#------------------------------------------------------------------------------
#$Date: 2016-03-21 10:23:07 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178648 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/59/4075959.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4075959
loop_
_publ_author_name
'Wei, Qiao-Hua'
'Zhang, Li-Yi'
'Yin, Gang-Qiang'
'Shi, Lin-Xi'
'Chen, Zhong-Ning'
_publ_section_title
;
 Luminescent Au6Ag13Cage Compounds of Arylacetylides, Metastable
 Intermediates to Au5Ag8Complexes of {1,2,3-C6(C6H4R-4)3}3-(R = H, CH3,
 But)
;
_journal_issue                   16
_journal_name_full               Organometallics
_journal_page_first              3818
_journal_paper_doi               10.1021/om050363d
_journal_volume                  24
_journal_year                    2005
_chemical_formula_sum            'C187 H138 Ag13 Au6 Cl0 F30 N0 O P6 Sb5'
_chemical_formula_weight         6349.65
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 91.52(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.281(5)
_cell_length_b                   21.627(4)
_cell_length_c                   42.693(9)
_cell_measurement_temperature    293(2)
_cell_volume                     21488(8)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.974
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.80000
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0338
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            21876
_diffrn_reflns_theta_full        23.56
_diffrn_reflns_theta_max         23.56
_diffrn_reflns_theta_min         1.45
_exptl_absorpt_coefficient_mu    5.961
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    1.963
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             11872
_refine_diff_density_max         2.540
_refine_diff_density_min         -3.562
_refine_diff_density_rms         0.291
_refine_ls_extinction_coef       0.000156(14)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.181
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     1415
_refine_ls_number_reflns         21876
_refine_ls_number_restraints     216
_refine_ls_restrained_S_all      1.179
_refine_ls_R_factor_all          0.1104
_refine_ls_R_factor_gt           0.0892
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1350P)²+375.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2638
_refine_ls_wR_factor_ref         0.2785
_reflns_number_gt                15936
_reflns_number_total             21876
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om050363dsi20050509_062135.cif
_cod_data_source_block           compound_1a(SbF6)5
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        21488(7)
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               4075959
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Au1 Au 0.12217(4) 0.05078(5) 0.12317(2) 0.0778(3) Uani 1 1 d .
Au2 Au 0.16757(5) 0.02179(6) 0.04995(3) 0.0988(4) Uani 1 1 d .
Au3 Au 0.31883(5) 0.02371(6) 0.02978(3) 0.0946(4) Uani 1 1 d .
Au4 Au 0.42129(5) 0.04682(5) 0.08926(3) 0.0852(4) Uani 1 1 d .
Au5 Au 0.36983(6) 0.07802(8) 0.16927(4) 0.1237(5) Uani 1 1 d .
Au6 Au 0.23395(6) 0.06491(8) 0.18521(4) 0.1251(5) Uani 1 1 d .
Ag1 Ag 0.12507(8) 0.13631(8) 0.17620(4) 0.0704(5) Uani 1 1 d .
Ag2 Ag 0.12905(7) -0.01199(8) 0.18564(4) 0.0679(5) Uani 1 1 d .
Ag3 Ag 0.19738(8) 0.14908(9) 0.08683(5) 0.0780(6) Uani 1 1 d .
Ag4 Ag 0.20887(7) -0.07117(9) 0.10589(5) 0.0732(5) Uani 1 1 d .
Ag5 Ag 0.22260(9) 0.08413(10) -0.00501(4) 0.0799(6) Uani 1 1 d .
Ag6 Ag 0.22777(8) -0.06300(9) 0.00822(4) 0.0738(5) Uani 1 1 d .
Ag7 Ag 0.33266(8) -0.06852(9) 0.08943(4) 0.0708(5) Uani 1 1 d .
Ag8 Ag 0.32504(8) 0.14639(9) 0.07307(4) 0.0735(5) Uani 1 1 d .
Ag9 Ag 0.46142(7) 0.14191(9) 0.13793(5) 0.0753(6) Uani 1 1 d .
Ag10 Ag 0.46363(7) -0.00325(9) 0.15021(5) 0.0750(6) Uani 1 1 d .
Ag11 Ag 0.27951(8) 0.17147(9) 0.13902(4) 0.0771(6) Uani 1 1 d .
Ag12 Ag 0.29681(8) -0.04825(9) 0.15660(4) 0.0716(5) Uani 1 1 d .
Ag13 Ag 0.2734(2) 0.0471(2) 0.10812(12) 0.2070(19) Uani 1 1 d .
Sb1 Sb 0.80307(8) 0.42634(11) -0.31971(5) 0.1008(7) Uani 1 1 d D
F11 F 0.8050(8) 0.3419(9) -0.3332(6) 0.169(9) Uani 1 1 d D
F12 F 0.8582(8) 0.4199(13) -0.2864(4) 0.187(12) Uani 1 1 d D
F13 F 0.7979(8) 0.5090(9) -0.3068(5) 0.159(8) Uani 1 1 d D
F14 F 0.7508(8) 0.4430(11) -0.3537(4) 0.162(9) Uani 1 1 d D
F15 F 0.8633(8) 0.4489(11) -0.3477(5) 0.174(10) Uani 1 1 d D
F16 F 0.7410(7) 0.4057(11) -0.2953(5) 0.163(9) Uani 1 1 d D
Sb2 Sb 0.9361(3) -0.0708(2) -0.40727(10) 0.252(3) Uani 1 1 d D
F21 F 0.918(2) -0.1568(13) -0.4023(11) 0.51(4) Uiso 1 1 d D
F22 F 0.8908(18) -0.051(2) -0.4430(8) 0.61(6) Uiso 1 1 d D
F23 F 0.9532(17) 0.0144(11) -0.4083(9) 0.34(2) Uiso 1 1 d D
F24 F 0.9906(12) -0.0833(16) -0.3729(6) 0.271(16) Uiso 1 1 d D
F25 F 1.0031(13) -0.0868(18) -0.4319(8) 0.33(2) Uiso 1 1 d D
F26 F 0.8806(13) -0.0549(17) -0.3769(7) 0.31(2) Uiso 1 1 d D
Sb3 Sb 0.54830(16) -0.03199(14) -0.35085(9) 0.1675(13) Uani 1 1 d D
F31 F 0.6276(11) -0.0090(18) -0.3484(9) 0.37(3) Uiso 1 1 d D
F32 F 0.5440(16) -0.0700(16) -0.3900(6) 0.32(2) Uiso 1 1 d D
F33 F 0.4709(11) -0.0572(17) -0.3513(9) 0.33(2) Uiso 1 1 d D
F34 F 0.5384(15) 0.0122(15) -0.3122(6) 0.300(19) Uiso 1 1 d D
F35 F 0.5230(14) 0.0458(11) -0.3690(8) 0.285(18) Uiso 1 1 d D
F36 F 0.5690(16) -0.0995(13) -0.3257(8) 0.33(2) Uiso 1 1 d D
P1 P 0.0475(3) 0.1343(3) 0.21167(16) 0.0697(17) Uani 1 1 d .
P2 P 0.0422(3) -0.0059(3) 0.21413(15) 0.0621(16) Uani 1 1 d .
P3 P 0.5545(3) 0.1379(3) 0.16450(15) 0.0703(17) Uani 1 1 d .
P4 P 0.5673(3) 0.0001(3) 0.15156(15) 0.0683(17) Uani 1 1 d .
P5 P 0.1856(3) 0.0567(3) -0.05653(15) 0.0729(18) Uani 1 1 d .
P6 P 0.2101(3) -0.0805(3) -0.04676(15) 0.0769(19) Uani 1 1 d .
C1 C 0.0000(11) 0.0659(9) 0.2073(7) 0.079(7) Uani 1 1 d .
C2 C 0.6035(9) 0.0773(11) 0.1489(5) 0.070(6) Uani 1 1 d .
C3 C 0.2201(10) -0.0134(10) -0.0731(5) 0.067(6) Uani 1 1 d .
C11 C -0.0011(8) 0.2003(7) 0.2053(5) 0.099(9) Uani 1 1 d G
C12 C -0.0544(9) 0.1944(8) 0.1901(7) 0.156(17) Uani 1 1 d G
C13 C -0.0881(8) 0.2465(11) 0.1844(8) 0.23(3) Uani 1 1 d G
C14 C -0.0686(10) 0.3044(9) 0.1939(7) 0.16(2) Uani 1 1 d G
C15 C -0.0153(12) 0.3103(6) 0.2091(6) 0.144(16) Uani 1 1 d G
C16 C 0.0184(9) 0.2583(9) 0.2148(5) 0.136(13) Uani 1 1 d G
C21 C 0.0704(10) 0.1417(8) 0.2531(4) 0.100(10) Uani 1 1 d G
C22 C 0.1287(9) 0.1472(9) 0.2605(5) 0.122(12) Uani 1 1 d G
C23 C 0.1471(8) 0.1534(11) 0.2916(6) 0.160(17) Uani 1 1 d G
C24 C 0.1072(12) 0.1541(12) 0.3152(4) 0.141(14) Uiso 1 1 d G
C25 C 0.0489(11) 0.1486(11) 0.3078(4) 0.130(12) Uiso 1 1 d G
C26 C 0.0305(8) 0.1424(9) 0.2767(5) 0.140(15) Uani 1 1 d G
C31 C -0.0073(7) -0.0679(6) 0.2028(5) 0.076(7) Uani 1 1 d G
C32 C -0.0569(8) -0.0578(7) 0.1847(6) 0.163(19) Uani 1 1 d G
C33 C -0.0913(8) -0.1075(10) 0.1755(6) 0.158(15) Uiso 1 1 d G
C34 C -0.0763(8) -0.1672(8) 0.1845(5) 0.119(11) Uani 1 1 d G
C35 C -0.0267(9) -0.1773(6) 0.2027(5) 0.095(9) Uani 1 1 d G
C36 C 0.0077(7) -0.1276(7) 0.2119(5) 0.108(10) Uani 1 1 d G
C41 C 0.0457(9) -0.0146(8) 0.2564(3) 0.097(9) Uani 1 1 d G
C42 C -0.0042(9) -0.0183(9) 0.2734(6) 0.147(18) Uani 1 1 d G
C43 C -0.0007(13) -0.0232(9) 0.3059(6) 0.16(2) Uani 1 1 d G
C44 C 0.0527(16) -0.0245(9) 0.3213(3) 0.18(3) Uani 1 1 d G
C45 C 0.1026(12) -0.0207(10) 0.3042(5) 0.20(3) Uani 1 1 d G
C46 C 0.0991(8) -0.0158(9) 0.2717(5) 0.131(14) Uani 1 1 d G
C51 C 0.5955(7) 0.2077(7) 0.1590(4) 0.086(8) Uani 1 1 d G
C52 C 0.5638(6) 0.2594(10) 0.1500(5) 0.097(9) Uani 1 1 d G
C53 C 0.5912(10) 0.3159(8) 0.1461(5) 0.126(11) Uiso 1 1 d G
C54 C 0.6502(11) 0.3207(8) 0.1513(5) 0.127(12) Uani 1 1 d G
C55 C 0.6819(7) 0.2689(11) 0.1603(5) 0.141(14) Uani 1 1 d G
C56 C 0.6545(7) 0.2124(9) 0.1642(5) 0.109(10) Uani 1 1 d G
C61 C 0.5541(7) 0.1241(11) 0.2060(3) 0.085(8) Uani 1 1 d G
C62 C 0.6053(6) 0.1128(13) 0.2224(4) 0.120(12) Uani 1 1 d G
C63 C 0.6046(9) 0.0974(14) 0.2540(5) 0.154(16) Uani 1 1 d G
C64 C 0.5526(13) 0.0935(14) 0.2692(4) 0.18(2) Uani 1 1 d G
C65 C 0.5014(9) 0.1048(14) 0.2528(5) 0.154(15) Uiso 1 1 d G
C66 C 0.5021(6) 0.1202(13) 0.2212(5) 0.146(17) Uani 1 1 d G
C71 C 0.5971(9) -0.0376(12) 0.1176(7) 0.083(8) Uani 1 1 d .
