14(17) . .
C21 Ru2 C21 48.2(2) 2_565 .
C1 Ru2 C22 100.8(3) . 2_565
C3 Ru2 C22 165.80(16) . 2_565
C21 Ru2 C22 37.34(12) 2_565 2_565
C21 Ru2 C22 14.67(19) . 2_565
C1 Ru2 C22 100.8(3) . .
C3 Ru2 C22 165.80(16) . .
C21 Ru2 C22 14.67(17) 2_565 .
C21 Ru2 C22 37.34(10) . .
C22 Ru2 C22 24.4(2) 2_565 .
C1 Ru2 C20 142.0(2) . 2_565
C3 Ru2 C20 118.9(2) . 2_565
C21 Ru2 C20 37.13(12) 2_565 2_565
C21 Ru2 C20 63.84(18) . 2_565
C22 Ru2 C20 61.87(15) 2_565 2_565
C22 Ru2 C20 49.02(13) . 2_565
C1 Ru2 C20 142.00(19) . .
C3 Ru2 C20 118.9(2) . .
C21 Ru2 C20 63.84(18) 2_565 .
C21 Ru2 C20 37.13(10) . .
C22 Ru2 C20 49.02(15) 2_565 .
C22 Ru2 C20 61.87(15) . .
C20 Ru2 C20 51.8(2) 2_565 .
C1 Ru2 C23 125.7(2) . 2_565
C3 Ru2 C23 129.45(19) . 2_565
C21 Ru2 C23 61.77(15) 2_565 2_565
C21 Ru2 C23 23.02(8) . 2_565
C22 Ru2 C23 36.90(11) 2_565 2_565
C22 Ru2 C23 55.37(17) . 2_565
C20 Ru2 C23 61.27(15) 2_565 2_565
C20 Ru2 C23 16.43(8) . 2_565
C1 Ru2 C23 125.7(2) . .
C3 Ru2 C23 129.45(19) . .
C21 Ru2 C23 23.02(12) 2_565 .
C21 Ru2 C23 61.77(15) . .
C22 Ru2 C23 55.4(2) 2_565 .
C22 Ru2 C23 36.90(10) . .
C20 Ru2 C23 16.43(11) 2_565 .
C20 Ru2 C23 61.27(15) . .
C23 Ru2 C23 66.47(19) 2_565 .
C1 Ru2 C19 161.4(2) . 2_565
C3 Ru2 C19 110.0(2) . 2_565
C21 Ru2 C19 61.54(15) 2_565 2_565
C21 Ru2 C19 53.14(15) . 2_565
C22 Ru2 C19 61.39(15) 2_565 2_565
C22 Ru2 C19 65.48(17) . 2_565
C20 Ru2 C19 36.58(10) 2_565 2_565
C20 Ru2 C19 20.79(19) . 2_565
C23 Ru2 C19 36.45(12) 2_565 2_565
C23 Ru2 C19 50.3(2) . 2_565
C1 Ru2 C19 161.4(2) . .
C3 Ru2 C19 110.0(2) . .
C21 Ru2 C19 53.14(14) 2_565 .
C21 Ru2 C19 61.54(15) . .
C22 Ru2 C19 65.48(16) 2_565 .
C22 Ru2 C19 61.39(15) . .
C20 Ru2 C19 20.79(16) 2_565 .
C20 Ru2 C19 36.58(10) . .
C23 Ru2 C19 50.30(17) 2_565 .
C23 Ru2 C19 36.45(10) . .
C19 Ru2 C19 17.4(2) 2_565 .
Ru2 C1 Ru1 85.5(3) . 2_565
Ru2 C1 Ru1 85.5(3) . .
Ru1 C1 Ru1 83.1(3) 2_565 .
C3 C2 C4 125.2(6) . .
C3 C2 Ru1 78.4(4) . .
C4 C2 Ru1 134.0(2) . .
C3 C2 Ru1 78.4(4) . 2_565
C4 C2 Ru1 134.0(2) . 2_565
Ru1 C2 Ru1 85.2(3) . 2_565
C2 C3 C5 115.0(6) . .
C2 C3 Ru2 128.0(5) . .
C5 C3 Ru2 117.0(5) . .
C2 C3 Ru1 61.2(3) . .
C5 C3 Ru1 141.05(19) . .
Ru2 C3 Ru1 78.3(2) . .
C2 C3 Ru1 61.2(3) . 2_565
C5 C3 Ru1 141.05(19) . 2_565
Ru2 C3 Ru1 78.3(2) . 2_565
Ru1 C3 Ru1 74.5(2) . 2_565
C6 C5 C6 117.8(7) . 2_565
C6 C5 C3 121.1(4) . .
C6 C5 C3 121.1(4) 2_565 .
C7 C6 C5 121.2(6) . .
C8 C7 C6 120.2(6) . .
C7 C8 C7 119.3(8) . 2_565
C13 C9 C10 107.2(5) . .
C13 C9 C14 126.2(6) . .
C10 C9 C14 126.3(6) . .
C13 C9 Ru1 71.5(3) . .
C10 C9 Ru1 71.7(3) . .
C14 C9 Ru1 126.7(4) . .
C11 C10 C9 108.4(5) . .
C11 C10 C15 124.6(6) . .
C9 C10 C15 126.7(6) . .
C11 C10 Ru1 70.9(3) . .
C9 C10 Ru1 71.4(3) . .
C15 C10 Ru1 128.4(4) . .
C12 C11 C10 108.2(5) . .
C12 C11 C16 126.4(7) . .
C10 C11 C16 125.1(7) . .
C12 C11 Ru1 72.0(3) . .
C10 C11 Ru1 72.1(3) . .
C16 C11 Ru1 126.3(4) . .
C11 C12 C13 107.8(5) . .
C11 C12 C17 125.7(8) . .
C13 C12 C17 126.3(8) . .
C11 C12 Ru1 71.2(3) . .
C13 C12 Ru1 71.5(3) . .
C17 C12 Ru1 126.4(5) . .
C9 C13 C12 108.3(6) . .
C9 C13 C18 124.4(7) . .
C12 C13 C18 127.1(7) . .
C9 C13 Ru1 71.5(3) . .
C12 C13 Ru1 71.3(3) . .
C18 C13 Ru1 127.1(5) . .
C19 C19 C20 141.2(4) 2_565 2_565
C19 C19 C20 21.13(11) 2_565 .
C20 C19 C20 120.1(4) 2_565 .
C19 C19 C23 129.13(12) 2_565 .
C20 C19 C23 12.1(4) 2_565 .
C20 C19 C23 108.0 . .
C19 C19 C24 104.87(12) 2_565 .
C20 C19 C24 113.9(4) 2_565 .
C20 C19 C24 126.0 . .
C23 C19 C24 126.0 . .
C19 C19 C24 53.6(2) 2_565 2_565
C20 C19 C24 165.2(6) 2_565 2_565
C20 C19 C24 74.7(3) . 2_565
C23 C19 C24 177.3(3) . 2_565
C24 C19 C24 51.3(3) . 2_565
C19 C19 C25 170.83(11) 2_565 2_565
C20 C19 C25 48.0(4) 2_565 2_565
C20 C19 C25 168.04(6) . 2_565
C23 C19 C25 60.04(7) . 2_565
C24 C19 C25 65.96(6) . 2_565
C24 C19 C25 117.2(3) 2_565 2_565
C19 C19 C23 34.81(19) 2_565 2_565
C20 C19 C23 106.4(3) 2_565 2_565
C20 C19 C23 13.68(16) . 2_565
C23 C19 C23 94.32(16) . 2_565
C24 C19 C23 139.68(16) . 2_565
C24 C19 C23 88.4(4) 2_565 2_565
C25 C19 C23 154.36(17) 2_565 2_565
C19 C19 C21 106.2(2) 2_565 2_565
C20 C19 C21 35.0(2) 2_565 2_565
C20 C19 C21 85.0(2) . 2_565
C23 C19 C21 23.0(2) . 2_565
C24 C19 C21 149.0(2) . 2_565
C24 C19 C21 159.8(4) 2_565 2_565
C25 C19 C21 83.0(3) 2_565 2_565
C23 C19 C21 71.3(2) 2_565 2_565
C19 C19 Ru2 81.31(11) 2_565 .
C20 C19 Ru2 77.5(2) 2_565 .
C20 C19 Ru2 70.53(18) . .
C23 C19 Ru2 71.23(19) . .
C24 C19 Ru2 123.87(17) . .
C24 C19 Ru2 110.0(3) 2_565 .
C25 C19 Ru2 103.67(19) 2_565 .
C23 C19 Ru2 64.47(17) 2_565 .
C21 C19 Ru2 61.78(19) 2_565 .
C23 C20 C19 152.6(10) 2_565 2_565
C23 C20 C21 26.9(7) 2_565 .
C19 C20 C21 125.7(3) 2_565 .
C23 C20 C19 134.9(7) 2_565 .
C19 C20 C19 17.7(3) 2_565 .
C21 C20 C19 108.0 . .
C23 C20 C25 99.1(7) 2_565 .
C19 C20 C25 108.3(3) 2_565 .
C21 C20 C25 126.0 . .
C19 C20 C25 126.0 . .
C23 C20 C28 50.2(6) 2_565 2_565
C19 C20 C28 157.2(4) 2_565 2_565
C21 C20 C28 77.11(12) . 2_565
C19 C20 C28 174.88(12) . 2_565
C25 C20 C28 48.89(12) . 2_565
C23 C20 C22 39.8(6) 2_565 2_565
C19 C20 C22 112.8(6) 2_565 2_565
C21 C20 C22 12.9(3) . 2_565
C19 C20 C22 95.1(3) . 2_565
C25 C20 C22 138.9(3) . 2_565
C28 C20 C22 90.0(2) 2_565 2_565
C23 C20 C20 113.8(7) 2_565 2_565
C19 C20 C20 38.8(3) 2_565 2_565
C21 C20 C20 86.9 . 2_565
C19 C20 C20 21.1 . 2_565
C25 C20 C20 147.1 . 2_565
C28 C20 C20 163.98(12) 2_565 2_565
C22 C20 C20 74.0(3) 2_565 2_565
C23 C20 C24 163.4(10) 2_565 2_565
C19 C20 C24 44.0(2) 2_565 2_565
C21 C20 C24 169.7(4) . 2_565
C19 C20 C24 61.7(4) . 2_565
C25 C20 C24 64.3(4) . 2_565
C28 C20 C24 113.2(4) 2_565 2_565
C22 C20 C24 156.8(5) 2_565 2_565
C20 C20 C24 82.8(4) 2_565 2_565
C23 C20 Ru2 83.2(4) 2_565 .
C19 C20 Ru2 81.7(4) 2_565 .
C21 C20 Ru2 70.14(18) . .
C19 C20 Ru2 72.89(18) . .
C25 C20 Ru2 122.64(18) . .
C28 C20 Ru2 109.26(17) 2_565 .
C22 C20 Ru2 64.8(2) 2_565 .
C20 C20 Ru2 64.12(18) 2_565 .
C24 C20 Ru2 105.0(3) 2_565 .
C22 C21 C23 152.2(11) 2_565 2_565
C22 C21 C20 133.2(6) 2_565 .
C23 C21 C20 19.0(5) 2_565 .
C22 C21 C22 25.2(6) 2_565 .
C23 C21 C22 127.0(5) 2_565 .
C20 C21 C22 108.0 . .
C22 C21 C26 100.8(6) 2_565 .
C23 C21 C26 107.0(5) 2_565 .
C20 C21 C26 126.0 . .
C22 C21 C26 126.0 . .
C22 C21 C27 53.5(2) 2_565 2_565
C23 C21 C27 154.3(9) 2_565 2_565
C20 C21 C27 173.3(4) . 2_565
C22 C21 C27 78.7(4) . 2_565
C26 C21 C27 47.3(4) . 2_565
C22 C21 C21 40.1(6) 2_565 2_565
C23 C21 C21 112.2(5) 2_565 2_565
C20 C21 C21 93.1 . 2_565
C22 C21 C21 14.9 . 2_565
C26 C21 C21 140.9 . 2_565
C27 C21 C21 93.6(4) 2_565 2_565
C22 C21 C19 113.9(7) 2_565 2_565
C23 C21 C19 38.3(4) 2_565 2_565
C20 C21 C19 19.3(2) . 2_565
C22 C21 C19 88.7(2) . 2_565
C26 C21 C19 145.3(2) . 2_565
C27 C21 C19 167.4(5) 2_565 2_565
C21 C21 C19 73.8(2) 2_565 2_565
C22 C21 Ru2 83.7(4) 2_565 .
