#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/32/51/4325191.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4325191
loop_
_publ_author_name
'Su-Yun Zhang'
'Jiang-Gao Mao'
_publ_section_title
;
 Syntheses, Crystal Structures, Magnetic and Luminescent Properties of two
 Classes of Molybdenum(VI) Rich Quaternary Lanthanide Selenites
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4934
_journal_page_last               4943
_journal_paper_doi               10.1021/ic200149y
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         'H7 La4 Mo9.50 O46 Se4'
_chemical_formula_sum            'H7 La4 Mo9.5 O46 Se4'
_chemical_formula_weight         2525.97
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                95.908(7)
_cell_angle_beta                 95.323(6)
_cell_angle_gamma                90.022(9)
_cell_formula_units_Z            1
_cell_length_a                   6.980(2)
_cell_length_b                   7.349(3)
_cell_length_c                   18.123(6)
_cell_measurement_reflns_used    2171
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.2694
_cell_volume                     920.7(6)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.942
_diffrn_measured_fraction_theta_max 0.942
_diffrn_measurement_device_type  'Saturn70 (4x4 bin mode)'
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0305
_diffrn_reflns_av_sigmaI/netI    0.0551
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            5427
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.79
_diffrn_standards_decay_%        <1.0
_exptl_absorpt_coefficient_mu    11.736
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.7774
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    4.556
_exptl_crystal_description       prism
_exptl_crystal_F_000             1138
_exptl_crystal_size_max          0.13
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.02
_refine_diff_density_max         3.699
_refine_diff_density_min         -1.055
_refine_diff_density_rms         0.245
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.011
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     289
_refine_ls_number_reflns         3053
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.010
_refine_ls_R_factor_all          0.0406
_refine_ls_R_factor_gt           0.0313
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0305P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0675
_refine_ls_wR_factor_ref         0.0699
_reflns_number_gt                2503
_reflns_number_total             3053
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic200149y_si_002_1.cif
_cod_data_source_block           H3La4Mo9.5O32(SeO3)4(H2O)2
_cod_original_cell_volume        920.6(5)
_cod_original_formula_sum        'H7 La4 Mo9.50 O46 Se4'
_cod_database_code               4325191
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
La1 La 0.90526(7) 0.25848(6) 0.03333(3) 0.00642(13) Uani 1 1 d .
La2 La 0.95047(7) -0.16967(7) 0.30955(3) 0.00715(13) Uani 1 1 d .
Mo1 Mo 0.46359(11) 0.28214(11) 0.12941(4) 0.00986(19) Uani 1 1 d .
Mo2 Mo 0.47388(10) 0.06566(9) 0.27981(4) 0.00477(17) Uani 1 1 d .
Mo3 Mo 0.47539(10) -0.42166(10) 0.27902(4) 0.00557(17) Uani 1 1 d .
Mo4 Mo 0.30194(14) -0.38005(13) 0.47578(5) 0.0055(2) Uani 0.75 1 d P
Mo5 Mo 0.69333(10) -0.12002(10) 0.51993(4) 0.00752(18) Uani 1 1 d .
Se1 Se 1.22986(12) 0.22538(11) -0.09563(5) 0.00651(19) Uani 1 1 d .
Se2 Se 0.90095(12) 0.31471(11) 0.25066(5) 0.00693(19) Uani 1 1 d .
O1 O 1.0806(9) 0.2031(8) -0.1752(3) 0.0150(15) Uani 1 1 d .
O2 O 1.1307(8) 0.4114(7) -0.0468(3) 0.0086(13) Uani 1 1 d U
O3 O 1.1325(8) 0.0663(7) -0.0469(3) 0.0105(13) Uani 1 1 d .
O4 O 0.7927(8) 0.5125(7) 0.2852(3) 0.0107(13) Uani 1 1 d .
O5 O 0.7979(8) 0.2905(8) 0.1609(3) 0.0090(13) Uani 1 1 d .
O6 O 0.7932(8) 0.1382(8) 0.2873(3) 0.0105(13) Uani 1 1 d .
O7 O 0.5058(8) 0.5342(7) 0.1619(3) 0.0074(13) Uani 1 1 d .