C72 C 0.6235(13) -0.1024(16) 0.1210(11) 0.140(15) Uani 1 1 d .
C73 C 0.6457(16) -0.129(2) 0.0927(10) 0.150(17) Uani 1 1 d .
C74 C 0.6360(14) -0.096(2) 0.0648(9) 0.139(16) Uani 1 1 d .
C75 C 0.6126(15) -0.0390(18) 0.0611(8) 0.125(13) Uani 1 1 d .
C76 C 0.5907(13) -0.0104(19) 0.0868(7) 0.119(12) Uani 1 1 d .
C81 C 0.5993(8) -0.0347(11) 0.1858(5) 0.090(8) Uani 1 1 d G
C82 C 0.6585(7) -0.0358(11) 0.1910(5) 0.104(10) Uani 1 1 d G
C83 C 0.6818(8) -0.0664(14) 0.2170(6) 0.163(16) Uiso 1 1 d G
C84 C 0.6459(13) -0.0958(15) 0.2378(5) 0.20(2) Uani 1 1 d G
C85 C 0.5868(12) -0.0947(14) 0.2326(6) 0.19(2) Uiso 1 1 d G
C86 C 0.5634(7) -0.0641(13) 0.2066(6) 0.166(16) Uiso 1 1 d G
C91 C 0.1970(8) 0.1152(9) -0.0867(4) 0.085(8) Uani 1 1 d G
C92 C 0.1781(10) 0.1745(11) -0.0799(4) 0.126(12) Uani 1 1 d G
C93 C 0.1831(11) 0.2215(8) -0.1019(7) 0.160(16) Uiso 1 1 d G
C94 C 0.2069(11) 0.2090(11) -0.1307(6) 0.18(2) Uani 1 1 d G
C95 C 0.2258(10) 0.1497(13) -0.1375(4) 0.152(16) Uani 1 1 d G
C96 C 0.2208(9) 0.1028(9) -0.1155(5) 0.118(11) Uani 1 1 d G
C100 C 0.1095(6) 0.0420(10) -0.0595(4) 0.084(8) Uani 1 1 d G
C102 C 0.0835(7) 0.0286(11) -0.0884(4) 0.108(10) Uani 1 1 d G
C103 C 0.0244(8) 0.0193(12) -0.0907(4) 0.124(11) Uiso 1 1 d G
C104 C -0.0086(6) 0.0234(13) -0.0641(6) 0.148(14) Uiso 1 1 d G
C105 C 0.0174(8) 0.0369(15) -0.0352(5) 0.18(2) Uani 1 1 d G
C106 C 0.0764(9) 0.0462(13) -0.0329(4) 0.132(13) Uani 1 1 d G
C111 C 0.1381(8) -0.1112(12) -0.0561(4) 0.105(10) Uani 1 1 d G
C112 C 0.1000(11) -0.1160(16) -0.0317(4) 0.158(17) Uani 1 1 d G
C113 C 0.0450(11) -0.139(2) -0.0373(6) 0.48(3) Uani 1 1 d G
C114 C 0.0281(9) -0.1576(18) -0.0674(8) 0.22(3) Uiso 1 1 d G
C115 C 0.0662(12) -0.1528(15) -0.0918(5) 0.21(3) Uani 1 1 d G
C116 C 0.1212(10) -0.1296(14) -0.0861(4) 0.159(17) Uani 1 1 d G
C121 C 0.2632(9) -0.1340(10) -0.0612(5) 0.099(9) Uani 1 1 d G
C122 C 0.2486(9) -0.1929(11) -0.0717(6) 0.170(17) Uiso 1 1 d G
C123 C 0.2914(13) -0.2339(8) -0.0804(6) 0.163(16) Uiso 1 1 d G
C124 C 0.3487(11) -0.2159(11) -0.0786(6) 0.138(13) Uiso 1 1 d G
C125 C 0.3633(8) -0.1570(12) -0.0681(5) 0.146(14) Uani 1 1 d G
C126 C 0.3205(10) -0.1160(8) -0.0594(5) 0.107(10) Uani 1 1 d G
C211 C 0.1137(10) 0.1444(14) 0.1193(6) 0.083(8) Uani 1 1 d .
C212 C 0.1001(10) 0.2007(13) 0.1182(6) 0.079(7) Uani 1 1 d .
C213 C 0.0875(11) 0.2626(10) 0.1175(7) 0.104(10) Uani 1 1 d G
C214 C 0.1267(12) 0.3031(17) 0.1047(10) 0.500 Uiso 1 1 d G
C215 C 0.1140(19) 0.3658(15) 0.1025(12) 0.500 Uiso 1 1 d G
C216 C 0.062(2) 0.3880(9) 0.1133(10) 0.23(3) Uiso 1 1 d G
C217 C 0.0229(13) 0.3474(14) 0.1262(8) 0.18(2) Uani 1 1 d G
C218 C 0.0356(9) 0.2847(12) 0.1283(6) 0.132(12) Uiso 1 1 d G
C221 C 0.1173(10) -0.0403(14) 0.1293(5) 0.080(8) Uani 1 1 d .
C222 C 0.1053(10) -0.0964(11) 0.1316(5) 0.071(7) Uani 1 1 d .
C223 C 0.0905(12) -0.1572(10) 0.1311(5) 0.099(9) Uani 1 1 d G
C224 C 0.1309(9) -0.2037(16) 0.1362(7) 0.186(19) Uiso 1 1 d G
C225 C 0.1139(15) -0.2653(13) 0.1356(8) 0.23(2) Uiso 1 1 d G
C226 C 0.0566(18) -0.2804(10) 0.1300(8) 0.177(17) Uiso 1 1 d G
C227 C 0.0162(11) -0.2339(16) 0.1249(7) 0.189(19) Uiso 1 1 d G
C228 C 0.0331(10) -0.1723(13) 0.1254(6) 0.142(13) Uiso 1 1 d G
C231 C 0.1587(10) 0.1133(14) 0.0395(6) 0.084(8) Uani 1 1 d .
C232 C 0.1466(15) 0.1611(14) 0.0281(7) 0.107(10) Uani 1 1 d .
C233 C 0.143(3) 0.223(3) 0.0158(8) 0.22(3) Uani 1 1 d G
C234 C 0.088(3) 0.225(3) 0.0023(12) 0.24(3) Uiso 1 1 d G
C235 C 0.066(2) 0.280(4) -0.0095(14) 0.500 Uiso 1 1 d G
C236 C 0.099(5) 0.334(3) -0.0076(17) 0.500 Uiso 1 1 d G
C237 C 0.154(4) 0.332(3) 0.006(2) 0.500 Uiso 1 1 d G
C238 C 0.176(2) 0.276(4) 0.0177(15) 0.500 Uiso 1 1 d G
C241 C 0.1687(10) -0.0746(17) 0.0519(5) 0.097(10) Uani 1 1 d .
C242 C 0.1605(13) -0.1305(12) 0.0513(6) 0.091(9) Uani 1 1 d .
C243 C 0.1467(15) -0.1825(11) 0.0543(7) 0.142(14) Uani 1 1 d G
C244 C 0.0915(13) -0.2046(16) 0.0481(8) 0.22(3) Uani 1 1 d G
C245 C 0.0815(15) -0.2679(18) 0.0465(9) 0.26(3) Uiso 1 1 d G
C246 C 0.127(2) -0.3091(11) 0.0512(11) 0.24(3) Uani 1 1 d G
C247 C 0.1819(17) -0.2870(14) 0.0574(11) 0.53(9) Uiso 1 1 d G
C248 C 0.1919(13) -0.2237(16) 0.0590(9) 0.26(4) Uani 1 1 d G
C251 C 0.3136(9) 0.1204(14) 0.0178(5) 0.079(8) Uani 1 1 d .
C252 C 0.3174(12) 0.1664(10) 0.0064(6) 0.080(8) Uani 1 1 d .
C253 C 0.3266(17) 0.2181(12) -0.0080(7) 0.137(13) Uani 1 1 d G
C254 C 0.2906(14) 0.2458(18) -0.0304(8) 0.23(3) Uani 1 1 d G
C255 C 0.3048(19) 0.3031(18) -0.0428(8) 0.21(2) Uiso 1 1 d G
C256 C 0.355(2) 0.3326(15) -0.0329(11) 0.25(3) Uiso 1 1 d G
C257 C 0.3911(17) 0.305(2) -0.0105(13) 0.72(13) Uiso 1 1 d G
C258 C 0.3768(16) 0.248(2) 0.0019(9) 0.27(3) Uiso 1 1 d G
C261 C 0.2253(10) 0.1623(15) 0.1822(6) 0.089(9) Uani 1 1 d .
