#------------------------------------------------------------------------------
#$Date: 2016-03-23 00:01:45 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179089 $
#$URL: svn://www.crystallography.net/cod/cif/4/30/51/4305110.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4305110
loop_
_publ_author_name
'Adel Hamada'
'Pierre Braunstein'
_publ_contact_author_address
;
Institut Le Bel, rue Blaise Pascal, 67000 STRASBOURG, FRANCE
;
_publ_contact_author_email       braunst@chimie.u-strasbg.fr
_publ_contact_author_fax         0390241322
_publ_contact_author_name
;
Pierre Braunstein
;
_publ_contact_author_phone       0390241308
_publ_section_title
;
Lithium-Palladium Complex Supported by Phosphonatophosphine and Chloride
Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3934
_journal_page_last               3936
_journal_paper_doi               10.1021/ic800355m
_journal_volume                  47
_journal_year                    2008
_chemical_formula_moiety         'C34 H44 Cl5 Li O6 P4 Pd2, 3 (C H2 Cl2)'
_chemical_formula_sum            'C37 H50 Cl11 Li O6 P4 Pd2'
_chemical_formula_weight         1324.34
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             10-05-07
_audit_creation_method           SHELXL-97
_cell_angle_alpha                110.906(2)
_cell_angle_beta                 95.971(2)
_cell_angle_gamma                91.575(2)
_cell_formula_units_Z            2
_cell_length_a                   11.1497(5)
_cell_length_b                   15.5662(6)
_cell_length_c                   16.6267(8)
_cell_measurement_reflns_used    20449
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      0.998
_cell_volume                     2674.6(2)
_computing_cell_refinement       'Denzo (Nonius B.V., 1998)'
_computing_data_collection       'Collect (Nonius B.V., 1998)'
_computing_data_reduction        'Denzo (Nonius B.V., 1998)'
_computing_molecular_graphics    'PLATON 98 (Spek, 1998)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0468
_diffrn_reflns_av_sigmaI/netI    0.0759
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            25125
_diffrn_reflns_theta_full        27.45
_diffrn_reflns_theta_max         27.45
_diffrn_reflns_theta_min         1.32
_exptl_absorpt_coefficient_mu    1.381
_exptl_absorpt_correction_T_max  0.87673
_exptl_absorpt_correction_T_min  0.79111
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'MULscanABS in PLATON (Spek, 2003)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.644
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1324
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.059
_refine_diff_density_min         -1.005
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     554
_refine_ls_number_reflns         12149
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.031
_refine_ls_R_factor_all          0.0812
_refine_ls_R_factor_gt           0.0466
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0384P)²+1.4926P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0922
_refine_ls_wR_factor_ref         0.1036
_reflns_number_gt                8525
_reflns_number_total             12149
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            ic800355m-file003_2.cif
_cod_data_source_block           hamada8
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4305110
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.3785(3) 0.1960(3) -0.0985(3) 0.0238(9) Uani 1 1 d . . .
C2 C 0.3507(4) 0.1042(3) -0.1518(3) 0.0277(9) Uani 1 1 d . . .
H2 H 0.3944 0.0573 -0.1407 0.033 Uiso 1 1 calc R . .
C3 C 0.2600(4) 0.0809(3) -0.2208(3) 0.0352(10) Uani 1 1 d . . .
H3 H 0.2402 0.0181 -0.2564 0.042 Uiso 1 1 calc R . .
C4 C 0.1984(4) 0.1499(3) -0.2375(3) 0.0376(11) Uani 1 1 d . . .
H4 H 0.1357 0.1343 -0.2847 0.045 Uiso 1 1 calc R . .
C5 C 0.2271(4) 0.2405(3) -0.1863(3) 0.0379(11) Uani 1 1 d . . .
H5 H 0.1854 0.2874 -0.1991 0.045 Uiso 1 1 calc R . .
C6 C 0.3162(4) 0.2642(3) -0.1165(3) 0.0311(10) Uani 1 1 d . . .
H6 H 0.3348 0.3271 -0.0808 0.037 Uiso 1 1 calc R . .
C7 C 0.5728(3) 0.3311(2) 0.0078(3) 0.0225(8) Uani 1 1 d . . .
C8 C 0.6026(4) 0.3453(3) -0.0663(3) 0.0325(10) Uani 1 1 d . . .
H8 H 0.5711 0.3031 -0.1222 0.039 Uiso 1 1 calc R . .
C9 C 0.6775(4) 0.4205(3) -0.0583(3) 0.0407(12) Uani 1 1 d . . .
H9 H 0.6969 0.4302 -0.1088 0.049 Uiso 1 1 calc R . .
C10 C 0.7242(4) 0.4814(3) 0.0222(3) 0.0389(12) Uani 1 1 d . . .
H10 H 0.7763 0.5329 0.0272 0.047 Uiso 1 1 calc R . .
C11 C 0.6955(4) 0.4680(3) 0.0963(3) 0.0360(11) Uani 1 1 d . . .
H11 H 0.7278 0.5101 0.1520 0.043 Uiso 1 1 calc R . .
C12 C 0.6195(4) 0.3927(3) 0.0885(3) 0.0294(10) Uani 1 1 d . . .
H12 H 0.5995 0.3835 0.1392 0.035 Uiso 1 1 calc R . .
C13 C 0.5981(3) 0.1388(2) -0.0331(3) 0.0235(9) Uani 1 1 d . . .
H13A H 0.5629 0.0812 -0.0298 0.028 Uiso 1 1 calc R . .
H13B H 0.6083 0.1262 -0.0946 0.028 Uiso 1 1 calc R . .
