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#$Date: 2025-08-20 17:12:52 +0300 (Wed, 20 Aug 2025) $
#$Revision: 301832 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/10/88/4108866.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4108866
loop_
_publ_author_name
'Michaela Zirngast'
'Michaela Flock'
'Judith Baumgartner'
'Christoph Marschner'
_publ_section_title
;
 Formation of Formal Disilene Fluoride Adducts
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              17460
_journal_page_last               17470
_journal_paper_doi               10.1021/ja805753d
_journal_volume                  130
_journal_year                    2008
_chemical_formula_sum            'C48 H108 F K O6 Si6'
_chemical_formula_weight         1007.98
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                103.33(3)
_cell_angle_beta                 93.43(3)
_cell_angle_gamma                97.87(3)
_cell_formula_units_Z            1
_cell_length_a                   10.700(2)
_cell_length_b                   11.556(2)
_cell_length_c                   12.860(3)
_cell_measurement_temperature    100(2)
_cell_volume                     1525.8(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.978
_diffrn_measured_fraction_theta_max 0.978
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0311
_diffrn_reflns_av_sigmaI/netI    0.0436
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            11982
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.63
_exptl_absorpt_coefficient_mu    0.247
_exptl_absorpt_correction_T_max  0.9295
_exptl_absorpt_correction_T_min  0.8904
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1998)'
_exptl_crystal_density_diffrn    1.097
_exptl_crystal_F_000             556
_exptl_crystal_size_max          0.48
_exptl_crystal_size_mid          0.36
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.967
_refine_diff_density_min         -0.448
_refine_diff_density_rms         0.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     295
_refine_ls_number_reflns         6106
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.040
_refine_ls_R_factor_all          0.0536
_refine_ls_R_factor_gt           0.0472
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0773P)²+0.6520P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1293
_refine_ls_wR_factor_ref         0.1347
_reflns_number_gt                5279
_reflns_number_total             6106
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja805753d_si_001_2.cif
_cod_data_source_block           409j_3b
_cod_original_cell_volume        1525.8(5)
_cod_database_code               4108866
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Si1 Si 0.26718(5) 0.05692(4) 0.46832(4) 0.02398(14) Uani 1 1 d .
Si2 Si 0.04548(5) 0.01652(5) 0.42365(5) 0.03297(16) Uani 1 1 d .
Si3 Si -0.01596(4) 0.18429(4) 0.36651(4) 0.02032(13) Uani 1 1 d .
F1 F 0.0267(2) -0.08431(18) 0.32522(16) 0.0259(4) Uani 0.50 1 d P
K1 K 0.5000 0.5000 0.0000 0.02564(15) Uani 1 2 d S
O1 O 0.40387(16) 0.70840(13) 0.01153(14) 0.0440(4) Uani 1 1 d .
O2 O 0.27630(16) 0.39169(15) -0.10992(13) 0.0466(4) Uani 1 1 d .
O3 O 0.39309(14) 0.48781(13) 0.18299(11) 0.0345(3) Uani 1 1 d .
C1 C 0.2725(2) 0.7074(2) 0.02457(19) 0.0408(5) Uani 1 1 d .
H1A H 0.2404 0.6423 0.0590 0.049 Uiso 1 1 calc R
H1B H 0.2233 0.6940 -0.0460 0.049 Uiso 1 1 calc R
C2 C 0.2598(2) 0.8300(2) 0.0955(2) 0.0428(5) Uani 1 1 d .
H2A H 0.1950 0.8673 0.0623 0.051 Uiso 1 1 calc R
H2B H 0.2365 0.8227 0.1673 0.051 Uiso 1 1 calc R
C3 C 0.3901(3) 0.9030(2) 0.1033(3) 0.0628(8) Uani 1 1 d .
H3A H 0.3843 0.9826 0.0886 0.075 Uiso 1 1 calc R
H3B H 0.4349 0.9151 0.1755 0.075 Uiso 1 1 calc R
C4 C 0.4560(3) 0.8306(2) 0.0210(3) 0.0678(9) Uani 1 1 d .
H4A H 0.4424 0.8525 -0.0484 0.081 Uiso 1 1 calc R
H4B H 0.5481 0.8442 0.0428 0.081 Uiso 1 1 calc R
C5 C 0.1802(3) 0.4140(2) -0.18043(19) 0.0486(6) Uani 1 1 d .