C262 C 0.2125(11) 0.2121(13) 0.1935(6) 0.084(8) Uani 1 1 d .
C263 C 0.1967(12) 0.2703(12) 0.2058(9) 0.123(12) Uani 1 1 d G
C264 C 0.1660(16) 0.313(2) 0.1874(7) 0.22(2) Uiso 1 1 d G
C265 C 0.1497(18) 0.3690(18) 0.2000(11) 0.500 Uiso 1 1 d G
C266 C 0.1642(18) 0.3832(15) 0.2310(12) 0.22(2) Uiso 1 1 d G
C267 C 0.1949(17) 0.341(2) 0.2494(7) 0.20(2) Uiso 1 1 d G
C268 C 0.2112(14) 0.2845(17) 0.2368(8) 0.21(2) Uiso 1 1 d G
C271 C 0.4263(10) 0.1404(14) 0.0831(6) 0.081(7) Uani 1 1 d .
C272 C 0.4419(10) 0.1926(12) 0.0797(6) 0.075(7) Uani 1 1 d .
C273 C 0.4603(10) 0.2562(9) 0.0766(6) 0.105(10) Uani 1 1 d G
C274 C 0.5016(11) 0.2683(13) 0.0546(6) 0.187(19) Uiso 1 1 d G
C275 C 0.5204(12) 0.3285(16) 0.0499(7) 0.20(2) Uiso 1 1 d G
C276 C 0.4978(15) 0.3766(11) 0.0673(9) 0.21(3) Uani 1 1 d G
C277 C 0.4564(15) 0.3646(11) 0.0893(8) 0.21(3) Uani 1 1 d G
C278 C 0.4377(11) 0.3043(13) 0.0940(6) 0.167(18) Uani 1 1 d G
C281 C 0.4326(10) -0.0442(12) 0.0967(6) 0.076(7) Uani 1 1 d .
C282 C 0.4505(10) -0.0943(12) 0.0999(7) 0.088(8) Uani 1 1 d .
C283 C 0.4752(13) -0.1497(13) 0.1057(10) 0.144(13) Uiso 1 1 d G
C284 C 0.4997(16) -0.185(2) 0.0823(6) 0.20(2) Uiso 1 1 d G
C285 C 0.5249(15) -0.2416(18) 0.0897(10) 0.22(2) Uiso 1 1 d G
C286 C 0.5256(16) -0.2628(14) 0.1205(12) 0.21(2) Uiso 1 1 d G
C287 C 0.5011(19) -0.228(2) 0.1438(8) 0.35(5) Uiso 1 1 d G
C288 C 0.4759(16) -0.1709(19) 0.1364(8) 0.21(2) Uiso 1 1 d G
C291 C 0.3736(11) 0.1764(15) 0.1634(7) 0.091(8) Uani 1 1 d .
C292 C 0.3759(10) 0.2294(14) 0.1666(7) 0.092(9) Uani 1 1 d .
C293 C 0.3785(12) 0.2951(10) 0.1700(6) 0.114(10) Uani 1 1 d G
C294 C 0.4280(9) 0.3257(13) 0.1802(7) 0.17(2) Uani 1 1 d G
C295 C 0.4288(13) 0.3899(13) 0.1816(7) 0.154(16) Uani 1 1 d G
C296 C 0.3801(19) 0.4235(10) 0.1728(8) 0.20(2) Uiso 1 1 d G
C297 C 0.3306(15) 0.3928(17) 0.1626(9) 0.26(3) Uiso 1 1 d G
C298 C 0.3298(10) 0.3286(18) 0.1612(8) 0.25(3) Uiso 1 1 d G
C301 C 0.3841(11) -0.0066(14) 0.1790(6) 0.088(8) Uani 1 1 d .
C302 C 0.3938(11) -0.0560(17) 0.1953(7) 0.107(11) Uani 1 1 d .
C303 C 0.4021(10) -0.1080(12) 0.2170(5) 0.112(11) Uani 1 1 d G
C304 C 0.4158(12) -0.0961(12) 0.2483(6) 0.166(19) Uani 1 1 d G
C305 C 0.4270(13) -0.1448(17) 0.2688(5) 0.21(3) Uiso 1 1 d G
C306 C 0.4246(14) -0.2054(14) 0.2581(8) 0.23(3) Uani 1 1 d G
C307 C 0.4110(15) -0.2173(11) 0.2267(9) 0.25(3) Uani 1 1 d G
C308 C 0.3998(13) -0.1686(15) 0.2062(6) 0.175(18) Uiso 1 1 d G
C311 C 0.3231(10) -0.0661(12) 0.0326(6) 0.073(7) Uani 1 1 d .
C312 C 0.3275(10) -0.1212(14) 0.0310(5) 0.080(8) Uani 1 1 d .
C313 C 0.3350(16) -0.1935(14) 0.0252(9) 0.130(12) Uiso 1 1 d G
C314 C 0.3029(17) -0.226(2) 0.0029(10) 0.500 Uiso 1 1 d G
C315 C 0.313(2) -0.289(2) -0.0015(11) 0.29(4) Uiso 1 1 d G
C316 C 0.356(2) -0.3188(14) 0.0164(13) 0.22(2) Uiso 1 1 d G
C317 C 0.388(2) -0.286(2) 0.0386(13) 0.500 Uiso 1 1 d G
C318 C 0.3775(18) -0.223(2) 0.0430(9) 0.33(4) Uiso 1 1 d G
C321 C 0.2288(9) -0.0237(13) 0.1962(5) 0.071(7) Uani 1 1 d .
C322 C 0.2226(9) -0.0760(13) 0.2065(6) 0.074(7) Uani 1 1 d .
C323 C 0.2164(14) -0.1367(12) 0.2214(6) 0.107(10) Uani 1 1 d G
C324 C 0.1674(12) -0.1722(18) 0.2161(7) 0.23(3) Uiso 1 1 d G
C325 C 0.1612(15) -0.2283(16) 0.2315(10) 0.26(3) Uiso 1 1 d G
C326 C 0.204(2) -0.2488(12) 0.2523(9) 0.178(18) Uiso 1 1 d G
C327 C 0.2531(17) -0.2133(19) 0.2576(8) 0.25(3) Uiso 1 1 d G
C328 C 0.2593(11) -0.1572(17) 0.2422(8) 0.23(3) Uiso 1 1 d G
C331 C 0.2656(11) 0.2180(11) 0.0926(6) 0.074(7) Uani 1 1 d .
C332 C 0.2687(13) 0.2704(14) 0.0863(8) 0.105(10) Uani 1 1 d .
C333 C 0.274(2) 0.3387(19) 0.0783(12) 0.21(3) Uani 1 1 d G
C334 C 0.313(2) 0.353(3) 0.0551(12) 0.25(3) Uiso 1 1 d G
C335 C 0.319(3) 0.413(4) 0.0453(14) 0.500 Uiso 1 1 d G
C336 C 0.287(4) 0.460(2) 0.059(2) 0.500 Uiso 1 1 d G
C337 C 0.248(3) 0.446(3) 0.082(2) 0.500 Uiso 1 1 d G
C338 C 0.242(2) 0.386(4) 0.0916(13) 0.500 Uiso 1 1 d G
C341 C 0.2836(10) -0.1288(12) 0.1224(6) 0.073(7) Uani 1 1 d .
C342 C 0.2930(9) -0.1794(11) 0.1281(6) 0.071(7) Uani 1 1 d .
C343 C 0.3106(13) -0.2401(12) 0.1380(9) 0.136(14) Uani 1 1 d G
C344 C 0.3491(16) -0.280(2) 0.1240(9) 0.500 Uiso 1 1 d G
C345 C 0.3590(17) -0.3385(17) 0.1366(13) 0.24(3) Uiso 1 1 d G
C346 C 0.330(2) -0.3570(14) 0.1632(13) 0.32(5) Uani 1 1 d G
C347 C 0.292(2) -0.317(2) 0.1772(10) 0.500 Uiso 1 1 d G
C348 C 0.2821(15) -0.2587(18) 0.1646(9) 0.21(2) Uiso 1 1 d G
Sb4 Sb -0.1546(6) 0.0591(6) 0.3191(3) 0.500 Uiso 1 1 d D
F41 F -0.147(2) 0.1427(15) 0.3045(13) 0.500 Uiso 1 1 d D
F42 F -0.145(2) 0.070(3) 0.3632(6) 0.500 Uiso 1 1 d D
F43 F -0.159(2) -0.0254(15) 0.3315(13) 0.500 Uiso 1 1 d D
F44 F -0.174(2) 0.037(2) 0.2763(7) 0.500 Uiso 1 1 d D
F45 F -0.2378(11) 0.064(3) 0.3229(13) 0.500 Uiso 1 1 d D
F46 F -0.0761(12) 0.050(2) 0.3106(13) 0.500 Uiso 1 1 d D
Sb5 Sb 0.5000 0.0000 0.0000 0.500 Uiso 1 2 d SD
F51 F 0.4999(17) -0.08093(10) -0.0009(9) 0.276(17) Uiso 1 1 d D
F52 F 0.5718(6) 0.0213(17) -0.0045(15) 0.500 Uiso 1 1 d D
F53 F 0.484(3) 0.0194(18) 0.0387(4) 0.500 Uiso 1 1 d D
Sb6 Sb 0.8058(11) 0.3988(13) 0.1102(6) 0.500 Uiso 0.50 1 d PD
F61 F 0.778(4) 0.483(2) 0.113(2) 0.500 Uiso 0.50 1 d PD
F62 F 0.824(4) 0.395(5) 0.0671(9) 0.500 Uiso 0.50 1 d PD
F63 F 0.830(4) 0.316(2) 0.108(2) 0.500 Uiso 0.50 1 d PD
F64 F 0.798(4) 0.394(5) 0.1548(8) 0.500 Uiso 0.50 1 d PD
F65 F 0.8847(19) 0.422(5) 0.120(2) 0.500 Uiso 0.50 1 d PD
F66 F 0.7284(17) 0.376(4) 0.106(2) 0.500 Uiso 0.50 1 d PD
O1 O 0.319(2) 0.067(3) 0.2564(13) 0.31(2) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C221 Au1 C211 170.7(9) . .
