#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/12/05/4120505.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4120505
loop_
_publ_author_name
'Wong, Joanne W. L.'
'Mailman, Aaron'
'Lekin, Kristina'
'Winter, Stephen M.'
'Yong, Wenjun'
'Zhao, Jianbao'
'Garimella, Subrahmanyam V.'
'Tse, John S.'
'Secco, Richard A.'
'Desgreniers, Serge'
'Ohishi, Yasuo'
'Borondics, Ferenc'
'Oakley, Richard T.'
_publ_section_title
;
 Pressure induced phase transitions and metallization of a neutral radical
 conductor.
;
_journal_issue                   3
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1070
_journal_page_last               1081
_journal_paper_doi               10.1021/ja411057x
_journal_volume                  136
_journal_year                    2014
_chemical_formula_moiety         'C6 H N2 O S4'
_chemical_formula_sum            'C6 H N2 O S4'
_chemical_formula_weight         245.33
_chemical_name_common            HBBO
_chemical_name_systematic        ' ?'
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2ab'
_symmetry_space_group_name_H-M   'P b n 21'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   12.8799(24)
_cell_length_b                   14.888(4)
_cell_length_c                   3.2737(5)
_cell_volume                     627.8(2)
_computing_structure_refinement  GSAS
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device_type  'SPring-8 BL10XU'
_diffrn_radiation_polarisn_ratio 0.95
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.41337
_diffrn_source                   synchrotron
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.596
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01
_pd_meas_2theta_range_max        27.6
_pd_meas_2theta_range_min        1.0
_pd_meas_number_of_points        2661
_pd_phase_name                   HBBO_18_again/HBBO_18_pbn21.cif
_pd_proc_2theta_range_inc        0.01
_pd_proc_2theta_range_max        27.67433
_pd_proc_2theta_range_min        1.07433
_pd_proc_info_datetime           2013-04-30T17:18:20
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with  8 terms.
 Shifted Chebyshev function of 1st kind
      1:    53714.7     2:    28763.3     3:   -1335.67     4:    7.16806    
      5:   -309.797     6:   -229.811     7:   -83.1807     8:   -29.6382    
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_profile_function
;
 CW Profile function number 2 with  18 terms
 Profile coefficients for Simpson's rule integration of pseudovoigt function
 C.J. Howard (1982). J. Appl. Cryst.,15,615-620.
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0049
_pd_proc_ls_prof_wR_expected     0.0042
_pd_proc_ls_prof_wR_factor       0.0085
_pd_proc_number_of_points        2661
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   2.01
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.71681
_refine_ls_shift/su_max          0.04
_refine_ls_shift/su_mean         0.02
_reflns_d_resolution_high        1.906
_reflns_d_resolution_low         7.444
_reflns_limit_h_max              8
_reflns_limit_h_min              0
_reflns_limit_k_max              9
_reflns_limit_k_min              0
_reflns_limit_l_max              2
_reflns_limit_l_min              0
_reflns_number_total             68
_cod_data_source_file            ja411057x_si_004.cif
_cod_data_source_block           HBBO_6.01GPa
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/usr/data/users/saulius/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (17
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to
/usr/data/users/saulius/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26 (24
times).

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_cell_volume        627.73(16)
_cod_original_sg_symbol_Hall     'c -2ab'
_cod_database_code               4120505
#BEGIN Tags that were not found in dictionaries:
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,+z
3 +x+1/2,-y+1/2,+z+1/2
4 -x,-y,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
S S3 -0.04327 0.33198 0.39727 1.0 Uiso 0.0247 4
S S4 0.02148 0.21633 0.10064 1.0 Uiso 0.0247 4
S S1 0.40041 0.55791 1.04627 1.0 Uiso 0.0247 4
S S2 0.23691 0.58532 1.08992 1.0 Uiso 0.0247 4
C C2 0.16899 0.3187 0.35784 1.0 Uiso 0.0247 4
C C1 0.28202 0.34835 0.41224 1.0 Uiso 0.0247 4