C14 C 0.9298(4) 0.2687(3) 0.0223(3) 0.0365(11) Uani 1 1 d . . .
H14A H 0.9804 0.2304 0.0466 0.044 Uiso 1 1 calc R . .
H14B H 0.9199 0.3275 0.0697 0.044 Uiso 1 1 calc R . .
C15 C 0.9876(5) 0.2866(4) -0.0475(4) 0.0634(17) Uani 1 1 d . . .
H15A H 0.9928 0.2282 -0.0954 0.095 Uiso 1 1 calc R . .
H15B H 1.0690 0.3160 -0.0244 0.095 Uiso 1 1 calc R . .
H15C H 0.9390 0.3274 -0.0687 0.095 Uiso 1 1 calc R . .
C16 C 0.7862(4) 0.0035(3) 0.0417(3) 0.0396(12) Uani 1 1 d . . .
H16A H 0.6991 -0.0163 0.0320 0.048 Uiso 1 1 calc R . .
H16B H 0.8111 0.0318 0.1050 0.048 Uiso 1 1 calc R . .
C17 C 0.8580(4) -0.0777(3) 0.0029(4) 0.0497(14) Uani 1 1 d . . .
H17A H 0.8378 -0.1020 -0.0603 0.075 Uiso 1 1 calc R . .
H17B H 0.8389 -0.1256 0.0258 0.075 Uiso 1 1 calc R . .
H17C H 0.9445 -0.0586 0.0176 0.075 Uiso 1 1 calc R . .
C18 C 0.6137(3) 0.1363(3) 0.4584(3) 0.0241(9) Uani 1 1 d . . .
C19 C 0.5603(4) 0.0611(3) 0.3890(3) 0.0284(9) Uani 1 1 d . . .
H19 H 0.5118 0.0698 0.3425 0.034 Uiso 1 1 calc R . .
C20 C 0.5780(4) -0.0276(3) 0.3878(3) 0.0339(10) Uani 1 1 d . . .
H20 H 0.5411 -0.0795 0.3403 0.041 Uiso 1 1 calc R . .
C21 C 0.6487(4) -0.0404(3) 0.4550(3) 0.0350(11) Uani 1 1 d . . .
H21 H 0.6607 -0.1011 0.4538 0.042 Uiso 1 1 calc R . .
C22 C 0.7021(4) 0.0345(3) 0.5240(3) 0.0363(11) Uani 1 1 d . . .
H22 H 0.7509 0.0256 0.5704 0.044 Uiso 1 1 calc R . .
C23 C 0.6847(4) 0.1225(3) 0.5257(3) 0.0302(10) Uani 1 1 d . . .
H23 H 0.7216 0.1741 0.5734 0.036 Uiso 1 1 calc R . .
C24 C 0.5717(3) 0.3238(3) 0.5674(2) 0.0236(9) Uani 1 1 d . . .
C25 C 0.5141(4) 0.2878(3) 0.6189(3) 0.0306(10) Uani 1 1 d . . .
H25 H 0.4878 0.2242 0.5975 0.037 Uiso 1 1 calc R . .
C26 C 0.4940(4) 0.3442(3) 0.7026(3) 0.0396(11) Uani 1 1 d . . .
H26 H 0.4554 0.3188 0.7382 0.048 Uiso 1 1 calc R . .
C27 C 0.5305(4) 0.4364(3) 0.7330(3) 0.0396(11) Uani 1 1 d . . .
H27 H 0.5177 0.4749 0.7899 0.048 Uiso 1 1 calc R . .
C28 C 0.5855(4) 0.4731(3) 0.6811(3) 0.0397(11) Uani 1 1 d . . .
H28 H 0.6104 0.5369 0.7023 0.048 Uiso 1 1 calc R . .
C29 C 0.6048(4) 0.4180(3) 0.5988(3) 0.0312(10) Uani 1 1 d . . .
H29 H 0.6411 0.4444 0.5630 0.037 Uiso 1 1 calc R . .
C30 C 0.7547(3) 0.2929(3) 0.4571(3) 0.0265(9) Uani 1 1 d . . .
H30A H 0.7529 0.3542 0.4519 0.032 Uiso 1 1 calc R . .
H30B H 0.8021 0.3010 0.5134 0.032 Uiso 1 1 calc R . .
C31 C 1.0120(5) 0.1929(4) 0.4743(4) 0.0592(15) Uani 1 1 d . . .
H31A H 1.0818 0.2050 0.4467 0.071 Uiso 1 1 calc R . .
H31B H 0.9931 0.2521 0.5176 0.071 Uiso 1 1 calc R . .
C32 C 1.0432(6) 0.1294(5) 0.5173(5) 0.088(2) Uani 1 1 d . . .
H32A H 0.9761 0.1207 0.5480 0.132 Uiso 1 1 calc R . .
H32B H 1.1158 0.1543 0.5589 0.132 Uiso 1 1 calc R . .
H32C H 1.0587 0.0700 0.4742 0.132 Uiso 1 1 calc R . .
C33 C 0.9984(4) 0.2715(3) 0.2911(3) 0.0415(12) Uani 1 1 d . . .
H33A H 0.9610 0.2190 0.2398 0.050 Uiso 1 1 calc R . .
H33B H 1.0784 0.2549 0.3106 0.050 Uiso 1 1 calc R . .
C34 C 1.0117(5) 0.3559(3) 0.2690(3) 0.0501(13) Uani 1 1 d . . .
H34A H 0.9333 0.3675 0.2437 0.075 Uiso 1 1 calc R . .