C221 Au1 Ag1 121.6(6) . .
C211 Au1 Ag1 55.6(7) . .
C221 Au1 Ag2 55.7(6) . .
C211 Au1 Ag2 121.7(7) . .
Ag1 Au1 Ag2 66.25(6) . .
C221 Au1 Ag3 139.3(7) . .
C211 Au1 Ag3 49.5(7) . .
Ag1 Au1 Ag3 87.32(6) . .
Ag2 Au1 Ag3 136.05(6) . .
C231 Au2 C241 168.6(9) . .
C231 Au2 Ag6 121.4(7) . .
C241 Au2 Ag6 52.8(7) . .
C231 Au2 Ag5 55.9(7) . .
C241 Au2 Ag5 118.2(6) . .
Ag6 Au2 Ag5 65.71(6) . .
C231 Au2 Ag3 45.6(7) . .
C241 Au2 Ag3 145.9(6) . .
Ag6 Au2 Ag3 136.56(7) . .
Ag5 Au2 Ag3 84.74(6) . .
C231 Au2 Ag4 142.0(7) . .
C241 Au2 Ag4 49.4(6) . .
Ag6 Au2 Ag4 85.58(6) . .
Ag5 Au2 Ag4 136.40(7) . .
Ag3 Au2 Ag4 96.51(6) . .
C311 Au3 C251 169.8(9) . .
C311 Au3 Ag6 54.7(7) . .
C251 Au3 Ag6 120.4(6) . .
C311 Au3 Ag5 120.5(7) . .
C251 Au3 Ag5 54.3(6) . .
Ag6 Au3 Ag5 66.24(6) . .
C311 Au3 Ag8 141.4(7) . .
C251 Au3 Ag8 48.7(6) . .
Ag6 Au3 Ag8 135.93(7) . .
Ag5 Au3 Ag8 86.92(6) . .
C311 Au3 Ag7 48.3(7) . .
C251 Au3 Ag7 141.8(6) . .
Ag6 Au3 Ag7 84.83(6) . .
Ag5 Au3 Ag7 136.35(7) . .
Ag8 Au3 Ag7 93.08(6) . .
C281 Au4 C271 169.1(9) . .
C281 Au4 Ag10 57.6(7) . .
C271 Au4 Ag10 117.1(7) . .
C281 Au4 Ag9 121.1(7) . .
C271 Au4 Ag9 53.3(7) . .
Ag10 Au4 Ag9 63.88(6) . .
C281 Au4 Ag8 142.0(6) . .
C271 Au4 Ag8 48.8(7) . .
Ag10 Au4 Ag8 131.02(7) . .
Ag9 Au4 Ag8 83.83(6) . .
C281 Au4 Ag7 47.6(6) . .
C271 Au4 Ag7 143.3(7) . .
Ag10 Au4 Ag7 85.04(6) . .
Ag9 Au4 Ag7 134.52(6) . .
Ag8 Au4 Ag7 94.42(6) . .
C301 Au5 C291 166.3(10) . .
C301 Au5 Ag9 115.7(7) . .
C291 Au5 Ag9 55.9(7) . .
C301 Au5 Ag10 50.1(7) . .
C291 Au5 Ag10 121.9(7) . .
Ag9 Au5 Ag10 66.14(6) . .
C301 Au5 Ag11 144.3(7) . .
C291 Au5 Ag11 49.3(7) . .
Ag9 Au5 Ag11 89.78(7) . .
Ag10 Au5 Ag11 139.45(8) . .
C301 Au5 Ag12 46.9(7) . .
C291 Au5 Ag12 146.7(7) . .
Ag9 Au5 Ag12 135.30(8) . .
Ag10 Au5 Ag12 80.83(7) . .
Ag11 Au5 Ag12 97.43(6) . .
C301 Au5 Au6 92.0(7) . .
C291 Au5 Au6 98.8(7) . .
Ag9 Au5 Au6 150.03(8) . .
Ag10 Au5 Au6 137.53(7) . .
Ag11 Au5 Au6 60.27(5) . .
Ag12 Au5 Au6 57.12(5) . .
C321 Au6 C261 166.3(9) . .
C321 Au6 Ag2 53.0(6) . .
C261 Au6 Ag2 118.8(6) . .
C321 Au6 Ag1 118.4(6) . .
C261 Au6 Ag1 53.0(6) . .
Ag2 Au6 Ag1 65.96(6) . .
C321 Au6 Ag12 50.5(6) . .
C261 Au6 Ag12 143.2(7) . .
Ag2 Au6 Ag12 87.55(7) . .
Ag1 Au6 Ag12 139.61(8) . .
C321 Au6 Ag11 149.2(6) . .
C261 Au6 Ag11 44.4(7) . .
Ag2 Au6 Ag11 133.63(8) . .
Ag1 Au6 Ag11 81.01(7) . .
Ag12 Au6 Ag11 98.97(7) . .
C321 Au6 Au5 101.5(6) . .
C261 Au6 Au5 89.6(6) . .
Ag2 Au6 Au5 148.81(7) . .
Ag1 Au6 Au5 138.80(7) . .
Ag12 Au6 Au5 61.26(5) . .
Ag11 Au6 Au5 58.36(5) . .
P1 Ag1 C261 133.2(6) . .
P1 Ag1 C211 124.6(6) . .
C261 Ag1 C211 99.6(8) . .
P1 Ag1 C262 114.5(6) . .
C261 Ag1 C262 26.9(8) . .
C211 Ag1 C262 106.8(8) . .
P1 Ag1 Au1 118.51(17) . .
C261 Ag1 Au1 103.4(7) . .
C211 Ag1 Au1 43.6(7) . .
C262 Ag1 Au1 126.7(6) . .
P1 Ag1 Au6 124.25(18) . .
C261 Ag1 Au6 44.7(8) . .
C211 Ag1 Au6 103.6(6) . .
C262 Ag1 Au6 69.4(6) . .
Au1 Ag1 Au6 76.97(6) . .
P1 Ag1 Ag2 85.55(15) . .
C261 Ag1 Ag2 101.2(8) . .
C211 Ag1 Ag2 101.3(7) . .
C262 Ag1 Ag2 123.3(6) . .
Au1 Ag1 Ag2 57.92(5) . .
Au6 Ag1 Ag2 56.58(5) . .
C321 Ag2 P2 138.4(6) . .
C321 Ag2 C221 103.8(8) . .
P2 Ag2 C221 115.6(6) . .
C321 Ag2 C322 26.8(7) . .
P2 Ag2 C322 123.0(6) . .
C221 Ag2 C322 104.9(7) . .
C321 Ag2 Au6 41.8(6) . .
P2 Ag2 Au6 133.01(16) . .
C221 Ag2 Au6 101.7(6) . .
C322 Ag2 Au6 68.4(6) . .
C321 Ag2 Au1 104.3(5) . .
P2 Ag2 Au1 113.74(17) . .
C221 Ag2 Au1 41.3(7) . .
C322 Ag2 Au1 123.2(5) . .
Au6 Ag2 Au1 76.35(6) . .
C321 Ag2 Ag1 98.9(7) . .
P2 Ag2 Ag1 89.24(15) . .
C221 Ag2 Ag1 97.0(7) . .
C322 Ag2 Ag1 124.6(6) . .
Au6 Ag2 Ag1 57.45(6) . .
Au1 Ag2 Ag1 55.83(5) . .
C331 Ag3 C231 126.0(9) . .
C331 Ag3 C211 123.9(9) . .
C231 Ag3 C211 100.6(8) . .
C331 Ag3 Ag11 49.2(6) . .
C231 Ag3 Ag11 160.8(6) . .
C211 Ag3 Ag11 95.2(6) . .
C331 Ag3 Ag13 92.7(6) . .
C231 Ag3 Ag13 103.5(8) . .
C211 Ag3 Ag13 106.1(7) . .
Ag11 Ag3 Ag13 61.15(11) . .
C331 Ag3 Ag8 47.5(6) . .
C231 Ag3 Ag8 100.6(6) . .
C211 Ag3 Ag8 156.0(6) . .
Ag11 Ag3 Ag8 62.00(7) . .
Ag13 Ag3 Ag8 57.71(11) . .
C331 Ag3 Au1 143.9(6) . .
C231 Ag3 Au1 89.8(7) . .
C211 Ag3 Au1 39.9(7) . .
Ag11 Ag3 Au1 95.50(7) . .
Ag13 Ag3 Au1 71.60(11) . .
Ag8 Ag3 Au1 129.30(8) . .
C331 Ag3 Au2 141.2(7) . .
C231 Ag3 Au2 38.8(8) . .
C211 Ag3 Au2 94.4(7) . .
Ag11 Ag3 Au2 129.49(8) . .
Ag13 Ag3 Au2 68.52(11) . .
Ag8 Ag3 Au2 95.03(7) . .
Au1 Ag3 Au2 63.62(5) . .
C341 Ag4 C241 123.4(9) . .
C341 Ag4 C221 134.0(8) . .
C241 Ag4 C221 94.4(8) . .
C341 Ag4 Ag13 94.7(7) . .
C241 Ag4 Ag13 103.6(8) . .
C221 Ag4 Ag13 101.3(7) . .
C341 Ag4 Ag12 49.5(7) . .
C241 Ag4 Ag12 156.9(6) . .
C221 Ag4 Ag12 104.1(5) . .
Ag13 Ag4 Ag12 59.73(11) . .
C341 Ag4 Ag7 48.5(6) . .
C241 Ag4 Ag7 97.2(6) . .
C221 Ag4 Ag7 159.9(6) . .
Ag13 Ag4 Ag7 59.98(11) . .
Ag12 Ag4 Ag7 61.25(6) . .
C341 Ag4 Au2 142.1(6) . .
C241 Ag4 Au2 40.0(9) . .
C221 Ag4 Au2 83.6(6) . .
Ag13 Ag4 Au2 68.27(11) . .
Ag12 Ag4 Au2 127.97(8) . .
Ag7 Ag4 Au2 94.82(7) . .
P5 Ag5 C251 136.8(6) . .
P5 Ag5 C231 123.0(6) . .
C251 Ag5 C231 98.2(8) . .
P5 Ag5 Au3 126.55(19) . .
C251 Ag5 Au3 45.8(7) . .
