#------------------------------------------------------------------------------
#$Date: 2016-03-23 02:32:26 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179185 $
#$URL: svn://www.crystallography.net/cod/cif/4/31/31/4313130.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4313130
loop_
_publ_author_name
'Richard D. Adams'
'Burjor Captain'
'Wei Fu'
_publ_section_title
;
 Germanium-Rich Pentaruthenium Carbonyl Clusters Including
 Ru5(CO)11(μ-GePh2)4(μ5-C) and Its Reactions with Hydrogen
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1328
_journal_page_last               1333
_journal_paper_doi               10.1021/ic020655w
_journal_volume                  42
_journal_year                    2003
_chemical_formula_sum            'C49 H30 Ge3 O12 Ru5'
_chemical_formula_weight         1533.85
_chemical_name_systematic
;
  ?
;
_space_group_IT_number           36
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.5433(9)
_cell_length_b                   13.8799(6)
_cell_length_c                   18.5911(8)
_cell_measurement_reflns_used    4989
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.03
_cell_measurement_theta_min      2.82
_cell_volume                     5301.0(4)
_computing_cell_refinement       'SAINT+ NT V6.02a (Bruker, 1998)'
_computing_data_collection       'SMART NT V5.619 (Bruker, 2000)'
_computing_data_reduction        'SAINT+ NT V6.02a'
_computing_molecular_graphics    'SHELXTL V5.1 (Sheldrick, 1997)'
_computing_publication_material  'SHELXTL V5.1'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker SMART APEX CCD diffractometer'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0390
_diffrn_reflns_av_sigmaI/netI    0.0489
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            20262
_diffrn_reflns_theta_full        28.29
_diffrn_reflns_theta_max         28.29
_diffrn_reflns_theta_min         1.77
_diffrn_standards_decay_%        <1
_exptl_absorpt_coefficient_mu    3.117
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.737
_exptl_absorpt_correction_type   SADABS
_exptl_absorpt_process_details   '(SADABS, Bruker, 1997)'
_exptl_crystal_colour            Red
_exptl_crystal_density_diffrn    1.922
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Plate
_exptl_crystal_F_000             2944
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.774
_refine_diff_density_min         -0.417
_refine_diff_density_rms         0.084
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.010(11)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.028
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     334
_refine_ls_number_reflns         6016
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.028
_refine_ls_R_factor_all          0.0394
_refine_ls_R_factor_gt           0.0319
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0222P)²+0.7366P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0649
_refine_ls_wR_factor_ref         0.0683
_reflns_number_gt                5301
_reflns_number_total             6016
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic020655w_1.cif
_cod_data_source_block           cmc21
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to the built-in table from CIF Core
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_database_code               4313130
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x, -y, z+1/2'
'-x, y, z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.5000 0.08521(3) -0.03278(3) 0.04310(13) Uani 1 2 d S . .
Ru2 Ru 0.569830(15) 0.23880(2) 0.03219(2) 0.03615(8) Uani 1 1 d . . .
Ru3 Ru 0.568771(19) 0.05131(3) 0.09625(2) 0.04778(11) Uani 1 1 d . . .
Ge1 Ge 0.66859(2) 0.13675(4) 0.05689(3) 0.04914(13) Uani 1 1 d . . .
Ge2 Ge 0.5000 0.36830(4) -0.01856(4) 0.03700(15) Uani 1 2 d S . .
O11 O 0.4008(2) 0.1217(4) -0.1514(3) 0.0892(15) Uani 1 1 d . . .
O12 O 0.5000 -0.1321(5) -0.0550(6) 0.188(6) Uani 1 2 d S . .
O21 O 0.6622(2) 0.3206(4) -0.0814(3) 0.0946(16) Uani 1 1 d . . .
O22 O 0.5939(2) 0.3699(3) 0.1585(3) 0.0826(14) Uani 1 1 d . . .
O31 O 0.6424(3) -0.1311(3) 0.0572(5) 0.141(3) Uani 1 1 d . . .
O32 O 0.6143(4) 0.0822(5) 0.2498(3) 0.135(3) Uani 1 1 d . . .
O33 O 0.5000 -0.1129(4) 0.1759(4) 0.0813(19) Uani 1 2 d S . .
