#------------------------------------------------------------------------------
#$Date: 2016-03-21 10:41:47 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178663 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/74/4077415.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4077415
loop_
_publ_author_name
'Zheng, Shao-Liang'
'Tong, Ming-Liang'
'Tan, Song-De'
'Wang, Yu'
'Shi, Jian-Xin'
'Tong, Ye-Xiang'
'Lee, Hung Kay'
'Chen, Xiao-Ming'
_publ_section_title
;
 Syntheses, Structures, and Properties of Three Novel Coordination
 Polymers of Silver(I) Aromatic Carboxylates with Hexamethylenetetramine
 Exhibiting Unique Metal−π Interaction
;
_journal_issue                   25
_journal_name_full               Organometallics
_journal_page_first              5319
_journal_paper_doi               10.1021/om010601e
_journal_volume                  20
_journal_year                    2001
_chemical_formula_sum            'C36 H43 Ag2 N9 O8'
_chemical_formula_weight         945.53
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 95.12(8)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.855(11)
_cell_length_b                   12.461(7)
_cell_length_c                   19.860(18)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      15
_cell_measurement_theta_min      7.5
_cell_volume                     3662(5)
_computing_cell_refinement       'SHELXTL-Plus (Sheldrick, 1990)'
_computing_data_collection       'SHELXTL-Plus (Sheldrick, 1990)'
_computing_data_reduction        'SHELXTL-Plus (Sheldrick, 1990)'
_computing_molecular_graphics    'SHELXTL V. 5.0 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.932
_diffrn_measured_fraction_theta_max 0.932
_diffrn_measurement_device_type  'Siemens R3m'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0630
_diffrn_reflns_av_sigmaI/netI    0.1080
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            7351
_diffrn_reflns_theta_full        26.04
_diffrn_reflns_theta_max         26.04
_diffrn_reflns_theta_min         2.06
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 200
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    1.136
_exptl_absorpt_correction_T_max  0.8217
_exptl_absorpt_correction_T_min  0.6469
_exptl_absorpt_correction_type   semi-empirical
_exptl_absorpt_process_details   'ψ-scans (North et al., 1968)'
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.715
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1920
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.18
_refine_diff_density_max         0.945
_refine_diff_density_min         -1.079
_refine_diff_density_rms         0.141
_refine_ls_extinction_coef       0.0020(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.969
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     500
_refine_ls_number_reflns         7067
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.969
_refine_ls_R_factor_all          0.1486
_refine_ls_R_factor_gt           0.0662
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0923P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1470
_refine_ls_wR_factor_ref         0.1874
_reflns_number_gt                3679
_reflns_number_total             7067
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om010601e.cif
_cod_data_source_block           complex2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0923P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0923P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      P2(1)/n
_cod_database_code               4077415
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 1.07451(5) -0.18693(6) 0.74742(4) 0.0481(2) Uani 1 d .
Ag2 Ag 0.67713(5) 0.22007(6) 0.50737(3) 0.0459(2) Uani 1 d .
O1 O 1.0406(4) 0.0005(5) 0.6627(3) 0.0536(17) Uani 1 d .
O2 O 0.9927(5) -0.0247(5) 0.7655(3) 0.0612(19) Uani 1 d .
O3 O 0.8960(4) 0.1170(5) 0.8173(3) 0.0435(15) Uani 1 d .
H3 H 0.9317 0.0638 0.8231 0.080 Uiso 1 d R
O4 O 0.7177(4) 0.5310(5) 0.9876(3) 0.0536(17) Uani 1 d .
O5 O 0.8365(5) 0.5541(5) 0.9269(3) 0.0593(19) Uani 1 d .
O6 O 0.8772(4) 0.4149(5) 0.8407(3) 0.0458(17) Uani 1 d .
H6 H 0.874(8) 0.463(9) 0.861(6) 0.080 Uiso 1 d .
N1 N 1.2237(4) -0.1888(5) 0.7094(3) 0.0367(16) Uani 1 d .
N2 N 1.3185(5) -0.2043(5) 0.6123(3) 0.0354(16) Uani 1 d .
N3 N 1.3762(5) -0.2701(7) 0.7263(4) 0.0482(19) Uani 1 d .
N4 N 1.3610(5) -0.0760(6) 0.7058(4) 0.049(2) Uani 1 d .
N5 N 1.0682(5) -0.2121(6) 0.8684(3) 0.0389(17) Uani 1 d .