C231 Ag5 Au3 100.7(7) . .
P5 Ag5 Au2 116.69(18) . .
C251 Ag5 Au2 102.4(6) . .
C231 Ag5 Au2 41.9(7) . .
Au3 Ag5 Au2 75.17(6) . .
P5 Ag5 Ag6 85.85(18) . .
C251 Ag5 Ag6 102.6(7) . .
C231 Ag5 Ag6 97.7(7) . .
Au3 Ag5 Ag6 56.88(5) . .
Au2 Ag5 Ag6 55.92(6) . .
C241 Ag6 P6 131.9(6) . .
C241 Ag6 C311 101.7(8) . .
P6 Ag6 C311 123.1(6) . .
C241 Ag6 Au2 44.7(9) . .
P6 Ag6 Au2 128.2(2) . .
C311 Ag6 Au2 101.7(6) . .
C241 Ag6 Au3 104.4(7) . .
P6 Ag6 Au3 120.43(18) . .
C311 Ag6 Au3 41.0(6) . .
Au2 Ag6 Au3 76.41(6) . .
C241 Ag6 Ag5 102.9(9) . .
P6 Ag6 Ag5 88.83(18) . .
C311 Ag6 Ag5 97.6(6) . .
Au2 Ag6 Ag5 58.37(6) . .
Au3 Ag6 Ag5 56.88(6) . .
C341 Ag7 C281 123.6(9) . .
C341 Ag7 C311 127.0(8) . .
C281 Ag7 C311 100.7(8) . .
C341 Ag7 Ag13 94.1(6) . .
C281 Ag7 Ag13 103.7(6) . .
C311 Ag7 Ag13 102.6(6) . .
C341 Ag7 Ag4 48.1(6) . .
C281 Ag7 Ag4 156.0(6) . .
C311 Ag7 Ag4 99.9(6) . .
Ag13 Ag7 Ag4 59.69(11) . .
C341 Ag7 Ag12 48.5(6) . .
C281 Ag7 Ag12 97.9(6) . .
C311 Ag7 Ag12 156.7(6) . .
Ag13 Ag7 Ag12 58.99(11) . .
Ag4 Ag7 Ag12 59.32(6) . .
C341 Ag7 Au4 141.4(6) . .
C281 Ag7 Au4 38.3(6) . .
C311 Ag7 Au4 91.3(6) . .
Ag13 Ag7 Au4 69.71(11) . .
Ag4 Ag7 Au4 129.40(8) . .
Ag12 Ag7 Au4 94.70(7) . .
C341 Ag7 Au3 143.6(6) . .
C281 Ag7 Au3 92.4(6) . .
C311 Ag7 Au3 36.8(6) . .
Ag13 Ag7 Au3 69.92(11) . .
Ag4 Ag7 Au3 96.90(7) . .
Ag12 Ag7 Au3 128.90(8) . .
Au4 Ag7 Au3 64.82(5) . .
C331 Ag8 C271 125.8(9) . .
C331 Ag8 C251 117.7(9) . .
C271 Ag8 C251 104.1(8) . .
C331 Ag8 Ag13 93.0(6) . .
C271 Ag8 Ag13 106.8(7) . .
C251 Ag8 Ag13 107.1(7) . .
C331 Ag8 Ag3 45.8(6) . .
C271 Ag8 Ag3 158.4(6) . .
C251 Ag8 Ag3 96.3(5) . .
Ag13 Ag8 Ag3 59.60(11) . .
C331 Ag8 Ag11 46.5(6) . .
C271 Ag8 Ag11 101.9(6) . .
C251 Ag8 Ag11 153.5(5) . .
Ag13 Ag8 Ag11 60.09(12) . .
Ag3 Ag8 Ag11 57.28(7) . .
C331 Ag8 Au4 145.5(6) . .
C271 Ag8 Au4 40.2(7) . .
C251 Ag8 Au4 96.5(6) . .
Ag13 Ag8 Au4 71.61(11) . .
Ag3 Ag8 Au4 131.19(8) . .
Ag11 Ag8 Au4 100.28(7) . .
C331 Ag8 Au3 139.2(6) . .
C271 Ag8 Au3 95.0(7) . .
C251 Ag8 Au3 41.8(7) . .
Ag13 Ag8 Au3 70.98(12) . .
Ag3 Ag8 Au3 95.55(7) . .
Ag11 Ag8 Au3 130.92(8) . .
Au4 Ag8 Au3 65.67(5) . .
P3 Ag9 C291 123.2(7) . .
P3 Ag9 C271 135.8(6) . .
C291 Ag9 C271 99.5(9) . .
P3 Ag9 Au5 115.28(18) . .
C291 Ag9 Au5 46.3(7) . .
C271 Ag9 Au5 101.7(6) . .
P3 Ag9 Au4 123.29(18) . .
C291 Ag9 Au4 105.2(7) . .
C271 Ag9 Au4 41.9(7) . .
Au5 Ag9 Au4 77.14(6) . .
P3 Ag9 Ag10 82.94(18) . .
C291 Ag9 Ag10 103.7(7) . .
C271 Ag9 Ag10 98.5(7) . .
Au5 Ag9 Ag10 57.49(6) . .
Au4 Ag9 Ag10 56.70(5) . .
C301 Ag10 P4 145.5(7) . .
C301 Ag10 C281 105.2(8) . .
P4 Ag10 C281 107.0(6) . .
C301 Ag10 Au5 40.5(8) . .
P4 Ag10 Au5 136.58(18) . .
C281 Ag10 Au5 105.2(6) . .
C301 Ag10 Au4 103.4(7) . .
P4 Ag10 Au4 108.63(17) . .
C281 Ag10 Au4 42.0(6) . .
Au5 Ag10 Au4 78.00(6) . .
C301 Ag10 Ag9 96.4(8) . .
P4 Ag10 Ag9 89.22(17) . .
C281 Ag10 Ag9 101.1(6) . .
Au5 Ag10 Ag9 56.37(6) . .
Au4 Ag10 Ag9 59.43(5) . .
C331 Ag11 C261 133.4(10) . .
C331 Ag11 C291 118.2(10) . .
C261 Ag11 C291 99.9(9) . .
C331 Ag11 Ag3 47.7(6) . .
C261 Ag11 Ag3 103.7(6) . .
C291 Ag11 Ag3 154.6(7) . .
C331 Ag11 Ag13 90.5(6) . .
C261 Ag11 Ag13 104.9(8) . .
C291 Ag11 Ag13 105.2(8) . .
Ag3 Ag11 Ag13 59.73(11) . .
C331 Ag11 Ag8 46.8(6) . .
C261 Ag11 Ag8 159.7(7) . .
C291 Ag11 Ag8 94.1(7) . .
Ag3 Ag11 Ag8 60.72(6) . .
Ag13 Ag11 Ag8 56.89(11) . .
C331 Ag11 Au5 136.6(6) . .
C261 Ag11 Au5 89.5(8) . .
C291 Ag11 Au5 42.6(8) . .
Ag3 Ag11 Au5 128.02(9) . .
Ag13 Ag11 Au5 68.29(11) . .
Ag8 Ag11 Au5 91.12(7) . .
C331 Ag11 Au6 145.0(6) . .
C261 Ag11 Au6 40.8(8) . .
C291 Ag11 Au6 94.4(7) . .
Ag3 Ag11 Au6 97.34(7) . .
Ag13 Ag11 Au6 67.41(11) . .
Ag8 Ag11 Au6 123.95(8) . .
Au5 Ag11 Au6 61.38(5) . .
C341 Ag12 C301 129.7(9) . .
C341 Ag12 C321 122.4(9) . .
C301 Ag12 C321 101.8(9) . .
C341 Ag12 Ag13 93.7(6) . .
C301 Ag12 Ag13 99.0(7) . .
C321 Ag12 Ag13 103.0(6) . .
C341 Ag12 Ag4 48.1(6) . .
C301 Ag12 Ag4 155.5(6) . .
C321 Ag12 Ag4 95.4(5) . .
Ag13 Ag12 Ag4 59.87(11) . .
C341 Ag12 Ag7 47.5(6) . .
C301 Ag12 Ag7 100.3(6) . .
C321 Ag12 Ag7 153.8(5) . .
Ag13 Ag12 Ag7 59.41(11) . .
Ag4 Ag12 Ag7 59.43(6) . .
C341 Ag12 Au6 142.3(6) . .
C301 Ag12 Au6 87.2(8) . .
C321 Ag12 Au6 39.4(6) . .
Ag13 Ag12 Au6 69.37(11) . .
Ag4 Ag12 Au6 95.43(7) . .
Ag7 Ag12 Au6 128.78(8) . .
C341 Ag12 Au5 143.7(6) . .
C301 Ag12 Au5 35.4(8) . .
C321 Ag12 Au5 92.8(7) . .
Ag13 Ag12 Au5 67.53(11) . .
Ag4 Ag12 Au5 127.28(8) . .
Ag7 Ag12 Au5 97.04(7) . .
Au6 Ag12 Au5 61.62(5) . .
Ag8 Ag13 Ag3 62.69(11) . .
Ag8 Ag13 Ag12 143.68(19) . .
Ag3 Ag13 Ag12 146.3(2) . .
Ag8 Ag13 Ag4 147.1(2) . .
Ag3 Ag13 Ag4 109.57(16) . .
Ag12 Ag13 Ag4 60.40(11) . .
Ag8 Ag13 Ag7 106.42(17) . .
Ag3 Ag13 Ag7 145.4(2) . .
Ag12 Ag13 Ag7 61.60(11) . .
Ag4 Ag13 Ag7 60.33(11) . .
Ag8 Ag13 Ag11 63.02(12) . .
Ag3 Ag13 Ag11 59.12(11) . .
Ag12 Ag13 Ag11 108.14(17) . .
Ag4 Ag13 Ag11 143.70(19) . .
Ag7 Ag13 Ag11 148.78(19) . .
F16 Sb1 F13 90.5(9) . .
F16 Sb1 F12 94.8(9) . .
F13 Sb1 F12 84.1(10) . .
F16 Sb1 F14 89.0(8) . .
F13 Sb1 F14 89.9(9) . .
F12 Sb1 F14 172.9(11) . .
F16 Sb1 F11 88.0(9) . .
F13 Sb1 F11 177.7(9) . .