C1 C 0.5000 0.1514(4) 0.0695(4) 0.0406(14) Uani 1 2 d S . .
C11 C 0.4342(3) 0.1115(5) -0.1032(3) 0.0605(15) Uani 1 1 d . . .
C12 C 0.5000 -0.0498(7) -0.0457(6) 0.112(4) Uani 1 2 d S . .
C21 C 0.6287(3) 0.2907(4) -0.0376(4) 0.0594(13) Uani 1 1 d . . .
C22 C 0.5872(2) 0.3210(4) 0.1096(3) 0.0520(13) Uani 1 1 d . . .
C31 C 0.6162(3) -0.0626(4) 0.0726(5) 0.088(2) Uani 1 1 d . . .
C32 C 0.5993(4) 0.0699(5) 0.1914(4) 0.081(2) Uani 1 1 d . . .
C33 C 0.5000 -0.0446(5) 0.1399(5) 0.060(2) Uani 1 2 d S . .
C41 C 0.7227(3) 0.0990(4) -0.0240(3) 0.0622(15) Uani 1 1 d . . .
C42 C 0.7108(3) 0.0224(5) -0.0698(4) 0.079(2) Uani 1 1 d . . .
H42 H 0.6749 -0.0169 -0.0615 0.095 Uiso 1 1 calc R . .
C43 C 0.7509(4) 0.0031(7) -0.1273(5) 0.104(3) Uani 1 1 d . . .
H43 H 0.7417 -0.0482 -0.1579 0.125 Uiso 1 1 calc R . .
C44 C 0.8034(5) 0.0589(8) -0.1389(5) 0.117(4) Uani 1 1 d . . .
H44 H 0.8310 0.0443 -0.1770 0.140 Uiso 1 1 calc R . .
C45 C 0.8172(4) 0.1358(8) -0.0966(5) 0.107(3) Uani 1 1 d . . .
H45 H 0.8532 0.1744 -0.1061 0.128 Uiso 1 1 calc R . .
C46 C 0.7765(3) 0.1557(5) -0.0386(4) 0.0809(19) Uani 1 1 d . . .
H46 H 0.7857 0.2082 -0.0091 0.097 Uiso 1 1 calc R . .
C51 C 0.7329(3) 0.1691(5) 0.1302(3) 0.0624(15) Uani 1 1 d . . .
C52 C 0.7792(3) 0.1016(6) 0.1458(4) 0.084(2) Uani 1 1 d . . .
H52 H 0.7802 0.0438 0.1205 0.101 Uiso 1 1 calc R . .
C53 C 0.8252(4) 0.1192(9) 0.1997(5) 0.109(3) Uani 1 1 d . . .
H53 H 0.8556 0.0717 0.2106 0.131 Uiso 1 1 calc R . .
C54 C 0.8268(4) 0.2001(10) 0.2352(5) 0.125(4) Uani 1 1 d . . .
H54 H 0.8584 0.2108 0.2702 0.150 Uiso 1 1 calc R . .
C55 C 0.7838(5) 0.2651(9) 0.2212(8) 0.169(6) Uani 1 1 d . . .
H55 H 0.7845 0.3225 0.2469 0.203 Uiso 1 1 calc R . .
C56 C 0.7359(4) 0.2516(8) 0.1679(7) 0.153(5) Uani 1 1 d . . .
H56 H 0.7059 0.3003 0.1588 0.183 Uiso 1 1 calc R . .
C61 C 0.5000 0.3985(5) -0.1207(4) 0.0413(14) Uani 1 2 d S . .
C62 C 0.5000 0.3284(5) -0.1730(4) 0.0486(17) Uani 1 2 d S . .
H62 H 0.5000 0.2640 -0.1594 0.058 Uiso 1 2 calc SR . .
C63 C 0.5000 0.3520(5) -0.2463(4) 0.0574(19) Uani 1 2 d S . .
H63 H 0.5000 0.3039 -0.2811 0.069 Uiso 1 2 calc SR . .
C64 C 0.5000 0.4465(6) -0.2656(4) 0.0558(19) Uani 1 2 d S . .
H64 H 0.5000 0.4631 -0.3141 0.067 Uiso 1 2 calc SR . .
C65 C 0.5000 0.5169(6) -0.2151(5) 0.071(2) Uani 1 2 d S . .