N6 N 0.9732(5) -0.2410(6) 0.9631(3) 0.0399(18) Uani 1 d .
N7 N 1.1292(5) -0.3115(6) 0.9706(4) 0.054(2) Uani 1 d .
N8 N 1.1029(5) -0.1161(6) 0.9776(4) 0.0459(19) Uani 1 d .
C1 C 0.8223(6) 0.2504(6) 0.7463(4) 0.0335(19) Uani 1 d .
C2 C 0.8827(5) 0.1642(6) 0.7545(4) 0.0341(19) Uani 1 d .
C3 C 0.9295(5) 0.1232(7) 0.6995(4) 0.0351(19) Uani 1 d .
C4 C 0.9138(5) 0.1703(7) 0.6356(4) 0.039(2) Uani 1 d .
H4A H 0.9451 0.1441 0.5987 0.080 Uiso 1 d R
C5 C 0.8314(5) 0.3054(7) 0.5588(4) 0.040(2) Uani 1 d .
H5A H 0.8605 0.2776 0.5211 0.080 Uiso 1 d R
C6 C 0.7713(6) 0.3905(7) 0.5485(4) 0.047(2) Uani 1 d .
H6A H 0.7567 0.4186 0.5039 0.080 Uiso 1 d R
C7 C 0.7318(6) 0.4357(7) 0.6043(5) 0.048(2) Uani 1 d .
H7A H 0.6930 0.4971 0.5976 0.080 Uiso 1 d R
C8 C 0.7489(5) 0.3918(7) 0.6690(4) 0.041(2) Uani 1 d .
H8A H 0.7208 0.4229 0.7061 0.080 Uiso 1 d R
C9 C 0.8076(5) 0.3006(7) 0.6808(4) 0.0352(19) Uani 1 d .
C10 C 0.8511(6) 0.2576(7) 0.6249(4) 0.035(2) Uani 1 d .
C11 C 0.7657(5) 0.2857(6) 0.8014(4) 0.0302(17) Uani 1 d .
C12 C 0.7928(5) 0.3699(6) 0.8452(4) 0.0310(18) Uani 1 d .
C13 C 0.7355(5) 0.4090(7) 0.8942(4) 0.0350(19) Uani 1 d .
C14 C 0.6506(5) 0.3625(7) 0.8982(4) 0.039(2) Uani 1 d .
H14A H 0.6124 0.3888 0.9311 0.080 Uiso 1 d R
C15 C 0.5322(6) 0.2296(8) 0.8574(4) 0.046(2) Uani 1 d .
H15A H 0.4932 0.2568 0.8894 0.080 Uiso 1 d R
C16 C 0.5027(6) 0.1455(7) 0.8151(4) 0.042(2) Uani 1 d .
H16A H 0.4433 0.1159 0.8167 0.080 Uiso 1 d R
C17 C 0.5631(6) 0.1037(7) 0.7687(5) 0.049(2) Uani 1 d .
H17A H 0.5441 0.0440 0.7404 0.080 Uiso 1 d R
C18 C 0.6480(6) 0.1476(7) 0.7642(4) 0.039(2) Uani 1 d .
H18A H 0.6866 0.1190 0.7323 0.080 Uiso 1 d R
C19 C 0.6786(6) 0.2356(6) 0.8068(4) 0.0348(19) Uani 1 d .
C20 C 0.6192(5) 0.2761(7) 0.8542(4) 0.037(2) Uani 1 d .
C21 C 0.9939(6) 0.0276(8) 0.7085(5) 0.044(2) Uani 1 d .
C22 C 0.7632(6) 0.5030(7) 0.9397(5) 0.047(2) Uani 1 d .
C23 C 1.2255(5) -0.2085(6) 0.6346(4) 0.0360(19) Uani 1 d .
H23A H 1.1889 -0.1555 0.6101 0.080 Uiso 1 d R
H23B H 1.1996 -0.2777 0.6239 0.080 Uiso 1 d R
C24 C 1.3743(6) -0.2860(7) 0.6522(4) 0.044(2) Uani 1 d .
H24A H 1.4351 -0.2830 0.6394 0.080 Uiso 1 d R
H24B H 1.3509 -0.3563 0.6411 0.080 Uiso 1 d R
C25 C 1.2833(6) -0.2722(8) 0.7458(5) 0.049(2) Uani 1 d .