F12 Sb1 F11 97.7(10) . .
F14 Sb1 F11 88.4(9) . .
F16 Sb1 F15 175.6(9) . .
F13 Sb1 F15 89.6(9) . .
F12 Sb1 F15 89.6(9) . .
F14 Sb1 F15 86.6(9) . .
F11 Sb1 F15 91.8(9) . .
F22 Sb2 F23 82.7(14) . .
F22 Sb2 F26 97.9(15) . .
F23 Sb2 F26 89.3(13) . .
F22 Sb2 F21 100.9(16) . .
F23 Sb2 F21 175.0(16) . .
F26 Sb2 F21 86.7(14) . .
F22 Sb2 F24 172.0(16) . .
F23 Sb2 F24 91.2(13) . .
F26 Sb2 F24 87.1(12) . .
F21 Sb2 F24 85.6(14) . .
F22 Sb2 F25 92.4(14) . .
F23 Sb2 F25 89.3(13) . .
F26 Sb2 F25 169.3(14) . .
F21 Sb2 F25 94.1(14) . .
F24 Sb2 F25 82.3(12) . .
F32 Sb3 F36 100.3(13) . .
F32 Sb3 F33 80.5(13) . .
F36 Sb3 F33 90.7(13) . .
F32 Sb3 F31 101.1(14) . .
F36 Sb3 F31 86.4(13) . .
F33 Sb3 F31 176.8(15) . .
F32 Sb3 F34 169.4(14) . .
F36 Sb3 F34 86.0(12) . .
F33 Sb3 F34 90.9(13) . .
F31 Sb3 F34 87.8(13) . .
F32 Sb3 F35 90.9(13) . .
F36 Sb3 F35 168.4(14) . .
F33 Sb3 F35 88.1(12) . .
F31 Sb3 F35 94.6(13) . .
F34 Sb3 F35 82.5(12) . .
C11 P1 C21 103.7(10) . .
C11 P1 C1 104.0(10) . .
C21 P1 C1 108.8(11) . .
C11 P1 Ag1 111.4(7) . .
C21 P1 Ag1 113.7(8) . .
C1 P1 Ag1 114.3(8) . .
C41 P2 C31 101.4(9) . .
C41 P2 C1 104.6(11) . .
C31 P2 C1 104.2(10) . .
C41 P2 Ag2 119.0(8) . .
C31 P2 Ag2 111.2(7) . .
C1 P2 Ag2 114.7(8) . .
C61 P3 C51 106.5(10) . .
C61 P3 C2 104.8(11) . .
C51 P3 C2 102.2(10) . .
C61 P3 Ag9 116.0(6) . .
C51 P3 Ag9 112.3(7) . .
C2 P3 Ag9 113.8(8) . .
C81 P4 C71 107.7(12) . .
C81 P4 C2 104.3(11) . .
C71 P4 C2 99.7(11) . .
C81 P4 Ag10 113.7(7) . .
C71 P4 Ag10 111.7(7) . .
C2 P4 Ag10 118.3(8) . .
C100 P5 C91 103.4(9) . .
C100 P5 C3 105.3(10) . .
C91 P5 C3 102.9(11) . .
C100 P5 Ag5 115.7(7) . .
C91 P5 Ag5 114.6(7) . .
C3 P5 Ag5 113.6(8) . .
C121 P6 C111 108.8(12) . .
C121 P6 C3 101.3(11) . .
C111 P6 C3 106.2(11) . .
C121 P6 Ag6 109.4(7) . .
C111 P6 Ag6 113.6(7) . .
C3 P6 Ag6 116.7(8) . .
P1 C1 P2 109.9(13) . .
P3 C2 P4 108.9(11) . .
P6 C3 P5 110.1(12) . .
C12 C11 C16 120.0 . .
C12 C11 P1 122.4(12) . .
C16 C11 P1 117.5(12) . .
C11 C12 C13 120.0 . .
C14 C13 C12 120.0 . .
C13 C14 C15 120.0 . .
C16 C15 C14 120.0 . .
C15 C16 C11 120.0 . .
C22 C21 C26 120.0 . .
C22 C21 P1 118.9(14) . .
C26 C21 P1 121.1(14) . .
C23 C22 C21 120.0 . .
C22 C23 C24 120.0 . .
C25 C24 C23 120.0 . .
C24 C25 C26 120.0 . .
C25 C26 C21 120.0 . .
C32 C31 C36 120.0 . .
C32 C31 P2 122.8(11) . .
C36 C31 P2 117.1(11) . .
C31 C32 C33 120.0 . .
C32 C33 C34 120.0 . .
C35 C34 C33 120.0 . .
C34 C35 C36 120.0 . .
C35 C36 C31 120.0 . .
C42 C41 C46 120.0 . .
C42 C41 P2 120.8(13) . .
C46 C41 P2 119.2(13) . .
C41 C42 C43 120.0 . .
C44 C43 C42 120.0 . .
C45 C44 C43 120.0 . .
C44 C45 C46 120.0 . .
C45 C46 C41 120.0 . .
C52 C51 C56 120.0 . .
C52 C51 P3 115.6(12) . .
C56 C51 P3 124.4(12) . .
C51 C52 C53 120.0 . .
C52 C53 C54 120.0 . .
C53 C54 C55 120.0 . .
C56 C55 C54 120.0 . .
C55 C56 C51 120.0 . .
C62 C61 C66 120.0 . .
C62 C61 P3 120.0(12) . .
C66 C61 P3 119.8(12) . .
C63 C62 C61 120.0 . .
C62 C63 C64 120.0 . .
C65 C64 C63 120.0 . .
C64 C65 C66 120.0 . .
C65 C66 C61 120.0 . .
C76 C71 C72 119(3) . .
C76 C71 P4 121(2) . .
C72 C71 P4 120(3) . .
C73 C72 C71 116(4) . .
C74 C73 C72 117(4) . .
C75 C74 C73 128(3) . .
C74 C75 C76 118(4) . .
C75 C76 C71 121(4) . .
C82 C81 C86 120.0 . .
C82 C81 P4 121.8(13) . .
C86 C81 P4 118.1(13) . .
C83 C82 C81 120.0 . .
C82 C83 C84 120.0 . .
C85 C84 C83 120.0 . .
C84 C85 C86 120.0 . .
C85 C86 C81 120.0 . .
C92 C91 C96 120.0 . .
C92 C91 P5 116.0(14) . .
C96 C91 P5 123.9(14) . .
C91 C92 C93 120.0 . .
C92 C93 C94 120.0 . .
C95 C94 C93 120.0 . .
C94 C95 C96 120.0 . .
C95 C96 C91 120.0 . .
C102 C100 C106 120.0 . .
C102 C100 P5 120.2(11) . .
C106 C100 P5 119.7(11) . .
C103 C102 C100 120.0 . .
C102 C103 C104 120.0 . .
C103 C104 C105 120.0 . .
C106 C105 C104 120.0 . .
C105 C106 C100 120.0 . .
C112 C111 C116 120.0 . .
C112 C111 P6 117.5(13) . .
C116 C111 P6 122.5(12) . .
C113 C112 C111 120.0 . .
C112 C113 C114 120.0 . .
C115 C114 C113 120.0 . .
C116 C115 C114 120.0 . .
C115 C116 C111 120.0 . .
C122 C121 C126 120.0 . .
C122 C121 P6 122.2(15) . .
C126 C121 P6 117.7(15) . .
C123 C122 C121 120.0 . .
C122 C123 C124 120.0 . .
C125 C124 C123 120.0 . .
C124 C125 C126 120.0 . .
C125 C126 C121 120.0 . .
C212 C211 Au1 171(2) . .
C212 C211 Ag3 98.3(18) . .
Au1 C211 Ag3 90.6(10) . .
C212 C211 Ag1 97.2(19) . .
Au1 C211 Ag1 80.8(9) . .
Ag3 C211 Ag1 120.3(9) . .
C211 C212 C213 178(3) . .
C212 C213 C214 119(2) . .
C212 C213 C218 121(2) . .
C214 C213 C218 120.0 . .
C213 C214 C215 120.0 . .
C214 C215 C216 120.0 . .
C217 C216 C215 120.0 . .
C218 C217 C216 120.0 . .
C217 C218 C213 120.0 . .
C222 C221 Au1 170(2) . .
C222 C221 Ag4 88.2(17) . .
Au1 C221 Ag4 99.3(11) . .
C222 C221 Ag2 100.4(18) . .
Au1 C221 Ag2 83.0(8) . .
Ag4 C221 Ag2 112.6(8) . .
C221 C222 C223 174(3) . .
C222 C223 C224 122(3) . .
C222 C223 C228 118(3) . .
C224 C223 C228 120.0 . .
C225 C224 C223 120.0 . .
C224 C225 C226 120.0 . .
C225 C226 C227 120.0 . .
C228 C227 C226 120.0 . .
C227 C228 C223 120.0 . .
C232 C231 Au2 165(3) . .
C232 C231 Ag3 99(2) . .
Au2 C231 Ag3 95.6(11) . .
C232 C231 Ag5 93(2) . .
Au2 C231 Ag5 82.2(9) . .
Ag3 C231 Ag5 121.0(10) . .
C231 C232 C233 169(5) . .
C234 C233 C238 120.0 . .
C234 C233 C232 103(6) . .
C238 C233 C232 137(6) . .
C233 C234 C235 120.0 . .
C236 C235 C234 120.0 . .
C235 C236 C237 120.0 . .
C238 C237 C236 120.0 . .
C237 C238 C233 120.0 . .
C242 C241 Au2 170(2) . .
C242 C241 Ag6 101(2) . .
Au2 C241 Ag6 82.5(11) . .
C242 C241 Ag4 96(2) . .
Au2 C241 Ag4 90.7(10) . .
Ag6 C241 Ag4 121.5(10) . .
C243 C242 C241 170(3) . .
C242 C243 C244 124(3) . .
C242 C243 C248 115(3) . .
C244 C243 C248 120.0 . .
C245 C244 C243 120.0 . .
C244 C245 C246 120.0 . .
C245 C246 C247 120.0 . .
C248 C247 C246 120.0 . .
C247 C248 C243 120.0 . .
C252 C251 Au3 165(2) . .
C252 C251 Ag8 102(2) . .
Au3 C251 Ag8 89.5(10) . .