H65 H 0.5000 0.5813 -0.2288 0.085 Uiso 1 2 calc SR . .
C66 C 0.5000 0.4927(6) -0.1438(5) 0.065(2) Uani 1 2 d S . .
H66 H 0.5000 0.5416 -0.1097 0.078 Uiso 1 2 calc SR . .
C71 C 0.5000 0.4970(4) 0.0247(3) 0.0405(14) Uani 1 2 d S . .
C72 C 0.5579(3) 0.5447(3) 0.0353(4) 0.0573(13) Uani 1 1 d . . .
H72 H 0.5973 0.5124 0.0295 0.069 Uiso 1 1 calc R . .
C73 C 0.5573(3) 0.6421(4) 0.0547(4) 0.0664(16) Uani 1 1 d . . .
H73 H 0.5963 0.6748 0.0613 0.080 Uiso 1 1 calc R . .
C74 C 0.5000 0.6889(5) 0.0641(5) 0.072(3) Uani 1 2 d S . .
H74 H 0.5000 0.7537 0.0770 0.087 Uiso 1 2 calc SR . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C12 Ru1 C11 95.8(3) . . ?
C12 Ru1 C11 95.8(3) . 4_655 ?
C11 Ru1 C11 89.6(3) . 4_655 ?
C12 Ru1 C1 123.1(4) . . ?
C11 Ru1 C1 122.2(2) . . ?
C11 Ru1 C1 122.2(2) 4_655 . ?
C12 Ru1 Ru3 86.7(3) . 4_655 ?
C11 Ru1 Ru3 105.05(17) . 4_655 ?
C11 Ru1 Ru3 164.81(17) 4_655 4_655 ?
C1 Ru1 Ru3 46.17(13) . 4_655 ?
C12 Ru1 Ru3 86.7(3) . . ?
C11 Ru1 Ru3 164.81(17) . . ?
C11 Ru1 Ru3 105.05(17) 4_655 . ?
C1 Ru1 Ru3 46.17(13) . . ?
Ru3 Ru1 Ru3 60.05(2) 4_655 . ?
C12 Ru1 Ru2 143.01(19) . . ?
C11 Ru1 Ru2 120.28(18) . . ?
C11 Ru1 Ru2 77.99(19) 4_655 . ?
C1 Ru1 Ru2 44.79(12) . . ?
Ru3 Ru1 Ru2 90.95(2) 4_655 . ?
Ru3 Ru1 Ru2 60.717(14) . . ?
C12 Ru1 Ru2 143.01(19) . 4_655 ?
C11 Ru1 Ru2 77.99(19) . 4_655 ?
C11 Ru1 Ru2 120.28(18) 4_655 4_655 ?
C1 Ru1 Ru2 44.79(12) . 4_655 ?
Ru3 Ru1 Ru2 60.717(14) 4_655 4_655 ?
Ru3 Ru1 Ru2 90.95(2) . 4_655 ?
Ru2 Ru1 Ru2 60.696(17) . 4_655 ?
C22 Ru2 C21 99.9(2) . . ?
C22 Ru2 C1 103.8(3) . . ?
C21 Ru2 C1 156.2(3) . . ?
C22 Ru2 Ge2 87.76(15) . . ?
C21 Ru2 Ge2 80.51(16) . . ?
C1 Ru2 Ge2 98.98(13) . . ?
C22 Ru2 Ge1 92.83(15) . . ?
C21 Ru2 Ge1 80.00(16) . . ?
C1 Ru2 Ge1 99.98(13) . . ?
Ge2 Ru2 Ge1 160.31(2) . . ?
C22 Ru2 Ru1 151.80(17) . . ?
C21 Ru2 Ru1 108.27(19) . . ?
C1 Ru2 Ru1 48.0(2) . . ?
Ge2 Ru2 Ru1 95.158(18) . . ?
Ge1 Ru2 Ru1 93.574(16) . . ?
C22 Ru2 Ru3 103.63(16) . . ?
C21 Ru2 Ru3 128.98(15) . . ?
C1 Ru2 Ru3 45.54(13) . . ?
Ge2 Ru2 Ru3 144.200(18) . . ?
Ge1 Ru2 Ru3 54.438(16) . . ?
Ru1 Ru2 Ru3 59.367(15) . . ?
