#------------------------------------------------------------------------------
#$Date: 2016-03-22 23:03:07 +0200 (Tue, 22 Mar 2016) $
#$Revision: 179047 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/09/4300950.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4300950
loop_
_publ_author_name
'Zdenek Spichal'
'Marek Necas'
'Jiri Pinkas'
_publ_section_title
;

From Parquets to Bricks: A Series of Lanthanide Coordination Polymers

with Bis(diphenylphosphino)ethane Dioxide

;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2074
_journal_page_last               2080
_journal_paper_doi               10.1021/ic048826f
_journal_volume                  44
_journal_year                    2005
_chemical_formula_sum            'C39 H36 Dy N3 O12 P3'
_chemical_formula_weight         994.12
_chemical_name_systematic
; 

 ? 

;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                96.74(6)
_cell_angle_beta                 94.47(6)
_cell_angle_gamma                106.69(7)
_cell_formula_units_Z            4
_cell_length_a                   14.284(12)
_cell_length_b                   14.768(12)
_cell_length_c                   19.818(11)
_cell_measurement_temperature    120(2)
_cell_volume                     3949(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.973
_diffrn_measured_fraction_theta_max 0.973
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0541
_diffrn_reflns_av_sigmaI/netI    0.0408
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            25311
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.85
_exptl_absorpt_coefficient_mu    2.081
_exptl_absorpt_correction_T_max  0.4898
_exptl_absorpt_correction_T_min  0.4226
_exptl_crystal_density_diffrn    1.672
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1992
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.40
_refine_diff_density_max         1.586
_refine_diff_density_min         -1.562
_refine_diff_density_rms         0.140
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.136
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1045
_refine_ls_number_reflns         13533
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.136
_refine_ls_R_factor_all          0.0452
_refine_ls_R_factor_gt           0.0420
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0355P)²+21.4888P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1029
_refine_ls_wR_factor_ref         0.1046
_reflns_number_gt                12344
_reflns_number_total             13533
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic048826fsi20040825_065511_05.cif
_cod_data_source_block           6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4300950
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy -0.011552(16) 1.319059(15) 0.736820(12) 0.01321(7) Uani 1 1 d . . .
Dy2 Dy -0.410049(16) 1.719149(15) 0.748035(12) 0.01307(7) Uani 1 1 d . . .
P2 P 0.16272(9) 1.56132(8) 0.74375(7) 0.0137(3) Uani 1 1 d . . .
P3 P -0.15116(9) 1.07240(8) 0.65978(7) 0.0145(3) Uani 1 1 d . . .
P5 P -0.31952(10) 1.97263(9) 0.82726(7) 0.0178(3) Uani 1 1 d . . .
P4 P -0.56441(9) 1.47977(9) 0.77044(7) 0.0155(3) Uani 1 1 d . . .
P1 P -0.23699(9) 1.39235(9) 0.69534(7) 0.0156(3) Uani 1 1 d . . .
P6 P -0.16853(9) 1.68429(9) 0.80007(7) 0.0162(3) Uani 1 1 d . . .
O21 O -0.0040(3) 1.3375(2) 0.61648(19) 0.0207(8) Uani 1 1 d . . .
O63 O -0.2517(4) 1.6925(3) 0.5882(3) 0.0519(14) Uani 1 1 d . . .
O13 O -0.1596(3) 1.3485(3) 0.9010(2) 0.0409(11) Uani 1 1 d . . .
O41 O -0.4347(3) 1.7164(2) 0.8703(2) 0.0237(8) Uani 1 1 d . . .
O22 O 0.1173(3) 1.3042(2) 0.66658(19) 0.0207(8) Uani 1 1 d . . .
O42 O -0.5518(3) 1.7318(2) 0.8035(2) 0.0221(8) Uani 1 1 d . . .
O4 O -0.4876(2) 1.5634(2) 0.75306(17) 0.0147(7) Uani 1 1 d . . .
O43 O -0.5645(4) 1.7400(3) 0.9105(2) 0.0419(12) Uani 1 1 d . . .
O2 O 0.0835(2) 1.4707(2) 0.74288(18) 0.0159(7) Uani 1 1 d . . .
O6 O -0.2686(3) 1.6971(3) 0.79233(19) 0.0203(8) Uani 1 1 d . . .
O23 O 0.1195(4) 1.3325(4) 0.5618(2) 0.0452(12) Uani 1 1 d . . .
O1 O -0.1385(2) 1.3769(2) 0.70635(18) 0.0178(7) Uani 1 1 d . . .
O32 O 0.1361(3) 1.3289(3) 0.8166(2) 0.0244(8) Uani 1 1 d . . .
O12 O -0.1290(3) 1.2616(2) 0.8155(2) 0.0279(9) Uani 1 1 d . . .
O11 O -0.0364(3) 1.4042(3) 0.84489(19) 0.0248(8) Uani 1 1 d . . .
C4 C -0.6764(4) 1.5061(4) 0.7876(3) 0.0195(11) Uani 1 1 d . . .
H4A H -0.7243 1.4476 0.7979 0.023 Uiso 1 1 calc R . .
H4B H -0.6623 1.5551 0.8287 0.023 Uiso 1 1 calc R . .
C1I C -0.2248(4) 2.0045(4) 0.8973(3) 0.0222(11) Uani 1 1 d . . .
O62 O -0.3554(3) 1.6280(3) 0.6556(2) 0.0297(9) Uani 1 1 d . . .
O5 O -0.3435(3) 1.8699(2) 0.80195(19) 0.0217(8) Uani 1 1 d . . .
O52 O -0.4762(3) 1.8295(3) 0.6878(2) 0.0390(11) Uani 1 1 d . . .
N50 N -0.5347(3) 1.7632(4) 0.6477(3) 0.0312(12) Uani 1 1 d . . .