H25A H 1.2580 -0.3421 0.7364 0.080 Uiso 1 d R
H25B H 1.2846 -0.2601 0.7936 0.080 Uiso 1 d R
C26 C 1.2662(7) -0.0797(7) 0.7247(5) 0.051(2) Uani 1 d .
H26A H 1.2656 -0.0646 0.7721 0.080 Uiso 1 d R
H26B H 1.2315 -0.0254 0.6999 0.080 Uiso 1 d R
C27 C 1.3580(6) -0.0956(7) 0.6315(5) 0.047(2) Uani 1 d .
H27A H 1.3222 -0.0408 0.6081 0.080 Uiso 1 d R
H27B H 1.4182 -0.0911 0.6177 0.080 Uiso 1 d R
C28 C 1.4146(7) -0.1605(9) 0.7421(6) 0.068(3) Uani 1 d .
H28A H 1.4751 -0.1574 0.7288 0.080 Uiso 1 d R
H28B H 1.4171 -0.1474 0.7899 0.080 Uiso 1 d R
C29 C 0.9755(6) -0.2321(7) 0.8875(4) 0.040(2) Uani 1 d .
H29A H 0.9530 -0.2973 0.8666 0.080 Uiso 1 d R
H29B H 0.9367 -0.1746 0.8709 0.080 Uiso 1 d R
C30 C 1.0356(6) -0.3290(7) 0.9882(4) 0.043(2) Uani 1 d .
H30A H 1.0143 -0.3958 0.9687 0.080 Uiso 1 d R
H30B H 1.0353 -0.3344 1.0363 0.080 Uiso 1 d R
C31 C 1.1272(6) -0.3018(7) 0.8960(5) 0.052(3) Uani 1 d .
H31A H 1.1875 -0.2916 0.8832 0.080 Uiso 1 d R
H31B H 1.1044 -0.3678 0.8763 0.080 Uiso 1 d R
C32 C 1.1017(6) -0.1107(7) 0.9019(4) 0.049(2) Uani 1 d .
H32A H 1.0632 -0.0525 0.8859 0.080 Uiso 1 d R
H32B H 1.1615 -0.0961 0.8895 0.080 Uiso 1 d R
C33 C 1.0088(6) -0.1383(7) 0.9937(5) 0.045(2) Uani 1 d .
H33A H 1.0072 -0.1424 1.0418 0.080 Uiso 1 d R
H33B H 0.9705 -0.0801 0.9774 0.080 Uiso 1 d R
C34 C 1.1587(7) -0.2079(8) 1.0016(5) 0.063(3) Uani 1 d .
H34A H 1.2202 -0.1947 0.9925 0.080 Uiso 1 d R
H34B H 1.1572 -0.2133 1.0497 0.080 Uiso 1 d R
O1W O 1.1603(5) 0.1315(7) 0.5899(4) 0.082(2) Uani 1 d .
H1WA H 1.1603 0.0915 0.5475 0.150 Uiso 1 d R
H1WB H 1.1285 0.0784 0.6152 0.150 Uiso 1 d R
O2W O 1.0506(6) -0.1038(7) 0.5274(4) 0.095(3) Uani 1 d .
H2WA H 1.0180 -0.0388 0.5104 0.150 Uiso 1 d R
H2WB H 1.1101 -0.0901 0.5521 0.150 Uiso 1 d R
N9 N 0.6657(7) 0.0053(10) 0.1045(5) 0.080(3) Uani 1 d .
C35 C 0.6230(8) 0.0614(10) 0.0709(6) 0.063(3) Uani 1 d .
C36 C 0.5676(9) 0.1369(13) 0.0298(8) 0.126(6) Uani 1 d .
H36A H 0.5872 0.2025 0.0104 0.080 Uiso 1 d R
H36B H 0.5095 0.1620 0.0113 0.080 Uiso 1 d R
H36C H 0.5853 0.0996 -0.0092 0.080 Uiso 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Ag1 N1 123.2(2) . .
O2 Ag1 N5 84.0(2) . .
N1 Ag1 N5 115.2(2) . .
O2 Ag1 C16 122.1(3) . 2_646
N1 Ag1 C16 102.7(3) . 2_646
N5 Ag1 C16 108.0(3) . 2_646
O2 Ag1 C15 99.7(3) . 2_646
N1 Ag1 C15 104.4(3) . 2_646
N5 Ag1 C15 129.6(3) . 2_646
C16 Ag1 C15 30.1(3) 2_646 2_646
N2 Ag2 N6 111.5(2) 3_756 2_656
N2 Ag2 O5 117.9(2) 3_756 2_646
N6 Ag2 O5 85.3(2) 2_656 2_646
N2 Ag2 C6 108.3(2) 3_756 .