C C4 0.10022 0.45662 0.73539 1.0 Uiso 0.0247 4
N N1 0.39374 0.46288 0.76495 1.0 Uiso 0.0247 4
O O1 0.35652 0.30677 0.24728 1.0 Uiso 0.0247 4
C C6 0.29586 0.43308 0.67009 1.0 Uiso 0.0247 4
N N2 0.14759 0.24069 0.15648 1.0 Uiso 0.0247 4
C C3 0.08314 0.37513 0.51441 1.0 Uiso 0.0247 4
C C5 0.20563 0.48451 0.81202 1.0 Uiso 0.0247 4
H H4 0.0408 0.49438 0.84909 1.0 Uiso 0.0494 4
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
S 16.0 0.000 0.000 6.90530 1.46790 5.20340 22.2151 1.43790 0.25360 1.58630
56.1720 0.86690 International_Tables_Vol_C
C 24.0 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
N 8.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630
0.58260 -11.529 International_Tables_Vol_C
O 4.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
H 4.0 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081
57.7997 0.00304 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
S4 S3 C3 91.798 1_555 1_555 n
S3 S4 N2 98.851 1_555 1_555 n
S2 S1 N1 98.355 1_555 1_555 n
S1 S2 C5 91.569 1_555 1_555 n
C1 C2 N2 119.5909 1_555 1_555 n
C1 C2 C3 120.410 1_555 1_555 n
N2 C2 C3 119.986 1_555 1_555 n
C2 C1 O1 122.079 1_555 1_555 n
C2 C1 C6 114.3916 1_555 1_555 n
O1 C1 C6 123.507 1_555 1_555 n
C3 C4 C5 118.5145 1_555 1_555 n
C3 C4 H4 122.477 1_555 1_555 n
C5 C4 H4 118.971 1_555 1_555 n
S1 N1 C6 116.145 1_555 1_555 n
C1 C6 N1 119.9390 1_555 1_555 n
C1 C6 C5 120.882 1_555 1_555 n
N1 C6 C5 119.167 1_555 1_555 n
S4 N2 C2 115.6818 1_555 1_555 n
S3 C3 C2 113.652 1_555 1_555 n
S3 C3 C4 123.5317 1_555 1_555 n
C2 C3 C4 122.815 1_555 1_555 n
S2 C5 C4 122.5913 1_555 1_555 n
S2 C5 C6 114.691 1_555 1_555 n
C4 C5 C6 122.717 1_555 1_555 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S3 S4 2.14545 1_555 n
S3 C3 1.79181 1_555 n
S4 N2 1.67429 1_555 n
S1 S2 2.1498 1_555 n
S1 N1 1.69030 1_555 n
S2 S1 2.1498 1_555 n
S2 C5 1.80068 1_555 n
C2 C1 1.53165 1_555 n
C2 N2 1.36357 1_555 n
C2 C3 1.48026 1_555 n
C1 O1 1.26316 1_555 n
C1 C6 1.52824 1_555 n
C4 C3 1.42953 1_555 n
C4 C5 1.44174 1_555 n
C4 H4 1.01994 1_555 n
N1 C6 1.37207 1_555 n
C6 C5 1.46722 1_555 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
0.0 0.0 11894.11816 .
0.0 0.0 11912.64648 .
0.0 0.0 11931.90625 .
0.0 0.0 11951.89844 .
0.0 0.0 11972.60645 .
0.0 0.0 11994.03320 .
0.0 0.0 12016.16309 .
0.0 0.0 12038.99512 .
0.0 0.0 12062.51465 .
0.0 0.0 12086.72559 .
0.0 0.0 12111.60938 .
0.0 0.0 12137.16797 .
0.0 0.0 12163.38770 .
0.0 0.0 12190.27051 .
0.0 0.0 12217.79688 .
0.0 0.0 12245.97266 .
0.0 0.0 12274.78320 .
0.0 0.0 12304.22852 .
0.0 0.0 12334.29199 .
0.0 0.0 12364.97754 .
0.0 0.0 12396.26953 .
0.0 0.0 12428.17090 .
0.0 0.0 12460.66602 .
0.0 0.0 12493.75879 .
0.0 0.0 12527.43164 .
0.0 0.0 12561.68848 .
0.0 0.0 12596.51465 .
0.0 0.0 12631.90625 .
0.0 0.0 12667.86426 .
0.0 0.0 12704.37500 .
0.0 0.0 12741.43555 .
0.0 0.0 12779.03613 .
0.0 0.0 12817.17773 .
0.0 0.0 12855.85059 .
0.0 0.0 12895.04395 .
0.0 0.0 12934.75781 .
0.0 0.0 12974.98828 .
0.0 0.0 13015.72363 .
0.0 0.0 13056.96484 .
0.0 0.0 13098.70020 .
0.0 0.0 13140.92969 .
0.0 0.0 13183.64355 .
0.0 0.0 13226.83789 .
0.0 0.0 13270.50488 .
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9750.0 0.0 16451.41602 .
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23244.0 0.0 23033.27734 .
23272.0 0.0 23106.84375 .
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23467.0 0.0 23254.04297 .
23556.0 0.0 23327.67383 .
23640.0 0.0 23401.32813 .
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23728.0 0.0000421 23548.68359 23963.99805
23799.0 0.0000420 23622.39063 24025.87891
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24177.0 0.0000414 23917.34961 24278.48633
24244.0 0.0000412 23991.12500 24342.78516
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26910.0 0.0000372 26646.61133 26851.46289
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27052.0 0.0000370 26793.72852 27007.73828
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27379.0 0.0000365 27087.71484 27355.44336
27433.0 0.0000365 27161.15625 27453.25977
27489.0 0.0000364 27234.57617 27556.28516
27593.0 0.0000362 27307.97070 27664.47656
27641.0 0.0000362 27381.34180 27777.33594
27758.0 0.0000360 27454.69141 27893.79688
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