#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/14/4321410.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4321410
loop_
_publ_author_name
'Allison M. Mills'
'Arthur Mar'
_publ_contact_author_address
; Department of Chemistry
  University of Alberta
  Edmonton, AB
  Canada  T6G 2G2
;
_publ_contact_author_email       arthur.mar@ualberta.ca
_publ_contact_author_fax         '(780) 492-8231'
_publ_contact_author_name        'Arthur Mar'
_publ_contact_author_phone       '(780) 492-5592'
_publ_section_title
;
 Rare-Earth Gallium Antimonides La13Ga8Sb21andRE12Ga4Sb23 (RE = La-Nd,
 Sm): Linking Sb Ribbons by Ga6-Rings or Ga2-Pairs
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4599
_journal_page_last               4607
_journal_paper_doi               10.1021/ic000519w
_journal_volume                  39
_journal_year                    2000
_chemical_formula_moiety         'Ga3.98 Pr12 Sb22.90'
_chemical_formula_sum            'Ga3.98 Pr12 Sb22.9'
_chemical_formula_weight         4756.48
_chemical_name_common            'praseodymium gallium antimonide'
_chemical_name_systematic        'praseodymium gallium antimonide'
_space_group_IT_number           71
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2'
_symmetry_space_group_name_H-M   'I m m m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   4.2612(3)
_cell_length_b                   19.4070(13)
_cell_length_c                   26.3972(18)
_cell_measurement_reflns_used    3256
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      32.85
_cell_measurement_theta_min      1.30
_cell_volume                     2183.0(3)
_computing_cell_refinement       'Bruker SAINT 5.0'
_computing_data_collection       'Bruker SMART 5.051'
_computing_data_reduction        'Bruker SAINT 5.0'
_computing_molecular_graphics    'ATOMS 4.0'
_computing_publication_material  'Bruker SHELXTL 5.1'
_computing_structure_refinement  'Bruker SHELXTL 5.1'
_computing_structure_solution    'Bruker SHELXTL 5.1'
_diffrn_ambient_temperature      295(2)
_diffrn_measured_fraction_theta_full 0.920
_diffrn_measured_fraction_theta_max 0.920
_diffrn_measurement_device_type  'Bruker P4/RA/SMART-1000 CCD'
_diffrn_measurement_method       'mixture of phi rotations and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0444
_diffrn_reflns_av_sigmaI/netI    0.0429
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -2
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       39
_diffrn_reflns_limit_l_min       -39
_diffrn_reflns_number            9014
_diffrn_reflns_theta_full        32.85
_diffrn_reflns_theta_max         32.85
_diffrn_reflns_theta_min         1.30
_exptl_absorpt_coefficient_mu    29.379
_exptl_absorpt_correction_T_max  0.9220
_exptl_absorpt_correction_T_min  0.8733
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'Bruker SHELXTL 5.1'
_exptl_crystal_colour            grey
_exptl_crystal_density_diffrn    7.236
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3999
_exptl_crystal_size_max          0.410
_exptl_crystal_size_mid          0.004
_exptl_crystal_size_min          0.002
_refine_diff_density_max         4.787
_refine_diff_density_min         -2.586
_refine_diff_density_rms         0.525
_refine_ls_extinction_coef       0.000066(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.985
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     75
_refine_ls_number_reflns         2178
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      0.984
_refine_ls_R_factor_all          0.0515
_refine_ls_R_factor_gt           0.0297
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0302P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0637
_refine_ls_wR_factor_ref         0.0723
_reflns_number_gt                1554
_reflns_number_total             2178
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic000519w_1.cif
_cod_data_source_block           immm
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_formula_sum        'Ga3.98 Pr12 Sb22.90'
_cod_database_code               4321410
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pr1 Pr 0.0000 0.27695(3) 0.40559(2) 0.00798(12) Uani 1 2 d S . .
Pr2 Pr 0.0000 0.38900(3) 0.26312(2) 0.00777(11) Uani 1 2 d S . .
Pr3 Pr 0.5000 0.0000 0.09340(3) 0.00822(15) Uani 1 4 d S . .
Pr4 Pr 0.5000 0.0000 0.38118(3) 0.00953(15) Uani 1 4 d S . .
Ga1 Ga 0.0000 0.0000 0.18986(7) 0.0225(6) Uani 0.964(7) 4 d SP . .
Ga2 Ga 0.0000 0.181(3) 0.5000 0.0126(17) Uani 0.027(2) 4 d SPU . .
Ga3 Ga 0.0000 0.43337(9) 0.0000 0.0134(3) Uani 1 4 d S . .
Sb1 Sb 0.0000 0.11138(4) 0.43300(3) 0.01520(19) Uani 0.973(2) 2 d SPU . .
Sb2 Sb 0.0000 0.11584(3) 0.14030(2) 0.00912(13) Uani 1 2 d S . .
Sb3 Sb 0.0000 0.22151(3) 0.28669(2) 0.00875(13) Uani 1 2 d S . .
Sb4 Sb 0.0000 0.33456(3) 0.14421(2) 0.00908(14) Uani 1 2 d S . .
Sb5 Sb 0.0000 0.0000 0.28911(3) 0.00957(18) Uani 1 4 d S . .
Sb6 Sb 0.0000 0.38335(5) 0.5000 0.01313(19) Uani 1 4 d S . .
Sb7 Sb 0.0000 0.23336(5) 0.0000 0.01133(19) Uani 1 4 d S . .
Sb8 Sb 0.0000 0.0000 0.0000 0.0088(2) Uani 1 8 d S . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pr Pr -0.2180 2.8214 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ga2 Pr1 Sb2 133.6(3) . 13 ?
Ga2 Pr1 Sb2 133.6(3) . 13_455 ?
Sb2 Pr1 Sb2 83.01(2) 13 13_455 ?
Ga2 Pr1 Sb6 76.4(8) . . ?