O31 O 0.0405(3) 1.1896(3) 0.7830(2) 0.0348(10) Uani 1 1 d . . .
C1D C 0.1782(4) 1.6321(4) 0.8250(3) 0.0182(11) Uani 1 1 d . . .
O33 O 0.1784(3) 1.2079(3) 0.8445(2) 0.0379(11) Uani 1 1 d . . .
C3K C -0.0529(4) 1.6075(4) 0.9693(3) 0.0312(14) Uani 1 1 d . . .
H3KA H -0.0033 1.5793 0.9817 0.037 Uiso 1 1 calc R . .
N10 N -0.1093(3) 1.3380(3) 0.8561(2) 0.0192(9) Uani 1 1 d . . .
C6D C 0.1788(4) 1.5855(4) 0.8812(3) 0.0221(11) Uani 1 1 d . . .
H6DA H 0.1696 1.5186 0.8748 0.027 Uiso 1 1 calc R . .
C1F C -0.0687(4) 1.0147(3) 0.6237(3) 0.0163(10) Uani 1 1 d . . .
C6H C -0.5838(4) 1.3738(4) 0.8791(3) 0.0325(14) Uani 1 1 d . . .
H6HA H -0.6511 1.3461 0.8615 0.039 Uiso 1 1 calc R . .
C5A C -0.4687(5) 1.1542(5) 0.6766(5) 0.049(2) Uani 1 1 d . . .
H5AA H -0.5058 1.1059 0.6407 0.059 Uiso 1 1 calc R . .
O53 O -0.5820(4) 1.7837(5) 0.5993(4) 0.078(2) Uani 1 1 d . . .
C6F C 0.0265(4) 1.0684(4) 0.6173(3) 0.0216(11) Uani 1 1 d . . .
H6FA H 0.0500 1.1340 0.6364 0.026 Uiso 1 1 calc R . .
C3B C -0.2148(4) 1.4356(4) 0.5005(3) 0.0287(13) Uani 1 1 d . . .
H3BA H -0.1662 1.4416 0.4699 0.034 Uiso 1 1 calc R . .
C5E C -0.3141(4) 1.1315(5) 0.5083(3) 0.0322(14) Uani 1 1 d . . .
H5EA H -0.3150 1.1869 0.4886 0.039 Uiso 1 1 calc R . .
C1G C -0.5994(4) 1.3870(4) 0.7001(3) 0.0214(12) Uani 1 1 d . . .
C6B C -0.3544(4) 1.4226(4) 0.5901(3) 0.0279(13) Uani 1 1 d . . .
H6BA H -0.4020 1.4195 0.6214 0.033 Uiso 1 1 calc R . .
C3 C -0.1997(4) 1.0097(3) 0.7271(3) 0.0183(11) Uani 1 1 d . . .
H3A H -0.2266 0.9409 0.7087 0.022 Uiso 1 1 calc R . .
H3B H -0.1448 1.0167 0.7629 0.022 Uiso 1 1 calc R . .
C2 C 0.2780(4) 1.5414(3) 0.7290(3) 0.0175(10) Uani 1 1 d . . .
H2A H 0.2678 1.4941 0.6873 0.021 Uiso 1 1 calc R . .
H2B H 0.3245 1.6020 0.7205 0.021 Uiso 1 1 calc R . .
C5B C -0.3748(5) 1.4389(5) 0.5251(3) 0.0386(16) Uani 1 1 d . . .
H5BA H -0.4372 1.4455 0.5109 0.046 Uiso 1 1 calc R . .
N30 N 0.1199(3) 1.2422(3) 0.8157(2) 0.0238(10) Uani 1 1 d . . .
C5K C -0.1818(4) 1.6708(4) 0.9997(3) 0.0314(13) Uani 1 1 d . . .
H5KA H -0.2202 1.6874 1.0333 0.038 Uiso 1 1 calc R . .
C1K C -0.1427(4) 1.6628(3) 0.8846(3) 0.0175(10) Uani 1 1 d . . .
C6C C 0.0431(4) 1.5830(4) 0.6376(3) 0.0194(11) Uani 1 1 d . . .
H6CA H -0.0018 1.5263 0.6477 0.023 Uiso 1 1 calc R . .
C2I C -0.1487(5) 2.0887(4) 0.9066(3) 0.0297(13) Uani 1 1 d . . .
H2IA H -0.1430 2.1312 0.8736 0.036 Uiso 1 1 calc R . .
C3C C 0.1726(5) 1.7480(4) 0.6087(3) 0.0297(13) Uani 1 1 d . . .
H3CA H 0.2163 1.8056 0.5991 0.036 Uiso 1 1 calc R . .
C5D C 0.1922(4) 1.6335(4) 0.9455(3) 0.0273(12) Uani 1 1 d . . .
H5DA H 0.1945 1.6010 0.9839 0.033 Uiso 1 1 calc R . .
C1C C 0.1332(4) 1.6228(3) 0.6774(3) 0.0174(10) Uani 1 1 d . . .
C1H C -0.5228(4) 1.4412(4) 0.8455(3) 0.0222(11) Uani 1 1 d . . .
C3I C -0.0815(5) 2.1106(5) 0.9636(4) 0.0387(16) Uani 1 1 d . . .
H3IA H -0.0290 2.1686 0.9705 0.046 Uiso 1 1 calc R . .
C2E C -0.3164(4) 0.9711(4) 0.5695(3) 0.0293(13) Uani 1 1 d . . .
H2EA H -0.3182 0.9167 0.5912 0.035 Uiso 1 1 calc R . .
C1J C -0.4221(4) 2.0023(4) 0.8602(3) 0.0249(12) Uani 1 1 d . . .
C5 C -0.2796(4) 2.0410(4) 0.7605(3) 0.0203(11) Uani 1 1 d . . .
H5A H -0.3361 2.0326 0.7257 0.024 Uiso 1 1 calc R . .