H34B H 1.0702 0.3467 0.2271 0.075 Uiso 1 1 calc R . .
H34C H 1.0404 0.4087 0.3217 0.075 Uiso 1 1 calc R . .
C35 C 0.7450(5) 0.5780(4) 0.4161(3) 0.0515(13) Uani 1 1 d . . .
H35A H 0.7005 0.6310 0.4487 0.062 Uiso 1 1 calc R . .
H35B H 0.6852 0.5258 0.3835 0.062 Uiso 1 1 calc R . .
C36 C 1.1150(5) 0.5642(4) 0.2401(4) 0.0680(17) Uani 1 1 d . . .
H36A H 1.1930 0.5357 0.2299 0.082 Uiso 1 1 calc R . .
H36B H 1.0812 0.5464 0.2851 0.082 Uiso 1 1 calc R . .
C37 C 0.2101(5) 0.0098(4) 0.2220(4) 0.0657(16) Uani 1 1 d . . .
H37A H 0.2556 0.0678 0.2608 0.079 Uiso 1 1 calc R . .
H37B H 0.2172 0.0038 0.1614 0.079 Uiso 1 1 calc R . .
O1 O 0.7451(2) 0.20882(18) 0.12246(17) 0.0282(6) Uani 1 1 d . . .
O2 O 0.8113(2) 0.22004(18) -0.01686(18) 0.0286(6) Uani 1 1 d . . .
O3 O 0.8080(2) 0.07054(18) 0.00053(18) 0.0294(7) Uani 1 1 d . . .
O4 O 0.7547(2) 0.16003(17) 0.29298(17) 0.0268(6) Uani 1 1 d . . .
O5 O 0.9085(2) 0.1554(2) 0.40893(19) 0.0332(7) Uani 1 1 d . . .
O6 O 0.9210(3) 0.29280(19) 0.36092(19) 0.0347(7) Uani 1 1 d . . .
P1 P 0.48795(9) 0.22664(7) -0.00138(7) 0.0211(2) Uani 1 1 d . . .
P2 P 0.74429(9) 0.16402(7) 0.02779(7) 0.0235(2) Uani 1 1 d . . .
P3 P 0.59963(9) 0.25238(7) 0.45909(7) 0.0217(2) Uani 1 1 d . . .
P4 P 0.83281(9) 0.21904(7) 0.37155(7) 0.0251(2) Uani 1 1 d . . .
Cl1 Cl 0.30827(9) 0.35923(7) 0.09963(7) 0.0313(2) Uani 1 1 d . . .
Cl2 Cl 0.48375(9) 0.10588(6) 0.13051(7) 0.0270(2) Uani 1 1 d . . .
Cl3 Cl 0.30543(9) 0.26039(7) 0.24542(7) 0.0291(2) Uani 1 1 d . . .
Cl4 Cl 0.32590(9) 0.20147(7) 0.41968(7) 0.0303(2) Uani 1 1 d . . .
Cl5 Cl 0.59746(9) 0.33963(6) 0.30463(7) 0.0266(2) Uani 1 1 d . . .
Cl6 Cl 0.84246(16) 0.54722(11) 0.48884(12) 0.0869(6) Uani 1 1 d . . .
Cl7 Cl 0.82454(15) 0.60788(14) 0.34279(11) 0.0872(5) Uani 1 1 d . . .
Cl8 Cl 1.01773(14) 0.52315(10) 0.14628(11) 0.0706(4) Uani 1 1 d . . .
Cl9 Cl 1.1401(2) 0.68339(13) 0.27740(13) 0.1100(7) Uani 1 1 d . . .
Cl10 Cl 0.05950(16) 0.01539(14) 0.23878(17) 0.1103(7) Uani 1 1 d . . .
Cl11 Cl 0.27424(16) -0.08367(13) 0.24158(10) 0.0831(5) Uani 1 1 d . . .
Pd1 Pd 0.40242(3) 0.237279(19) 0.117087(19) 0.02081(8) Uani 1 1 d . . .
Pd2 Pd 0.46216(3) 0.26284(2) 0.356844(19) 0.02137(8) Uani 1 1 d . . .
Li1 Li 0.6638(7) 0.1974(4) 0.2110(4) 0.0291(16) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 C1 C2 119.3(4) . . ?
C6 C1 P1 119.8(3) . . ?
C2 C1 P1 120.7(3) . . ?
C3 C2 C1 120.4(4) . . ?
C3 C2 H2 119.8 . . ?
C1 C2 H2 119.8 . . ?
C2 C3 C4 119.4(4) . . ?
C2 C3 H3 120.3 . . ?
C4 C3 H3 120.3 . . ?
C5 C4 C3 120.4(4) . . ?
C5 C4 H4 119.8 . . ?
C3 C4 H4 119.8 . . ?
C4 C5 C6 120.5(4) . . ?
C4 C5 H5 119.7 . . ?
C6 C5 H5 119.7 . . ?
C5 C6 C1 119.9(4) . . ?
C5 C6 H6 120.1 . . ?
C1 C6 H6 120.1 . . ?
C12 C7 C8 119.3(3) . . ?
C12 C7 P1 119.8(3) . . ?
C8 C7 P1 120.5(3) . . ?
C9 C8 C7 120.0(4) . . ?
C9 C8 H8 120.0 . . ?
C7 C8 H8 120.0 . . ?
C10 C9 C8 120.4(4) . . ?
C10 C9 H9 119.8 . . ?
C8 C9 H9 119.8 . . ?
C9 C10 C11 120.1(4) . . ?
C9 C10 H10 120.0 . . ?