C252 C251 Ag5 101(2) . .
Au3 C251 Ag5 79.9(9) . .
Ag8 C251 Ag5 122.2(10) . .
C251 C252 C253 174(4) . .
C252 C253 C254 126(3) . .
C252 C253 C258 114(3) . .
C254 C253 C258 120.0 . .
C255 C254 C253 120.0 . .
C256 C255 C254 120.0 . .
C255 C256 C257 120.0 . .
C258 C257 C256 120.0 . .
C257 C258 C253 120.0 . .
C262 C261 Au6 151(2) . .
C262 C261 Ag11 113(2) . .
Au6 C261 Ag11 94.8(11) . .
C262 C261 Ag1 90.1(17) . .
Au6 C261 Ag1 82.3(9) . .
Ag11 C261 Ag1 119.6(11) . .
C261 C262 C263 178(3) . .
C261 C262 Ag1 63.0(15) . .
C263 C262 Ag1 116.1(18) . .
C264 C263 C268 120.0 . .
C264 C263 C262 121(3) . .
C268 C263 C262 119(3) . .
C263 C264 C265 120.0 . .
C264 C265 C266 120.0 . .
C267 C266 C265 120.0 . .
C266 C267 C268 120.0 . .
C267 C268 C263 120.0 . .
C272 C271 Au4 166(2) . .
C272 C271 Ag8 103.2(19) . .
Au4 C271 Ag8 91.0(10) . .
C272 C271 Ag9 91(2) . .
Au4 C271 Ag9 84.8(9) . .
Ag8 C271 Ag9 118.2(10) . .
C271 C272 C273 178(3) . .
C274 C273 C278 120.0 . .
C274 C273 C272 117(2) . .
C278 C273 C272 123(2) . .
C273 C274 C275 120.0 . .
C276 C275 C274 120.0 . .
C275 C276 C277 120.0 . .
C278 C277 C276 120.0 . .
C277 C278 C273 120.0 . .
C282 C281 Au4 166(2) . .
C282 C281 Ag7 98.9(19) . .
Au4 C281 Ag7 94.1(10) . .
C282 C281 Ag10 97(2) . .
Au4 C281 Ag10 80.4(8) . .
Ag7 C281 Ag10 116.4(10) . .
C281 C282 C283 174(3) . .
C282 C283 C284 123(4) . .
C282 C283 C288 117(4) . .
C284 C283 C288 120.0 . .
C283 C284 C285 120.0 . .
C284 C285 C286 120.0 . .
C287 C286 C285 120.0 . .
C286 C287 C288 120.0 . .
C287 C288 C283 120.0 . .
C292 C291 Au5 167(3) . .
C292 C291 Ag11 98(2) . .
Au5 C291 Ag11 88.1(10) . .
C292 C291 Ag9 108(2) . .
Au5 C291 Ag9 77.8(9) . .
Ag11 C291 Ag9 123.6(12) . .
C291 C292 C293 179(4) . .
C294 C293 C298 120.0 . .
C294 C293 C292 123(2) . .
C298 C293 C292 117(2) . .
C295 C294 C293 120.0 . .
C294 C295 C296 120.0 . .
C297 C296 C295 120.0 . .
C296 C297 C298 120.0 . .
C297 C298 C293 120.0 . .
C302 C301 Au5 160(3) . .
C302 C301 Ag10 101(2) . .
Au5 C301 Ag10 89.5(10) . .
C302 C301 Ag12 92.3(18) . .
Au5 C301 Ag12 97.6(11) . .
Ag10 C301 Ag12 119.7(11) . .
C301 C302 C303 173(3) . .
C304 C303 C308 120.0 . .
C304 C303 C302 119(2) . .
C308 C303 C302 121(2) . .
C305 C304 C303 120.0 . .
C304 C305 C306 120.0 . .
C305 C306 C307 120.0 . .
C306 C307 C308 120.0 . .
C307 C308 C303 120.0 . .
C312 C311 Au3 173(2) . .
C312 C311 Ag6 94.7(18) . .
Au3 C311 Ag6 84.3(9) . .
C312 C311 Ag7 91.6(18) . .
Au3 C311 Ag7 94.9(10) . .
Ag6 C311 Ag7 119.1(10) . .
C311 C312 C313 174(3) . .
C314 C313 C318 120.0 . .
C314 C313 C312 123(3) . .
C318 C313 C312 117(3) . .
C315 C314 C313 120.0 . .
C314 C315 C316 120.0 . .
C317 C316 C315 120.0 . .
C316 C317 C318 120.0 . .
C317 C318 C313 120.0 . .
C322 C321 Au6 172(2) . .
C322 C321 Ag2 92.4(17) . .
Au6 C321 Ag2 85.2(8) . .
C322 C321 Ag12 97.8(18) . .
Au6 C321 Ag12 90.2(8) . .
Ag2 C321 Ag12 123.4(10) . .
C321 C322 C323 175(3) . .
C321 C322 Ag2 60.8(14) . .
C323 C322 Ag2 120.8(18) . .
C324 C323 C328 120.0 . .
C324 C323 C322 121(3) . .
C328 C323 C322 119(3) . .
C323 C324 C325 120.0 . .
C326 C325 C324 120.0 . .
C325 C326 C327 120.0 . .
C326 C327 C328 120.0 . .
C327 C328 C323 120.0 . .
C332 C331 Ag3 133(2) . .
C332 C331 Ag11 129(2) . .
Ag3 C331 Ag11 83.1(8) . .
C332 C331 Ag8 123(2) . .
Ag3 C331 Ag8 86.7(8) . .
Ag11 C331 Ag8 86.7(8) . .
C331 C332 C333 179(4) . .
C334 C333 C338 120.0 . .
C334 C333 C332 115(5) . .
C338 C333 C332 125(5) . .
C333 C334 C335 120.0 . .
C336 C335 C334 120.0 . .
C335 C336 C337 120.0 . .
C338 C337 C336 120.0 . .
C337 C338 C333 120.0 . .
C342 C341 Ag4 138(2) . .
C342 C341 Ag7 126(2) . .
Ag4 C341 Ag7 83.3(8) . .
C342 C341 Ag12 125(2) . .
Ag4 C341 Ag12 82.4(8) . .
Ag7 C341 Ag12 84.0(9) . .
C341 C342 C343 173(3) . .
C344 C343 C348 120.0 . .
C344 C343 C342 129(3) . .
C348 C343 C342 111(3) . .
C343 C344 C345 120.0 . .
C344 C345 C346 120.0 . .
C345 C346 C347 120.0 . .
C348 C347 C346 120.0 . .
C347 C348 C343 120.0 . .
F46 Sb4 F43 90.8(15) . .
F46 Sb4 F42 96.2(15) . .
F43 Sb4 F42 81.3(14) . .
F46 Sb4 F41 86.5(14) . .
F43 Sb4 F41 176.5(17) . .
F42 Sb4 F41 101.2(16) . .
F46 Sb4 F44 89.7(14) . .
F43 Sb4 F44 91.0(15) . .
F42 Sb4 F44 170.3(17) . .
F41 Sb4 F44 86.7(14) . .
F46 Sb4 F45 173.0(17) . .
F43 Sb4 F45 88.0(14) . .
F42 Sb4 F45 90.5(15) . .
F41 Sb4 F45 94.3(15) . .
F44 Sb4 F45 83.4(14) . .
F53 Sb5 F53 180(4) 3_655 .
F53 Sb5 F52 74.8(2) 3_655 .
F53 Sb5 F52 105.2(2) . .
F53 Sb5 F52 105.2(2) 3_655 3_655
F53 Sb5 F52 74.8(2) . 3_655
F52 Sb5 F52 180(5) . 3_655
F53 Sb5 F51 105.2(2) 3_655 3_655
F53 Sb5 F51 74.8(2) . 3_655
F52 Sb5 F51 74.9(2) . 3_655
F52 Sb5 F51 105.1(2) 3_655 3_655
F53 Sb5 F51 74.8(2) 3_655 .
F53 Sb5 F51 105.2(2) . .
F52 Sb5 F51 105.1(2) . .
F52 Sb5 F51 74.9(2) 3_655 .
F51 Sb5 F51 180.000(1) 3_655 .
F66 Sb6 F63 92.3(16) . .
F66 Sb6 F62 97.4(16) . .
F63 Sb6 F62 81.0(15) . .
F66 Sb6 F64 88.2(15) . .
F63 Sb6 F64 91.6(16) . .
F62 Sb6 F64 170.8(18) . .
F66 Sb6 F61 86.0(15) . .
F63 Sb6 F61 178.2(19) . .
F62 Sb6 F61 99.9(17) . .
F64 Sb6 F61 87.6(15) . .
F66 Sb6 F65 172.8(18) . .
F63 Sb6 F65 88.4(15) . .
F62 Sb6 F65 89.8(15) . .
F64 Sb6 F65 84.6(15) . .
F61 Sb6 F65 93.1(16) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Au1 C221 1.99(3) .
Au1 C211 2.04(3) .
Au1 Ag1 2.923(2) .
Au1 Ag2 2.993(2) .
Au1 Ag3 3.184(2) .
Au2 C231 2.04(3) .
Au2 C241 2.09(4) .
Au2 Ag6 2.938(2) .
Au2 Ag5 3.021(3) .
Au2 Ag3 3.237(2) .
Au2 Ag4 3.248(2) .
Au3 C311 1.95(3) .
Au3 C251 2.16(3) .
Au3 Ag6 2.959(2) .
Au3 Ag5 2.959(2) .
Au3 Ag8 3.235(2) .
Au3 Ag7 3.244(2) .
Au4 C281 2.01(3) .
Au4 C271 2.04(3) .
Au4 Ag10 2.963(2) .
Au4 Ag9 3.052(2) .
Au4 Ag8 3.171(2) .
Au4 Ag7 3.237(2) .
Au5 C301 1.90(3) .
Au5 C291 2.14(3) .
Au5 Ag9 2.898(2) .
Au5 Ag10 2.935(3) .
Au5 Ag11 3.167(3) .
Au5 Ag12 3.255(3) .
Au5 Au6 3.266(2) .
Au6 C321 1.98(3) .
Au6 C261 2.12(3) .
Au6 Ag2 2.955(2) .
Au6 Ag1 2.984(2) .
Au6 Ag12 3.117(3) .