H5B H -0.2539 2.1097 0.7797 0.024 Uiso 1 1 calc R . .
C6A C -0.3921(4) 1.2290(4) 0.6619(4) 0.0319(14) Uani 1 1 d . . .
H6AA H -0.3778 1.2327 0.6161 0.038 Uiso 1 1 calc R . .
C5C C 0.0187(4) 1.6260(4) 0.5832(3) 0.0264(12) Uani 1 1 d . . .
H5CA H -0.0431 1.5990 0.5560 0.032 Uiso 1 1 calc R . .
C5I C -0.1652(5) 1.9646(5) 1.0016(3) 0.0382(15) Uani 1 1 d . . .
H5IA H -0.1701 1.9219 1.0344 0.046 Uiso 1 1 calc R . .
C4F C 0.0535(4) 0.9316(4) 0.5553(3) 0.0282(13) Uani 1 1 d . . .
H4FA H 0.0949 0.9031 0.5308 0.034 Uiso 1 1 calc R . .
C6I C -0.2326(4) 1.9426(4) 0.9450(3) 0.0297(13) Uani 1 1 d . . .
H6IA H -0.2850 1.8846 0.9384 0.036 Uiso 1 1 calc R . .
C2A C -0.3586(5) 1.2909(5) 0.7801(4) 0.0359(15) Uani 1 1 d . . .
H2AA H -0.3200 1.3372 0.8167 0.043 Uiso 1 1 calc R . .
C1E C -0.2476(4) 1.0580(4) 0.5934(3) 0.0186(11) Uani 1 1 d . . .
C6 C -0.1603(4) 1.5848(4) 0.7424(3) 0.0218(11) Uani 1 1 d . . .
H6A H -0.1665 1.5983 0.6948 0.026 Uiso 1 1 calc R . .
H6B H -0.0954 1.5747 0.7523 0.026 Uiso 1 1 calc R . .
C4D C 0.2024(5) 1.7302(5) 0.9546(3) 0.0343(15) Uani 1 1 d . . .
H4DA H 0.2112 1.7644 0.9995 0.041 Uiso 1 1 calc R . .
C4A C -0.4907(5) 1.1491(6) 0.7399(5) 0.055(2) Uani 1 1 d . . .
H4AA H -0.5445 1.0983 0.7484 0.067 Uiso 1 1 calc R . .
C1A C -0.3374(4) 1.2974(4) 0.7143(3) 0.0232(12) Uani 1 1 d . . .
C6E C -0.2463(4) 1.1374(4) 0.5631(3) 0.0240(12) Uani 1 1 d . . .
H6EA H -0.1983 1.1968 0.5802 0.029 Uiso 1 1 calc R . .
C2B C -0.1952(4) 1.4170(4) 0.5650(3) 0.0223(11) Uani 1 1 d . . .
H2BA H -0.1336 1.4084 0.5788 0.027 Uiso 1 1 calc R . .
C2H C -0.4260(4) 1.4830(4) 0.8731(3) 0.0222(11) Uani 1 1 d . . .
H2HA H -0.3839 1.5307 0.8517 0.027 Uiso 1 1 calc R . .
C3L C 0.0016(4) 1.9565(4) 0.8179(3) 0.0270(12) Uani 1 1 d . . .
H3LA H 0.0056 2.0146 0.8459 0.032 Uiso 1 1 calc R . .
C3A C -0.4373(5) 1.2158(6) 0.7934(5) 0.052(2) Uani 1 1 d . . .
H3AA H -0.4533 1.2111 0.8388 0.062 Uiso 1 1 calc R . .
C1L C -0.0756(4) 1.7880(4) 0.7861(3) 0.0186(11) Uani 1 1 d . . .
C4K C -0.1081(4) 1.6317(4) 1.0175(3) 0.0310(14) Uani 1 1 d . . .
H4KA H -0.0959 1.6217 1.0634 0.037 Uiso 1 1 calc R . .
C4B C -0.3054(5) 1.4458(5) 0.4796(3) 0.0349(14) Uani 1 1 d . . .
H4BA H -0.3198 1.4575 0.4344 0.042 Uiso 1 1 calc R . .
C4L C 0.0651(4) 1.9561(4) 0.7694(3) 0.0246(12) Uani 1 1 d . . .
H4LA H 0.1136 2.0135 0.7642 0.030 Uiso 1 1 calc R . .
C1B C -0.2647(4) 1.4107(3) 0.6103(3) 0.0176(10) Uani 1 1 d . . .
C6L C -0.0118(5) 1.7887(4) 0.7370(3) 0.0318(14) Uani 1 1 d . . .
H6LA H -0.0158 1.7310 0.7086 0.038 Uiso 1 1 calc R . .
N20 N 0.0798(3) 1.3249(3) 0.6134(2) 0.0212(10) Uani 1 1 d . . .
O3 O -0.1038(3) 1.1761(2) 0.68301(19) 0.0200(8) Uani 1 1 d . . .
O61 O -0.3048(3) 1.7790(2) 0.66230(19) 0.0237(8) Uani 1 1 d . . .
O51 O -0.5366(3) 1.6821(3) 0.6519(2) 0.0415(11) Uani 1 1 d . . .
N40 N -0.5174(3) 1.7301(3) 0.8633(2) 0.0225(10) Uani 1 1 d . . .
N60 N -0.3035(3) 1.6998(3) 0.6329(2) 0.0256(10) Uani 1 1 d . . .
C1 C -0.2406(4) 1.4962(4) 0.7500(3) 0.0191(11) Uani 1 1 d . . .
H1A H -0.3051 1.5070 0.7397 0.023 Uiso 1 1 calc R . .
H1B H -0.2349 1.4846 0.7981 0.023 Uiso 1 1 calc R . .
C2K C -0.0684(4) 1.6235(4) 0.9033(3) 0.0262(12) Uani 1 1 d . . .