N6 Ag2 C6 103.9(3) 2_656 .
O5 Ag2 C6 125.4(3) 2_646 .
N2 Ag2 C5 108.5(2) 3_756 .
N6 Ag2 C5 127.9(3) 2_656 .
O5 Ag2 C5 104.0(3) 2_646 .
C6 Ag2 C5 30.5(3) . .
C21 O1 O1W 128.5(6) . .
C21 O2 Ag1 104.1(5) . .
C21 O2 O3 93.2(5) . .
Ag1 O2 O3 162.6(3) . .
C2 O3 O2 88.4(5) . .
C22 O5 Ag2 101.4(6) . 2_656
C22 O5 O6 92.9(6) . .
Ag2 O5 O6 164.4(3) 2_656 .
C12 O6 O5 87.8(4) . .
C25 N1 C23 107.4(6) . .
C25 N1 C26 107.8(7) . .
C23 N1 C26 107.4(6) . .
C25 N1 Ag1 112.0(5) . .
C23 N1 Ag1 114.1(5) . .
C26 N1 Ag1 107.9(5) . .
C23 N2 C24 107.7(6) . .
C23 N2 C27 107.9(6) . .
C24 N2 C27 107.0(7) . .
C23 N2 Ag2 113.6(5) . 3_756
C24 N2 Ag2 114.1(5) . 3_756
C27 N2 Ag2 106.2(5) . 3_756
C25 N3 C24 109.0(7) . .
C25 N3 C28 108.1(8) . .
C24 N3 C28 107.6(7) . .
C28 N4 C26 109.7(8) . .
C28 N4 C27 109.5(7) . .
C26 N4 C27 107.4(7) . .
C29 N5 C32 108.0(7) . .
C29 N5 C31 108.0(6) . .
C32 N5 C31 107.9(7) . .
C29 N5 Ag1 113.2(5) . .
C32 N5 Ag1 106.9(5) . .
C31 N5 Ag1 112.7(5) . .
C33 N6 C30 107.9(7) . .
C33 N6 C29 107.6(6) . .
C30 N6 C29 108.4(6) . .
C33 N6 Ag2 112.2(5) . 2_646
C30 N6 Ag2 109.5(5) . 2_646
C29 N6 Ag2 111.2(5) . 2_646
C30 N7 C34 106.2(8) . .
C30 N7 C31 108.1(7) . .
C34 N7 C31 108.8(7) . .
C34 N8 C33 107.4(7) . .
C34 N8 C32 108.4(8) . .
C33 N8 C32 107.1(7) . .
C2 C1 C9 118.7(7) . .
C2 C1 C11 122.3(7) . .
C9 C1 C11 118.7(7) . .
O3 C2 C1 118.1(7) . .
O3 C2 C3 119.7(7) . .
C1 C2 C3 122.2(7) . .
C4 C3 C2 119.1(7) . .
C4 C3 C21 119.0(7) . .
C2 C3 C21 121.9(7) . .
C3 C4 C10 120.4(8) . .
C6 C5 C10 121.4(8) . .
C6 C5 Ag2 74.2(5) . .
C10 C5 Ag2 106.4(5) . .
C5 C6 C7 119.7(8) . .
C5 C6 Ag2 75.3(5) . .
C7 C6 Ag2 108.5(6) . .
C8 C7 C6 120.6(8) . .
C7 C8 C9 121.0(8) . .
C10 C9 C8 118.4(7) . .
C10 C9 C1 119.6(7) . .
C8 C9 C1 121.9(7) . .
C4 C10 C9 119.9(7) . .
C4 C10 C5 121.4(8) . .
C9 C10 C5 118.7(7) . .
C12 C11 C19 119.1(7) . .
C12 C11 C1 121.6(7) . .
C19 C11 C1 119.2(7) . .
O6 C12 C11 118.4(7) . .
O6 C12 C13 120.1(7) . .
C11 C12 C13 121.5(7) . .
C14 C13 C12 119.4(7) . .
C14 C13 C22 119.1(7) . .
C12 C13 C22 121.5(7) . .
C13 C14 C20 121.4(7) . .
C16 C15 C20 121.3(9) . .
C16 C15 Ag1 72.1(5) . 2_656
C20 C15 Ag1 106.3(6) . 2_656
C15 C16 C17 118.6(8) . .