Sb2 Pr1 Sb6 82.95(2) 13 . ?
Sb2 Pr1 Sb6 82.95(2) 13_455 . ?
Ga2 Pr1 Sb7 49.9(5) . 13 ?
Sb2 Pr1 Sb7 83.997(16) 13 13 ?
Sb2 Pr1 Sb7 139.03(3) 13_455 13 ?
Sb6 Pr1 Sb7 56.951(18) . 13 ?
Ga2 Pr1 Sb7 49.9(5) . 13_455 ?
Sb2 Pr1 Sb7 139.03(3) 13 13_455 ?
Sb2 Pr1 Sb7 83.997(16) 13_455 13_455 ?
Sb6 Pr1 Sb7 56.951(18) . 13_455 ?
Sb7 Pr1 Sb7 80.874(13) 13 13_455 ?
Ga2 Pr1 Sb1 40.5(8) . . ?
Sb2 Pr1 Sb1 135.573(13) 13 . ?
Sb2 Pr1 Sb1 135.573(13) 13_455 . ?
Sb6 Pr1 Sb1 116.95(3) . . ?
Sb7 Pr1 Sb1 76.94(2) 13 . ?
Sb7 Pr1 Sb1 76.94(2) 13_455 . ?
Ga2 Pr1 Sb4 85.8(7) . 13_455 ?
Sb2 Pr1 Sb4 134.45(2) 13 13_455 ?
Sb2 Pr1 Sb4 81.190(16) 13_455 13_455 ?
Sb6 Pr1 Sb4 136.312(13) . 13_455 ?
Sb7 Pr1 Sb4 132.78(3) 13 13_455 ?
Sb7 Pr1 Sb4 81.023(16) 13_455 13_455 ?
Sb1 Pr1 Sb4 56.585(16) . 13_455 ?
Ga2 Pr1 Sb4 85.8(6) . 13 ?
Sb2 Pr1 Sb4 81.190(16) 13 13 ?
Sb2 Pr1 Sb4 134.45(2) 13_455 13 ?
Sb6 Pr1 Sb4 136.312(13) . 13 ?
Sb7 Pr1 Sb4 81.023(16) 13 13 ?
Sb7 Pr1 Sb4 132.78(3) 13_455 13 ?
Sb1 Pr1 Sb4 56.585(16) . 13 ?
Sb4 Pr1 Sb4 80.162(19) 13_455 13 ?
Ga2 Pr1 Sb3 124.3(8) . . ?
Sb2 Pr1 Sb3 81.572(18) 13 . ?
Sb2 Pr1 Sb3 81.572(18) 13_455 . ?
Sb6 Pr1 Sb3 159.28(3) . . ?
Sb7 Pr1 Sb3 134.263(14) 13 . ?
Sb7 Pr1 Sb3 134.263(14) 13_455 . ?
Sb1 Pr1 Sb3 83.77(2) . . ?
Sb4 Pr1 Sb3 53.997(15) 13_455 . ?
Sb4 Pr1 Sb3 53.997(15) 13 . ?
Ga1 Pr2 Ga1 81.19(2) 13 13_455 ?
Ga1 Pr2 Sb3 178.77(4) 13 13_455 ?
Ga1 Pr2 Sb3 99.129(14) 13_455 13_455 ?
Ga1 Pr2 Sb3 99.129(14) 13 13 ?
Ga1 Pr2 Sb3 178.77(4) 13_455 13 ?
Sb3 Pr2 Sb3 80.528(19) 13_455 13 ?
Ga1 Pr2 Sb3 125.09(2) 13 . ?
Ga1 Pr2 Sb3 125.09(2) 13_455 . ?
Sb3 Pr2 Sb3 55.667(17) 13_455 . ?
Sb3 Pr2 Sb3 55.667(17) 13 . ?
Ga1 Pr2 Sb4 124.69(3) 13 . ?
Ga1 Pr2 Sb4 124.69(3) 13_455 . ?
Sb3 Pr2 Sb4 54.161(14) 13_455 . ?
Sb3 Pr2 Sb4 54.161(14) 13 . ?
Sb3 Pr2 Sb4 82.23(2) . . ?
Ga1 Pr2 Sb2 46.43(2) 13 13 ?
Ga1 Pr2 Sb2 98.33(3) 13_455 13 ?
Sb3 Pr2 Sb2 134.57(2) 13_455 13 ?
Sb3 Pr2 Sb2 82.717(15) 13 13 ?
Sb3 Pr2 Sb2 80.098(17) . 13 ?
Sb4 Pr2 Sb2 135.884(13) . 13 ?
Ga1 Pr2 Sb2 98.33(3) 13 13_455 ?
Ga1 Pr2 Sb2 46.43(2) 13_455 13_455 ?
Sb3 Pr2 Sb2 82.717(15) 13_455 13_455 ?
Sb3 Pr2 Sb2 134.57(2) 13 13_455 ?
Sb3 Pr2 Sb2 80.098(18) . 13_455 ?
Sb4 Pr2 Sb2 135.884(13) . 13_455 ?
Sb2 Pr2 Sb2 79.73(2) 13 13_455 ?
Ga1 Pr2 Sb5 46.74(3) 13 13 ?
Ga1 Pr2 Sb5 98.495(19) 13_455 13 ?
Sb3 Pr2 Sb5 132.03(2) 13_455 13 ?
Sb3 Pr2 Sb5 80.919(13) 13 13 ?
Sb3 Pr2 Sb5 135.518(10) . 13 ?
Sb4 Pr2 Sb5 79.278(19) . 13 ?
Sb2 Pr2 Sb5 85.738(17) 13 13 ?
Sb2 Pr2 Sb5 138.26(2) 13_455 13 ?
Ga1 Pr2 Sb5 98.495(19) 13 13_455 ?
Ga1 Pr2 Sb5 46.74(3) 13_455 13_455 ?
Sb3 Pr2 Sb5 80.919(13) 13_455 13_455 ?