H2KA H -0.0286 1.6078 0.8703 0.031 Uiso 1 1 calc R . .
C6K C -0.1996(4) 1.6859(4) 0.9337(3) 0.0246(12) Uani 1 1 d . . .
H6KA H -0.2509 1.7121 0.9215 0.030 Uiso 1 1 calc R . .
C2D C 0.1877(4) 1.7279(4) 0.8339(3) 0.0271(13) Uani 1 1 d . . .
H2DA H 0.1858 1.7604 0.7954 0.032 Uiso 1 1 calc R . .
C2G C -0.5933(4) 1.4131(4) 0.6360(3) 0.0254(12) Uani 1 1 d . . .
H2GA H -0.5626 1.4779 0.6312 0.031 Uiso 1 1 calc R . .
C3H C -0.3902(5) 1.4558(5) 0.9314(3) 0.0333(14) Uani 1 1 d . . .
H3HA H -0.3233 1.4841 0.9499 0.040 Uiso 1 1 calc R . .
C4C C 0.0840(5) 1.7077(4) 0.5688(3) 0.0290(13) Uani 1 1 d . . .
H4CA H 0.0678 1.7365 0.5309 0.035 Uiso 1 1 calc R . .
C2C C 0.1986(4) 1.7062(4) 0.6625(3) 0.0226(11) Uani 1 1 d . . .
H2CA H 0.2606 1.7338 0.6894 0.027 Uiso 1 1 calc R . .
C2L C -0.0680(4) 1.8731(4) 0.8262(3) 0.0250(12) Uani 1 1 d . . .
H2LA H -0.1112 1.8743 0.8601 0.030 Uiso 1 1 calc R . .
C3D C 0.2000(5) 1.7763(4) 0.8993(4) 0.0401(17) Uani 1 1 d . . .
H3DA H 0.2069 1.8428 0.9058 0.048 Uiso 1 1 calc R . .
C3F C -0.0408(4) 0.8778(4) 0.5631(3) 0.0291(13) Uani 1 1 d . . .
H3FA H -0.0636 0.8120 0.5445 0.035 Uiso 1 1 calc R . .
C3E C -0.3825(5) 0.9647(5) 0.5135(4) 0.0407(17) Uani 1 1 d . . .
H3EA H -0.4301 0.9053 0.4958 0.049 Uiso 1 1 calc R . .
C2J C -0.5159(4) 1.9558(4) 0.8282(4) 0.0355(15) Uani 1 1 d . . .
H2JA H -0.5259 1.9103 0.7883 0.043 Uiso 1 1 calc R . .
C2F C -0.1016(4) 0.9193(4) 0.5976(3) 0.0231(12) Uani 1 1 d . . .
H2FA H -0.1660 0.8820 0.6033 0.028 Uiso 1 1 calc R . .
C5F C 0.0869(4) 1.0259(4) 0.5831(3) 0.0253(12) Uani 1 1 d . . .
H5FA H 0.1522 1.0624 0.5787 0.030 Uiso 1 1 calc R . .
C3G C -0.6312(5) 1.3463(5) 0.5786(3) 0.0362(15) Uani 1 1 d . . .
H3GA H -0.6283 1.3648 0.5343 0.043 Uiso 1 1 calc R . .
C4G C -0.6733(5) 1.2525(5) 0.5861(4) 0.0418(17) Uani 1 1 d . . .
H4GA H -0.6991 1.2057 0.5469 0.050 Uiso 1 1 calc R . .
C5L C 0.0581(5) 1.8729(4) 0.7288(4) 0.0371(15) Uani 1 1 d . . .
H5LA H 0.1013 1.8723 0.6947 0.044 Uiso 1 1 calc R . .
C5H C -0.5483(5) 1.3471(5) 0.9368(4) 0.0451(18) Uani 1 1 d . . .
H5HA H -0.5907 1.3005 0.9588 0.054 Uiso 1 1 calc R . .
C6G C -0.6416(5) 1.2922(4) 0.7074(4) 0.0361(15) Uani 1 1 d . . .
H6GA H -0.6452 1.2733 0.7516 0.043 Uiso 1 1 calc R . .
C5G C -0.6780(5) 1.2264(4) 0.6501(4) 0.049(2) Uani 1 1 d . . .
H5GA H -0.7071 1.1613 0.6547 0.059 Uiso 1 1 calc R . .
C4E C -0.3794(5) 1.0457(5) 0.4828(3) 0.0422(17) Uani 1 1 d . . .
H4EA H -0.4239 1.0404 0.4433 0.051 Uiso 1 1 calc R . .
C6J C -0.4090(5) 2.0683(5) 0.9177(3) 0.0350(14) Uani 1 1 d . . .
H6JA H -0.3447 2.1002 0.9402 0.042 Uiso 1 1 calc R . .
C4I C -0.0901(5) 2.0488(5) 1.0108(3) 0.0418(16) Uani 1 1 d . . .
H4IA H -0.0434 2.0646 1.0504 0.050 Uiso 1 1 calc R . .
C4H C -0.4517(5) 1.3871(5) 0.9631(4) 0.0430(17) Uani 1 1 d . . .
H4HA H -0.4268 1.3678 1.0031 0.052 Uiso 1 1 calc R . .
C5J C -0.4902(7) 2.0883(6) 0.9430(4) 0.050(2) Uani 1 1 d . . .
H5JA H -0.4812 2.1344 0.9825 0.059 Uiso 1 1 calc R . .
C4J C -0.5812(7) 2.0426(6) 0.9116(5) 0.057(2) Uani 1 1 d . . .
H4JA H -0.6363 2.0567 0.9290 0.068 Uiso 1 1 calc R . .
C3J C -0.5950(5) 1.9761(5) 0.8549(5) 0.052(2) Uani 1 1 d . . .
H3JA H -0.6598 1.9434 0.8337 0.062 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Dy1 O2 154.93(14) . . ?