C23 C21 Ru2 81.7(3) 2_565 .
C20 C21 Ru2 72.73(19) . .
C22 C21 Ru2 71.72(19) . .
C26 C21 Ru2 121.29(18) . .
C27 C21 Ru2 110.1(3) 2_565 .
C21 C21 Ru2 65.91(19) 2_565 .
C19 C21 Ru2 65.1(2) 2_565 .
C21 C22 C22 139.9(6) 2_565 2_565
C21 C22 C23 17.1(6) 2_565 .
C22 C22 C23 122.9 2_565 .
C21 C22 C21 125.1(6) 2_565 .
C22 C22 C21 14.9 2_565 .
C23 C22 C21 108.0 . .
C21 C22 C27 108.9(6) 2_565 .
C22 C22 C27 111.1 2_565 .
C23 C22 C27 126.0 . .
C21 C22 C27 126.0 . .
C21 C22 C26 60.2(7) 2_565 2_565
C22 C22 C26 159.87(16) 2_565 2_565
C23 C22 C26 77.26(16) . 2_565
C21 C22 C26 174.74(16) . 2_565
C27 C22 C26 48.74(16) . 2_565
C21 C22 C20 33.9(4) 2_565 2_565
C22 C22 C20 106.0(3) 2_565 2_565
C23 C22 C20 16.9(3) . 2_565
C21 C22 C20 91.1(3) . 2_565
C27 C22 C20 142.9(3) . 2_565
C26 C22 C20 94.1(4) 2_565 2_565
C21 C22 Ru2 81.6(3) 2_565 .
C22 C22 Ru2 77.81(18) 2_565 .
C23 C22 Ru2 73.08(18) . .
C21 C22 Ru2 70.93(18) . .
C27 C22 Ru2 121.70(18) . .
C26 C22 Ru2 111.5(2) 2_565 .
C20 C22 Ru2 66.1(2) 2_565 .
C20 C23 C21 134.1(12) 2_565 2_565
C20 C23 C22 123.4(7) 2_565 .
C21 C23 C22 10.7(5) 2_565 .
C20 C23 C19 15.4(7) 2_565 .
C21 C23 C19 118.7(5) 2_565 .
C22 C23 C19 108.0 . .
C20 C23 C28 110.6(7) 2_565 .
C21 C23 C28 115.3(5) 2_565 .
C22 C23 C28 126.0 . .
C19 C23 C28 126.0 . .
C20 C23 C25 59.4(4) 2_565 2_565
C21 C23 C25 166.6(8) 2_565 2_565
C22 C23 C25 177.3(4) . 2_565
C19 C23 C25 74.7(4) . 2_565
C28 C23 C25 51.3(3) . 2_565
C20 C23 C19 31.4(6) 2_565 2_565
C21 C23 C19 102.7(6) 2_565 2_565
C22 C23 C19 91.94(17) . 2_565
C19 C23 C19 16.06(16) . 2_565
C28 C23 C19 142.06(16) . 2_565
C25 C23 C19 90.8(3) 2_565 2_565
C20 C23 C26 178.6(9) 2_565 2_565
C21 C23 C26 47.2(2) 2_565 2_565
C22 C23 C26 58.0(4) . 2_565
C19 C23 C26 166.0(4) . 2_565
C28 C23 C26 68.0(4) . 2_565
C25 C23 C26 119.3(6) 2_565 2_565
C19 C23 C26 149.9(4) 2_565 2_565
C20 C23 Ru2 80.3(5) 2_565 .
C21 C23 Ru2 75.3(3) 2_565 .
C22 C23 Ru2 70.02(18) . .
C19 C23 Ru2 72.32(19) . .
C28 C23 Ru2 123.30(17) . .
C25 C23 Ru2 111.4(2) 2_565 .
C19 C23 Ru2 65.23(18) 2_565 .
C26 C23 Ru2 100.7(2) 2_565 .
C24 C24 C19 75.1 2_565 .
C24 C24 C19 53.6(2) 2_565 2_565
C19 C24 C19 21.5(2) . 2_565
C24 C24 C25 142.8(2) 2_565 2_565
C19 C24 C25 67.7(2) . 2_565
C19 C24 C25 89.19(19) 2_565 2_565
C24 C24 C20 97.2(2) 2_565 2_565
C19 C24 C20 22.1(2) . 2_565
C19 C24 C20 43.60(12) 2_565 2_565
C25 C24 C20 45.59(10) 2_565 2_565
C28 C25 C20 77.7(5) 2_565 .
C28 C25 C23 56.2(3) 2_565 2_565
C20 C25 C23 21.5(2) . 2_565
C28 C25 C24 147.8(7) 2_565 2_565
C20 C25 C24 70.1(2) . 2_565
C23 C25 C24 91.6(4) 2_565 2_565
C28 C25 C19 101.4(5) 2_565 2_565
C20 C25 C19 23.70(7) . 2_565
C23 C25 C19 45.2(2) 2_565 2_565
C24 C25 C19 46.4(3) 2_565 2_565
C27 C26 C21 76.8(4) 2_565 .
C27 C26 C22 57.8(5) 2_565 2_565
C21 C26 C22 19.00(11) . 2_565
C27 C26 C23 102.6(5) 2_565 2_565
C21 C26 C23 25.8(2) . 2_565
C22 C26 C23 44.78(17) 2_565 2_565
C27 C26 C28 147.6(6) 2_565 2_565
C21 C26 C28 70.7(4) . 2_565
C22 C26 C28 89.7(3) 2_565 2_565
C23 C26 C28 44.96(18) 2_565 2_565
C26 C27 C22 73.4(4) 2_565 .
C26 C27 C21 55.86(14) 2_565 2_565
C22 C27 C21 17.6(3) . 2_565
C25 C28 C23 72.5(5) 2_565 .
C25 C28 C20 53.4(4) 2_565 2_565
C23 C28 C20 19.15(8) . 2_565
C25 C28 C26 139.5(8) 2_565 2_565
C23 C28 C26 67.0(4) . 2_565
C20 C28 C26 86.1(4) 2_565 2_565
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ru1 C2 1.980(5) .
Ru1 C1 2.020(6) .
Ru1 C3 2.213(6) .
Ru1 C11 2.235(6) .
Ru1 C12 2.245(6) .
Ru1 C13 2.246(6) .
Ru1 C9 2.247(5) .
Ru1 C10 2.251(5) .
Ru1 Ru1 2.6799(13) 2_565
Ru1 Ru2 2.7024(13) .
Ru2 C1 1.960(7) .
Ru2 C3 2.064(8) .
Ru2 C21 2.228(5) 2_565
Ru2 C21 2.228(5) .
Ru2 C22 2.239(5) 2_565
Ru2 C22 2.239(6) .
Ru2 C20 2.262(5) 2_565
Ru2 C20 2.262(5) .
Ru2 C23 2.279(5) 2_565
Ru2 C23 2.279(5) .
Ru2 C19 2.293(5) 2_565
Ru2 C19 2.293(5) .
C1 Ru1 2.020(6) 2_565
C4 C2 1.514(11) .
C2 C3 1.466(10) .
C2 Ru1 1.980(5) 2_565
C3 C5 1.480(10) .
C3 Ru1 2.213(6) 2_565
C5 C6 1.394(7) .
C5 C6 1.394(7) 2_565
C6 C7 1.390(9) .
C7 C8 1.386(8) .
C8 C7 1.386(8) 2_565
C9 C13 1.425(9) .
C9 C10 1.426(8) .
C9 C14 1.502(8) .
C10 C11 1.425(8) .
C10 C15 1.502(9) .
C11 C12 1.412(10) .
C11 C16 1.506(9) .
C12 C13 1.433(10) .
C12 C17 1.497(9) .
C13 C18 1.500(10) .
C19 C19 0.693(9) 2_565
C19 C20 0.823(6) 2_565
C19 C20 1.430(3) .
C19 C23 1.430(3) .
C19 C24 1.520(3) .
C19 C24 1.825(8) 2_565
C19 C25 1.943(10) 2_565
C19 C23 1.943(6) 2_565
C19 C21 2.023(4) 2_565
C20 C23 0.649(3) 2_565
C20 C19 0.823(7) 2_565
C20 C21 1.430(3) .
C20 C25 1.520(3) .
C20 C28 1.851(10) 2_565
C20 C22 1.867(5) 2_565
C20 C20 1.975(8) 2_565
C20 C24 2.000(5) 2_565
C21 C22 0.570(8) 2_565
C21 C23 0.901(3) 2_565
C21 C22 1.430(3) .
C21 C26 1.520(3) .
C21 C27 1.788(4) 2_565
C21 C21 1.819(8) 2_565
C21 C19 2.023(5) 2_565
C22 C21 0.570(7) 2_565
C22 C22 0.946(9) 2_565
C22 C23 1.430(3) .
C22 C27 1.520(3) .
C22 C26 1.721(11) 2_565
C22 C20 1.867(4) 2_565
C23 C20 0.649(4) 2_565
C23 C21 0.901(5) 2_565
C23 C28 1.520(3) .
C23 C25 1.745(6) 2_565
C23 C19 1.943(8) 2_565
C23 C26 1.980(5) 2_565
C24 C24 1.473(12) 2_565
C24 C19 1.825(7) 2_565
C24 C25 1.918(8) 2_565
C24 C20 2.000(4) 2_565
C25 C28 1.427(3) 2_565
C25 C23 1.745(8) 2_565
C25 C24 1.918(12) 2_565
C25 C19 1.943(9) 2_565
C26 C27 1.350(12) 2_565
C26 C22 1.721(10) 2_565
C26 C23 1.980(7) 2_565
C26 C28 1.995(3) 2_565
C27 C26 1.350(9) 2_565
C27 C21 1.788(4) 2_565
C28 C25 1.427(7) 2_565
C28 C20 1.851(11) 2_565
C28 C26 1.995(8) 2_565
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C3 Ru2 C1 Ru1 -41.72(13) . 2_565
C21 Ru2 C1 Ru1 163.74(16) 2_565 2_565
C21 Ru2 C1 Ru1 112.8(2) . 2_565
C22 Ru2 C1 Ru1 125.87(18) 2_565 2_565
C22 Ru2 C1 Ru1 150.70(17) . 2_565
C20 Ru2 C1 Ru1 -176.6(2) 2_565 2_565
C20 Ru2 C1 Ru1 93.1(4) . 2_565
C23 Ru2 C1 Ru1 95.8(3) 2_565 2_565
C23 Ru2 C1 Ru1 -179.28(16) . 2_565
C19 Ru2 C1 Ru1 110.1(6) 2_565 2_565
C19 Ru2 C1 Ru1 166.5(4) . 2_565
C3 Ru2 C1 Ru1 41.72(13) . .
C21 Ru2 C1 Ru1 -112.8(2) 2_565 .
C21 Ru2 C1 Ru1 -163.74(16) . .
C22 Ru2 C1 Ru1 -150.70(17) 2_565 .
C22 Ru2 C1 Ru1 -125.87(18) . .
C20 Ru2 C1 Ru1 -93.1(4) 2_565 .
C20 Ru2 C1 Ru1 176.6(2) . .
C23 Ru2 C1 Ru1 179.28(16) 2_565 .
C23 Ru2 C1 Ru1 -95.8(3) . .
C19 Ru2 C1 Ru1 -166.5(4) 2_565 .
C19 Ru2 C1 Ru1 -110.1(6) . .
C2 Ru1 C1 Ru2 -76.9(2) . .
C3 Ru1 C1 Ru2 -38.8(2) . .
C11 Ru1 C1 Ru2 150.5(2) . .
C12 Ru1 C1 Ru2 173.9(2) . .
C13 Ru1 C1 Ru2 133.4(7) . .
C9 Ru1 C1 Ru2 89.7(3) . .