Sb3 Pr2 Sb5 132.03(2) 13 13_455 ?
Sb3 Pr2 Sb5 135.518(10) . 13_455 ?
Sb4 Pr2 Sb5 79.278(19) . 13_455 ?
Sb2 Pr2 Sb5 138.26(2) 13 13_455 ?
Sb2 Pr2 Sb5 85.738(16) 13_455 13_455 ?
Sb5 Pr2 Sb5 79.593(17) 13 13_455 ?
Sb8 Pr3 Sb8 81.665(18) . 1_655 ?
Sb8 Pr3 Ga1 179.09(3) . 1_655 ?
Sb8 Pr3 Ga1 99.25(2) 1_655 1_655 ?
Sb8 Pr3 Ga1 99.25(2) . . ?
Sb8 Pr3 Ga1 179.09(3) 1_655 . ?
Ga1 Pr3 Ga1 79.84(4) 1_655 . ?
Sb8 Pr3 Sb2 134.304(16) . 1_655 ?
Sb8 Pr3 Sb2 82.136(11) 1_655 1_655 ?
Ga1 Pr3 Sb2 46.009(14) 1_655 1_655 ?
Ga1 Pr3 Sb2 97.20(2) . 1_655 ?
Sb8 Pr3 Sb2 82.136(11) . 2 ?
Sb8 Pr3 Sb2 134.304(16) 1_655 2 ?
Ga1 Pr3 Sb2 97.20(2) 1_655 2 ?
Ga1 Pr3 Sb2 46.009(14) . 2 ?
Sb2 Pr3 Sb2 136.43(3) 1_655 2 ?
Sb8 Pr3 Sb2 134.304(16) . 2_655 ?
Sb8 Pr3 Sb2 82.136(11) 1_655 2_655 ?
Ga1 Pr3 Sb2 46.009(14) 1_655 2_655 ?
Ga1 Pr3 Sb2 97.20(2) . 2_655 ?
Sb2 Pr3 Sb2 84.75(2) 1_655 2_655 ?
Sb2 Pr3 Sb2 79.396(17) 2 2_655 ?
Sb8 Pr3 Sb2 82.136(11) . . ?
Sb8 Pr3 Sb2 134.304(16) 1_655 . ?
Ga1 Pr3 Sb2 97.20(2) 1_655 . ?
Ga1 Pr3 Sb2 46.009(14) . . ?
Sb2 Pr3 Sb2 79.396(17) 1_655 . ?
Sb2 Pr3 Sb2 84.75(2) 2 . ?
Sb2 Pr3 Sb2 136.43(3) 2_655 . ?
Sb8 Pr3 Sb6 56.130(13) . 5_544 ?
Sb8 Pr3 Sb6 56.130(13) 1_655 5_544 ?
Ga1 Pr3 Sb6 124.396(14) 1_655 5_544 ?
Ga1 Pr3 Sb6 124.396(14) . 5_544 ?
Sb2 Pr3 Sb6 136.822(15) 1_655 5_544 ?
Sb2 Pr3 Sb6 79.486(15) 2 5_544 ?
Sb2 Pr3 Sb6 79.487(15) 2_655 5_544 ?
Sb2 Pr3 Sb6 136.822(15) . 5_544 ?
Sb8 Pr3 Sb6 56.130(13) . 13 ?
Sb8 Pr3 Sb6 56.130(13) 1_655 13 ?
Ga1 Pr3 Sb6 124.396(14) 1_655 13 ?
Ga1 Pr3 Sb6 124.396(14) . 13 ?
Sb2 Pr3 Sb6 79.486(15) 1_655 13 ?
Sb2 Pr3 Sb6 136.822(15) 2 13 ?
Sb2 Pr3 Sb6 136.822(15) 2_655 13 ?
Sb2 Pr3 Sb6 79.486(15) . 13 ?
Sb6 Pr3 Sb6 85.12(3) 5_544 13 ?
Sb5 Pr4 Sb5 82.48(3) . 1_655 ?
Sb5 Pr4 Sb4 81.161(14) . 14_545 ?
Sb5 Pr4 Sb4 81.161(14) 1_655 14_545 ?
Sb5 Pr4 Sb4 81.161(14) . 13 ?
Sb5 Pr4 Sb4 81.161(14) 1_655 13 ?
Sb4 Pr4 Sb4 156.42(3) 14_545 13 ?
Sb5 Pr4 Sb1 136.958(16) . 1_655 ?
Sb5 Pr4 Sb1 83.516(15) 1_655 1_655 ?
Sb4 Pr4 Sb1 136.017(12) 14_545 1_655 ?
Sb4 Pr4 Sb1 56.521(14) 13 1_655 ?
Sb5 Pr4 Sb1 83.516(15) . 2 ?
Sb5 Pr4 Sb1 136.958(16) 1_655 2 ?
Sb4 Pr4 Sb1 56.521(14) 14_545 2 ?
Sb4 Pr4 Sb1 136.017(12) 13 2 ?
Sb1 Pr4 Sb1 131.48(3) 1_655 2 ?
Sb5 Pr4 Sb1 136.958(16) . 2_655 ?
Sb5 Pr4 Sb1 83.516(15) 1_655 2_655 ?
Sb4 Pr4 Sb1 56.521(14) 14_545 2_655 ?
Sb4 Pr4 Sb1 136.017(12) 13 2_655 ?
Sb1 Pr4 Sb1 80.98(2) 1_655 2_655 ?
Sb1 Pr4 Sb1 79.585(19) 2 2_655 ?
Sb5 Pr4 Sb1 83.516(15) . . ?
Sb5 Pr4 Sb1 136.958(16) 1_655 . ?
Sb4 Pr4 Sb1 136.017(12) 14_545 . ?
Sb4 Pr4 Sb1 56.521(14) 13 . ?
Sb1 Pr4 Sb1 79.585(19) 1_655 . ?