O3 Dy1 O1 87.78(15) . . ?
O2 Dy1 O1 85.09(14) . . ?
O3 Dy1 O12 76.07(15) . . ?
O2 Dy1 O12 125.13(13) . . ?
O1 Dy1 O12 76.74(15) . . ?
O3 Dy1 O22 87.97(14) . . ?
O2 Dy1 O22 76.87(14) . . ?
O1 Dy1 O22 125.55(13) . . ?
O12 Dy1 O22 152.50(13) . . ?
O3 Dy1 O21 77.25(14) . . ?
O2 Dy1 O21 77.68(14) . . ?
O1 Dy1 O21 74.17(13) . . ?
O12 Dy1 O21 140.90(14) . . ?
O22 Dy1 O21 52.01(13) . . ?
O3 Dy1 O11 127.41(14) . . ?
O2 Dy1 O11 73.94(14) . . ?
O1 Dy1 O11 76.33(14) . . ?
O12 Dy1 O11 51.65(13) . . ?
O22 Dy1 O11 141.47(13) . . ?
O21 Dy1 O11 140.35(13) . . ?
O3 Dy1 O31 69.38(14) . . ?
O2 Dy1 O31 125.20(14) . . ?
O1 Dy1 O31 147.28(14) . . ?
O12 Dy1 O31 75.23(16) . . ?
O22 Dy1 O31 78.25(15) . . ?
O21 Dy1 O31 120.31(15) . . ?
O11 Dy1 O31 98.73(15) . . ?
O3 Dy1 O32 118.87(14) . . ?
O2 Dy1 O32 75.93(14) . . ?
O1 Dy1 O32 149.76(13) . . ?
O12 Dy1 O32 95.05(15) . . ?
O22 Dy1 O32 73.01(14) . . ?
O21 Dy1 O32 122.90(13) . . ?
O11 Dy1 O32 75.90(14) . . ?
O31 Dy1 O32 50.23(14) . . ?
O3 Dy1 N20 82.88(15) . . ?
O2 Dy1 N20 74.75(14) . . ?
O1 Dy1 N20 99.89(14) . . ?
O12 Dy1 N20 158.76(13) . . ?
O22 Dy1 N20 25.86(13) . . ?
O21 Dy1 N20 26.19(13) . . ?
O11 Dy1 N20 148.67(13) . . ?
O31 Dy1 N20 100.11(16) . . ?
O32 Dy1 N20 97.58(14) . . ?
O3 Dy1 N10 101.41(15) . . ?
O2 Dy1 N10 99.48(14) . . ?
O1 Dy1 N10 73.27(13) . . ?
O12 Dy1 N10 25.72(13) . . ?
O22 Dy1 N10 159.71(12) . . ?
O21 Dy1 N10 147.44(12) . . ?
O11 Dy1 N10 26.03(13) . . ?
O31 Dy1 N10 88.18(15) . . ?
O32 Dy1 N10 86.71(14) . . ?
N20 Dy1 N10 171.61(12) . . ?
O3 Dy1 N30 94.19(15) . . ?
O2 Dy1 N30 100.13(15) . . ?
O1 Dy1 N30 161.53(13) . . ?
O12 Dy1 N30 85.90(15) . . ?
O22 Dy1 N30 72.90(14) . . ?
O21 Dy1 N30 124.17(13) . . ?
O11 Dy1 N30 88.03(14) . . ?
O31 Dy1 N30 25.39(13) . . ?
O32 Dy1 N30 24.89(12) . . ?
N20 Dy1 N30 98.57(14) . . ?
N10 Dy1 N30 88.36(14) . . ?
O5 Dy2 O6 84.26(15) . . ?
O5 Dy2 O4 149.23(13) . . ?
O6 Dy2 O4 88.53(15) . . ?
O5 Dy2 O51 121.06(16) . . ?
O6 Dy2 O51 146.98(16) . . ?
O4 Dy2 O51 79.03(16) . . ?
O5 Dy2 O42 82.80(15) . . ?
O6 Dy2 O42 129.67(14) . . ?
O4 Dy2 O42 78.98(14) . . ?
O51 Dy2 O42 78.05(17) . . ?
O5 Dy2 O61 82.51(14) . . ?
O6 Dy2 O61 80.65(15) . . ?
O4 Dy2 O61 125.75(13) . . ?
O51 Dy2 O61 82.14(16) . . ?
O42 Dy2 O61 144.37(13) . . ?
O5 Dy2 O62 130.99(14) . . ?
O6 Dy2 O62 73.64(15) . . ?
O4 Dy2 O62 74.41(13) . . ?
O51 Dy2 O62 73.58(17) . . ?
O42 Dy2 O62 144.07(14) . . ?
O61 Dy2 O62 51.48(13) . . ?
O5 Dy2 O52 70.23(16) . . ?
O6 Dy2 O52 143.02(15) . . ?
O4 Dy2 O52 126.82(15) . . ?
O51 Dy2 O52 51.02(17) . . ?
O42 Dy2 O52 74.41(15) . . ?
O61 Dy2 O52 70.10(15) . . ?
O62 Dy2 O52 103.06(16) . . ?
O5 Dy2 O41 73.11(14) . . ?
O6 Dy2 O41 78.09(14) . . ?
O4 Dy2 O41 76.14(13) . . ?
O51 Dy2 O41 126.90(16) . . ?
O42 Dy2 O41 51.61(13) . . ?
O61 Dy2 O41 148.95(13) . . ?
O62 Dy2 O41 139.25(13) . . ?
O52 Dy2 O41 117.10(15) . . ?
O5 Dy2 N50 96.09(16) . . ?
O6 Dy2 N50 155.33(15) . . ?
O4 Dy2 N50 102.60(16) . . ?
O51 Dy2 N50 25.05(15) . . ?