C22 Ru2 Ru2 100.97(16) . 4_655 ?
C21 Ru2 Ru2 129.17(17) . 4_655 ?
C1 Ru2 Ru2 44.25(13) . 4_655 ?
Ge2 Ru2 Ru2 54.753(11) . 4_655 ?
Ge1 Ru2 Ru2 143.723(14) . 4_655 ?
Ru1 Ru2 Ru2 59.652(8) . 4_655 ?
Ru3 Ru2 Ru2 89.565(11) . 4_655 ?
C32 Ru3 C31 99.2(3) . . ?
C32 Ru3 C1 111.3(3) . . ?
C31 Ru3 C1 149.4(3) . . ?
C32 Ru3 C33 87.0(3) . . ?
C31 Ru3 C33 84.7(3) . . ?
C1 Ru3 C33 93.42(18) . . ?
C32 Ru3 Ge1 86.3(2) . . ?
C31 Ru3 Ge1 84.6(2) . . ?
C1 Ru3 Ge1 100.07(13) . . ?
C33 Ru3 Ge1 166.38(14) . . ?
C32 Ru3 Ru1 159.4(2) . . ?
C31 Ru3 Ru1 101.4(3) . . ?
C1 Ru3 Ru1 48.2(2) . . ?
C33 Ru3 Ru1 95.6(2) . . ?
Ge1 Ru3 Ru1 94.79(2) . . ?
C32 Ru3 Ru3 109.3(2) . 4_655 ?
C31 Ru3 Ru3 120.7(2) . 4_655 ?
C1 Ru3 Ru3 46.24(12) . 4_655 ?
C33 Ru3 Ru3 47.82(14) . 4_655 ?
Ge1 Ru3 Ru3 145.802(15) . 4_655 ?
Ru1 Ru3 Ru3 59.974(10) . 4_655 ?
C32 Ru3 Ru2 105.2(2) . . ?
C31 Ru3 Ru2 130.8(2) . . ?
C1 Ru3 Ru2 44.41(13) . . ?
C33 Ru3 Ru2 137.80(14) . . ?
Ge1 Ru3 Ru2 55.665(15) . . ?
Ru1 Ru3 Ru2 59.916(14) . . ?
Ru3 Ru3 Ru2 90.435(11) 4_655 . ?
C41 Ge1 C51 102.4(2) . . ?
C41 Ge1 Ru3 124.95(18) . . ?
C51 Ge1 Ru3 117.66(19) . . ?
C41 Ge1 Ru2 118.17(17) . . ?
C51 Ge1 Ru2 122.96(18) . . ?
Ru3 Ge1 Ru2 69.897(17) . . ?
C61 Ge2 C71 101.8(3) . . ?
C61 Ge2 Ru2 121.76(14) . 4_655 ?
C71 Ge2 Ru2 120.24(14) . 4_655 ?
C61 Ge2 Ru2 121.76(14) . . ?
C71 Ge2 Ru2 120.24(14) . . ?
Ru2 Ge2 Ru2 70.49(2) 4_655 . ?
Ru2 C1 Ru2 91.5(3) . 4_655 ?
Ru2 C1 Ru3 172.6(4) . 4_655 ?
Ru2 C1 Ru3 90.05(3) 4_655 4_655 ?
Ru2 C1 Ru3 90.05(3) . . ?
Ru2 C1 Ru3 172.6(4) 4_655 . ?
Ru3 C1 Ru3 87.5(2) 4_655 . ?
Ru2 C1 Ru1 87.2(2) . . ?
Ru2 C1 Ru1 87.2(2) 4_655 . ?
Ru3 C1 Ru1 85.6(2) 4_655 . ?
Ru3 C1 Ru1 85.6(2) . . ?
O11 C11 Ru1 170.9(6) . . ?
O12 C12 Ru1 178.7(11) . . ?
O21 C21 Ru2 177.3(6) . . ?
O22 C22 Ru2 175.6(5) . . ?
O31 C31 Ru3 177.5(8) . . ?
O32 C32 Ru3 176.3(8) . . ?
O33 C33 Ru3 137.68(16) . 4_655 ?
O33 C33 Ru3 137.68(16) . . ?
Ru3 C33 Ru3 84.4(3) 4_655 . ?