Sb1 Pr4 Sb1 80.98(2) 2 . ?
Sb1 Pr4 Sb1 131.48(3) 2_655 . ?
Sb5 Pr4 Ga3 134.044(16) . 13 ?
Sb5 Pr4 Ga3 134.044(16) 1_655 13 ?
Sb4 Pr4 Ga3 124.20(3) 14_545 13 ?
Sb4 Pr4 Ga3 79.39(3) 13 13 ?
Sb1 Pr4 Ga3 51.15(2) 1_655 13 ?
Sb1 Pr4 Ga3 82.39(3) 2 13 ?
Sb1 Pr4 Ga3 82.39(3) 2_655 13 ?
Sb1 Pr4 Ga3 51.15(2) . 13 ?
Sb5 Pr4 Ga3 134.044(16) . 5_545 ?
Sb5 Pr4 Ga3 134.044(16) 1_655 5_545 ?
Sb4 Pr4 Ga3 79.39(3) 14_545 5_545 ?
Sb4 Pr4 Ga3 124.20(3) 13 5_545 ?
Sb1 Pr4 Ga3 82.39(3) 1_655 5_545 ?
Sb1 Pr4 Ga3 51.15(2) 2 5_545 ?
Sb1 Pr4 Ga3 51.15(2) 2_655 5_545 ?
Sb1 Pr4 Ga3 82.39(3) . 5_545 ?
Ga3 Pr4 Ga3 44.81(6) 13 5_545 ?
Sb2 Ga1 Sb2 119.61(7) 2 . ?
Sb2 Ga1 Sb5 120.20(4) 2 . ?
Sb2 Ga1 Sb5 120.20(4) . . ?
Sb2 Ga1 Pr2 139.404(12) 2 13 ?
Sb2 Ga1 Pr2 67.792(15) . 13 ?
Sb5 Ga1 Pr2 67.72(3) . 13 ?
Sb2 Ga1 Pr2 139.404(12) 2 13_455 ?
Sb2 Ga1 Pr2 67.792(15) . 13_455 ?
Sb5 Ga1 Pr2 67.72(3) . 13_455 ?
Pr2 Ga1 Pr2 81.19(2) 13 13_455 ?
Sb2 Ga1 Pr2 67.792(15) 2 14_445 ?
Sb2 Ga1 Pr2 139.404(12) . 14_445 ?
Sb5 Ga1 Pr2 67.72(3) . 14_445 ?
Pr2 Ga1 Pr2 135.44(6) 13 14_445 ?
Pr2 Ga1 Pr2 82.28(3) 13_455 14_445 ?
Sb2 Ga1 Pr2 67.792(15) 2 14_545 ?
Sb2 Ga1 Pr2 139.404(12) . 14_545 ?
Sb5 Ga1 Pr2 67.72(3) . 14_545 ?
Pr2 Ga1 Pr2 82.28(3) 13 14_545 ?
Pr2 Ga1 Pr2 135.44(6) 13_455 14_545 ?
Pr2 Ga1 Pr2 81.19(2) 14_445 14_545 ?
Sb2 Ga1 Pr3 67.31(3) 2 1_455 ?
Sb2 Ga1 Pr3 67.31(3) . 1_455 ?
Sb5 Ga1 Pr3 140.08(2) . 1_455 ?
Pr2 Ga1 Pr3 135.10(3) 13 1_455 ?
Pr2 Ga1 Pr3 82.714(15) 13_455 1_455 ?
Pr2 Ga1 Pr3 82.714(15) 14_445 1_455 ?
Pr2 Ga1 Pr3 135.10(3) 14_545 1_455 ?
Sb2 Ga1 Pr3 67.31(3) 2 . ?
Sb2 Ga1 Pr3 67.31(3) . . ?
Sb5 Ga1 Pr3 140.08(2) . . ?
Pr2 Ga1 Pr3 82.714(15) 13 . ?
Pr2 Ga1 Pr3 135.10(3) 13_455 . ?
Pr2 Ga1 Pr3 135.10(3) 14_445 . ?
Pr2 Ga1 Pr3 82.714(15) 14_545 . ?
Pr3 Ga1 Pr3 79.84(4) 1_455 . ?
Sb1 Ga2 Sb1 105(2) . 10_556 ?
Sb1 Ga2 Sb7 111.93(13) . 13 ?
Sb1 Ga2 Sb7 111.93(13) 10_556 13 ?
Sb1 Ga2 Sb7 111.93(13) . 13_455 ?
Sb1 Ga2 Sb7 111.93(13) 10_556 13_455 ?
Sb7 Ga2 Sb7 104.1(19) 13 13_455 ?
Sb1 Ga2 Pr1 179(2) . 10_556 ?
Sb1 Ga2 Pr1 74.1(3) 10_556 10_556 ?
Sb7 Ga2 Pr1 68.4(9) 13 10_556 ?
Sb7 Ga2 Pr1 68.4(9) 13_455 10_556 ?
Sb1 Ga2 Pr1 74.1(3) . . ?
Sb1 Ga2 Pr1 179(2) 10_556 . ?
Sb7 Ga2 Pr1 68.4(9) 13 . ?
Sb7 Ga2 Pr1 68.4(9) 13_455 . ?
Pr1 Ga2 Pr1 106.5(17) 10_556 . ?
Ga3 Ga3 Sb1 107.41(4) 9_565 6_454 ?
Ga3 Ga3 Sb1 107.41(4) 9_565 13 ?
Sb1 Ga3 Sb1 145.18(7) 6_454 13 ?
Ga3 Ga3 Sb1 107.41(4) 9_565 13_455 ?
Sb1 Ga3 Sb1 75.10(3) 6_454 13_455 ?
Sb1 Ga3 Sb1 94.48(3) 13 13_455 ?
Ga3 Ga3 Sb1 107.41(4) 9_565 6_554 ?
Sb1 Ga3 Sb1 94.48(3) 6_454 6_554 ?