H5A H 0.1805 0.3636 -0.2540 0.058 Uiso 1 1 calc R
H5B H 0.1924 0.4998 -0.1829 0.058 Uiso 1 1 calc R
C6 C 0.0587(3) 0.3812(3) -0.1340(2) 0.0598(7) Uani 1 1 d .
H6A H -0.0147 0.3627 -0.1890 0.072 Uiso 1 1 calc R
H6B H 0.0440 0.4466 -0.0733 0.072 Uiso 1 1 calc R
C7 C 0.0821(3) 0.2709(3) -0.0968(2) 0.0608(8) Uani 1 1 d .
H7A H 0.0519 0.1967 -0.1536 0.073 Uiso 1 1 calc R
H7B H 0.0390 0.2659 -0.0315 0.073 Uiso 1 1 calc R
C8 C 0.2254(2) 0.2891(2) -0.0729(2) 0.0500(6) Uani 1 1 d .
H8A H 0.2484 0.3028 0.0052 0.060 Uiso 1 1 calc R
H8B H 0.2595 0.2169 -0.1105 0.060 Uiso 1 1 calc R
C9 C 0.3722(2) 0.5931(2) 0.26089(18) 0.0432(5) Uani 1 1 d .
H9A H 0.2811 0.6009 0.2572 0.052 Uiso 1 1 calc R
H9B H 0.4208 0.6664 0.2471 0.052 Uiso 1 1 calc R
C10 C 0.4164(2) 0.5773(2) 0.37029(17) 0.0370(5) Uani 1 1 d .
H10A H 0.3448 0.5434 0.4051 0.044 Uiso 1 1 calc R
H10B H 0.4581 0.6547 0.4179 0.044 Uiso 1 1 calc R
C11 C 0.5099(2) 0.4894(2) 0.34375(17) 0.0397(5) Uani 1 1 d .
H11A H 0.5171 0.4428 0.3989 0.048 Uiso 1 1 calc R
H11B H 0.5949 0.5314 0.3366 0.048 Uiso 1 1 calc R
C12 C 0.4492(2) 0.40938(19) 0.23686(17) 0.0387(5) Uani 1 1 d .
H12A H 0.5138 0.3717 0.1946 0.046 Uiso 1 1 calc R
H12B H 0.3840 0.3451 0.2481 0.046 Uiso 1 1 calc R
C13 C 0.36323(18) 0.15235(19) 0.39047(17) 0.0321(4) Uani 1 1 d .
H13A H 0.4536 0.1497 0.4052 0.048 Uiso 1 1 calc R
H13B H 0.3476 0.2357 0.4125 0.048 Uiso 1 1 calc R
H13C H 0.3381 0.1209 0.3135 0.048 Uiso 1 1 calc R
C14 C 0.31624(18) 0.13189(17) 0.61546(16) 0.0289(4) Uani 1 1 d .
H14A H 0.2488 0.1095 0.6587 0.043 Uiso 1 1 calc R
H14B H 0.3308 0.2195 0.6254 0.043 Uiso 1 1 calc R
H14C H 0.3944 0.1054 0.6382 0.043 Uiso 1 1 calc R
C15 C 0.33142(18) -0.09003(17) 0.43264(16) 0.0294(4) Uani 1 1 d .
H15A H 0.3029 -0.1312 0.3578 0.044 Uiso 1 1 calc R
H15B H 0.3005 -0.1411 0.4797 0.044 Uiso 1 1 calc R
H15C H 0.4243 -0.0741 0.4419 0.044 Uiso 1 1 calc R
C16 C 0.00847(17) 0.33404(15) 0.47302(14) 0.0232(4) Uani 1 1 d .
H16 H -0.0209 0.3954 0.4377 0.028 Uiso 1 1 calc R
C17 C -0.0693(2) 0.33077(17) 0.56870(16) 0.0313(4) Uani 1 1 d .
H17A H -0.0455 0.2692 0.6038 0.047 Uiso 1 1 calc R
H17B H -0.1597 0.3115 0.5435 0.047 Uiso 1 1 calc R
H17C H -0.0526 0.4096 0.6200 0.047 Uiso 1 1 calc R
C18 C 0.14847(19) 0.37833(17) 0.51366(18) 0.0335(5) Uani 1 1 d .
H18A H 0.1561 0.4537 0.5690 0.050 Uiso 1 1 calc R
H18B H 0.1962 0.3921 0.4538 0.050 Uiso 1 1 calc R
H18C H 0.1825 0.3175 0.5441 0.050 Uiso 1 1 calc R
C19 C 0.08813(19) 0.21774(17) 0.25716(15) 0.0271(4) Uani 1 1 d .