C11 C10 H10 120.0 . . ?
C12 C11 C10 119.7(4) . . ?
C12 C11 H11 120.2 . . ?
C10 C11 H11 120.2 . . ?
C7 C12 C11 120.4(4) . . ?
C7 C12 H12 119.8 . . ?
C11 C12 H12 119.8 . . ?
P2 C13 P1 117.4(2) . . ?
P2 C13 H13A 107.9 . . ?
P1 C13 H13A 107.9 . . ?
P2 C13 H13B 107.9 . . ?
P1 C13 H13B 107.9 . . ?
H13A C13 H13B 107.2 . . ?
O2 C14 C15 107.2(4) . . ?
O2 C14 H14A 110.3 . . ?
C15 C14 H14A 110.3 . . ?
O2 C14 H14B 110.3 . . ?
C15 C14 H14B 110.3 . . ?
H14A C14 H14B 108.5 . . ?
C14 C15 H15A 109.5 . . ?
C14 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C14 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
O3 C16 C17 108.4(3) . . ?
O3 C16 H16A 110.0 . . ?
C17 C16 H16A 110.0 . . ?
O3 C16 H16B 110.0 . . ?
C17 C16 H16B 110.0 . . ?
H16A C16 H16B 108.4 . . ?
C16 C17 H17A 109.5 . . ?
C16 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C16 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C19 C18 C23 119.6(4) . . ?
C19 C18 P3 120.7(3) . . ?
C23 C18 P3 119.6(3) . . ?
C18 C19 C20 119.6(4) . . ?
C18 C19 H19 120.2 . . ?
C20 C19 H19 120.2 . . ?
C21 C20 C19 120.3(4) . . ?
C21 C20 H20 119.9 . . ?
C19 C20 H20 119.9 . . ?
C20 C21 C22 120.1(4) . . ?
C20 C21 H21 120.0 . . ?
C22 C21 H21 120.0 . . ?
C21 C22 C23 119.9(4) . . ?
C21 C22 H22 120.0 . . ?
C23 C22 H22 120.0 . . ?
C22 C23 C18 120.5(4) . . ?
C22 C23 H23 119.7 . . ?
C18 C23 H23 119.7 . . ?
C25 C24 C29 118.7(4) . . ?
C25 C24 P3 121.4(3) . . ?
C29 C24 P3 119.8(3) . . ?
C24 C25 C26 120.4(4) . . ?
C24 C25 H25 119.8 . . ?
C26 C25 H25 119.8 . . ?
C27 C26 C25 119.7(4) . . ?
C27 C26 H26 120.1 . . ?
C25 C26 H26 120.1 . . ?
C28 C27 C26 120.0(4) . . ?
C28 C27 H27 120.0 . . ?
C26 C27 H27 120.0 . . ?
C27 C28 C29 120.5(4) . . ?
C27 C28 H28 119.8 . . ?
C29 C28 H28 119.8 . . ?
C28 C29 C24 120.6(4) . . ?
C28 C29 H29 119.7 . . ?
C24 C29 H29 119.7 . . ?
P4 C30 P3 115.7(2) . . ?
P4 C30 H30A 108.4 . . ?
P3 C30 H30A 108.4 . . ?
P4 C30 H30B 108.4 . . ?
P3 C30 H30B 108.4 . . ?
H30A C30 H30B 107.4 . . ?
C32 C31 O5 110.6(5) . . ?
C32 C31 H31A 109.5 . . ?
O5 C31 H31A 109.5 . . ?
C32 C31 H31B 109.5 . . ?
O5 C31 H31B 109.5 . . ?
H31A C31 H31B 108.1 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C31 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
O6 C33 C34 107.0(4) . . ?
O6 C33 H33A 110.3 . . ?
C34 C33 H33A 110.3 . . ?
O6 C33 H33B 110.3 . . ?
C34 C33 H33B 110.3 . . ?
H33A C33 H33B 108.6 . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
Cl6 C35 Cl7 111.4(3) . . ?
Cl6 C35 H35A 109.3 . . ?
Cl7 C35 H35A 109.3 . . ?
Cl6 C35 H35B 109.4 . . ?
Cl7 C35 H35B 109.3 . . ?
H35A C35 H35B 108.0 . . ?
Cl8 C36 Cl9 111.9(3) . . ?
Cl8 C36 H36A 109.2 . . ?
Cl9 C36 H36A 109.2 . . ?
Cl8 C36 H36B 109.2 . . ?
Cl9 C36 H36B 109.2 . . ?
H36A C36 H36B 107.9 . . ?
Cl10 C37 Cl11 111.9(3) . . ?
Cl10 C37 H37A 109.2 . . ?
Cl11 C37 H37A 109.2 . . ?
Cl10 C37 H37B 109.2 . . ?
Cl11 C37 H37B 109.2 . . ?
H37A C37 H37B 107.9 . . ?
P2 O1 Li1 139.2(3) . . ?
C14 O2 P2 120.8(2) . . ?
C16 O3 P2 120.5(2) . . ?
P4 O4 Li1 127.3(3) . . ?
C31 O5 P4 121.1(3) . . ?
C33 O6 P4 122.9(3) . . ?
C7 P1 C1 107.07(17) . . ?
C7 P1 C13 103.02(17) . . ?
C1 P1 C13 103.16(18) . . ?
C7 P1 Pd1 113.74(13) . . ?
C1 P1 Pd1 112.84(12) . . ?
C13 P1 Pd1 115.90(12) . . ?
O1 P2 O2 115.74(16) . . ?