Sb1 Ga3 Sb1 75.10(3) 13 6_554 ?
Sb1 Ga3 Sb1 145.18(7) 13_455 6_554 ?
Ga3 Ga3 Pr4 67.59(3) 9_565 13 ?
Sb1 Ga3 Pr4 132.649(13) 6_454 13 ?
Sb1 Ga3 Pr4 63.295(16) 13 13 ?
Sb1 Ga3 Pr4 63.295(16) 13_455 13 ?
Sb1 Ga3 Pr4 132.649(13) 6_554 13 ?
Ga3 Ga3 Pr4 67.59(3) 9_565 5_454 ?
Sb1 Ga3 Pr4 63.295(16) 6_454 5_454 ?
Sb1 Ga3 Pr4 132.649(13) 13 5_454 ?
Sb1 Ga3 Pr4 132.649(13) 13_455 5_454 ?
Sb1 Ga3 Pr4 63.295(16) 6_554 5_454 ?
Pr4 Ga3 Pr4 135.19(6) 13 5_454 ?
Ga2 Sb1 Ga3 72.4(8) . 13 ?
Ga2 Sb1 Ga3 72.4(8) . 13_455 ?
Ga3 Sb1 Ga3 94.48(3) 13 13_455 ?
Ga2 Sb1 Sb4 108.3(8) . 13_455 ?
Ga3 Sb1 Sb4 175.60(3) 13 13_455 ?
Ga3 Sb1 Sb4 89.851(15) 13_455 13_455 ?
Ga2 Sb1 Sb4 108.3(8) . 13 ?
Ga3 Sb1 Sb4 89.851(15) 13 13 ?
Ga3 Sb1 Sb4 175.60(3) 13_455 13 ?
Sb4 Sb1 Sb4 85.81(3) 13_455 13 ?
Ga2 Sb1 Pr1 65.3(12) . . ?
Ga3 Sb1 Pr1 115.20(4) 13 . ?
Ga3 Sb1 Pr1 115.20(4) 13_455 . ?
Sb4 Sb1 Pr1 61.956(17) 13_455 . ?
Sb4 Sb1 Pr1 61.956(17) 13 . ?
Ga2 Sb1 Pr4 136.1(5) . 1_455 ?
Ga3 Sb1 Pr4 121.74(4) 13 1_455 ?
Ga3 Sb1 Pr4 65.56(3) 13_455 1_455 ?
Sb4 Sb1 Pr4 60.949(16) 13_455 1_455 ?
Sb4 Sb1 Pr4 112.70(3) 13 1_455 ?
Pr1 Sb1 Pr4 122.900(19) . 1_455 ?
Ga2 Sb1 Pr4 136.1(5) . . ?
Ga3 Sb1 Pr4 65.56(3) 13 . ?
Ga3 Sb1 Pr4 121.74(4) 13_455 . ?
Sb4 Sb1 Pr4 112.70(3) 13_455 . ?
Sb4 Sb1 Pr4 60.949(16) 13 . ?
Pr1 Sb1 Pr4 122.900(19) . . ?
Pr4 Sb1 Pr4 79.585(19) 1_455 . ?
Ga1 Sb2 Pr1 138.493(10) . 13 ?
Ga1 Sb2 Pr1 138.493(10) . 13_455 ?
Pr1 Sb2 Pr1 83.01(2) 13 13_455 ?
Ga1 Sb2 Pr2 65.78(3) . 13 ?
Pr1 Sb2 Pr2 83.252(13) 13 13 ?
Pr1 Sb2 Pr2 137.06(2) 13_455 13 ?
Ga1 Sb2 Pr2 65.78(3) . 13_455 ?
Pr1 Sb2 Pr2 137.06(2) 13 13_455 ?
Pr1 Sb2 Pr2 83.252(13) 13_455 13_455 ?
Pr2 Sb2 Pr2 79.73(2) 13 13_455 ?
Ga1 Sb2 Pr3 66.68(3) . 1_455 ?
Pr1 Sb2 Pr3 136.03(3) 13 1_455 ?
Pr1 Sb2 Pr3 82.706(13) 13_455 1_455 ?
Pr2 Sb2 Pr3 132.46(2) 13 1_455 ?
Pr2 Sb2 Pr3 81.733(16) 13_455 1_455 ?
Ga1 Sb2 Pr3 66.68(3) . . ?
Pr1 Sb2 Pr3 82.706(13) 13 . ?
Pr1 Sb2 Pr3 136.03(3) 13_455 . ?
Pr2 Sb2 Pr3 81.733(15) 13 . ?
Pr2 Sb2 Pr3 132.46(2) 13_455 . ?
Pr3 Sb2 Pr3 79.396(17) 1_455 . ?
Sb4 Sb3 Sb4 90.18(2) 13 13_455 ?
Sb4 Sb3 Sb3 178.40(3) 13 13_455 ?
Sb4 Sb3 Sb3 91.216(13) 13_455 13_455 ?
Sb4 Sb3 Sb3 91.216(13) 13 13 ?
Sb4 Sb3 Sb3 178.40(3) 13_455 13 ?
Sb3 Sb3 Sb3 87.38(3) 13_455 13 ?
Sb4 Sb3 Pr2 117.66(3) 13 13_455 ?
Sb4 Sb3 Pr2 63.180(17) 13_455 13_455 ?
Sb3 Sb3 Pr2 62.378(18) 13_455 13_455 ?
Sb3 Sb3 Pr2 115.42(3) 13 13_455 ?
Sb4 Sb3 Pr2 63.180(17) 13 13 ?
Sb4 Sb3 Pr2 117.66(3) 13_455 13 ?
Sb3 Sb3 Pr2 115.42(3) 13_455 13 ?
Sb3 Sb3 Pr2 62.378(18) 13 13 ?
Pr2 Sb3 Pr2 80.528(19) 13_455 13 ?
Sb4 Sb3 Pr2 117.98(2) 13 . ?