H19 H 0.1746 0.2493 0.2953 0.033 Uiso 1 1 calc R
C20 C 0.0521(2) 0.31996(18) 0.20847(17) 0.0350(5) Uani 1 1 d .
H20A H 0.1195 0.3447 0.1661 0.053 Uiso 1 1 calc R
H20B H 0.0413 0.3887 0.2663 0.053 Uiso 1 1 calc R
H20C H -0.0274 0.2915 0.1620 0.053 Uiso 1 1 calc R
C21 C 0.1061(2) 0.10940(19) 0.16772(17) 0.0368(5) Uani 1 1 d .
H21A H 0.0289 0.0838 0.1180 0.055 Uiso 1 1 calc R
H21B H 0.1230 0.0430 0.1993 0.055 Uiso 1 1 calc R
H21C H 0.1777 0.1323 0.1288 0.055 Uiso 1 1 calc R
C22 C -0.19182(17) 0.15010(16) 0.31254(15) 0.0247(4) Uani 1 1 d .
H22 H -0.2369 0.1092 0.3633 0.030 Uiso 1 1 calc R
C23 C -0.2157(2) 0.06001(18) 0.20230(16) 0.0339(5) Uani 1 1 d .
H23A H -0.3068 0.0310 0.1858 0.051 Uiso 1 1 calc R
H23B H -0.1709 -0.0082 0.2036 0.051 Uiso 1 1 calc R
H23C H -0.1847 0.0998 0.1472 0.051 Uiso 1 1 calc R
C24 C -0.25722(19) 0.25994(18) 0.30901(18) 0.0340(5) Uani 1 1 d .
H24A H -0.2168 0.3035 0.2598 0.051 Uiso 1 1 calc R
H24B H -0.2494 0.3134 0.3811 0.051 Uiso 1 1 calc R
H24C H -0.3471 0.2329 0.2839 0.051 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C15 Si1 C13 102.54(9) . .
C15 Si1 C14 109.03(9) . .
C13 Si1 C14 105.57(10) . .
C15 Si1 Si2 108.26(7) . .
C13 Si1 Si2 116.82(7) . .
C14 Si1 Si2 113.87(7) . .
F1 Si2 Si2 118.27(10) . 2_556
F1 Si2 Si1 104.44(9) . .
Si2 Si2 Si1 106.68(5) 2_556 .
F1 Si2 Si3 105.30(9) . .
Si2 Si2 Si3 113.66(4) 2_556 .
Si1 Si2 Si3 107.73(4) . .
C16 Si3 C19 103.73(9) . .
C16 Si3 C22 107.35(8) . .
C19 Si3 C22 110.48(9) . .
C16 Si3 Si2 116.08(6) . .
C19 Si3 Si2 108.84(6) . .
C22 Si3 Si2 110.17(6) . .
O2 K1 O2 180.0 2_665 .
O2 K1 O3 88.27(5) 2_665 2_665
O2 K1 O3 91.73(5) . 2_665
O2 K1 O3 91.73(5) 2_665 .
O2 K1 O3 88.27(5) . .
O3 K1 O3 180.00(6) 2_665 .
O2 K1 O1 85.20(6) 2_665 2_665
O2 K1 O1 94.80(6) . 2_665
O3 K1 O1 86.91(5) 2_665 2_665
O3 K1 O1 93.09(5) . 2_665
O2 K1 O1 94.80(6) 2_665 .
O2 K1 O1 85.20(6) . .
O3 K1 O1 93.09(5) 2_665 .
O3 K1 O1 86.91(5) . .
O1 K1 O1 180.0 2_665 .
O2 K1 C8 22.48(5) 2_665 2_665
O2 K1 C8 157.51(5) . 2_665
O3 K1 C8 73.30(6) 2_665 2_665
O3 K1 C8 106.70(6) . 2_665
O1 K1 C8 100.88(6) 2_665 2_665
O1 K1 C8 79.12(6) . 2_665
O2 K1 C12 97.35(6) 2_665 2_665
O2 K1 C12 82.65(6) . 2_665
O3 K1 C12 22.44(5) 2_665 2_665
O3 K1 C12 157.56(5) . 2_665
O1 K1 C12 108.04(6) 2_665 2_665
O1 K1 C12 71.96(6) . 2_665
C8 K1 C12 77.25(7) 2_665 2_665
C4 O1 C1 105.96(18) . .