C10 Ru1 C1 Ru2 112.9(2) . .
Ru1 Ru1 C1 Ru2 -86.0(2) 2_565 .
C2 Ru1 C1 Ru1 9.1(3) . 2_565
C3 Ru1 C1 Ru1 47.2(2) . 2_565
C11 Ru1 C1 Ru1 -123.5(2) . 2_565
C12 Ru1 C1 Ru1 -100.1(3) . 2_565
C13 Ru1 C1 Ru1 -140.6(6) . 2_565
C9 Ru1 C1 Ru1 175.68(19) . 2_565
C10 Ru1 C1 Ru1 -161.0(2) . 2_565
Ru2 Ru1 C1 Ru1 86.0(2) . 2_565
C1 Ru1 C2 C3 69.8(3) . .
C11 Ru1 C2 C3 176.2(3) . .
C12 Ru1 C2 C3 -158.6(3) . .
C13 Ru1 C2 C3 -120.5(3) . .
C9 Ru1 C2 C3 -96.2(4) . .
C10 Ru1 C2 C3 -143.7(7) . .
Ru1 Ru1 C2 C3 79.1(3) 2_565 .
Ru2 Ru1 C2 C3 24.7(3) . .
C1 Ru1 C2 C4 -162.0(7) . .
C3 Ru1 C2 C4 128.2(8) . .
C11 Ru1 C2 C4 -55.5(8) . .
C12 Ru1 C2 C4 -30.3(7) . .
C13 Ru1 C2 C4 7.7(7) . .
C9 Ru1 C2 C4 32.0(9) . .
C10 Ru1 C2 C4 -15.4(12) . .
Ru1 Ru1 C2 C4 -152.7(8) 2_565 .
Ru2 Ru1 C2 C4 153.0(7) . .
C1 Ru1 C2 Ru1 -9.3(3) . 2_565
C3 Ru1 C2 Ru1 -79.1(3) . 2_565
C11 Ru1 C2 Ru1 97.2(3) . 2_565
C12 Ru1 C2 Ru1 122.3(3) . 2_565
C13 Ru1 C2 Ru1 160.4(2) . 2_565
C9 Ru1 C2 Ru1 -175.3(2) . 2_565
C10 Ru1 C2 Ru1 137.2(6) . 2_565
Ru2 Ru1 C2 Ru1 -54.34(18) . 2_565
C4 C2 C3 C5 0.000(3) . .
Ru1 C2 C3 C5 136.28(12) . .
Ru1 C2 C3 C5 -136.28(12) 2_565 .
C4 C2 C3 Ru2 180.000(2) . .
Ru1 C2 C3 Ru2 -43.72(12) . .
Ru1 C2 C3 Ru2 43.72(12) 2_565 .
C4 C2 C3 Ru1 -136.28(12) . .
Ru1 C2 C3 Ru1 87.4(2) 2_565 .
C4 C2 C3 Ru1 136.28(12) . 2_565
Ru1 C2 C3 Ru1 -87.4(2) . 2_565
C1 Ru2 C3 C2 0.000(2) . .
C21 Ru2 C3 C2 122.3(4) 2_565 .
C21 Ru2 C3 C2 -122.3(4) . .
C22 Ru2 C3 C2 -120.6(9) 2_565 .
C22 Ru2 C3 C2 120.6(9) . .
C20 Ru2 C3 C2 150.09(14) 2_565 .
C20 Ru2 C3 C2 -150.09(14) . .
C23 Ru2 C3 C2 -134.8(2) 2_565 .
C23 Ru2 C3 C2 134.8(2) . .
C19 Ru2 C3 C2 -170.75(12) 2_565 .
C19 Ru2 C3 C2 170.75(12) . .
C1 Ru2 C3 C5 180.000(2) . .
C21 Ru2 C3 C5 -57.7(4) 2_565 .
C21 Ru2 C3 C5 57.7(4) . .
C22 Ru2 C3 C5 59.4(9) 2_565 .
C22 Ru2 C3 C5 -59.4(9) . .
C20 Ru2 C3 C5 -29.91(14) 2_565 .
C20 Ru2 C3 C5 29.91(14) . .
C23 Ru2 C3 C5 45.2(2) 2_565 .
C23 Ru2 C3 C5 -45.2(2) . .
C19 Ru2 C3 C5 9.25(12) 2_565 .
C19 Ru2 C3 C5 -9.25(12) . .
C1 Ru2 C3 Ru1 -38.20(9) . .
C21 Ru2 C3 Ru1 84.1(5) 2_565 .
C21 Ru2 C3 Ru1 -160.5(3) . .
C22 Ru2 C3 Ru1 -158.8(8) 2_565 .
C22 Ru2 C3 Ru1 82.4(9) . .
C20 Ru2 C3 Ru1 111.9(2) 2_565 .
C20 Ru2 C3 Ru1 171.71(14) . .
C23 Ru2 C3 Ru1 -172.98(17) 2_565 .
C23 Ru2 C3 Ru1 96.6(3) . .
C19 Ru2 C3 Ru1 151.05(14) 2_565 .
C19 Ru2 C3 Ru1 132.55(16) . .
C1 Ru2 C3 Ru1 38.20(9) . 2_565
C21 Ru2 C3 Ru1 160.5(4) 2_565 2_565
C21 Ru2 C3 Ru1 -84.1(5) . 2_565
C22 Ru2 C3 Ru1 -82.4(9) 2_565 2_565
C22 Ru2 C3 Ru1 158.8(8) . 2_565
C20 Ru2 C3 Ru1 -171.71(14) 2_565 2_565
C20 Ru2 C3 Ru1 -111.9(2) . 2_565
C23 Ru2 C3 Ru1 -96.6(3) 2_565 2_565
C23 Ru2 C3 Ru1 172.98(17) . 2_565
C19 Ru2 C3 Ru1 -132.55(16) 2_565 2_565
C19 Ru2 C3 Ru1 -151.05(14) . 2_565
C1 Ru1 C3 C2 -108.9(3) . .
C11 Ru1 C3 C2 -18.1(16) . .
C12 Ru1 C3 C2 32.3(4) . .
C13 Ru1 C3 C2 74.2(3) . .
C9 Ru1 C3 C2 117.6(3) . .
C10 Ru1 C3 C2 157.2(4) . .
Ru1 Ru1 C3 C2 -65.3(3) 2_565 .
Ru2 Ru1 C3 C2 -146.2(3) . .
C2 Ru1 C3 C5 -95.0(9) . .
C1 Ru1 C3 C5 156.1(8) . .
C11 Ru1 C3 C5 -113.1(13) . .
C12 Ru1 C3 C5 -62.7(9) . .
C13 Ru1 C3 C5 -20.8(9) . .
C9 Ru1 C3 C5 22.6(9) . .
C10 Ru1 C3 C5 62.2(11) . .
Ru1 Ru1 C3 C5 -160.3(9) 2_565 .
Ru2 Ru1 C3 C5 118.8(8) . .
C2 Ru1 C3 Ru2 146.2(3) . .
C1 Ru1 C3 Ru2 37.32(19) . .
C11 Ru1 C3 Ru2 128.1(14) . .
C12 Ru1 C3 Ru2 178.5(3) . .
C13 Ru1 C3 Ru2 -139.6(2) . .
C9 Ru1 C3 Ru2 -96.2(2) . .
C10 Ru1 C3 Ru2 -56.6(5) . .
Ru1 Ru1 C3 Ru2 80.92(16) 2_565 .
C2 Ru1 C3 Ru1 65.3(3) . 2_565
C1 Ru1 C3 Ru1 -43.6(2) . 2_565
C11 Ru1 C3 Ru1 47.2(15) . 2_565
C12 Ru1 C3 Ru1 97.6(3) . 2_565
C13 Ru1 C3 Ru1 139.5(2) . 2_565
C9 Ru1 C3 Ru1 -177.13(19) . 2_565
C10 Ru1 C3 Ru1 -137.5(4) . 2_565
Ru2 Ru1 C3 Ru1 -80.92(16) . 2_565
C2 C3 C5 C6 -89.3(6) . .
Ru2 C3 C5 C6 90.7(6) . .
Ru1 C3 C5 C6 -14.9(12) . .
Ru1 C3 C5 C6 -163.8(6) 2_565 .
C2 C3 C5 C6 89.3(6) . 2_565
Ru2 C3 C5 C6 -90.7(6) . 2_565
Ru1 C3 C5 C6 163.8(6) . 2_565
Ru1 C3 C5 C6 14.9(12) 2_565 2_565
C6 C5 C6 C7 -0.9(11) 2_565 .
C3 C5 C6 C7 177.8(6) . .
C5 C6 C7 C8 0.0(10) . .
C6 C7 C8 C7 0.9(13) . 2_565
C2 Ru1 C9 C13 -41.9(5) . .
C1 Ru1 C9 C13 156.5(4) . .
C3 Ru1 C9 C13 -93.6(4) . .
C11 Ru1 C9 C13 79.1(4) . .
C12 Ru1 C9 C13 37.3(4) . .
C10 Ru1 C9 C13 116.1(5) . .
Ru1 Ru1 C9 C13 -135(2) 2_565 .
Ru2 Ru1 C9 C13 -149.7(3) . .
C2 Ru1 C9 C10 -158.0(4) . .
C1 Ru1 C9 C10 40.4(5) . .
C3 Ru1 C9 C10 150.3(4) . .
C11 Ru1 C9 C10 -37.0(4) . .
C12 Ru1 C9 C10 -78.7(4) . .
C13 Ru1 C9 C10 -116.1(5) . .
Ru1 Ru1 C9 C10 109(2) 2_565 .
Ru2 Ru1 C9 C10 94.2(3) . .
C2 Ru1 C9 C14 79.9(7) . .
C1 Ru1 C9 C14 -81.7(6) . .
C3 Ru1 C9 C14 28.2(7) . .
C11 Ru1 C9 C14 -159.1(6) . .
C12 Ru1 C9 C14 159.1(6) . .
C13 Ru1 C9 C14 121.8(7) . .
C10 Ru1 C9 C14 -122.1(7) . .
Ru1 Ru1 C9 C14 -13(3) 2_565 .
Ru2 Ru1 C9 C14 -27.9(6) . .
C13 C9 C10 C11 -1.5(6) . .
C14 C9 C10 C11 -176.0(5) . .
Ru1 C9 C10 C11 61.5(4) . .
C13 C9 C10 C15 172.5(6) . .
C14 C9 C10 C15 -1.9(9) . .
Ru1 C9 C10 C15 -124.4(6) . .
C13 C9 C10 Ru1 -63.1(4) . .
C14 C9 C10 Ru1 122.5(6) . .
C2 Ru1 C10 C11 -54.1(9) . .
C1 Ru1 C10 C11 92.0(4) . .
C3 Ru1 C10 C11 -178.8(5) . .
C12 Ru1 C10 C11 -37.4(4) . .
C13 Ru1 C10 C11 -80.0(4) . .
C9 Ru1 C10 C11 -118.0(5) . .
Ru1 Ru1 C10 C11 67.5(5) 2_565 .
Ru2 Ru1 C10 C11 138.4(3) . .
C2 Ru1 C10 C9 63.9(8) . .
C1 Ru1 C10 C9 -149.9(4) . .
C3 Ru1 C10 C9 -60.7(6) . .
C11 Ru1 C10 C9 118.0(5) . .
C12 Ru1 C10 C9 80.6(4) . .
C13 Ru1 C10 C9 38.0(4) . .
Ru1 Ru1 C10 C9 -174.4(3) 2_565 .
Ru2 Ru1 C10 C9 -103.5(3) . .
C2 Ru1 C10 C15 -173.6(7) . .
C1 Ru1 C10 C15 -27.4(6) . .
C3 Ru1 C10 C15 61.8(8) . .
C11 Ru1 C10 C15 -119.5(7) . .
C12 Ru1 C10 C15 -156.9(7) . .
C13 Ru1 C10 C15 160.5(7) . .
C9 Ru1 C10 C15 122.5(7) . .
Ru1 Ru1 C10 C15 -51.9(7) 2_565 .
Ru2 Ru1 C10 C15 19.0(6) . .
C9 C10 C11 C12 1.5(6) . .