O1 P2 O3 113.34(16) . . ?
O2 P2 O3 102.83(14) . . ?
O1 P2 C13 115.00(17) . . ?
O2 P2 C13 102.49(16) . . ?
O3 P2 C13 106.05(17) . . ?
C24 P3 C18 107.04(17) . . ?
C24 P3 C30 101.52(19) . . ?
C18 P3 C30 103.95(17) . . ?
C24 P3 Pd2 112.68(13) . . ?
C18 P3 Pd2 114.34(14) . . ?
C30 P3 Pd2 116.05(13) . . ?
O4 P4 O6 116.69(16) . . ?
O4 P4 O5 108.33(16) . . ?
O6 P4 O5 108.68(16) . . ?
O4 P4 C30 115.36(18) . . ?
O6 P4 C30 99.46(17) . . ?
O5 P4 C30 107.74(17) . . ?
O6 P4 Li1 94.73(17) . . ?
O5 P4 Li1 137.36(18) . . ?
C30 P4 Li1 102.67(19) . . ?
Pd1 Cl2 Li1 89.72(16) . . ?
Pd2 Cl3 Pd1 106.21(4) . . ?
Pd2 Cl5 Li1 91.84(16) . . ?
P1 Pd1 Cl1 86.26(4) . . ?
P1 Pd1 Cl2 94.84(4) . . ?
Cl1 Pd1 Cl2 175.41(4) . . ?
P1 Pd1 Cl3 175.54(4) . . ?
Cl1 Pd1 Cl3 89.40(3) . . ?
Cl2 Pd1 Cl3 89.57(3) . . ?
P1 Pd1 Li1 90.50(11) . . ?
Cl1 Pd1 Li1 138.53(12) . . ?
Cl2 Pd1 Li1 45.99(11) . . ?
Cl3 Pd1 Li1 92.07(11) . . ?
P3 Pd2 Cl4 85.74(4) . . ?
P3 Pd2 Cl5 93.41(4) . . ?
Cl4 Pd2 Cl5 173.98(4) . . ?
P3 Pd2 Cl3 174.63(4) . . ?
Cl4 Pd2 Cl3 90.12(3) . . ?
Cl5 Pd2 Cl3 91.06(3) . . ?
P3 Pd2 Li1 89.94(12) . . ?
Cl4 Pd2 Li1 140.87(11) . . ?
Cl5 Pd2 Li1 45.01(11) . . ?
Cl3 Pd2 Li1 91.11(12) . . ?
O1 Li1 O4 116.2(4) . . ?
O1 Li1 Cl5 114.0(3) . . ?
O4 Li1 Cl5 100.2(3) . . ?
O1 Li1 Cl2 101.6(3) . . ?
O4 Li1 Cl2 118.9(3) . . ?
Cl5 Li1 Cl2 106.0(3) . . ?
O1 Li1 P4 112.4(3) . . ?
O4 Li1 P4 22.90(13) . . ?
Cl5 Li1 P4 81.99(19) . . ?
Cl2 Li1 P4 138.3(2) . . ?
O1 Li1 Pd1 91.0(2) . . ?
O4 Li1 Pd1 152.2(3) . . ?
Cl5 Li1 Pd1 71.57(17) . . ?
Cl2 Li1 Pd1 44.29(12) . . ?
P4 Li1 Pd1 150.3(2) . . ?
O1 Li1 Pd2 153.1(3) . . ?
O4 Li1 Pd2 86.0(2) . . ?
Cl5 Li1 Pd2 43.15(11) . . ?
Cl2 Li1 Pd2 77.95(19) . . ?
P4 Li1 Pd2 81.90(15) . . ?
Pd1 Li1 Pd2 69.73(14) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C6 1.387(5) . ?
C1 C2 1.392(5) . ?
C1 P1 1.826(4) . ?
C2 C3 1.383(6) . ?
C2 H2 0.9500 . ?
C3 C4 1.384(6) . ?
C3 H3 0.9500 . ?
C4 C5 1.371(6) . ?
C4 H4 0.9500 . ?
C5 C6 1.380(6) . ?
C5 H5 0.9500 . ?
C6 H6 0.9500 . ?
C7 C12 1.379(6) . ?
C7 C8 1.398(5) . ?
C7 P1 1.808(4) . ?
C8 C9 1.378(6) . ?
C8 H8 0.9500 . ?
C9 C10 1.373(7) . ?
C9 H9 0.9500 . ?
C10 C11 1.388(6) . ?
C10 H10 0.9500 . ?
C11 C12 1.387(5) . ?
C11 H11 0.9500 . ?
C12 H12 0.9500 . ?
C13 P2 1.782(4) . ?
C13 P1 1.836(4) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C14 O2 1.468(5) . ?
C14 C15 1.489(6) . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 O3 1.466(4) . ?
C16 C17 1.496(6) . ?
C16 H16A 0.9900 . ?
C16 H16B 0.9900 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 C19 1.382(6) . ?
C18 C23 1.386(5) . ?
C18 P3 1.815(4) . ?
C19 C20 1.393(5) . ?
C19 H19 0.9500 . ?
C20 C21 1.377(6) . ?
C20 H20 0.9500 . ?
C21 C22 1.378(6) . ?
C21 H21 0.9500 . ?
C22 C23 1.379(5) . ?
C22 H22 0.9500 . ?
C23 H23 0.9500 . ?
C24 C25 1.378(5) . ?
C24 C29 1.394(5) . ?
C24 P3 1.812(4) . ?
C25 C26 1.399(6) . ?
C25 H25 0.9500 . ?
C26 C27 1.375(6) . ?