O42 Dy2 N50 74.57(15) . . ?
O61 Dy2 N50 74.96(15) . . ?
O62 Dy2 N50 88.07(17) . . ?
O52 Dy2 N50 25.97(15) . . ?
O41 Dy2 N50 125.72(15) . . ?
O5 Dy2 N40 75.46(14) . . ?
O6 Dy2 N40 104.01(15) . . ?
O4 Dy2 N40 77.40(13) . . ?
O51 Dy2 N40 102.91(17) . . ?
O42 Dy2 N40 25.74(13) . . ?
O61 Dy2 N40 156.77(12) . . ?
O62 Dy2 N40 151.74(12) . . ?
O52 Dy2 N40 95.20(15) . . ?
O41 Dy2 N40 25.92(13) . . ?
N50 Dy2 N40 99.91(16) . . ?
O5 Dy2 N60 106.60(15) . . ?
O6 Dy2 N60 75.11(15) . . ?
O4 Dy2 N60 100.29(14) . . ?
O51 Dy2 N60 77.21(17) . . ?
O42 Dy2 N60 154.90(14) . . ?
O61 Dy2 N60 25.59(13) . . ?
O62 Dy2 N60 25.91(13) . . ?
O52 Dy2 N60 86.75(16) . . ?
O41 Dy2 N60 153.05(14) . . ?
N50 Dy2 N60 81.23(16) . . ?
N40 Dy2 N60 177.58(13) . . ?
O2 P2 C1C 110.1(2) . . ?
O2 P2 C1D 109.0(2) . . ?
C1C P2 C1D 111.0(2) . . ?
O2 P2 C2 112.1(2) . . ?
C1C P2 C2 106.4(2) . . ?
C1D P2 C2 108.3(3) . . ?
O3 P3 C1E 108.8(2) . . ?
O3 P3 C3 112.7(2) . . ?
C1E P3 C3 109.3(3) . . ?
O3 P3 C1F 112.6(2) . . ?
C1E P3 C1F 105.9(2) . . ?
C3 P3 C1F 107.2(2) . . ?
O5 P5 C1I 109.5(2) . . ?
O5 P5 C5 110.1(2) . . ?
C1I P5 C5 109.7(3) . . ?
O5 P5 C1J 111.9(3) . . ?
C1I P5 C1J 105.6(3) . . ?
C5 P5 C1J 109.9(3) . . ?
O4 P4 C1G 109.9(2) . . ?
O4 P4 C1H 110.9(2) . . ?
C1G P4 C1H 111.9(3) . . ?
O4 P4 C4 113.1(2) . . ?
C1G P4 C4 105.0(3) . . ?
C1H P4 C4 105.8(3) . . ?
O1 P1 C1B 111.8(2) . . ?
O1 P1 C1 110.6(2) . . ?
C1B P1 C1 106.8(3) . . ?
O1 P1 C1A 114.6(2) . . ?
C1B P1 C1A 107.6(3) . . ?
C1 P1 C1A 104.9(3) . . ?
O6 P6 C1K 108.6(2) . . ?
O6 P6 C1L 111.9(2) . . ?
C1K P6 C1L 108.1(2) . . ?
O6 P6 C6 112.1(2) . . ?
C1K P6 C6 107.9(3) . . ?
C1L P6 C6 108.1(3) . . ?
N20 O21 Dy1 95.8(3) . . ?
N40 O41 Dy2 94.3(3) . . ?
N20 O22 Dy1 96.3(3) . . ?
N40 O42 Dy2 97.2(3) . . ?
P4 O4 Dy2 157.2(2) . . ?
P2 O2 Dy1 167.9(2) . . ?
P6 O6 Dy2 162.8(2) . . ?
P1 O1 Dy1 164.3(2) . . ?
N30 O32 Dy1 96.7(3) . . ?
N10 O12 Dy1 97.3(3) . . ?
N10 O11 Dy1 95.3(3) . . ?
C2 C4 P4 113.2(4) 1_455 . ?
C2I C1I C6I 120.1(6) . . ?
C2I C1I P5 122.9(4) . . ?
C6I C1I P5 116.9(4) . . ?
N60 O62 Dy2 95.9(3) . . ?
P5 O5 Dy2 166.2(3) . . ?
N50 O52 Dy2 92.7(3) . . ?
O51 N50 O52 119.7(5) . . ?
O51 N50 O53 121.7(6) . . ?
O52 N50 O53 118.1(6) . . ?
O51 N50 Dy2 58.4(3) . . ?
O52 N50 Dy2 61.3(3) . . ?
O53 N50 Dy2 173.5(5) . . ?
N30 O31 Dy1 96.5(3) . . ?
C2D C1D C6D 119.7(5) . . ?
C2D C1D P2 123.8(4) . . ?
C6D C1D P2 116.5(4) . . ?
C4K C3K C2K 120.6(6) . . ?
O13 N10 O12 122.0(5) . . ?
O13 N10 O11 122.6(5) . . ?
O12 N10 O11 115.3(4) . . ?
O13 N10 Dy1 171.6(4) . . ?
O12 N10 Dy1 57.0(3) . . ?
O11 N10 Dy1 58.7(2) . . ?
C5D C6D C1D 121.1(5) . . ?
C2F C1F C6F 120.1(5) . . ?
C2F C1F P3 120.2(4) . . ?
C6F C1F P3 119.6(4) . . ?
C5H C6H C1H 121.0(6) . . ?
C4A C5A C6A 121.1(8) . . ?
C5F C6F C1F 119.6(5) . . ?
C2B C3B C4B 120.1(6) . . ?
C4E C5E C6E 119.1(6) . . ?
C2G C1G C6G 120.0(5) . . ?
C2G C1G P4 117.1(4) . . ?
C6G C1G P4 122.5(5) . . ?
C5B C6B C1B 119.9(6) . . ?
C5 C3 P3 116.0(4) 1_545 . ?