C15 C10 C11 C12 -172.6(5) . .
Ru1 C10 C11 C12 63.4(4) . .
C9 C10 C11 C16 175.9(6) . .
C15 C10 C11 C16 1.7(9) . .
Ru1 C10 C11 C16 -122.3(6) . .
C9 C10 C11 Ru1 -61.8(4) . .
C15 C10 C11 Ru1 124.0(6) . .
C2 Ru1 C11 C12 44.2(5) . .
C1 Ru1 C11 C12 148.9(4) . .
C3 Ru1 C11 C12 59.6(15) . .
C13 Ru1 C11 C12 -37.7(4) . .
C9 Ru1 C11 C12 -79.9(4) . .
C10 Ru1 C11 C12 -116.8(5) . .
Ru1 Ru1 C11 C12 102.4(3) 2_565 .
Ru2 Ru1 C11 C12 -179.7(3) . .
C2 Ru1 C11 C10 161.0(3) . .
C1 Ru1 C11 C10 -94.3(4) . .
C3 Ru1 C11 C10 176.4(13) . .
C12 Ru1 C11 C10 116.8(5) . .
C13 Ru1 C11 C10 79.0(4) . .
C9 Ru1 C11 C10 36.9(3) . .
Ru1 Ru1 C11 C10 -140.8(3) 2_565 .
Ru2 Ru1 C11 C10 -62.9(4) . .
C2 Ru1 C11 C16 -78.2(8) . .
C1 Ru1 C11 C16 26.5(8) . .
C3 Ru1 C11 C16 -62.8(18) . .
C12 Ru1 C11 C16 -122.4(9) . .
C13 Ru1 C11 C16 -160.1(8) . .
C9 Ru1 C11 C16 157.7(8) . .
C10 Ru1 C11 C16 120.8(9) . .
Ru1 Ru1 C11 C16 -20.0(8) 2_565 .
Ru2 Ru1 C11 C16 57.9(8) . .
C10 C11 C12 C13 -0.9(6) . .
C16 C11 C12 C13 -175.2(6) . .
Ru1 C11 C12 C13 62.5(4) . .
C10 C11 C12 C17 174.7(6) . .
C16 C11 C12 C17 0.4(10) . .
Ru1 C11 C12 C17 -121.9(6) . .
C10 C11 C12 Ru1 -63.4(4) . .
C16 C11 C12 Ru1 122.3(6) . .
C2 Ru1 C12 C11 -147.4(4) . .
C1 Ru1 C12 C11 -41.1(4) . .
C3 Ru1 C12 C11 -168.1(3) . .
C13 Ru1 C12 C11 117.0(5) . .
C9 Ru1 C12 C11 79.9(4) . .
C10 Ru1 C12 C11 37.7(3) . .
Ru1 Ru1 C12 C11 -100.7(3) 2_565 .
Ru2 Ru1 C12 C11 1.8(17) . .
C2 Ru1 C12 C13 95.6(4) . .
C1 Ru1 C12 C13 -158.1(4) . .
C3 Ru1 C12 C13 74.9(4) . .
C11 Ru1 C12 C13 -117.0(5) . .
C9 Ru1 C12 C13 -37.1(4) . .
C10 Ru1 C12 C13 -79.3(4) . .
Ru1 Ru1 C12 C13 142.3(3) 2_565 .
Ru2 Ru1 C12 C13 -115.2(14) . .
C2 Ru1 C12 C17 -26.3(9) . .
C1 Ru1 C12 C17 80.0(9) . .
C3 Ru1 C12 C17 -47.0(10) . .
C11 Ru1 C12 C17 121.1(10) . .
C13 Ru1 C12 C17 -121.9(10) . .
C9 Ru1 C12 C17 -159.0(10) . .
C10 Ru1 C12 C17 158.8(10) . .
Ru1 Ru1 C12 C17 20.4(10) 2_565 .
Ru2 Ru1 C12 C17 122.8(14) . .
C10 C9 C13 C12 1.0(6) . .
C14 C9 C13 C12 175.4(5) . .
Ru1 C9 C13 C12 -62.2(4) . .
C10 C9 C13 C18 -174.0(6) . .
C14 C9 C13 C18 0.4(10) . .
Ru1 C9 C13 C18 122.8(7) . .
C10 C9 C13 Ru1 63.2(4) . .
C14 C9 C13 Ru1 -122.4(6) . .
C11 C12 C13 C9 0.0(7) . .
C17 C12 C13 C9 -175.6(6) . .
Ru1 C12 C13 C9 62.3(4) . .
C11 C12 C13 C18 174.7(6) . .
C17 C12 C13 C18 -0.8(11) . .
Ru1 C12 C13 C18 -122.9(7) . .
C11 C12 C13 Ru1 -62.4(4) . .
C17 C12 C13 Ru1 122.0(7) . .
C2 Ru1 C13 C9 149.9(4) . .
C1 Ru1 C13 C9 -61.0(9) . .
C3 Ru1 C13 C9 110.1(4) . .
C11 Ru1 C13 C9 -80.3(4) . .
C12 Ru1 C13 C9 -117.6(6) . .
C10 Ru1 C13 C9 -38.0(3) . .
Ru1 Ru1 C13 C9 175.7(2) 2_565 .
Ru2 Ru1 C13 C9 52.2(5) . .
C2 Ru1 C13 C12 -92.5(4) . .
C1 Ru1 C13 C12 56.5(9) . .
C3 Ru1 C13 C12 -132.3(4) . .
C11 Ru1 C13 C12 37.3(4) . .
C9 Ru1 C13 C12 117.6(6) . .
C10 Ru1 C13 C12 79.6(4) . .
Ru1 Ru1 C13 C12 -66.8(5) 2_565 .
Ru2 Ru1 C13 C12 169.7(3) . .
C2 Ru1 C13 C18 30.3(8) . .
C1 Ru1 C13 C18 179.4(8) . .
C3 Ru1 C13 C18 -9.5(8) . .
C11 Ru1 C13 C18 160.1(8) . .
C12 Ru1 C13 C18 122.8(9) . .
C9 Ru1 C13 C18 -119.6(9) . .
C10 Ru1 C13 C18 -157.6(8) . .
Ru1 Ru1 C13 C18 56.1(9) 2_565 .
Ru2 Ru1 C13 C18 -67.4(8) . .
C1 Ru2 C19 C19 -117.0(5) . 2_565
C3 Ru2 C19 C19 93.18(6) . 2_565
C21 Ru2 C19 C19 -113.7(2) 2_565 2_565
C21 Ru2 C19 C19 -56.47(12) . 2_565
C22 Ru2 C19 C19 -72.27(16) 2_565 2_565
C22 Ru2 C19 C19 -99.21(13) . 2_565
C20 Ru2 C19 C19 -147.3(4) 2_565 2_565
C20 Ru2 C19 C19 -18.77(13) . 2_565
C23 Ru2 C19 C19 -32.06(18) 2_565 2_565
C23 Ru2 C19 C19 -136.57(14) . 2_565
C1 Ru2 C19 C20 30.3(7) . 2_565
C3 Ru2 C19 C20 -119.5(3) . 2_565
C21 Ru2 C19 C20 33.6(2) 2_565 2_565
C21 Ru2 C19 C20 90.8(4) . 2_565
C22 Ru2 C19 C20 75.0(3) 2_565 2_565
C22 Ru2 C19 C20 48.1(4) . 2_565
C20 Ru2 C19 C20 128.5(3) . 2_565
C23 Ru2 C19 C20 115.2(3) 2_565 2_565
C23 Ru2 C19 C20 10.7(3) . 2_565
C19 Ru2 C19 C20 147.3(4) 2_565 2_565
C1 Ru2 C19 C20 -98.2(5) . .
C3 Ru2 C19 C20 111.96(13) . .
C21 Ru2 C19 C20 -94.9(2) 2_565 .
C21 Ru2 C19 C20 -37.69(7) . .
C22 Ru2 C19 C20 -53.5(2) 2_565 .
C22 Ru2 C19 C20 -80.43(11) . .
C20 Ru2 C19 C20 -128.5(3) 2_565 .
C23 Ru2 C19 C20 -13.29(15) 2_565 .
C23 Ru2 C19 C20 -117.80(11) . .
C19 Ru2 C19 C20 18.77(13) 2_565 .
C1 Ru2 C19 C23 19.6(5) . .
C3 Ru2 C19 C23 -130.25(14) . .
C21 Ru2 C19 C23 22.9(2) 2_565 .
C21 Ru2 C19 C23 80.11(13) . .
C22 Ru2 C19 C23 64.3(2) 2_565 .
C22 Ru2 C19 C23 37.36(8) . .
C20 Ru2 C19 C23 -10.7(3) 2_565 .
C20 Ru2 C19 C23 117.80(10) . .
C23 Ru2 C19 C23 104.51(18) 2_565 .
C19 Ru2 C19 C23 136.57(14) 2_565 .
C1 Ru2 C19 C24 140.9(5) . .
C3 Ru2 C19 C24 -8.95(13) . .
C21 Ru2 C19 C24 144.2(3) 2_565 .
C21 Ru2 C19 C24 -158.6 . .
C22 Ru2 C19 C24 -174.4(2) 2_565 .
C22 Ru2 C19 C24 158.7 . .
C20 Ru2 C19 C24 110.6(4) 2_565 .
C20 Ru2 C19 C24 -120.90(10) . .
C23 Ru2 C19 C24 -134.2(2) 2_565 .
C23 Ru2 C19 C24 121.30(11) . .
C19 Ru2 C19 C24 -102.13(12) 2_565 .
C1 Ru2 C19 C24 -163.0(4) . 2_565
C3 Ru2 C19 C24 47.2(3) . 2_565
C21 Ru2 C19 C24 -159.7(4) 2_565 2_565
C21 Ru2 C19 C24 -102.5(3) . 2_565
C22 Ru2 C19 C24 -118.3(4) 2_565 2_565
C22 Ru2 C19 C24 -145.2(3) . 2_565
C20 Ru2 C19 C24 166.7(6) 2_565 2_565
C20 Ru2 C19 C24 -64.8(3) . 2_565
C23 Ru2 C19 C24 -78.1(4) 2_565 2_565
C23 Ru2 C19 C24 177.4(3) . 2_565
C19 Ru2 C19 C24 -46.0(3) 2_565 2_565
C1 Ru2 C19 C25 70.9(5) . 2_565
C3 Ru2 C19 C25 -78.96(14) . 2_565
C21 Ru2 C19 C25 74.2(3) 2_565 2_565
C21 Ru2 C19 C25 131.39(10) . 2_565
C22 Ru2 C19 C25 115.6(2) 2_565 2_565
C22 Ru2 C19 C25 88.65(11) . 2_565
C20 Ru2 C19 C25 40.6(4) 2_565 2_565
C20 Ru2 C19 C25 169.08(6) . 2_565
C23 Ru2 C19 C25 155.79(16) 2_565 2_565
C23 Ru2 C19 C25 51.28(9) . 2_565
C19 Ru2 C19 C25 -172.15(13) 2_565 2_565
C1 Ru2 C19 C23 -84.9(6) . 2_565
C3 Ru2 C19 C23 125.25(16) . 2_565
C21 Ru2 C19 C23 -81.6(2) 2_565 2_565
C21 Ru2 C19 C23 -24.40(18) . 2_565
C22 Ru2 C19 C23 -40.21(15) 2_565 2_565
C22 Ru2 C19 C23 -67.1(2) . 2_565
C20 Ru2 C19 C23 -115.2(3) 2_565 2_565
C20 Ru2 C19 C23 13.29(15) . 2_565
C23 Ru2 C19 C23 -104.51(18) . 2_565
C19 Ru2 C19 C23 32.06(18) 2_565 2_565
C1 Ru2 C19 C21 -3.3(6) . 2_565
C3 Ru2 C19 C21 -153.15(18) . 2_565
C21 Ru2 C19 C21 57.2(3) . 2_565
C22 Ru2 C19 C21 41.40(17) 2_565 2_565
C22 Ru2 C19 C21 14.5(3) . 2_565
C20 Ru2 C19 C21 -33.6(2) 2_565 2_565
C20 Ru2 C19 C21 94.9(2) . 2_565
C23 Ru2 C19 C21 81.6(2) 2_565 2_565
C23 Ru2 C19 C21 -22.9(2) . 2_565
C19 Ru2 C19 C21 113.7(2) 2_565 2_565
C19 C19 C20 C23 179(100) 2_565 2_565
C20 C19 C20 C23 -0.7 2_565 2_565
C23 C19 C20 C23 -0.4 . 2_565
C24 C19 C20 C23 179.6 . 2_565
C24 C19 C20 C23 179.5 2_565 2_565
C25 C19 C20 C23 -1.4 2_565 2_565
C21 C19 C20 C23 -0.5 2_565 2_565
Ru2 C19 C20 C23 61.27(19) . 2_565
C20 C19 C20 C19 180.0(5) 2_565 2_565
C23 C19 C20 C19 -179.8(5) . 2_565
C24 C19 C20 C19 0.2(5) . 2_565
C24 C19 C20 C19 0.2(5) 2_565 2_565
C25 C19 C20 C19 179(100) 2_565 2_565
C23 C19 C20 C19 -179(100) 2_565 2_565
C21 C19 C20 C19 -179.8(5) 2_565 2_565
Ru2 C19 C20 C19 -118.1(5) . 2_565
C19 C19 C20 C21 179.8(5) 2_565 .