C26 H26 0.9500 . ?
C27 C28 1.373(6) . ?
C27 H27 0.9500 . ?
C28 C29 1.374(6) . ?
C28 H28 0.9500 . ?
C29 H29 0.9500 . ?
C30 P4 1.802(4) . ?
C30 P3 1.832(4) . ?
C30 H30A 0.9900 . ?
C30 H30B 0.9900 . ?
C31 C32 1.441(7) . ?
C31 O5 1.451(6) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?
C33 O6 1.467(5) . ?
C33 C34 1.493(6) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 Cl6 1.744(5) . ?
C35 Cl7 1.759(5) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 Cl8 1.708(6) . ?
C36 Cl9 1.737(6) . ?
C36 H36A 0.9900 . ?
C36 H36B 0.9900 . ?
C37 Cl10 1.731(6) . ?
C37 Cl11 1.755(6) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
O1 P2 1.476(3) . ?
O1 Li1 1.864(7) . ?
O2 P2 1.553(3) . ?
O3 P2 1.575(3) . ?
O4 P4 1.474(3) . ?
O4 Li1 1.880(7) . ?
O5 P4 1.567(3) . ?
O6 P4 1.560(3) . ?
P1 Pd1 2.2323(10) . ?
P3 Pd2 2.2214(10) . ?
P4 Li1 3.011(7) . ?
Cl1 Pd1 2.2868(9) . ?
Cl2 Pd1 2.3327(9) . ?
Cl2 Li1 2.403(7) . ?
Cl3 Pd2 2.3999(10) . ?
Cl3 Pd1 2.4095(10) . ?
Cl4 Pd2 2.2967(9) . ?
Cl5 Pd2 2.3178(9) . ?
Cl5 Li1 2.397(7) . ?
Pd1 Li1 3.341(7) . ?
Pd2 Li1 3.387(7) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6 C1 C2 C3 -1.5(6) . . . . ?
P1 C1 C2 C3 174.2(3) . . . . ?
C1 C2 C3 C4 1.2(6) . . . . ?
C2 C3 C4 C5 0.2(6) . . . . ?
C3 C4 C5 C6 -1.3(7) . . . . ?
C4 C5 C6 C1 1.0(6) . . . . ?
C2 C1 C6 C5 0.5(6) . . . . ?
P1 C1 C6 C5 -175.3(3) . . . . ?
C12 C7 C8 C9 -0.2(6) . . . . ?
P1 C7 C8 C9 -173.4(3) . . . . ?
C7 C8 C9 C10 0.6(7) . . . . ?
C8 C9 C10 C11 -0.5(7) . . . . ?
C9 C10 C11 C12 0.0(7) . . . . ?
C8 C7 C12 C11 -0.2(6) . . . . ?
P1 C7 C12 C11 173.1(3) . . . . ?
C10 C11 C12 C7 0.3(6) . . . . ?
C23 C18 C19 C20 0.3(6) . . . . ?
P3 C18 C19 C20 176.4(3) . . . . ?
C18 C19 C20 C21 -0.3(6) . . . . ?
C19 C20 C21 C22 0.2(6) . . . . ?
C20 C21 C22 C23 0.0(7) . . . . ?
C21 C22 C23 C18 0.0(6) . . . . ?
C19 C18 C23 C22 -0.1(6) . . . . ?
P3 C18 C23 C22 -176.3(3) . . . . ?
C29 C24 C25 C26 -2.7(6) . . . . ?
P3 C24 C25 C26 179.6(3) . . . . ?
C24 C25 C26 C27 1.0(6) . . . . ?
C25 C26 C27 C28 0.5(7) . . . . ?
C26 C27 C28 C29 -0.2(7) . . . . ?
C27 C28 C29 C24 -1.6(7) . . . . ?
C25 C24 C29 C28 3.0(6) . . . . ?
P3 C24 C29 C28 -179.3(3) . . . . ?
C15 C14 O2 P2 160.6(3) . . . . ?
C17 C16 O3 P2 179.9(3) . . . . ?
C32 C31 O5 P4 162.2(4) . . . . ?
C34 C33 O6 P4 147.8(3) . . . . ?
C12 C7 P1 C1 150.3(3) . . . . ?
C8 C7 P1 C1 -36.5(4) . . . . ?
C12 C7 P1 C13 -101.3(3) . . . . ?
C8 C7 P1 C13 71.9(3) . . . . ?
C12 C7 P1 Pd1 25.0(4) . . . . ?
C8 C7 P1 Pd1 -161.8(3) . . . . ?
C6 C1 P1 C7 -41.9(3) . . . . ?
C2 C1 P1 C7 142.4(3) . . . . ?
C6 C1 P1 C13 -150.2(3) . . . . ?
C2 C1 P1 C13 34.1(3) . . . . ?
C6 C1 P1 Pd1 84.0(3) . . . . ?
C2 C1 P1 Pd1 -91.7(3) . . . . ?
P2 C13 P1 C7 48.3(2) . . . . ?
P2 C13 P1 C1 159.6(2) . . . . ?
P2 C13 P1 Pd1 -76.5(2) . . . . ?
Li1 O1 P2 O2 164.0(4) . . . . ?
Li1 O1 P2 O3 -77.5(4) . . . . ?
Li1 O1 P2 C13 44.7(4) . . . . ?
C14 O2 P2 O1 43.5(3) . . . . ?
C14 O2 P2 O3 -80.6(3) . . . . ?
C14 O2 P2 C13 169.5(3) . . . . ?
C16 O3 P2 O1 43.4(4) . . . . ?