C15 C16 Ag1 77.8(5) . 2_656
C17 C16 Ag1 104.8(6) . 2_656
C18 C17 C16 121.4(8) . .
C17 C18 C19 120.4(8) . .
C18 C19 C20 118.3(7) . .
C18 C19 C11 121.6(7) . .
C20 C19 C11 120.1(7) . .
C15 C20 C14 121.6(8) . .
C15 C20 C19 119.9(8) . .
C14 C20 C19 118.4(7) . .
O1 C21 O2 123.5(8) . .
O1 C21 C3 120.9(8) . .
O2 C21 C3 115.6(7) . .
O4 C22 O5 121.5(9) . .
O4 C22 C13 121.9(8) . .
O5 C22 C13 116.7(8) . .
N2 C23 N1 112.7(6) . .
N3 C24 N2 113.2(7) . .
N3 C25 N1 112.8(7) . .
N4 C26 N1 111.3(7) . .
N4 C27 N2 111.8(7) . .
N4 C28 N3 111.7(8) . .
N5 C29 N6 111.9(7) . .
N7 C30 N6 112.5(7) . .
N7 C31 N5 112.7(7) . .
N5 C32 N8 112.5(7) . .
N8 C33 N6 112.2(7) . .
N8 C34 N7 114.1(8) . .
O1 O1W O4 100.3(3) . 4_665
O4 O2W O2W 92.5(4) 4_665 3_756
N9 C35 C36 177.6(14) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O2 2.402(6) .
Ag1 N1 2.405(6) .
Ag1 N5 2.433(7) .
Ag1 C16 2.639(9) 2_646
Ag1 C15 2.710(9) 2_646
Ag2 N2 2.391(7) 3_756
Ag2 N6 2.408(7) 2_656
Ag2 O5 2.463(6) 2_646
Ag2 C6 2.633(9) .
Ag2 C5 2.647(9) .
O1 C21 1.239(10) .
O1 O1W 2.894(10) .
O2 C21 1.310(11) .
O2 O3 2.549(8) .
O3 C2 1.377(9) .
O4 C22 1.265(11) .
O5 C22 1.306(11) .
O5 Ag2 2.463(6) 2_656
O5 O6 2.548(8) .
O6 C12 1.384(10) .
N1 C25 1.507(11) .
N1 C23 1.509(10) .
N1 C26 1.517(11) .
N2 C23 1.489(10) .
N2 C24 1.496(10) .
N2 C27 1.511(11) .
N2 Ag2 2.391(7) 3_756
N3 C25 1.466(11) .
N3 C24 1.483(11) .
N3 C28 1.502(13) .
N4 C28 1.470(12) .
N4 C26 1.490(11) .
N4 C27 1.494(11) .
N5 C29 1.481(10) .
N5 C32 1.492(11) .
N5 C31 1.494(11) .
N6 C33 1.492(11) .
N6 C30 1.493(11) .
N6 C29 1.509(10) .
N6 Ag2 2.408(7) 2_646
N7 C30 1.480(11) .
N7 C34 1.480(13) .
N7 C31 1.485(12) .
N8 C34 1.467(12) .
N8 C33 1.488(11) .
N8 C32 1.504(11) .
C1 C2 1.400(11) .
C1 C9 1.442(11) .
C1 C11 1.504(10) .
C2 C3 1.440(11) .
C3 C4 1.399(11) .
C3 C21 1.528(12) .
C4 C10 1.436(11) .
C5 C6 1.390(12) .
C5 C10 1.448(11) .
C6 C7 1.415(12) .
C7 C8 1.399(12) .
C8 C9 1.439(11) .
C9 C10 1.436(11) .
C11 C12 1.398(11) .
C11 C19 1.449(11) .
C12 C13 1.434(11) .
C13 C14 1.397(11) .
C13 C22 1.513(12) .
C14 C20 1.437(12) .
C15 C16 1.390(12) .
C15 C20 1.423(11) .
C15 Ag1 2.710(9) 2_656
C16 C17 1.439(12) .
C16 Ag1 2.639(9) 2_656
C17 C18 1.386(12) .
C18 C19 1.434(11) .
C19 C20 1.438(11) .
O1W O4 3.042(11) 4_665
O2W O4 2.821(10) 4_665
O2W O2W 3.138(18) 3_756
N9 C35 1.122(14) .
C35 C36 1.452(18) .