Au6 Ag11 3.230(3) .
Ag1 P1 2.388(6) .
Ag1 C261 2.41(2) .
Ag1 C211 2.44(3) .
Ag1 C262 2.70(2) .
Ag1 Ag2 3.233(3) .
Ag2 C321 2.37(2) .
Ag2 P2 2.390(6) .
Ag2 C221 2.49(2) .
Ag2 C322 2.71(2) .
Ag3 C331 2.19(2) .
Ag3 C231 2.32(2) .
Ag3 C211 2.42(2) .
Ag3 Ag11 2.938(3) .
Ag3 Ag13 2.956(5) .
Ag3 Ag8 3.045(3) .
Ag4 C341 2.24(2) .
Ag4 C241 2.46(2) .
Ag4 C221 2.47(2) .
Ag4 Ag13 2.966(5) .
Ag4 Ag12 2.982(3) .
Ag4 Ag7 2.985(3) .
Ag5 P5 2.415(7) .
Ag5 C251 2.44(2) .
Ag5 C231 2.52(2) .
Ag5 Ag6 3.233(3) .
Ag6 C241 2.36(2) .
Ag6 P6 2.402(6) .
Ag6 C311 2.43(2) .
Ag7 C341 2.25(2) .
Ag7 C281 2.40(2) .
Ag7 C311 2.43(2) .
Ag7 Ag13 2.975(5) .
Ag7 Ag12 3.040(3) .
Ag8 C331 2.25(2) .
Ag8 C271 2.39(2) .
Ag8 C251 2.43(2) .
Ag8 Ag13 2.897(5) .
Ag8 Ag11 3.083(3) .
Ag9 P3 2.422(6) .
Ag9 C291 2.46(3) .
Ag9 C271 2.46(2) .
Ag9 Ag10 3.183(3) .
Ag10 C301 2.25(2) .
Ag10 P4 2.415(6) .
Ag10 C281 2.54(2) .
Ag11 C331 2.24(2) .
Ag11 C261 2.27(2) .
Ag11 C291 2.40(3) .
Ag11 Ag13 2.998(6) .
Ag12 C341 2.29(3) .
Ag12 C301 2.40(2) .
Ag12 C321 2.40(2) .
Ag12 Ag13 2.962(5) .
Sb1 F16 1.859(15) .
Sb1 F13 1.875(19) .
Sb1 F12 1.895(17) .
Sb1 F14 1.904(16) .
Sb1 F11 1.92(2) .
Sb1 F15 1.928(17) .
Sb2 F22 1.88(2) .
Sb2 F23 1.88(2) .
Sb2 F26 1.89(2) .
Sb2 F21 1.92(2) .
Sb2 F24 1.94(2) .
Sb2 F25 1.94(2) .
Sb3 F32 1.86(2) .
Sb3 F36 1.87(2) .
Sb3 F33 1.88(2) .
Sb3 F31 1.91(2) .
Sb3 F34 1.93(2) .
Sb3 F35 1.94(2) .
P1 C11 1.839(15) .
P1 C21 1.839(17) .
P1 C1 1.85(2) .
P2 C41 1.812(16) .
P2 C31 1.826(14) .
P2 C1 1.86(2) .
P3 C61 1.797(15) .
P3 C51 1.803(15) .
P3 C2 1.87(2) .
P4 C81 1.787(17) .
P4 C71 1.82(3) .
P4 C2 1.87(2) .
P5 C100 1.801(14) .
P5 C91 1.830(16) .
P5 C3 1.86(2) .
P6 C121 1.814(18) .
P6 C111 1.837(16) .
P6 C3 1.86(2) .
C11 C12 1.3900 .
C11 C16 1.3900 .
C12 C13 1.3900 .
C13 C14 1.3900 .
C14 C15 1.3900 .
C15 C16 1.3900 .
C21 C22 1.3900 .
C21 C26 1.3900 .
C22 C23 1.3900 .
C23 C24 1.3900 .
C24 C25 1.3900 .
C25 C26 1.3900 .
C31 C32 1.3900 .
C31 C36 1.3900 .
C32 C33 1.3900 .
C33 C34 1.3900 .
C34 C35 1.3900 .
C35 C36 1.3900 .
C41 C42 1.3900 .
C41 C46 1.3900 .
C42 C43 1.3900 .
C43 C44 1.3900 .
C44 C45 1.3900 .
C45 C46 1.3900 .
C51 C52 1.3900 .
C51 C56 1.3900 .
C52 C53 1.3900 .
C53 C54 1.3900 .
C54 C55 1.3900 .
C55 C56 1.3900 .
C61 C62 1.3900 .
C61 C66 1.3900 .
C62 C63 1.3900 .
C63 C64 1.3900 .
C64 C65 1.3900 .
C65 C66 1.3900 .
C71 C76 1.44(4) .
C71 C72 1.54(4) .
C72 C73 1.44(5) .
C73 C74 1.40(6) .
C74 C75 1.36(5) .
C75 C76 1.37(4) .
C81 C82 1.3900 .
C81 C86 1.3900 .
C82 C83 1.3900 .
C83 C84 1.3900 .
C84 C85 1.3900 .
C85 C86 1.3900 .
C91 C92 1.3900 .
C91 C96 1.3900 .
C92 C93 1.3900 .
C93 C94 1.3900 .
C94 C95 1.3900 .
C95 C96 1.3900 .
C100 C102 1.3900 .
C100 C106 1.3900 .
C102 C103 1.3900 .
C103 C104 1.3900 .
C104 C105 1.3900 .
C105 C106 1.3900 .
C111 C112 1.3900 .
C111 C116 1.3900 .
C112 C113 1.3900 .
C113 C114 1.3900 .
C114 C115 1.3900 .
C115 C116 1.3900 .
C121 C122 1.3900 .
C121 C126 1.3900 .
C122 C123 1.3900 .
C123 C124 1.3900 .
C124 C125 1.3900 .
C125 C126 1.3900 .
C211 C212 1.26(3) .
C212 C213 1.37(3) .
C213 C214 1.3900 .
C213 C218 1.3900 .
C214 C215 1.3900 .
C215 C216 1.3900 .
C216 C217 1.3900 .
C217 C218 1.3900 .
C221 C222 1.25(3) .
C222 C223 1.36(3) .
C223 C224 1.3900 .
C223 C228 1.3900 .
C224 C225 1.3900 .
C225 C226 1.3900 .
C226 C227 1.3900 .
C227 C228 1.3900 .
C231 C232 1.17(4) .
C232 C233 1.44(5) .
C233 C234 1.3900 .
C233 C238 1.3900 .
C234 C235 1.3900 .
C235 C236 1.3900 .
C236 C237 1.3900 .
C237 C238 1.3900 .
C241 C242 1.22(4) .
C242 C243 1.18(3) .
C243 C244 1.3900 .
C243 C248 1.3900 .
C244 C245 1.3900 .
C245 C246 1.3900 .
C246 C247 1.3900 .
C247 C248 1.3900 .
C251 C252 1.11(3) .
C252 C253 1.30(3) .
C253 C254 1.3900 .
C253 C258 1.3900 .
C254 C255 1.3900 .
C255 C256 1.3900 .
C256 C257 1.3900 .
C257 C258 1.3900 .
C261 C262 1.22(3) .
C262 C263 1.42(3) .
C263 C264 1.3900 .
C263 C268 1.3900 .
C264 C265 1.3900 .
C265 C266 1.3900 .
C266 C267 1.3900 .
C267 C268 1.3900 .
C271 C272 1.20(3) .
C272 C273 1.45(3) .
C273 C274 1.3900 .
C273 C278 1.3900 .
C274 C275 1.3900 .
C275 C276 1.3900 .
C276 C277 1.3900 .
C277 C278 1.3900 .
C281 C282 1.17(3) .
C282 C283 1.35(3) .
C283 C284 1.3900 .
C283 C288 1.3900 .
C284 C285 1.3900 .
C285 C286 1.3900 .
C286 C287 1.3900 .
C287 C288 1.3900 .
C291 C292 1.16(3) .
C292 C293 1.43(4) .
C293 C294 1.3900 .
C293 C298 1.3900 .
C294 C295 1.3900 .
C295 C296 1.3900 .
C296 C297 1.3900 .
C297 C298 1.3900 .
C301 C302 1.29(4) .
C302 C303 1.47(4) .
C303 C304 1.3900 .
C303 C308 1.3900 .
C304 C305 1.3900 .
C305 C306 1.3900 .
C306 C307 1.3900 .
C307 C308 1.3900 .
C311 C312 1.20(3) .
C312 C313 1.59(4) .
C313 C314 1.3900 .
C313 C318 1.3900 .
C314 C315 1.3900 .
C315 C316 1.3900 .
C316 C317 1.3900 .
C317 C318 1.3900 .
C321 C322 1.22(3) .
C322 C323 1.47(3) .
C323 C324 1.3900 .
C323 C328 1.3900 .
C324 C325 1.3900 .
C325 C326 1.3900 .
C326 C327 1.3900 .
C327 C328 1.3900 .
C331 C332 1.17(3) .
C332 C333 1.52(5) .
C333 C334 1.3900 .
C333 C338 1.3900 .
C334 C335 1.3900 .
C335 C336 1.3900 .
C336 C337 1.3900 .
C337 C338 1.3900 .
C341 C342 1.14(3) .
C342 C343 1.43(3) .
C343 C344 1.3900 .
C343 C348 1.3900 .
C344 C345 1.3900 .
C345 C346 1.3900 .
C346 C347 1.3900 .
C347 C348 1.3900 .
Sb4 F46 1.88(2) .
Sb4 F43 1.91(2) .
Sb4 F42 1.91(2) .
Sb4 F41 1.92(2) .
Sb4 F44 1.93(2) .
Sb4 F45 1.95(2) .
Sb5 F53 1.750(2) 3_655
Sb5 F53 1.750(2) .
Sb5 F52 1.750(2) .
Sb5 F52 1.750(2) 3_655
Sb5 F51 1.751(2) 3_655
Sb5 F51 1.751(2) .
Sb6 F66 1.87(2) .
Sb6 F63 1.88(2) .
Sb6 F62 1.90(2) .
Sb6 F64 1.92(2) .
Sb6 F61 1.93(3) .
Sb6 F65 1.94(2) .