C16 O3 P2 O2 169.1(3) . . . . ?
C16 O3 P2 C13 -83.7(3) . . . . ?
P1 C13 P2 O1 41.8(3) . . . . ?
P1 C13 P2 O2 -84.6(2) . . . . ?
P1 C13 P2 O3 167.88(18) . . . . ?
C25 C24 P3 C18 -28.5(4) . . . . ?
C29 C24 P3 C18 153.8(3) . . . . ?
C25 C24 P3 C30 -137.2(3) . . . . ?
C29 C24 P3 C30 45.2(4) . . . . ?
C25 C24 P3 Pd2 98.0(3) . . . . ?
C29 C24 P3 Pd2 -79.6(3) . . . . ?
C19 C18 P3 C24 137.9(3) . . . . ?
C23 C18 P3 C24 -46.0(4) . . . . ?
C19 C18 P3 C30 -115.2(3) . . . . ?
C23 C18 P3 C30 60.9(3) . . . . ?
C19 C18 P3 Pd2 12.3(4) . . . . ?
C23 C18 P3 Pd2 -171.6(3) . . . . ?
P4 C30 P3 C24 164.0(2) . . . . ?
P4 C30 P3 C18 52.9(3) . . . . ?
P4 C30 P3 Pd2 -73.5(2) . . . . ?
Li1 O4 P4 O6 -46.1(4) . . . . ?
Li1 O4 P4 O5 -169.1(3) . . . . ?
Li1 O4 P4 C30 70.1(4) . . . . ?
C33 O6 P4 O4 -47.9(4) . . . . ?
C33 O6 P4 O5 74.9(3) . . . . ?
C33 O6 P4 C30 -172.6(3) . . . . ?
C33 O6 P4 Li1 -68.9(3) . . . . ?
C31 O5 P4 O4 166.2(3) . . . . ?
C31 O5 P4 O6 38.5(4) . . . . ?
C31 O5 P4 C30 -68.3(4) . . . . ?
C31 O5 P4 Li1 158.3(3) . . . . ?
P3 C30 P4 O4 26.3(3) . . . . ?
P3 C30 P4 O6 152.0(2) . . . . ?
P3 C30 P4 O5 -94.8(2) . . . . ?
P3 C30 P4 Li1 54.9(2) . . . . ?
C7 P1 Pd1 Cl1 57.18(14) . . . . ?
C1 P1 Pd1 Cl1 -65.05(14) . . . . ?
C13 P1 Pd1 Cl1 176.33(15) . . . . ?
C7 P1 Pd1 Cl2 -127.29(14) . . . . ?
C1 P1 Pd1 Cl2 110.48(13) . . . . ?
C13 P1 Pd1 Cl2 -8.14(15) . . . . ?
C7 P1 Pd1 Li1 -81.45(18) . . . . ?
C1 P1 Pd1 Li1 156.33(17) . . . . ?
C13 P1 Pd1 Li1 37.71(18) . . . . ?
Li1 Cl2 Pd1 P1 86.00(16) . . . . ?
Li1 Cl2 Pd1 Cl3 -93.30(16) . . . . ?
Pd2 Cl3 Pd1 Cl1 -130.21(4) . . . . ?
Pd2 Cl3 Pd1 Cl2 54.27(4) . . . . ?
Pd2 Cl3 Pd1 Li1 8.33(12) . . . . ?
C24 P3 Pd2 Cl4 -63.15(14) . . . . ?
C18 P3 Pd2 Cl4 59.37(13) . . . . ?
C30 P3 Pd2 Cl4 -179.58(15) . . . . ?
C24 P3 Pd2 Cl5 110.88(14) . . . . ?
C18 P3 Pd2 Cl5 -126.60(13) . . . . ?
C30 P3 Pd2 Cl5 -5.56(15) . . . . ?
C24 P3 Pd2 Li1 155.78(17) . . . . ?
C18 P3 Pd2 Li1 -81.70(17) . . . . ?
C30 P3 Pd2 Li1 39.34(18) . . . . ?
Li1 Cl5 Pd2 P3 86.50(17) . . . . ?
Li1 Cl5 Pd2 Cl3 -90.51(17) . . . . ?
Pd1 Cl3 Pd2 Cl4 -149.10(4) . . . . ?
Pd1 Cl3 Pd2 Cl5 36.80(4) . . . . ?
Pd1 Cl3 Pd2 Li1 -8.22(11) . . . . ?
P2 O1 Li1 O4 112.5(4) . . . . ?
P2 O1 Li1 Cl5 -131.6(3) . . . . ?
P2 O1 Li1 Cl2 -18.1(5) . . . . ?
P2 O1 Li1 P4 137.3(3) . . . . ?
P2 O1 Li1 Pd1 -61.4(4) . . . . ?
P2 O1 Li1 Pd2 -104.3(7) . . . . ?
P4 O4 Li1 O1 85.6(4) . . . . ?
P4 O4 Li1 Cl5 -37.7(4) . . . . ?
P4 O4 Li1 Cl2 -152.5(2) . . . . ?
P4 O4 Li1 Pd1 -107.5(6) . . . . ?
P4 O4 Li1 Pd2 -78.6(3) . . . . ?
Pd2 Cl5 Li1 O1 162.4(3) . . . . ?
Pd2 Cl5 Li1 O4 -72.8(3) . . . . ?
Pd2 Cl5 Li1 Cl2 51.42(19) . . . . ?
Pd2 Cl5 Li1 P4 -86.67(11) . . . . ?
Pd2 Cl5 Li1 Pd1 79.72(7) . . . . ?