Sb4 Sb3 Pr2 117.98(2) 13_455 . ?
Sb3 Sb3 Pr2 61.95(2) 13_455 . ?
Sb3 Sb3 Pr2 61.95(2) 13 . ?
Pr2 Sb3 Pr2 124.333(17) 13_455 . ?
Pr2 Sb3 Pr2 124.333(17) 13 . ?
Sb4 Sb3 Pr1 62.850(17) 13 . ?
Sb4 Sb3 Pr1 62.850(17) 13_455 . ?
Sb3 Sb3 Pr1 118.54(3) 13_455 . ?
Sb3 Sb3 Pr1 118.54(3) 13 . ?
Pr2 Sb3 Pr1 126.029(17) 13_455 . ?
Pr2 Sb3 Pr1 126.029(17) 13 . ?
Pr2 Sb3 Pr1 81.92(2) . . ?
Sb3 Sb4 Sb3 90.18(2) 13 13_455 ?
Sb3 Sb4 Sb1 176.63(3) 13 13_455 ?
Sb3 Sb4 Sb1 91.948(14) 13_455 13_455 ?
Sb3 Sb4 Sb1 91.948(14) 13 13 ?
Sb3 Sb4 Sb1 176.63(3) 13_455 13 ?
Sb1 Sb4 Sb1 85.81(3) 13_455 13 ?
Sb3 Sb4 Pr4 118.55(2) 13 13 ?
Sb3 Sb4 Pr4 118.55(2) 13_455 13 ?
Sb1 Sb4 Pr4 62.530(19) 13_455 13 ?
Sb1 Sb4 Pr4 62.530(19) 13 13 ?
Sb3 Sb4 Pr1 117.41(2) 13 13_455 ?
Sb3 Sb4 Pr1 63.152(16) 13_455 13_455 ?
Sb1 Sb4 Pr1 61.459(17) 13_455 13_455 ?
Sb1 Sb4 Pr1 113.51(3) 13 13_455 ?
Pr4 Sb4 Pr1 123.984(19) 13 13_455 ?
Sb3 Sb4 Pr1 63.152(16) 13 13 ?
Sb3 Sb4 Pr1 117.41(2) 13_455 13 ?
Sb1 Sb4 Pr1 113.51(3) 13_455 13 ?
Sb1 Sb4 Pr1 61.459(17) 13 13 ?
Pr4 Sb4 Pr1 123.984(19) 13 13 ?
Pr1 Sb4 Pr1 80.162(19) 13_455 13 ?
Sb3 Sb4 Pr2 62.659(17) 13 . ?
Sb3 Sb4 Pr2 62.659(17) 13_455 . ?
Sb1 Sb4 Pr2 120.68(2) 13_455 . ?
Sb1 Sb4 Pr2 120.68(2) 13 . ?
Pr4 Sb4 Pr2 83.19(2) 13 . ?
Pr1 Sb4 Pr2 125.811(17) 13_455 . ?
Pr1 Sb4 Pr2 125.811(17) 13 . ?
Ga1 Sb5 Pr4 138.762(14) . . ?
Ga1 Sb5 Pr4 138.762(14) . 1_455 ?
Pr4 Sb5 Pr4 82.48(3) . 1_455 ?
Ga1 Sb5 Pr2 65.535(17) . 14_445 ?
Pr4 Sb5 Pr2 137.168(16) . 14_445 ?
Pr4 Sb5 Pr2 83.656(12) 1_455 14_445 ?
Ga1 Sb5 Pr2 65.535(17) . 13 ?
Pr4 Sb5 Pr2 83.656(12) . 13 ?
Pr4 Sb5 Pr2 137.168(16) 1_455 13 ?
Pr2 Sb5 Pr2 131.07(3) 14_445 13 ?
Ga1 Sb5 Pr2 65.535(17) . 13_455 ?
Pr4 Sb5 Pr2 137.168(16) . 13_455 ?
Pr4 Sb5 Pr2 83.656(12) 1_455 13_455 ?
Pr2 Sb5 Pr2 80.654(19) 14_445 13_455 ?
Pr2 Sb5 Pr2 79.593(17) 13 13_455 ?
Ga1 Sb5 Pr2 65.535(17) . 14_545 ?
Pr4 Sb5 Pr2 83.656(12) . 14_545 ?
Pr4 Sb5 Pr2 137.168(16) 1_455 14_545 ?
Pr2 Sb5 Pr2 79.593(17) 14_445 14_545 ?
Pr2 Sb5 Pr2 80.654(19) 13 14_545 ?
Pr2 Sb5 Pr2 131.07(3) 13_455 14_545 ?
Sb8 Sb6 Sb8 86.53(3) 5 5_455 ?
Sb8 Sb6 Sb7 179.99(3) 5 13_455 ?
Sb8 Sb6 Sb7 93.488(14) 5_455 13_455 ?
Sb8 Sb6 Sb7 93.488(14) 5 13 ?
Sb8 Sb6 Sb7 179.99(3) 5_455 13 ?
Sb7 Sb6 Sb7 86.50(3) 13_455 13 ?
Sb8 Sb6 Pr1 117.685(7) 5 . ?
Sb8 Sb6 Pr1 117.685(7) 5_455 . ?
Sb7 Sb6 Pr1 62.308(17) 13_455 . ?
Sb7 Sb6 Pr1 62.308(17) 13 . ?
Sb8 Sb6 Pr1 117.685(7) 5 10_556 ?
Sb8 Sb6 Pr1 117.685(7) 5_455 10_556 ?
Sb7 Sb6 Pr1 62.308(17) 13_455 10_556 ?
Sb7 Sb6 Pr1 62.308(17) 13 10_556 ?
Pr1 Sb6 Pr1 100.71(3) . 10_556 ?
Sb8 Sb6 Pr3 60.493(15) 5 5_455 ?
Sb8 Sb6 Pr3 60.493(15) 5_455 5_455 ?