C4 C2 P2 113.5(4) 1_655 . ?
C6B C5B C4B 120.6(6) . . ?
O32 N30 O33 122.5(5) . . ?
O32 N30 O31 116.4(4) . . ?
O33 N30 O31 121.1(5) . . ?
O32 N30 Dy1 58.5(3) . . ?
O33 N30 Dy1 175.0(4) . . ?
O31 N30 Dy1 58.1(3) . . ?
C6K C5K C4K 120.3(6) . . ?
C6K C1K C2K 119.2(5) . . ?
C6K C1K P6 118.2(4) . . ?
C2K C1K P6 122.6(4) . . ?
C5C C6C C1C 119.9(5) . . ?
C3I C2I C1I 119.5(6) . . ?
C2C C3C C4C 120.8(5) . . ?
C6D C5D C4D 119.4(6) . . ?
C6C C1C C2C 119.8(5) . . ?
C6C C1C P2 117.8(4) . . ?
C2C C1C P2 122.4(4) . . ?
C2H C1H C6H 118.8(5) . . ?
C2H C1H P4 117.9(4) . . ?
C6H C1H P4 123.3(5) . . ?
C2I C3I C4I 119.9(6) . . ?
C3E C2E C1E 118.6(6) . . ?
C6J C1J C2J 119.6(6) . . ?
C6J C1J P5 121.1(5) . . ?
C2J C1J P5 119.3(5) . . ?
C3 C5 P5 110.7(4) 1_565 . ?
C1A C6A C5A 119.1(7) . . ?
C4C C5C C6C 119.8(6) . . ?
C6I C5I C4I 119.4(6) . . ?
C5F C4F C3F 119.8(5) . . ?
C5I C6I C1I 120.1(6) . . ?
C1A C2A C3A 119.9(7) . . ?
C6E C1E C2E 120.9(5) . . ?
C6E C1E P3 116.4(4) . . ?
C2E C1E P3 122.6(4) . . ?
C1 C6 P6 110.1(4) . . ?
C3D C4D C5D 119.9(5) . . ?
C5A C4A C3A 121.2(7) . . ?
C2A C1A C6A 119.7(6) . . ?
C2A C1A P1 121.2(5) . . ?
C6A C1A P1 119.0(5) . . ?
C1E C6E C5E 120.5(6) . . ?
C3B C2B C1B 120.2(5) . . ?
C3H C2H C1H 120.1(5) . . ?
C4L C3L C2L 120.4(5) . . ?
C4A C3A C2A 118.9(7) . . ?
C2L C1L C6L 118.0(5) . . ?
C2L C1L P6 117.7(4) . . ?
C6L C1L P6 124.3(4) . . ?
C3K C4K C5K 120.1(6) . . ?
C5B C4B C3B 119.3(6) . . ?
C5L C4L C3L 119.5(5) . . ?
C6B C1B C2B 119.8(5) . . ?
C6B C1B P1 120.0(4) . . ?
C2B C1B P1 120.2(4) . . ?
C1L C6L C5L 120.8(5) . . ?
O23 N20 O22 123.2(5) . . ?
O23 N20 O21 121.0(5) . . ?
O22 N20 O21 115.8(4) . . ?
O23 N20 Dy1 176.6(4) . . ?
O22 N20 Dy1 57.8(2) . . ?
O21 N20 Dy1 58.0(2) . . ?
P3 O3 Dy1 165.9(2) . . ?
N60 O61 Dy2 97.2(3) . . ?
N50 O51 Dy2 96.6(3) . . ?
O43 N40 O42 119.9(5) . . ?
O43 N40 O41 123.5(5) . . ?
O42 N40 O41 116.6(4) . . ?
O43 N40 Dy2 175.5(4) . . ?
O42 N40 Dy2 57.0(2) . . ?
O41 N40 Dy2 59.7(3) . . ?
O63 N60 O61 122.4(5) . . ?
O63 N60 O62 122.1(5) . . ?
O61 N60 O62 115.3(4) . . ?
O63 N60 Dy2 174.4(4) . . ?
O61 N60 Dy2 57.2(3) . . ?
O62 N60 Dy2 58.2(3) . . ?
C6 C1 P1 113.3(4) . . ?
C3K C2K C1K 119.8(5) . . ?
C5K C6K C1K 120.0(5) . . ?
C1D C2D C3D 119.1(6) . . ?
C1G C2G C3G 120.5(6) . . ?
C2H C3H C4H 120.1(6) . . ?
C3C C4C C5C 120.4(5) . . ?
C3C C2C C1C 119.4(5) . . ?
C1L C2L C3L 120.9(5) . . ?
C4D C3D C2D 120.8(6) . . ?
C2F C3F C4F 120.3(5) . . ?
C2E C3E C4E 119.8(6) . . ?
C3J C2J C1J 119.3(7) . . ?
C1F C2F C3F 119.8(5) . . ?
C4F C5F C6F 120.5(5) . . ?
C4G C3G C2G 119.2(7) . . ?
C5G C4G C3G 120.1(6) . . ?
C4L C5L C6L 120.3(6) . . ?
C6H C5H C4H 120.1(6) . . ?
C5G C6G C1G 118.9(7) . . ?
C6G C5G C4G 121.2(6) . . ?
C5E C4E C3E 121.1(6) . . ?
C1J C6J C5J 119.8(7) . . ?
C3I C4I C5I 120.9(6) . . ?
C5H C4H C3H 119.9(6) . . ?
C4J C5J C6J 120.1(7) . . ?
C5J C4J C3J 120.5(7) . . ?
C4J C3J C2J 120.7(8) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O3 2.233(4) . ?
Dy1 O2 2.244(4) . ?
Dy1 O1 2.286(4) . ?
Dy1 O12 2.422(4) . ?
Dy1 O22 2.436(4) . ?