C20 C19 C20 C21 -0.2 2_565 .
C23 C19 C20 C21 0.0 . .
C24 C19 C20 C21 180.0 . .
C24 C19 C20 C21 179.9 2_565 .
C25 C19 C20 C21 -0.9 2_565 .
C23 C19 C20 C21 0.4 2_565 .
C21 C19 C20 C21 -0.1 2_565 .
Ru2 C19 C20 C21 61.72(19) . .
C19 C19 C20 C25 -0.2(5) 2_565 .
C20 C19 C20 C25 179.8 2_565 .
C23 C19 C20 C25 180.0 . .
C24 C19 C20 C25 0.0 . .
C24 C19 C20 C25 -0.1 2_565 .
C25 C19 C20 C25 179(100) 2_565 .
C23 C19 C20 C25 -179.6 2_565 .
C21 C19 C20 C25 179.9 2_565 .
Ru2 C19 C20 C25 -118.28(19) . .
C19 C19 C20 C28 2.5(5) 2_565 2_565
C20 C19 C20 C28 -177(100) 2_565 2_565
C23 C19 C20 C28 -177(100) . 2_565
C24 C19 C20 C28 2.74(11) . 2_565
C24 C19 C20 C28 2.67(11) 2_565 2_565
C25 C19 C20 C28 -178(100) 2_565 2_565
C23 C19 C20 C28 -177(100) 2_565 2_565
C21 C19 C20 C28 -177(100) 2_565 2_565
Ru2 C19 C20 C28 -115.54(19) . 2_565
C19 C19 C20 C22 179.7(5) 2_565 2_565
C20 C19 C20 C22 -0.3 2_565 2_565
C23 C19 C20 C22 0.0 . 2_565
C24 C19 C20 C22 180.0 . 2_565
C24 C19 C20 C22 179.9 2_565 2_565
C25 C19 C20 C22 -1.0 2_565 2_565
C23 C19 C20 C22 0.4 2_565 2_565
C21 C19 C20 C22 -0.1 2_565 2_565
Ru2 C19 C20 C22 61.68(19) . 2_565
C19 C19 C20 C20 180.0(5) 2_565 2_565
C23 C19 C20 C20 0.2 . 2_565
C24 C19 C20 C20 -179.8 . 2_565
C24 C19 C20 C20 -179.8 2_565 2_565
C25 C19 C20 C20 -0.7 2_565 2_565
C23 C19 C20 C20 0.7 2_565 2_565
C21 C19 C20 C20 0.2 2_565 2_565
Ru2 C19 C20 C20 61.95(19) . 2_565
C19 C19 C20 C24 -0.2(5) 2_565 2_565
C20 C19 C20 C24 179.8 2_565 2_565
C23 C19 C20 C24 -179.9 . 2_565
C24 C19 C20 C24 0.1 . 2_565
C25 C19 C20 C24 179(100) 2_565 2_565
C23 C19 C20 C24 -179.5 2_565 2_565
C21 C19 C20 C24 180.0 2_565 2_565
Ru2 C19 C20 C24 -118.21(19) . 2_565
C19 C19 C20 Ru2 118.1(5) 2_565 .
C20 C19 C20 Ru2 -61.95(19) 2_565 .
C23 C19 C20 Ru2 -61.72(19) . .
C24 C19 C20 Ru2 118.28(19) . .
C24 C19 C20 Ru2 118.21(19) 2_565 .
C25 C19 C20 Ru2 -62.6(2) 2_565 .
C23 C19 C20 Ru2 -61.27(19) 2_565 .
C21 C19 C20 Ru2 -61.79(19) 2_565 .
C1 Ru2 C20 C23 7.8(8) . 2_565
C3 Ru2 C20 C23 133.9(6) . 2_565
C21 Ru2 C20 C23 -78.6(6) 2_565 2_565
C21 Ru2 C20 C23 -24.2(7) . 2_565
C22 Ru2 C20 C23 -36.9(5) 2_565 2_565
C22 Ru2 C20 C23 -62.3(7) . 2_565
C20 Ru2 C20 C23 -120.6(6) 2_565 2_565
C23 Ru2 C20 C23 -104.4(6) . 2_565
C19 Ru2 C20 C23 -157.0(9) 2_565 2_565
C19 Ru2 C20 C23 -141.3(6) . 2_565
C1 Ru2 C20 C19 164.8(4) . 2_565
C3 Ru2 C20 C19 -69.1(4) . 2_565
C21 Ru2 C20 C19 78.4(4) 2_565 2_565
C21 Ru2 C20 C19 132.8(3) . 2_565
C22 Ru2 C20 C19 120.1(5) 2_565 2_565
C22 Ru2 C20 C19 94.7(3) . 2_565
C20 Ru2 C20 C19 36.4(3) 2_565 2_565
C23 Ru2 C20 C19 157.0(9) 2_565 2_565
C23 Ru2 C20 C19 52.5(3) . 2_565
C19 Ru2 C20 C19 15.7(3) . 2_565
C1 Ru2 C20 C21 32.0(3) . .
C3 Ru2 C20 C21 158.09(18) . .
C21 Ru2 C20 C21 -54.41(18) 2_565 .
C22 Ru2 C20 C21 -12.7(3) 2_565 .
C22 Ru2 C20 C21 -38.06(8) . .
C20 Ru2 C20 C21 -96.36(12) 2_565 .
C23 Ru2 C20 C21 24.2(7) 2_565 .
C23 Ru2 C20 C21 -80.24(12) . .
C19 Ru2 C20 C21 -132.8(3) 2_565 .
C19 Ru2 C20 C21 -117.06(10) . .
C1 Ru2 C20 C19 149.1(3) . .
C3 Ru2 C20 C19 -84.84(18) . .
C21 Ru2 C20 C19 62.65(16) 2_565 .
C21 Ru2 C20 C19 117.06(10) . .
C22 Ru2 C20 C19 104.4(3) 2_565 .
C22 Ru2 C20 C19 79.00(12) . .
C20 Ru2 C20 C19 20.7 2_565 .
C23 Ru2 C20 C19 141.3(6) 2_565 .
C23 Ru2 C20 C19 36.83(7) . .
C19 Ru2 C20 C19 -15.7(3) 2_565 .
C1 Ru2 C20 C25 -88.7(3) . .
C3 Ru2 C20 C25 37.37(18) . .
C21 Ru2 C20 C25 -175.13(16) 2_565 .
C21 Ru2 C20 C25 -120.72(10) . .
C22 Ru2 C20 C25 -133.4(3) 2_565 .
C22 Ru2 C20 C25 -158.8 . .
C20 Ru2 C20 C25 142.92(7) 2_565 .
C23 Ru2 C20 C25 -96.5(7) 2_565 .
C23 Ru2 C20 C25 159.0 . .
C19 Ru2 C20 C25 106.5(3) 2_565 .
C19 Ru2 C20 C25 122.22(10) . .
C1 Ru2 C20 C28 -35.8(4) . 2_565
C3 Ru2 C20 C28 90.3(2) . 2_565
C21 Ru2 C20 C28 -122.2(2) 2_565 2_565
C21 Ru2 C20 C28 -67.83(19) . 2_565
C22 Ru2 C20 C28 -80.5(2) 2_565 2_565
C22 Ru2 C20 C28 -105.89(19) . 2_565
C20 Ru2 C20 C28 -164.18(12) 2_565 2_565
C23 Ru2 C20 C28 -43.6(5) 2_565 2_565
C23 Ru2 C20 C28 -148.06(14) . 2_565
C19 Ru2 C20 C28 159.4(4) 2_565 2_565
C19 Ru2 C20 C28 175.11(11) . 2_565
C1 Ru2 C20 C22 44.7(4) . 2_565
C3 Ru2 C20 C22 170.8(2) . 2_565
C21 Ru2 C20 C22 -41.71(19) 2_565 2_565
C21 Ru2 C20 C22 12.7(3) . 2_565
C22 Ru2 C20 C22 -25.4(3) . 2_565
C20 Ru2 C20 C22 -83.7(3) 2_565 2_565
C23 Ru2 C20 C22 36.9(5) 2_565 2_565
C23 Ru2 C20 C22 -67.5(3) . 2_565
C19 Ru2 C20 C22 -120.1(5) 2_565 2_565
C19 Ru2 C20 C22 -104.4(3) . 2_565
C1 Ru2 C20 C20 128.4(3) . 2_565
C3 Ru2 C20 C20 -105.55(18) . 2_565
C21 Ru2 C20 C20 41.95(15) 2_565 2_565
C21 Ru2 C20 C20 96.36(12) . 2_565
C22 Ru2 C20 C20 83.7(3) 2_565 2_565
C22 Ru2 C20 C20 58.30(10) . 2_565
C23 Ru2 C20 C20 120.6(6) 2_565 2_565
C23 Ru2 C20 C20 16.1 . 2_565
C19 Ru2 C20 C20 -36.4(3) 2_565 2_565
C19 Ru2 C20 C20 -20.7 . 2_565
C1 Ru2 C20 C24 -157.5(4) . 2_565
C3 Ru2 C20 C24 -31.4(4) . 2_565
C21 Ru2 C20 C24 116.1(4) 2_565 2_565
C21 Ru2 C20 C24 170.5(3) . 2_565
C22 Ru2 C20 C24 157.8(4) 2_565 2_565
C22 Ru2 C20 C24 132.4(3) . 2_565
C20 Ru2 C20 C24 74.1(4) 2_565 2_565
C23 Ru2 C20 C24 -165.3(9) 2_565 2_565
C23 Ru2 C20 C24 90.2(4) . 2_565
C19 Ru2 C20 C24 37.7(2) 2_565 2_565
C19 Ru2 C20 C24 53.4(4) . 2_565
C23 C20 C21 C22 179(100) 2_565 2_565
C19 C20 C21 C22 -0.11(19) 2_565 2_565
C19 C20 C21 C22 -0.2 . 2_565
C25 C20 C21 C22 179.8 . 2_565
C28 C20 C21 C22 179.6 2_565 2_565
C20 C20 C21 C22 -0.3 2_565 2_565
C24 C20 C21 C22 0.1 2_565 2_565
Ru2 C20 C21 C22 63.30(19) . 2_565
C19 C20 C21 C23 -179.22(19) 2_565 2_565
C19 C20 C21 C23 -179.3 . 2_565
C25 C20 C21 C23 0.7 . 2_565
C28 C20 C21 C23 0.4 2_565 2_565
C22 C20 C21 C23 -179(100) 2_565 2_565
C20 C20 C21 C23 -179.4 2_565 2_565
C24 C20 C21 C23 -179(100) 2_565 2_565
Ru2 C20 C21 C23 -115.81(18) . 2_565
C23 C20 C21 C22 179.3 2_565 .
C19 C20 C21 C22 0.08(19) 2_565 .
C19 C20 C21 C22 0.0 . .
C25 C20 C21 C22 180.0 . .