Sb7 Sb6 Pr3 119.514(9) 13_455 5_455 ?
Sb7 Sb6 Pr3 119.514(9) 13 5_455 ?
Pr1 Sb6 Pr3 177.08(3) . 5_455 ?
Pr1 Sb6 Pr3 82.203(14) 10_556 5_455 ?
Sb8 Sb6 Pr3 60.493(15) 5 13 ?
Sb8 Sb6 Pr3 60.493(15) 5_455 13 ?
Sb7 Sb6 Pr3 119.514(9) 13_455 13 ?
Sb7 Sb6 Pr3 119.514(9) 13 13 ?
Pr1 Sb6 Pr3 82.203(14) . 13 ?
Pr1 Sb6 Pr3 177.08(3) 10_556 13 ?
Pr3 Sb6 Pr3 94.88(3) 5_455 13 ?
Ga2 Sb7 Ga2 104.1(19) 13 13_455 ?
Ga2 Sb7 Sb6 171.2(10) 13 13_455 ?
Ga2 Sb7 Sb6 84.7(10) 13_455 13_455 ?
Ga2 Sb7 Sb6 84.7(10) 13 13 ?
Ga2 Sb7 Sb6 171.2(10) 13_455 13 ?
Sb6 Sb7 Sb6 86.50(3) 13_455 13 ?
Ga2 Sb7 Pr1 123.3(4) 13 6_454 ?
Ga2 Sb7 Pr1 61.7(5) 13_455 6_454 ?
Sb6 Sb7 Pr1 60.741(13) 13_455 6_454 ?
Sb6 Sb7 Pr1 113.58(2) 13 6_454 ?
Ga2 Sb7 Pr1 61.7(5) 13 6_554 ?
Ga2 Sb7 Pr1 123.3(4) 13_455 6_554 ?
Sb6 Sb7 Pr1 113.58(2) 13_455 6_554 ?
Sb6 Sb7 Pr1 60.741(13) 13 6_554 ?
Pr1 Sb7 Pr1 80.874(13) 6_454 6_554 ?
Ga2 Sb7 Pr1 61.7(5) 13 13 ?
Ga2 Sb7 Pr1 123.3(4) 13_455 13 ?
Sb6 Sb7 Pr1 113.58(2) 13_455 13 ?
Sb6 Sb7 Pr1 60.741(13) 13 13 ?
Pr1 Sb7 Pr1 173.02(4) 6_454 13 ?
Pr1 Sb7 Pr1 98.696(13) 6_554 13 ?
Ga2 Sb7 Pr1 123.3(4) 13 13_455 ?
Ga2 Sb7 Pr1 61.7(5) 13_455 13_455 ?
Sb6 Sb7 Pr1 60.741(13) 13_455 13_455 ?
Sb6 Sb7 Pr1 113.58(2) 13 13_455 ?
Pr1 Sb7 Pr1 98.696(13) 6_454 13_455 ?
Pr1 Sb7 Pr1 173.02(4) 6_554 13_455 ?
Pr1 Sb7 Pr1 80.874(13) 13 13_455 ?
Sb6 Sb8 Sb6 180.00(2) 13 5_444 ?
Sb6 Sb8 Sb6 86.53(3) 13 13_455 ?
Sb6 Sb8 Sb6 93.47(3) 5_444 13_455 ?
Sb6 Sb8 Sb6 93.47(3) 13 5_544 ?
Sb6 Sb8 Sb6 86.53(3) 5_444 5_544 ?
Sb6 Sb8 Sb6 180.00(2) 13_455 5_544 ?
Sb6 Sb8 Pr3 63.377(9) 13 . ?
Sb6 Sb8 Pr3 116.623(9) 5_444 . ?
Sb6 Sb8 Pr3 116.623(9) 13_455 . ?
Sb6 Sb8 Pr3 63.377(9) 5_544 . ?
Sb6 Sb8 Pr3 116.623(9) 13 9 ?
Sb6 Sb8 Pr3 63.377(9) 5_444 9 ?
Sb6 Sb8 Pr3 63.377(9) 13_455 9 ?
Sb6 Sb8 Pr3 116.623(9) 5_544 9 ?
Pr3 Sb8 Pr3 180.000(17) . 9 ?
Sb6 Sb8 Pr3 116.623(9) 13 1_455 ?
Sb6 Sb8 Pr3 63.377(9) 5_444 1_455 ?
Sb6 Sb8 Pr3 63.377(9) 13_455 1_455 ?
Sb6 Sb8 Pr3 116.623(9) 5_544 1_455 ?
Pr3 Sb8 Pr3 81.665(18) . 1_455 ?
Pr3 Sb8 Pr3 98.335(18) 9 1_455 ?
Sb6 Sb8 Pr3 63.377(9) 13 9_655 ?
Sb6 Sb8 Pr3 116.623(9) 5_444 9_655 ?
Sb6 Sb8 Pr3 116.623(9) 13_455 9_655 ?
Sb6 Sb8 Pr3 63.377(9) 5_544 9_655 ?
Pr3 Sb8 Pr3 98.335(18) . 9_655 ?
Pr3 Sb8 Pr3 81.665(18) 9 9_655 ?
Pr3 Sb8 Pr3 180.000(17) 1_455 9_655 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pr1 Ga2 3.11(3) . ?
Pr1 Sb2 3.2150(6) 13 ?
Pr1 Sb2 3.2150(6) 13_455 ?
Pr1 Sb6 3.2365(8) . ?
Pr1 Sb7 3.2849(4) 13 ?
Pr1 Sb7 3.2849(4) 13_455 ?
Pr1 Sb1 3.2936(9) . ?
Pr1 Sb4 3.3091(6) 13_455 ?
Pr1 Sb4 3.3091(6) 13 ?
Pr1 Sb3 3.3180(8) . ?
Pr2 Ga1 3.2743(8) 13 ?