C4 O1 K1 135.29(16) . .
C1 O1 K1 118.24(13) . .
C5 O2 C8 107.22(18) . .
C5 O2 K1 140.14(15) . .
C8 O2 K1 111.43(13) . .
C12 O3 C9 109.34(15) . .
C12 O3 K1 111.49(12) . .
C9 O3 K1 122.69(13) . .
O1 C1 C2 106.71(19) . .
C3 C2 C1 103.95(19) . .
C4 C3 C2 104.6(2) . .
O1 C4 C3 106.5(2) . .
O2 C5 C6 104.7(2) . .
C5 C6 C7 102.1(2) . .
C6 C7 C8 103.7(2) . .
O2 C8 C7 107.3(2) . .
O3 C9 C10 106.87(17) . .
C9 C10 C11 102.81(17) . .
C10 C11 C12 101.72(18) . .
O3 C12 C11 105.23(17) . .
C17 C16 C18 109.46(16) . .
C17 C16 Si3 113.50(13) . .
C18 C16 Si3 112.35(13) . .
C21 C19 C20 110.21(16) . .
C21 C19 Si3 116.55(14) . .
C20 C19 Si3 113.85(13) . .
C23 C22 C24 109.50(16) . .
C23 C22 Si3 112.47(14) . .
C24 C22 Si3 116.10(13) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Si1 C15 1.888(2) .
Si1 C13 1.897(2) .
Si1 C14 1.899(2) .
Si1 Si2 2.3632(9) .
Si2 F1 1.492(2) .
Si2 Si2 2.3286(13) 2_556
Si2 Si3 2.3830(9) .
Si3 C16 1.9182(19) .
Si3 C19 1.920(2) .
Si3 C22 1.9214(19) .
K1 O2 2.6929(18) 2_665
K1 O2 2.6929(18) .
K1 O3 2.7013(15) 2_665
K1 O3 2.7013(15) .
K1 O1 2.7224(16) 2_665
K1 O1 2.7225(16) .
K1 C8 3.480(3) 2_665
K1 C12 3.490(2) 2_665
O1 C4 1.420(3) .
O1 C1 1.424(3) .
O2 C5 1.419(3) .
O2 C8 1.430(3) .
O3 C12 1.432(3) .
O3 C9 1.440(3) .
C1 C2 1.527(3) .
C2 C3 1.512(4) .
C3 C4 1.469(4) .
C5 C6 1.501(4) .
C6 C7 1.507(4) .
C7 C8 1.522(4) .
C9 C10 1.517(3) .
C10 C11 1.519(3) .
C11 C12 1.520(3) .
C16 C17 1.531(3) .
C16 C18 1.534(3) .
C19 C21 1.535(3) .
C19 C20 1.540(3) .
C22 C23 1.537(3) .
C22 C24 1.539(2) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C15 Si1 Si2 F1 -34.61(11) . .
C13 Si1 Si2 F1 80.41(12) . .
C14 Si1 Si2 F1 -156.04(11) . .
C15 Si1 Si2 Si2 91.38(8) . 2_556
C13 Si1 Si2 Si2 -153.60(8) . 2_556
C14 Si1 Si2 Si2 -30.05(8) . 2_556
C15 Si1 Si2 Si3 -146.23(7) . .
C13 Si1 Si2 Si3 -31.21(9) . .
C14 Si1 Si2 Si3 92.34(8) . .
F1 Si2 Si3 C16 -175.65(11) . .
Si2 Si2 Si3 C16 53.36(8) 2_556 .
Si1 Si2 Si3 C16 -64.62(8) . .
F1 Si2 Si3 C19 -59.15(12) . .
Si2 Si2 Si3 C19 169.85(7) 2_556 .
Si1 Si2 Si3 C19 51.88(8) . .
F1 Si2 Si3 C22 62.11(12) . .
Si2 Si2 Si3 C22 -68.88(8) 2_556 .
Si1 Si2 Si3 C22 173.14(7) . .
O2 K1 O1 C4 27.3(3) 2_665 .
O2 K1 O1 C4 -152.7(3) . .
O3 K1 O1 C4 -61.2(3) 2_665 .
O3 K1 O1 C4 118.8(3) . .
O1 K1 O1 C4 2(5) 2_665 .