Pd1 Cl2 Li1 O1 -79.3(2) . . . . ?
Pd1 Cl2 Li1 O4 151.8(3) . . . . ?
Pd1 Cl2 Li1 Cl5 40.10(19) . . . . ?
Pd1 Cl2 Li1 P4 136.1(4) . . . . ?
Pd1 Cl2 Li1 Pd2 73.24(8) . . . . ?
O4 P4 Li1 O1 -104.7(5) . . . . ?
O6 P4 Li1 O1 35.1(3) . . . . ?
O5 P4 Li1 O1 -89.3(3) . . . . ?
C30 P4 Li1 O1 135.9(3) . . . . ?
O6 P4 Li1 O4 139.8(3) . . . . ?
O5 P4 Li1 O4 15.4(4) . . . . ?
C30 P4 Li1 O4 -119.4(3) . . . . ?
O4 P4 Li1 Cl5 142.6(4) . . . . ?
O6 P4 Li1 Cl5 -77.65(18) . . . . ?
O5 P4 Li1 Cl5 158.00(17) . . . . ?
C30 P4 Li1 Cl5 23.2(2) . . . . ?
O4 P4 Li1 Cl2 37.5(3) . . . . ?
O6 P4 Li1 Cl2 177.2(4) . . . . ?
O5 P4 Li1 Cl2 52.9(5) . . . . ?
C30 P4 Li1 Cl2 -81.9(4) . . . . ?
O4 P4 Li1 Pd1 115.8(6) . . . . ?
O6 P4 Li1 Pd1 -104.5(4) . . . . ?
O5 P4 Li1 Pd1 131.2(4) . . . . ?
C30 P4 Li1 Pd1 -3.7(5) . . . . ?
O4 P4 Li1 Pd2 99.0(3) . . . . ?
O6 P4 Li1 Pd2 -121.25(14) . . . . ?
O5 P4 Li1 Pd2 114.4(2) . . . . ?
C30 P4 Li1 Pd2 -20.44(17) . . . . ?
P1 Pd1 Li1 O1 9.5(2) . . . . ?
Cl1 Pd1 Li1 O1 -75.4(3) . . . . ?
Cl2 Pd1 Li1 O1 105.7(3) . . . . ?
Cl3 Pd1 Li1 O1 -166.9(2) . . . . ?
P1 Pd1 Li1 O4 -158.8(7) . . . . ?
Cl1 Pd1 Li1 O4 116.3(6) . . . . ?
Cl2 Pd1 Li1 O4 -62.6(6) . . . . ?
Cl3 Pd1 Li1 O4 24.8(7) . . . . ?
P1 Pd1 Li1 Cl5 124.48(12) . . . . ?
Cl1 Pd1 Li1 Cl5 39.6(2) . . . . ?
Cl2 Pd1 Li1 Cl5 -139.3(2) . . . . ?
Cl3 Pd1 Li1 Cl5 -51.87(13) . . . . ?
P1 Pd1 Li1 Cl2 -96.25(12) . . . . ?
Cl1 Pd1 Li1 Cl2 178.83(6) . . . . ?
Cl3 Pd1 Li1 Cl2 87.40(12) . . . . ?
P1 Pd1 Li1 P4 152.6(4) . . . . ?
Cl1 Pd1 Li1 P4 67.7(5) . . . . ?
Cl2 Pd1 Li1 P4 -111.2(5) . . . . ?
Cl3 Pd1 Li1 P4 -23.8(4) . . . . ?
P1 Pd1 Li1 Pd2 170.32(8) . . . . ?
Cl1 Pd1 Li1 Pd2 85.40(15) . . . . ?
Cl2 Pd1 Li1 Pd2 -93.43(13) . . . . ?
Cl3 Pd1 Li1 Pd2 -6.03(8) . . . . ?
P3 Pd2 Li1 O1 -132.7(7) . . . . ?
Cl4 Pd2 Li1 O1 144.2(6) . . . . ?
Cl5 Pd2 Li1 O1 -37.8(7) . . . . ?
Cl3 Pd2 Li1 O1 52.6(7) . . . . ?
P3 Pd2 Li1 O4 14.7(2) . . . . ?
Cl4 Pd2 Li1 O4 -68.5(3) . . . . ?
Cl5 Pd2 Li1 O4 109.6(3) . . . . ?
Cl3 Pd2 Li1 O4 -160.0(2) . . . . ?
P3 Pd2 Li1 Cl5 -94.88(12) . . . . ?
Cl4 Pd2 Li1 Cl5 -178.05(6) . . . . ?
Cl3 Pd2 Li1 Cl5 90.39(12) . . . . ?
P3 Pd2 Li1 Cl2 135.33(13) . . . . ?
Cl4 Pd2 Li1 Cl2 52.2(2) . . . . ?
Cl5 Pd2 Li1 Cl2 -129.8(2) . . . . ?
Cl3 Pd2 Li1 Cl2 -39.40(13) . . . . ?
P3 Pd2 Li1 P4 -7.97(11) . . . . ?
Cl4 Pd2 Li1 P4 -91.14(19) . . . . ?
Cl5 Pd2 Li1 P4 86.91(17) . . . . ?
Cl3 Pd2 Li1 P4 177.30(11) . . . . ?
P3 Pd2 Li1 Pd1 -179.22(8) . . . . ?
Cl4 Pd2 Li1 Pd1 97.62(15) . . . . ?
Cl5 Pd2 Li1 Pd1 -84.33(13) . . . . ?
Cl3 Pd2 Li1 Pd1 6.06(8) . . . . ?