C28 C20 C21 C22 179.7 2_565 .
C22 C20 C21 C22 0.2 2_565 .
C20 C20 C21 C22 -0.1 2_565 .
C24 C20 C21 C22 0.3 2_565 .
Ru2 C20 C21 C22 63.49(19) . .
C23 C20 C21 C26 -0.7 2_565 .
C19 C20 C21 C26 -179.91(19) 2_565 .
C19 C20 C21 C26 180.0 . .
C25 C20 C21 C26 0.0 . .
C28 C20 C21 C26 -0.2 2_565 .
C22 C20 C21 C26 -180(100) 2_565 .
C20 C20 C21 C26 179.9 2_565 .
C24 C20 C21 C26 -180(100) 2_565 .
Ru2 C20 C21 C26 -116.51(19) . .
C23 C20 C21 C27 0.1 2_565 2_565
C19 C20 C21 C27 -179(100) 2_565 2_565
C19 C20 C21 C27 -179(100) . 2_565
C25 C20 C21 C27 0.81(6) . 2_565
C28 C20 C21 C27 0.56(6) 2_565 2_565
C22 C20 C21 C27 -179(100) 2_565 2_565
C20 C20 C21 C27 -179(100) 2_565 2_565
C24 C20 C21 C27 -179(100) 2_565 2_565
Ru2 C20 C21 C27 -115.70(18) . 2_565
C23 C20 C21 C21 179.4 2_565 2_565
C19 C20 C21 C21 0.17(19) 2_565 2_565
C19 C20 C21 C21 0.1 . 2_565
C25 C20 C21 C21 -179.9 . 2_565
C28 C20 C21 C21 179.8 2_565 2_565
C22 C20 C21 C21 0.3 2_565 2_565
C20 C20 C21 C21 0.0 2_565 2_565
C24 C20 C21 C21 0.4 2_565 2_565
Ru2 C20 C21 C21 63.57(19) . 2_565
C23 C20 C21 C19 179.2(2) 2_565 2_565
C19 C20 C21 C19 -0.08(19) . 2_565
C25 C20 C21 C19 179.92(19) . 2_565
C28 C20 C21 C19 179.66(19) 2_565 2_565
C22 C20 C21 C19 0.11(19) 2_565 2_565
C20 C20 C21 C19 -0.17(19) 2_565 2_565
C24 C20 C21 C19 0.25(19) 2_565 2_565
Ru2 C20 C21 C19 63.4(4) . 2_565
C23 C20 C21 Ru2 115.81(18) 2_565 .
C19 C20 C21 Ru2 -63.4(4) 2_565 .
C19 C20 C21 Ru2 -63.49(19) . .
C25 C20 C21 Ru2 116.51(19) . .
C28 C20 C21 Ru2 116.26(19) 2_565 .
C22 C20 C21 Ru2 -63.30(19) 2_565 .
C20 C20 C21 Ru2 -63.57(19) 2_565 .
C24 C20 C21 Ru2 -63.16(19) 2_565 .
C1 Ru2 C21 C22 61.1(5) . 2_565
C3 Ru2 C21 C22 178.4(6) . 2_565
C21 Ru2 C21 C22 -37.4(5) 2_565 2_565
C22 Ru2 C21 C22 -22.7(5) . 2_565
C20 Ru2 C21 C22 -78.6(6) 2_565 2_565
C20 Ru2 C21 C22 -139.0(5) . 2_565
C23 Ru2 C21 C22 -156.3(9) 2_565 2_565
C23 Ru2 C21 C22 -60.3(5) . 2_565
C19 Ru2 C21 C22 -120.0(6) 2_565 2_565
C19 Ru2 C21 C22 -101.9(5) . 2_565
C1 Ru2 C21 C23 -142.6(5) . 2_565
C3 Ru2 C21 C23 -25.3(7) . 2_565
C21 Ru2 C21 C23 118.9(5) 2_565 2_565
C22 Ru2 C21 C23 156.3(9) 2_565 2_565
C22 Ru2 C21 C23 133.6(5) . 2_565
C20 Ru2 C21 C23 77.7(5) 2_565 2_565
C20 Ru2 C21 C23 17.3(5) . 2_565
C23 Ru2 C21 C23 96.0(5) . 2_565
C19 Ru2 C21 C23 36.3(4) 2_565 2_565
C19 Ru2 C21 C23 54.4(5) . 2_565
C1 Ru2 C21 C20 -159.89(16) . .
C3 Ru2 C21 C20 -42.6(4) . .
C21 Ru2 C21 C20 101.63(11) 2_565 .
C22 Ru2 C21 C20 139.0(5) 2_565 .
C22 Ru2 C21 C20 116.33(10) . .
C20 Ru2 C21 C20 60.43(16) 2_565 .
C23 Ru2 C21 C20 -17.3(5) 2_565 .
C23 Ru2 C21 C20 78.77(11) . .
C19 Ru2 C21 C20 19.0(2) 2_565 .
C19 Ru2 C21 C20 37.13(7) . .
C1 Ru2 C21 C22 83.78(16) . .
C3 Ru2 C21 C22 -158.9(5) . .
C21 Ru2 C21 C22 -14.7 2_565 .
C22 Ru2 C21 C22 22.7(5) 2_565 .
C20 Ru2 C21 C22 -55.90(15) 2_565 .
C20 Ru2 C21 C22 -116.33(10) . .
C23 Ru2 C21 C22 -133.6(5) 2_565 .
C23 Ru2 C21 C22 -37.56(7) . .
C19 Ru2 C21 C22 -97.3(2) 2_565 .
C19 Ru2 C21 C22 -79.19(11) . .
C1 Ru2 C21 C26 -37.79(16) . .
C3 Ru2 C21 C26 79.5(4) . .
C21 Ru2 C21 C26 -136.27(8) 2_565 .
C22 Ru2 C21 C26 -98.9(5) 2_565 .
C22 Ru2 C21 C26 -121.58(10) . .
C20 Ru2 C21 C26 -177.48(15) 2_565 .
C20 Ru2 C21 C26 122.10(10) . .
C23 Ru2 C21 C26 104.8(5) 2_565 .
C23 Ru2 C21 C26 -159.1 . .
C19 Ru2 C21 C26 141.1(2) 2_565 .
C19 Ru2 C21 C26 159.2 . .
C1 Ru2 C21 C27 13.7(4) . 2_565
C3 Ru2 C21 C27 131.0(5) . 2_565
C21 Ru2 C21 C27 -84.8(5) 2_565 2_565
C22 Ru2 C21 C27 -47.38(18) 2_565 2_565
C22 Ru2 C21 C27 -70.1(5) . 2_565
C20 Ru2 C21 C27 -126.0(5) 2_565 2_565
C20 Ru2 C21 C27 173.6(4) . 2_565
C23 Ru2 C21 C27 156.3(8) 2_565 2_565
C23 Ru2 C21 C27 -107.7(5) . 2_565
C19 Ru2 C21 C27 -167.4(5) 2_565 2_565
C19 Ru2 C21 C27 -149.3(4) . 2_565
C1 Ru2 C21 C21 98.48(16) . 2_565
C3 Ru2 C21 C21 -144.2(5) . 2_565
C22 Ru2 C21 C21 37.4(5) 2_565 2_565
C22 Ru2 C21 C21 14.7 . 2_565
C20 Ru2 C21 C21 -41.20(15) 2_565 2_565
C20 Ru2 C21 C21 -101.63(10) . 2_565
C23 Ru2 C21 C21 -118.9(5) 2_565 2_565
C23 Ru2 C21 C21 -22.9 . 2_565
C19 Ru2 C21 C21 -82.6(2) 2_565 2_565
C19 Ru2 C21 C21 -64.50(10) . 2_565
C1 Ru2 C21 C19 -178.89(19) . 2_565
C3 Ru2 C21 C19 -61.6(5) . 2_565
C21 Ru2 C21 C19 82.6(2) 2_565 2_565
C22 Ru2 C21 C19 120.0(6) 2_565 2_565
C22 Ru2 C21 C19 97.3(2) . 2_565
C20 Ru2 C21 C19 41.42(14) 2_565 2_565
C20 Ru2 C21 C19 -19.0(2) . 2_565
C23 Ru2 C21 C19 -36.3(4) 2_565 2_565
C23 Ru2 C21 C19 59.8(2) . 2_565
C19 Ru2 C21 C19 18.1(2) . 2_565
C22 C21 C22 C21 180.0 2_565 2_565
C23 C21 C22 C21 0.6 2_565 2_565
C20 C21 C22 C21 0.3 . 2_565
C26 C21 C22 C21 -179.7 . 2_565
C27 C21 C22 C21 -179.8 2_565 2_565
C19 C21 C22 C21 0.35(6) 2_565 2_565
Ru2 C21 C22 C21 64.47(19) . 2_565
C23 C21 C22 C22 -179(100) 2_565 2_565
C20 C21 C22 C22 -179.7 . 2_565
C26 C21 C22 C22 0.3 . 2_565
C27 C21 C22 C22 0.2 2_565 2_565
C21 C21 C22 C22 180.0 2_565 2_565
C19 C21 C22 C22 -179.65(6) 2_565 2_565
Ru2 C21 C22 C22 -115.5(2) . 2_565
C22 C21 C22 C23 179.7 2_565 .
C23 C21 C22 C23 0.3 2_565 .
C20 C21 C22 C23 0.0 . .
C26 C21 C22 C23 180.0 . .
C27 C21 C22 C23 179.9 2_565 .
C21 C21 C22 C23 -0.3 2_565 .
C19 C21 C22 C23 0.03(6) 2_565 .
Ru2 C21 C22 C23 64.15(19) . .
C22 C21 C22 C27 -0.3 2_565 .
C23 C21 C22 C27 -179.7 2_565 .
C20 C21 C22 C27 180.0 . .
C26 C21 C22 C27 0.0 . .
C27 C21 C22 C27 -0.1 2_565 .
C21 C21 C22 C27 179.7 2_565 .
C19 C21 C22 C27 -179.97(6) 2_565 .
Ru2 C21 C22 C27 -115.86(19) . .
C22 C21 C22 C26 -2.50(9) 2_565 2_565
C23 C21 C22 C26 178(100) 2_565 2_565
C20 C21 C22 C26 178(100) . 2_565
C26 C21 C22 C26 -2.18(9) . 2_565
C27 C21 C22 C26 -2.27(9) 2_565 2_565
C21 C21 C22 C26 177(100) 2_565 2_565
C19 C21 C22 C26 178(100) 2_565 2_565
Ru2 C21 C22 C26 -118.0(2) . 2_565
C22 C21 C22 C20 179.8 2_565 2_565
C23 C21 C22 C20 0.4 2_565 2_565
C20 C21 C22 C20 0.1 . 2_565
C26 C21 C22 C20 -179.9 . 2_565
C27 C21 C22 C20 180.0 2_565 2_565
C21 C21 C22 C20 -0.2 2_565 2_565
C19 C21 C22 C20 0.12(6) 2_565 2_565
Ru2 C21 C22 C20 64.23(19) . 2_565
C22 C21 C22 Ru2 115.5(2) 2_565 .
C23 C21 C22 Ru2 -63.86(19) 2_565 .
C20 C21 C22 Ru2 -64.14(19) . .
C26 C21 C22 Ru2 115.85(19) . .
C27 C21 C22 Ru2 115.76(19) 2_565 .
C21 C21 C22 Ru2 -64.47(19) 2_565 .
C19 C21 C22 Ru2 -64.1(2) 2_565 .
C1 Ru2 C22 C21 122.2(5) . 2_565
C3 Ru2 C22 C21 3.2(12) . 2_565
C21 Ru2 C22 C21 -131.7(5) . 2_565
C22 Ru2 C22 C21 -145.4(5) 2_565 2_565
C20 Ru2 C22 C21 -31.6(4) 2_565 2_565
C20 Ru2 C22 C21 -93.9(6) . 2_565
C23 Ru2 C22 C21 -111.6(5) 2_565 2_565
C23 Ru2 C22 C21 -15.2(5) . 2_565
C19 Ru2 C22 C21 -71.0(5) 2_565 2_565
C19 Ru2 C22 C21 -52.1(6) . 2_565
C1 Ru2 C22 C22 -92.35(14) . 2_565
C3 Ru2 C22 C22 148.6(9) . 2_565
C21 Ru2 C22 C22 145.4(5) 2_565 2_565
C21 Ru2 C22 C22 13.7 . 2_565
C20 Ru2 C22 C22 113.8(2) 2_565 2_565
C20 Ru2 C22 C22 51.55(9) . 2_565
C23 Ru2 C22 C22 33.84(14) 2_565 2_565
C23 Ru2 C22 C22 130.25(9) . 2_565
C19 Ru2 C22 C22 74.4(2) 2_565 2_565
C19 Ru2 C22 C22 93.34(11) . 2_565
C1 Ru2 C22 C23 137.40(13) . .