C8 K1 O1 C4 11.1(3) 2_665 .
C12 K1 O1 C4 -68.9(3) 2_665 .
O2 K1 O1 C1 -143.16(15) 2_665 .
O2 K1 O1 C1 36.84(15) . .
O3 K1 O1 C1 128.31(15) 2_665 .
O3 K1 O1 C1 -51.69(15) . .
O1 K1 O1 C1 -168(5) 2_665 .
C8 K1 O1 C1 -159.35(16) 2_665 .
C12 K1 O1 C1 120.65(16) 2_665 .
O2 K1 O2 C5 26(5) 2_665 .
O3 K1 O2 C5 -62.1(2) 2_665 .
O3 K1 O2 C5 117.9(2) . .
O1 K1 O2 C5 -149.2(2) 2_665 .
O1 K1 O2 C5 30.8(2) . .
C8 K1 O2 C5 -14.9(3) 2_665 .
C12 K1 O2 C5 -41.6(2) 2_665 .
O2 K1 O2 C8 -139(5) 2_665 .
O3 K1 O2 C8 132.76(17) 2_665 .
O3 K1 O2 C8 -47.24(17) . .
O1 K1 O2 C8 45.72(17) 2_665 .
O1 K1 O2 C8 -134.28(17) . .
C8 K1 O2 C8 180.0 2_665 .
C12 K1 O2 C8 153.33(17) 2_665 .
O2 K1 O3 C12 -65.90(13) 2_665 .
O2 K1 O3 C12 114.10(13) . .
O3 K1 O3 C12 -148(58) 2_665 .
O1 K1 O3 C12 19.39(13) 2_665 .
O1 K1 O3 C12 -160.61(13) . .
C8 K1 O3 C12 -82.95(14) 2_665 .
C12 K1 O3 C12 180.001(1) 2_665 .
O2 K1 O3 C9 66.61(15) 2_665 .
O2 K1 O3 C9 -113.39(15) . .
O3 K1 O3 C9 -16(58) 2_665 .
O1 K1 O3 C9 151.90(15) 2_665 .
O1 K1 O3 C9 -28.10(15) . .
C8 K1 O3 C9 49.56(16) 2_665 .
C12 K1 O3 C9 -47.5(2) 2_665 .
C4 O1 C1 C2 -28.1(3) . .
K1 O1 C1 C2 144.88(15) . .
O1 C1 C2 C3 9.3(3) . .
C1 C2 C3 C4 12.1(3) . .
C1 O1 C4 C3 36.6(3) . .
K1 O1 C4 C3 -134.6(2) . .
C2 C3 C4 O1 -29.8(4) . .
C8 O2 C5 C6 34.9(3) . .
K1 O2 C5 C6 -130.6(2) . .
O2 C5 C6 C7 -38.9(3) . .
C5 C6 C7 C8 27.8(3) . .
C5 O2 C8 C7 -16.6(3) . .
K1 O2 C8 C7 153.49(17) . .
C6 C7 C8 O2 -8.0(3) . .
C12 O3 C9 C10 -1.0(2) . .
K1 O3 C9 C10 -134.40(15) . .
O3 C9 C10 C11 23.4(2) . .
C9 C10 C11 C12 -35.3(2) . .
C9 O3 C12 C11 -22.0(2) . .
K1 O3 C12 C11 116.93(15) . .
C10 C11 C12 O3 35.7(2) . .
C19 Si3 C16 C17 178.37(13) . .
C22 Si3 C16 C17 61.40(15) . .
Si2 Si3 C16 C17 -62.31(14) . .
C19 Si3 C16 C18 -56.76(15) . .
C22 Si3 C16 C18 -173.74(13) . .
Si2 Si3 C16 C18 62.55(15) . .
C16 Si3 C19 C21 170.58(15) . .
C22 Si3 C19 C21 -74.65(16) . .
Si2 Si3 C19 C21 46.42(16) . .
C16 Si3 C19 C20 -59.39(16) . .
C22 Si3 C19 C20 55.37(16) . .
Si2 Si3 C19 C20 176.45(13) . .
C16 Si3 C22 C23 159.70(13) . .
C19 Si3 C22 C23 47.23(15) . .
Si2 Si3 C22 C23 -73.05(14) . .
C16 Si3 C22 C24 32.49(17) . .
C19 Si3 C22 C24 -79.97(16) . .
Si2 Si3 C22 C24 159.75(13) . .
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1 PubChem 139117558