C42 C41 C46 117.3(6) . . ?
C42 C41 Ge1 125.6(5) . . ?
C46 C41 Ge1 117.1(5) . . ?
C43 C42 C41 121.4(8) . . ?
C44 C43 C42 119.5(8) . . ?
C43 C44 C45 121.8(9) . . ?
C44 C45 C46 118.7(9) . . ?
C41 C46 C45 121.2(8) . . ?
C56 C51 C52 116.3(7) . . ?
C56 C51 Ge1 126.2(5) . . ?
C52 C51 Ge1 117.5(5) . . ?
C51 C52 C53 120.1(8) . . ?
C54 C53 C52 122.0(9) . . ?
C55 C54 C53 118.9(9) . . ?
C54 C55 C56 121.9(10) . . ?
C51 C56 C55 120.7(8) . . ?
C62 C61 C66 116.8(7) . . ?
C62 C61 Ge2 122.6(5) . . ?
C66 C61 Ge2 120.6(6) . . ?
C61 C62 C63 121.5(7) . . ?
C64 C63 C62 118.8(7) . . ?
C65 C64 C63 120.9(8) . . ?
C64 C65 C66 119.6(7) . . ?
C65 C66 C61 122.4(8) . . ?
C72 C71 C72 119.8(6) 4_655 . ?
C72 C71 Ge2 119.8(3) 4_655 . ?
C72 C71 Ge2 119.8(3) . . ?
C71 C72 C73 119.5(5) . . ?
C74 C73 C72 120.3(6) . . ?
C73 C74 C73 120.5(7) 4_655 . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 C12 1.890(9) . ?
Ru1 C11 1.917(6) . ?
Ru1 C11 1.917(6) 4_655 ?
Ru1 C1 2.112(7) . ?
Ru1 Ru3 2.8234(7) 4_655 ?
Ru1 Ru3 2.8234(7) . ?
Ru1 Ru2 2.8393(5) . ?
Ru1 Ru2 2.8393(5) 4_655 ?
Ru2 C22 1.871(6) . ?
Ru2 C21 1.914(6) . ?
Ru2 C1 2.003(5) . ?
Ru2 Ge2 2.4858(6) . ?
Ru2 Ge1 2.5166(6) . ?
Ru2 Ru3 2.8620(5) . ?
Ru2 Ru2 2.8691(6) 4_655 ?
Ru3 C32 1.894(8) . ?
Ru3 C31 1.909(6) . ?
Ru3 C1 2.043(5) . ?
Ru3 C33 2.104(6) . ?
Ru3 Ge1 2.4792(7) . ?
Ru3 Ru3 2.8256(8) 4_655 ?
Ge1 C41 1.943(6) . ?
Ge1 C51 1.951(6) . ?
Ge2 C61 1.945(7) . ?
Ge2 C71 1.959(6) . ?
Ge2 Ru2 2.4858(6) 4_655 ?
O11 C11 1.137(7) . ?
O12 C12 1.155(11) . ?
O21 C21 1.146(7) . ?
O22 C22 1.143(6) . ?
O31 C31 1.130(7) . ?
O32 C32 1.142(9) . ?
O33 C33 1.161(9) . ?
C1 Ru2 2.003(5) 4_655 ?
C1 Ru3 2.043(5) 4_655 ?
C33 Ru3 2.104(6) 4_655 ?
C41 C42 1.383(9) . ?
C41 C46 1.384(9) . ?
C42 C43 1.375(11) . ?
C43 C44 1.346(12) . ?
C44 C45 1.356(13) . ?
C45 C46 1.392(11) . ?
C51 C56 1.344(10) . ?
C51 C52 1.366(9) . ?
C52 C53 1.399(11) . ?
C53 C54 1.303(14) . ?
C54 C55 1.289(14) . ?
C55 C56 1.409(13) . ?
C61 C62 1.375(10) . ?
C61 C66 1.376(10) . ?
C62 C63 1.402(11) . ?
C63 C64 1.360(10) . ?
C64 C65 1.354(11) . ?
C65 C66 1.367(12) . ?
C71 C72 1.376(6) 4_655 ?
C71 C72 1.376(6) . ?
C72 C73 1.400(7) . ?
C73 C74 1.356(7) . ?
C74 C73 1.356(7) 4_655 ?