C3 Ru2 C22 C23 18.4(9) . .
C21 Ru2 C22 C23 15.2(5) 2_565 .
C21 Ru2 C22 C23 -116.54(10) . .
C22 Ru2 C22 C23 -130.25(9) 2_565 .
C20 Ru2 C22 C23 -16.4(2) 2_565 .
C20 Ru2 C22 C23 -78.70(11) . .
C23 Ru2 C22 C23 -96.41(17) 2_565 .
C19 Ru2 C22 C23 -55.8(2) 2_565 .
C19 Ru2 C22 C23 -36.91(7) . .
C1 Ru2 C22 C21 -106.06(13) . .
C3 Ru2 C22 C21 134.9(9) . .
C21 Ru2 C22 C21 131.7(5) 2_565 .
C22 Ru2 C22 C21 -13.7 2_565 .
C20 Ru2 C22 C21 100.1(2) 2_565 .
C20 Ru2 C22 C21 37.84(7) . .
C23 Ru2 C22 C21 20.13(14) 2_565 .
C23 Ru2 C22 C21 116.54(10) . .
C19 Ru2 C22 C21 60.7(2) 2_565 .
C19 Ru2 C22 C21 79.63(11) . .
C1 Ru2 C22 C27 15.10(12) . .
C3 Ru2 C22 C27 -103.9(9) . .
C21 Ru2 C22 C27 -107.1(6) 2_565 .
C21 Ru2 C22 C27 121.16(10) . .
C22 Ru2 C22 C27 107.46(11) 2_565 .
C20 Ru2 C22 C27 -138.7(3) 2_565 .
C20 Ru2 C22 C27 159.0 . .
C23 Ru2 C22 C27 141.30(18) 2_565 .
C23 Ru2 C22 C27 -122.29(10) . .
C19 Ru2 C22 C27 -178.1(2) 2_565 .
C19 Ru2 C22 C27 -159.2 . .
C1 Ru2 C22 C26 68.95(17) . 2_565
C3 Ru2 C22 C26 -50.1(9) . 2_565
C21 Ru2 C22 C26 -53.3(7) 2_565 2_565
C21 Ru2 C22 C26 175.01(15) . 2_565
C22 Ru2 C22 C26 161.30(16) 2_565 2_565
C20 Ru2 C22 C26 -84.9(4) 2_565 2_565
C20 Ru2 C22 C26 -147.15(14) . 2_565
C23 Ru2 C22 C26 -164.9(2) 2_565 2_565
C23 Ru2 C22 C26 -68.45(16) . 2_565
C19 Ru2 C22 C26 -124.3(3) 2_565 2_565
C19 Ru2 C22 C26 -105.36(15) . 2_565
C1 Ru2 C22 C20 153.8(2) . 2_565
C3 Ru2 C22 C20 34.8(10) . 2_565
C21 Ru2 C22 C20 31.6(4) 2_565 2_565
C21 Ru2 C22 C20 -100.1(2) . 2_565
C22 Ru2 C22 C20 -113.8(2) 2_565 2_565
C20 Ru2 C22 C20 -62.3(3) . 2_565
C23 Ru2 C22 C20 -80.0(2) 2_565 2_565
C23 Ru2 C22 C20 16.4(2) . 2_565
C19 Ru2 C22 C20 -39.39(15) 2_565 2_565
C19 Ru2 C22 C20 -20.5(3) . 2_565
C21 C22 C23 C20 -179(100) 2_565 2_565
C22 C22 C23 C20 0.4 2_565 2_565
C21 C22 C23 C20 0.3 . 2_565
C27 C22 C23 C20 -179.7 . 2_565
C26 C22 C23 C20 -179.5 2_565 2_565
Ru2 C22 C23 C20 63.05(19) . 2_565
C22 C22 C23 C21 179(100) 2_565 2_565
C21 C22 C23 C21 179(100) . 2_565
C27 C22 C23 C21 -0.9 . 2_565
C26 C22 C23 C21 -0.7 2_565 2_565
C20 C22 C23 C21 179(100) 2_565 2_565
Ru2 C22 C23 C21 -118.1(2) . 2_565
C21 C22 C23 C19 -179(100) 2_565 .
C22 C22 C23 C19 0.1 2_565 .
C21 C22 C23 C19 0.0 . .
C27 C22 C23 C19 180.0 . .
C26 C22 C23 C19 -179.8 2_565 .
C20 C22 C23 C19 -0.3 2_565 .
Ru2 C22 C23 C19 62.75(19) . .
C21 C22 C23 C28 0.9 2_565 .
C22 C22 C23 C28 -179.9 2_565 .
C21 C22 C23 C28 180.0 . .
C27 C22 C23 C28 0.0 . .
C26 C22 C23 C28 0.2 2_565 .
C20 C22 C23 C28 179.7 2_565 .
Ru2 C22 C23 C28 -117.25(19) . .
C21 C22 C23 C25 -3.6(6) 2_565 2_565
C22 C22 C23 C25 176(100) 2_565 2_565
C21 C22 C23 C25 175(100) . 2_565
C27 C22 C23 C25 -4.5(7) . 2_565
C26 C22 C23 C25 -4.3(7) 2_565 2_565
C20 C22 C23 C25 175(100) 2_565 2_565
Ru2 C22 C23 C25 -121.8(7) . 2_565
C21 C22 C23 C19 -179(100) 2_565 2_565
C22 C22 C23 C19 0.07(7) 2_565 2_565
C21 C22 C23 C19 -0.03(7) . 2_565
C27 C22 C23 C19 179.97(7) . 2_565
C26 C22 C23 C19 -179.83(7) 2_565 2_565
C20 C22 C23 C19 -0.33(7) 2_565 2_565
Ru2 C22 C23 C19 62.72(15) . 2_565
C21 C22 C23 C26 0.7 2_565 2_565
C22 C22 C23 C26 179.9 2_565 2_565
C21 C22 C23 C26 179.8 . 2_565
C27 C22 C23 C26 -0.2 . 2_565
C20 C22 C23 C26 179.5 2_565 2_565
Ru2 C22 C23 C26 -117.46(19) . 2_565
C21 C22 C23 Ru2 118.1(2) 2_565 .
C22 C22 C23 Ru2 -62.65(19) 2_565 .
C21 C22 C23 Ru2 -62.75(19) . .
C27 C22 C23 Ru2 117.25(19) . .
C26 C22 C23 Ru2 117.46(19) 2_565 .
C20 C22 C23 Ru2 -63.05(19) 2_565 .
C19 C19 C23 C20 -179(100) 2_565 2_565
C20 C19 C23 C20 -179(100) . 2_565
C24 C19 C23 C20 0.9 . 2_565
C24 C19 C23 C20 2.3(2) 2_565 2_565
C25 C19 C23 C20 0.7 2_565 2_565
C23 C19 C23 C20 -179(100) 2_565 2_565
C21 C19 C23 C20 -179(100) 2_565 2_565
Ru2 C19 C23 C20 119.7(2) . 2_565
C19 C19 C23 C21 -0.3(2) 2_565 2_565
C20 C19 C23 C21 179(100) 2_565 2_565
C20 C19 C23 C21 -0.2 . 2_565
C24 C19 C23 C21 179.8 . 2_565
C24 C19 C23 C21 -179(100) 2_565 2_565
C25 C19 C23 C21 179.6 2_565 2_565
C23 C19 C23 C21 -0.3 2_565 2_565
Ru2 C19 C23 C21 -61.46(18) . 2_565
C19 C19 C23 C22 -0.1(2) 2_565 .
C20 C19 C23 C22 179(100) 2_565 .
C20 C19 C23 C22 0.0 . .
C24 C19 C23 C22 180.0 . .
C24 C19 C23 C22 -179(100) 2_565 .
C25 C19 C23 C22 179.8 2_565 .
C23 C19 C23 C22 -0.1 2_565 .
C21 C19 C23 C22 0.2 2_565 .
Ru2 C19 C23 C22 -61.27(18) . .
C19 C19 C23 C28 179.9(2) 2_565 .
C20 C19 C23 C28 -0.9 2_565 .
C20 C19 C23 C28 180.0 . .
C24 C19 C23 C28 0.0 . .
C24 C19 C23 C28 1.4(2) 2_565 .
C25 C19 C23 C28 -0.2 2_565 .
C23 C19 C23 C28 179.9 2_565 .
C21 C19 C23 C28 -179.8 2_565 .
Ru2 C19 C23 C28 118.73(18) . .
C19 C19 C23 C25 -179.9(2) 2_565 2_565
C20 C19 C23 C25 -0.7 2_565 2_565
C20 C19 C23 C25 -179.8 . 2_565
C24 C19 C23 C25 0.2 . 2_565
C24 C19 C23 C25 1.6(2) 2_565 2_565
C23 C19 C23 C25 -179.9 2_565 2_565
C21 C19 C23 C25 -179.6 2_565 2_565
Ru2 C19 C23 C25 118.95(18) . 2_565
C20 C19 C23 C19 179(100) 2_565 2_565
C20 C19 C23 C19 0.1(2) . 2_565
C24 C19 C23 C19 -179.9(2) . 2_565
C24 C19 C23 C19 -178(100) 2_565 2_565
C25 C19 C23 C19 179.9(2) 2_565 2_565
C23 C19 C23 C19 0.0(2) 2_565 2_565
C21 C19 C23 C19 0.3(2) 2_565 2_565
Ru2 C19 C23 C19 -61.2(2) . 2_565
C19 C19 C23 C26 -0.8(2) 2_565 2_565
C20 C19 C23 C26 178(100) 2_565 2_565
C20 C19 C23 C26 -0.7 . 2_565
C24 C19 C23 C26 179(100) . 2_565
C24 C19 C23 C26 -179(100) 2_565 2_565
C25 C19 C23 C26 179(100) 2_565 2_565
C23 C19 C23 C26 -0.8 2_565 2_565
C21 C19 C23 C26 -0.5 2_565 2_565
Ru2 C19 C23 C26 -61.99(19) . 2_565
C19 C19 C23 Ru2 61.2(2) 2_565 .
C20 C19 C23 Ru2 -119.7(2) 2_565 .
C20 C19 C23 Ru2 61.27(18) . .
C24 C19 C23 Ru2 -118.72(18) . .
C24 C19 C23 Ru2 -117.3(3) 2_565 .
C25 C19 C23 Ru2 -118.95(18) 2_565 .
C23 C19 C23 Ru2 61.17(18) 2_565 .
C21 C19 C23 Ru2 61.46(18) 2_565 .
C1 Ru2 C23 C20 174.1(6) . 2_565
C3 Ru2 C23 C20 54.8(7) . 2_565
C21 Ru2 C23 C20 -140.7(10) 2_565 2_565
C21 Ru2 C23 C20 -92.9(6) . 2_565
C22 Ru2 C23 C20 -108.4(7) 2_565 2_565
C22 Ru2 C23 C20 -131.0(6) . 2_565
C20 Ru2 C23 C20 -50.5(6) . 2_565
C23 Ru2 C23 C20 -67.8(6) 2_565 2_565
C19 Ru2 C23 C20 -29.0(5) 2_565 2_565
C19 Ru2 C23 C20 -13.5(6) . 2_565
C1 Ru2 C23 C21 -45.2(5) . 2_565
C3 Ru2 C23 C21 -164.5(4) . 2_565
C21 Ru2 C23 C21 47.8(5) . 2_565
C22 Ru2 C23 C21 32.3(4) 2_565 2_565
C22 Ru2 C23 C21 9.8(5) . 2_565
C20 Ru2 C23 C21 140.7(10) 2_565 2_565
C20 Ru2 C23 C21 90.3(5) . 2_565
C23 Ru2 C23 C21 72.9(5) 2_565 2_565
C19 Ru2 C23 C21 111.7(5) 2_565 2_565
C19 Ru2 C23 C21 127.2(4) . 2_565
C1 Ru2 C23 C22 -55.0(2) . .