Dy1 O21 2.439(4) . ?
Dy1 O11 2.457(4) . ?
Dy1 O31 2.483(4) . ?
Dy1 O32 2.494(4) . ?
Dy1 N20 2.860(5) . ?
Dy1 N10 2.864(5) . ?
Dy1 N30 2.906(5) . ?
Dy2 O5 2.251(4) . ?
Dy2 O6 2.265(4) . ?
Dy2 O4 2.266(4) . ?
Dy2 O51 2.419(5) . ?
Dy2 O42 2.420(4) . ?
Dy2 O61 2.432(4) . ?
Dy2 O62 2.453(4) . ?
Dy2 O52 2.478(4) . ?
Dy2 O41 2.480(4) . ?
Dy2 N50 2.822(5) . ?
Dy2 N40 2.862(5) . ?
Dy2 N60 2.871(5) . ?
P2 O2 1.481(4) . ?
P2 C1C 1.774(5) . ?
P2 C1D 1.775(5) . ?
P2 C2 1.794(5) . ?
P3 O3 1.485(4) . ?
P3 C1E 1.777(6) . ?
P3 C3 1.784(5) . ?
P3 C1F 1.785(5) . ?
P5 O5 1.472(4) . ?
P5 C1I 1.780(6) . ?
P5 C5 1.788(6) . ?
P5 C1J 1.793(6) . ?
P4 O4 1.493(4) . ?
P4 C1G 1.766(6) . ?
P4 C1H 1.774(6) . ?
P4 C4 1.799(5) . ?
P1 O1 1.492(4) . ?
P1 C1B 1.770(5) . ?
P1 C1 1.787(5) . ?
P1 C1A 1.793(6) . ?
P6 O6 1.493(4) . ?
P6 C1K 1.772(5) . ?
P6 C1L 1.781(6) . ?
P6 C6 1.790(5) . ?
O21 N20 1.269(6) . ?
O63 N60 1.212(6) . ?
O13 N10 1.209(6) . ?
O41 N40 1.255(6) . ?
O22 N20 1.255(6) . ?
O42 N40 1.253(6) . ?
O43 N40 1.215(6) . ?
O23 N20 1.208(6) . ?
O32 N30 1.231(6) . ?
O12 N10 1.253(6) . ?
O11 N10 1.263(6) . ?
C4 C2 1.506(7) 1_455 ?
C1I C2I 1.378(8) . ?
C1I C6I 1.380(8) . ?
O62 N60 1.261(6) . ?
O52 N50 1.237(7) . ?
N50 O51 1.203(7) . ?
N50 O53 1.247(7) . ?
O31 N30 1.254(6) . ?
C1D C2D 1.371(7) . ?
C1D C6D 1.376(8) . ?
O33 N30 1.231(6) . ?
C3K C4K 1.364(9) . ?
C3K C2K 1.369(8) . ?
C6D C5D 1.354(8) . ?
C1F C2F 1.373(7) . ?
C1F C6F 1.388(7) . ?
C6H C5H 1.360(9) . ?
C6H C1H 1.393(8) . ?
C5A C4A 1.321(12) . ?
C5A C6A 1.392(9) . ?
C6F C5F 1.379(8) . ?
C3B C2B 1.363(8) . ?
C3B C4B 1.382(8) . ?
C5E C4E 1.352(10) . ?
C5E C6E 1.375(8) . ?
C1G C2G 1.373(8) . ?
C1G C6G 1.386(8) . ?
C6B C5B 1.362(9) . ?
C6B C1B 1.378(7) . ?
C3 C5 1.517(7) 1_545 ?
C2 C4 1.506(7) 1_655 ?
C5B C4B 1.381(9) . ?
C5K C6K 1.368(8) . ?
C5K C4K 1.380(9) . ?
C1K C6K 1.388(8) . ?
C1K C2K 1.395(7) . ?
C6C C5C 1.384(8) . ?
C6C C1C 1.386(7) . ?
C2I C3I 1.368(9) . ?
C3C C2C 1.371(8) . ?
C3C C4C 1.372(9) . ?
C5D C4D 1.381(9) . ?
C1C C2C 1.394(7) . ?
C1H C2H 1.380(8) . ?
C3I C4I 1.370(10) . ?
C2E C3E 1.375(9) . ?
C2E C1E 1.379(8) . ?
C1J C6J 1.374(8) . ?
C1J C2J 1.380(9) . ?
C5 C3 1.517(7) 1_565 ?
C6A C1A 1.373(9) . ?
C5C C4C 1.373(9) . ?
C5I C6I 1.363(9) . ?
C5I C4I 1.372(10) . ?
C4F C5F 1.366(8) . ?
C4F C3F 1.384(8) . ?
C2A C1A 1.370(9) . ?
C2A C3A 1.400(10) . ?
C1E C6E 1.374(8) . ?
C6 C1 1.503(7) . ?
C4D C3D 1.361(10) . ?
C4A C3A 1.368(12) . ?
C2B C1B 1.381(8) . ?
C2H C3H 1.376(8) . ?
C3L C4L 1.372(8) . ?
C3L C2L 1.380(8) . ?
C1L C2L 1.377(8) . ?
C1L C6L 1.383(8) . ?
C4L C5L 1.362(9) . ?
C6L C5L 1.388(9) . ?
O61 N60 1.250(6) . ?
C2D C3D 1.377(9) . ?
C2G C3G 1.377(8) . ?
C3H C4H 1.386(10) . ?
C3F C2F 1.377(8) . ?
C3E C4E 1.395(10) . ?
C2J C3J 1.376(9) . ?
C3G C4G 1.373(10) . ?
C4G C5G 1.368(11) . ?
C5H C4H 1.369(10) . ?
C6G C5G 1.365(10) . ?
C6J C5J 1.391(10) . ?
C5J C4J 1.343(12) . ?
C4J C3J 1.364(12) . ?