Pr2 Ga1 3.2743(8) 13_455 ?
Pr2 Sb3 3.2966(7) 13_455 ?
Pr2 Sb3 3.2966(7) 13 ?
Pr2 Sb3 3.3095(8) . ?
Pr2 Sb4 3.3119(8) . ?
Pr2 Sb2 3.3239(7) 13 ?
Pr2 Sb2 3.3239(7) 13_455 ?
Pr2 Sb5 3.3287(6) 13 ?
Pr2 Sb5 3.3287(6) 13_455 ?
Pr3 Sb8 3.2585(6) . ?
Pr3 Sb8 3.2585(6) 1_655 ?
Pr3 Ga1 3.3201(15) 1_655 ?
Pr3 Ga1 3.3201(15) . ?
Pr3 Sb2 3.3356(6) 1_655 ?
Pr3 Sb2 3.3356(6) 2 ?
Pr3 Sb2 3.3356(6) 2_655 ?
Pr3 Sb2 3.3356(6) . ?
Pr3 Sb6 3.3472(9) 5_544 ?
Pr3 Sb6 3.3472(9) 13 ?
Pr4 Sb5 3.2322(9) . ?
Pr4 Sb5 3.2322(9) 1_655 ?
Pr4 Sb4 3.2800(7) 14_545 ?
Pr4 Sb4 3.2800(7) 13 ?
Pr4 Sb1 3.3290(7) 1_655 ?
Pr4 Sb1 3.3290(7) 2 ?
Pr4 Sb1 3.3290(7) 2_655 ?
Pr4 Sb1 3.3290(7) . ?
Pr4 Ga3 3.3925(10) 13 ?
Pr4 Ga3 3.3925(10) 5_545 ?
Ga1 Sb2 2.6011(11) 2 ?
Ga1 Sb2 2.6011(11) . ?
Ga1 Sb5 2.620(2) . ?
Ga1 Pr2 3.2743(8) 13 ?
Ga1 Pr2 3.2743(8) 13_455 ?
Ga1 Pr2 3.2743(8) 14_445 ?
Ga1 Pr2 3.2743(8) 14_545 ?
Ga1 Pr3 3.3201(15) 1_455 ?
Ga2 Sb1 2.23(3) . ?
Ga2 Sb1 2.23(3) 10_556 ?
Ga2 Sb7 2.70(4) 13 ?
Ga2 Sb7 2.70(4) 13_455 ?
Ga2 Pr1 3.11(3) 10_556 ?
Ga3 Ga3 2.586(4) 9_565 ?
Ga3 Sb1 2.9020(7) 6_454 ?
Ga3 Sb1 2.9020(7) 13 ?
Ga3 Sb1 2.9020(7) 13_455 ?
Ga3 Sb1 2.9020(7) 6_554 ?
Ga3 Pr4 3.3925(10) 13 ?
Ga3 Pr4 3.3925(10) 5_454 ?
Sb1 Ga3 2.9020(7) 13 ?
Sb1 Ga3 2.9020(7) 13_455 ?
Sb1 Sb4 3.1296(7) 13_455 ?
Sb1 Sb4 3.1296(7) 13 ?
Sb1 Pr4 3.3290(7) 1_455 ?
Sb2 Pr1 3.2150(6) 13 ?
Sb2 Pr1 3.2150(6) 13_455 ?
Sb2 Pr2 3.3239(7) 13 ?
Sb2 Pr2 3.3239(7) 13_455 ?
Sb2 Pr3 3.3356(6) 1_455 ?
Sb3 Sb4 3.0085(7) 13 ?
Sb3 Sb4 3.0085(7) 13_455 ?
Sb3 Sb3 3.0844(9) 13_455 ?
Sb3 Sb3 3.0844(9) 13 ?
Sb3 Pr2 3.2966(7) 13_455 ?
Sb3 Pr2 3.2966(7) 13 ?
Sb4 Sb3 3.0085(7) 13 ?
Sb4 Sb3 3.0085(7) 13_455 ?
Sb4 Sb1 3.1296(7) 13_455 ?
Sb4 Sb1 3.1296(7) 13 ?
Sb4 Pr4 3.2800(7) 13 ?
Sb4 Pr1 3.3091(6) 13_455 ?
Sb4 Pr1 3.3091(6) 13 ?
Sb5 Pr4 3.2322(9) 1_455 ?
Sb5 Pr2 3.3287(6) 14_445 ?
Sb5 Pr2 3.3287(6) 13 ?
Sb5 Pr2 3.3287(6) 13_455 ?
Sb5 Pr2 3.3287(6) 14_545 ?
Sb6 Sb8 3.1088(7) 5 ?
Sb6 Sb8 3.1088(7) 5_455 ?
Sb6 Sb7 3.1095(10) 13_455 ?
Sb6 Sb7 3.1095(10) 13 ?
Sb6 Pr1 3.2365(8) 10_556 ?
Sb6 Pr3 3.3472(9) 5_455 ?
Sb6 Pr3 3.3472(9) 13 ?
Sb7 Ga2 2.70(4) 13 ?
Sb7 Ga2 2.70(4) 13_455 ?
Sb7 Sb6 3.1095(10) 13_455 ?
Sb7 Sb6 3.1095(10) 13 ?
Sb7 Pr1 3.2849(4) 6_454 ?
Sb7 Pr1 3.2849(4) 6_554 ?
Sb7 Pr1 3.2849(4) 13 ?
Sb7 Pr1 3.2849(4) 13_455 ?
Sb8 Sb6 3.1088(7) 13 ?
Sb8 Sb6 3.1088(7) 5_444 ?
Sb8 Sb6 3.1088(7) 13_455 ?
Sb8 Sb6 3.1088(7) 5_544 ?
Sb8 Pr3 3.2585(6) 9 ?
Sb8 Pr3 3.2585(6) 1_455 ?
Sb8 Pr3 3.2585(6) 9_655 ?