C3 Ru2 C23 C22 -174.3(2) . .
C21 Ru2 C23 C22 -9.8(5) 2_565 .
C21 Ru2 C23 C22 38.02(7) . .
C22 Ru2 C23 C22 22.52(16) 2_565 .
C20 Ru2 C23 C22 131.0(6) 2_565 .
C20 Ru2 C23 C22 80.49(11) . .
C23 Ru2 C23 C22 63.11(10) 2_565 .
C19 Ru2 C23 C22 101.97(16) 2_565 .
C19 Ru2 C23 C22 117.45(11) . .
C1 Ru2 C23 C19 -172.4(2) . .
C3 Ru2 C23 C19 68.3(2) . .
C21 Ru2 C23 C19 -127.2(4) 2_565 .
C21 Ru2 C23 C19 -79.43(12) . .
C22 Ru2 C23 C19 -94.93(17) 2_565 .
C22 Ru2 C23 C19 -117.45(10) . .
C20 Ru2 C23 C19 13.5(6) 2_565 .
C20 Ru2 C23 C19 -36.96(7) . .
C23 Ru2 C23 C19 -54.34(10) 2_565 .
C19 Ru2 C23 C19 -15.48(17) 2_565 .
C1 Ru2 C23 C28 65.7(2) . .
C3 Ru2 C23 C28 -53.6(3) . .
C21 Ru2 C23 C28 110.9(5) 2_565 .
C21 Ru2 C23 C28 158.6 . .
C22 Ru2 C23 C28 143.15(15) 2_565 .
C22 Ru2 C23 C28 120.63(10) . .
C20 Ru2 C23 C28 -108.4(6) 2_565 .
C20 Ru2 C23 C28 -158.9 . .
C23 Ru2 C23 C28 -176.3 2_565 .
C19 Ru2 C23 C28 -137.40(16) 2_565 .
C19 Ru2 C23 C28 -121.92(11) . .
C1 Ru2 C23 C25 122.5(4) . 2_565
C3 Ru2 C23 C25 3.3(5) . 2_565
C21 Ru2 C23 C25 167.8(7) 2_565 2_565
C21 Ru2 C23 C25 -144.5(3) . 2_565
C22 Ru2 C23 C25 -160.0(4) 2_565 2_565
C22 Ru2 C23 C25 177.5(3) . 2_565
C20 Ru2 C23 C25 -51.5(3) 2_565 2_565
C20 Ru2 C23 C25 -102.0(4) . 2_565
C23 Ru2 C23 C25 -119.4(4) 2_565 2_565
C19 Ru2 C23 C25 -80.5(3) 2_565 2_565
C19 Ru2 C23 C25 -65.0(4) . 2_565
C1 Ru2 C23 C19 -156.9(2) . 2_565
C3 Ru2 C23 C19 83.8(3) . 2_565
C21 Ru2 C23 C19 -111.7(5) 2_565 2_565
C21 Ru2 C23 C19 -63.95(16) . 2_565
C22 Ru2 C23 C19 -79.5(2) 2_565 2_565
C22 Ru2 C23 C19 -101.97(16) . 2_565
C20 Ru2 C23 C19 29.0(5) 2_565 2_565
C20 Ru2 C23 C19 -21.48(16) . 2_565
C23 Ru2 C23 C19 -38.86(16) 2_565 2_565
C19 Ru2 C23 C19 15.48(17) . 2_565
C1 Ru2 C23 C26 -5.0(4) . 2_565
C3 Ru2 C23 C26 -124.3(3) . 2_565
C21 Ru2 C23 C26 40.2(2) 2_565 2_565
C21 Ru2 C23 C26 88.0(4) . 2_565
C22 Ru2 C23 C26 72.5(3) 2_565 2_565
C22 Ru2 C23 C26 50.0(4) . 2_565
C20 Ru2 C23 C26 -179.1(8) 2_565 2_565
C20 Ru2 C23 C26 130.4(3) . 2_565
C23 Ru2 C23 C26 113.1(3) 2_565 2_565
C19 Ru2 C23 C26 151.9(4) 2_565 2_565
C19 Ru2 C23 C26 167.4(3) . 2_565
C19 C19 C24 C24 0.00(19) 2_565 2_565
C20 C19 C24 C24 -179.9 2_565 2_565
C20 C19 C24 C24 -0.1 . 2_565
C23 C19 C24 C24 179.9 . 2_565
C25 C19 C24 C24 -179.9 2_565 2_565
C23 C19 C24 C24 0.1 2_565 2_565
C21 C19 C24 C24 -179.9 2_565 2_565
Ru2 C19 C24 C24 89.4(2) . 2_565
C20 C19 C24 C19 -179.87(19) 2_565 2_565
C20 C19 C24 C19 -0.08(19) . 2_565
C23 C19 C24 C19 179.91(19) . 2_565
C24 C19 C24 C19 0.00(19) 2_565 2_565
C25 C19 C24 C19 -179.87(19) 2_565 2_565
C23 C19 C24 C19 0.08(19) 2_565 2_565
C21 C19 C24 C19 -179.9(2) 2_565 2_565
Ru2 C19 C24 C19 89.43(12) . 2_565
C19 C19 C24 C25 179.87(19) 2_565 2_565
C20 C19 C24 C25 0.0 2_565 2_565
C20 C19 C24 C25 179.8 . 2_565
C23 C19 C24 C25 -0.2 . 2_565
C24 C19 C24 C25 179.9 2_565 2_565
C23 C19 C24 C25 180.0 2_565 2_565
C21 C19 C24 C25 -0.1 2_565 2_565
Ru2 C19 C24 C25 -90.7(2) . 2_565
C19 C19 C24 C20 179.87(19) 2_565 2_565
C20 C19 C24 C20 179.8 . 2_565
C23 C19 C24 C20 -0.2 . 2_565
C24 C19 C24 C20 179.9 2_565 2_565
C25 C19 C24 C20 0.0 2_565 2_565
C23 C19 C24 C20 179.9 2_565 2_565
C21 C19 C24 C20 -0.1 2_565 2_565
Ru2 C19 C24 C20 -90.7(2) . 2_565
C23 C20 C25 C28 0.0 2_565 2_565
C19 C20 C25 C28 179.60(17) 2_565 2_565
C21 C20 C25 C28 -0.3 . 2_565
C19 C20 C25 C28 179.7 . 2_565
C22 C20 C25 C28 -0.3 2_565 2_565
C20 C20 C25 C28 179.8 2_565 2_565
C24 C20 C25 C28 179.6 2_565 2_565
Ru2 C20 C25 C28 87.8(2) . 2_565
C19 C20 C25 C23 179.61(16) 2_565 2_565
C21 C20 C25 C23 -0.3 . 2_565
C19 C20 C25 C23 179.7 . 2_565
C28 C20 C25 C23 0.0 2_565 2_565
C22 C20 C25 C23 -0.3 2_565 2_565
C20 C20 C25 C23 179.8 2_565 2_565
C24 C20 C25 C23 179.6 2_565 2_565
Ru2 C20 C25 C23 87.8(2) . 2_565
C23 C20 C25 C24 -179.6 2_565 2_565
C19 C20 C25 C24 0.00(17) 2_565 2_565
C21 C20 C25 C24 -179.9 . 2_565
C19 C20 C25 C24 0.1 . 2_565
C28 C20 C25 C24 -179.6 2_565 2_565
C22 C20 C25 C24 -179.9 2_565 2_565
C20 C20 C25 C24 0.2 2_565 2_565
Ru2 C20 C25 C24 -91.8(2) . 2_565
C23 C20 C25 C19 -179.61(16) 2_565 2_565
C21 C20 C25 C19 -179.93(16) . 2_565
C19 C20 C25 C19 0.07(17) . 2_565
C28 C20 C25 C19 -179.60(17) 2_565 2_565
C22 C20 C25 C19 -179.87(16) 2_565 2_565
C20 C20 C25 C19 0.22(17) 2_565 2_565
C24 C20 C25 C19 0.00(16) 2_565 2_565
Ru2 C20 C25 C19 -91.8(3) . 2_565
C22 C21 C26 C27 0.0 2_565 2_565
C23 C21 C26 C27 179.6 2_565 2_565
C20 C21 C26 C27 179.9 . 2_565
C22 C21 C26 C27 -0.1 . 2_565
C21 C21 C26 C27 -0.3 2_565 2_565
C19 C21 C26 C27 179.82(11) 2_565 2_565
Ru2 C21 C26 C27 89.2(2) . 2_565
C23 C21 C26 C22 179.6 2_565 2_565
C20 C21 C26 C22 179.9 . 2_565
C22 C21 C26 C22 -0.1 . 2_565
C27 C21 C26 C22 0.0 2_565 2_565
C21 C21 C26 C22 -0.3 2_565 2_565
C19 C21 C26 C22 179.81(11) 2_565 2_565
Ru2 C21 C26 C22 89.2(2) . 2_565
C22 C21 C26 C23 -179.6 2_565 2_565
C20 C21 C26 C23 0.2 . 2_565
C22 C21 C26 C23 -179.8 . 2_565
C27 C21 C26 C23 -179.6 2_565 2_565
C21 C21 C26 C23 -179.9 2_565 2_565
C19 C21 C26 C23 0.19(11) 2_565 2_565
Ru2 C21 C26 C23 -90.5(2) . 2_565
C22 C21 C26 C28 -179.6 2_565 2_565
C23 C21 C26 C28 0.0 2_565 2_565
C20 C21 C26 C28 0.2 . 2_565
C22 C21 C26 C28 -179.8 . 2_565
C27 C21 C26 C28 -179.6 2_565 2_565
C21 C21 C26 C28 -179.9 2_565 2_565
C19 C21 C26 C28 0.19(11) 2_565 2_565
Ru2 C21 C26 C28 -90.5(2) . 2_565
C21 C22 C27 C26 0.0 2_565 2_565
C22 C22 C27 C26 -179.8 2_565 2_565
C23 C22 C27 C26 0.3 . 2_565
C21 C22 C27 C26 -179.7 . 2_565
C20 C22 C27 C26 0.1 2_565 2_565
Ru2 C22 C27 C26 91.7(2) . 2_565
C22 C22 C27 C21 -179.8 2_565 2_565
C23 C22 C27 C21 0.3 . 2_565
C21 C22 C27 C21 -179.7 . 2_565
C26 C22 C27 C21 0.0 2_565 2_565
C20 C22 C27 C21 0.1 2_565 2_565
Ru2 C22 C27 C21 91.8(2) . 2_565
C20 C23 C28 C25 0.0 2_565 2_565
C21 C23 C28 C25 -179.5 2_565 2_565
C22 C23 C28 C25 -179.7 . 2_565
C19 C23 C28 C25 0.3 . 2_565
C19 C23 C28 C25 0.32(11) 2_565 2_565
C26 C23 C28 C25 -179.5 2_565 2_565
Ru2 C23 C28 C25 91.9(2) . 2_565
C21 C23 C28 C20 -179.5 2_565 2_565
C22 C23 C28 C20 -179.7 . 2_565
C19 C23 C28 C20 0.3 . 2_565
C25 C23 C28 C20 0.0 2_565 2_565
C19 C23 C28 C20 0.31(11) 2_565 2_565
C26 C23 C28 C20 -179.5 2_565 2_565
Ru2 C23 C28 C20 91.9(2) . 2_565
C20 C23 C28 C26 179.5 2_565 2_565
C21 C23 C28 C26 0.0 2_565 2_565
C22 C23 C28 C26 -0.2 . 2_565
C19 C23 C28 C26 179.8 . 2_565
C25 C23 C28 C26 179.5 2_565 2_565
C19 C23 C28 C26 179.86(11) 2_565 2_565
Ru2 C23 C28 C26 -88.6(2) . 2_565