O8 O 0.5448(8) 0.2591(8) 0.0409(3) 0.0135(14) Uani 1 1 d .
O9 O 0.2148(8) 0.2792(8) 0.1125(3) 0.0130(14) Uani 1 1 d .
O10 O 0.4497(8) 0.3156(7) 0.2539(3) 0.0085(13) Uani 1 1 d .
O11 O 0.5050(8) 0.0476(8) 0.1626(3) 0.0104(13) Uani 1 1 d .
O12 O 0.4916(8) 0.1140(8) 0.3746(3) 0.0105(13) Uani 1 1 d .
O13 O 0.2354(8) 0.0015(8) 0.2636(3) 0.0102(13) Uani 1 1 d .
O14 O 0.5867(8) -0.1787(8) 0.2763(3) 0.0102(13) Uani 1 1 d .
O15 O 0.2376(8) -0.3638(8) 0.2623(3) 0.0104(13) Uani 1 1 d .
O16 O 0.4959(8) -0.4269(8) 0.3737(3) 0.0110(13) Uani 1 1 d .
O17 O 0.1180(9) -0.3678(9) 0.4048(3) 0.0176(15) Uani 1 1 d .
O18 O 0.1774(11) -0.3564(10) 0.5521(4) 0.036(2) Uani 1 1 d .
O19 O 0.6210(10) -0.3664(8) 0.5244(4) 0.0203(16) Uani 1 1 d .
O20 O 0.5985(8) 0.1307(8) 0.5261(3) 0.0123(14) Uani 1 1 d .
O21 O 0.8008(8) -0.1352(8) 0.4376(3) 0.0131(14) Uani 1 1 d .
O22 O 0.8778(8) -0.0719(9) 0.5898(3) 0.0157(15) Uani 1 1 d .
O1W O 0.7491(9) 0.2281(9) -0.0992(3) 0.0206(16) Uani 1 1 d .
H1WA H 0.8358 0.2209 -0.1294 0.031 Uiso 1 1 d R
H1WB H 0.6792 0.1321 -0.1067 0.031 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
La La -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 La1 O3 162.49(19) 2_765 2_755
O2 La1 O9 91.95(19) 2_765 1_655
O3 La1 O9 92.3(2) 2_755 1_655
O2 La1 O5 82.28(19) 2_765 .
O3 La1 O5 82.03(19) 2_755 .
O9 La1 O5 77.81(19) 1_655 .
O2 La1 O8 83.41(18) 2_765 .
O3 La1 O8 82.78(19) 2_755 .
O9 La1 O8 141.9(2) 1_655 .
O5 La1 O8 64.09(19) . .
O2 La1 O1W 92.6(2) 2_765 .
O3 La1 O1W 93.6(2) 2_755 .
O9 La1 O1W 145.0(2) 1_655 .
O5 La1 O1W 137.2(2) . .
O8 La1 O1W 73.1(2) . .
O2 La1 O2 69.0(2) 2_765 .
O3 La1 O2 128.54(18) 2_755 .
O9 La1 O2 77.0(2) 1_655 .
O5 La1 O2 140.71(18) . .
O8 La1 O2 134.07(19) . .
O1W La1 O2 72.37(19) . .
O2 La1 O3 128.00(19) 2_765 .
O3 La1 O3 69.5(2) 2_755 .
O9 La1 O3 76.96(19) 1_655 .
O5 La1 O3 140.75(19) . .
O8 La1 O3 134.09(19) . .
O1W La1 O3 73.02(19) . .
O2 La1 O3 59.04(17) . .
O2 La1 Se1 98.70(13) 2_765 .
O3 La1 Se1 98.80(13) 2_755 .
O9 La1 Se1 78.01(15) 1_655 .
O5 La1 Se1 155.82(13) . .
O8 La1 Se1 140.09(14) . .
O1W La1 Se1 67.03(15) . .
O2 La1 Se1 29.87(12) . .
O3 La1 Se1 29.45(13) . .
O2 La1 Mo1 81.66(13) 2_765 .
O3 La1 Mo1 81.28(13) 2_755 .
O9 La1 Mo1 117.00(15) 1_655 .
O5 La1 Mo1 39.19(13) . .
O8 La1 Mo1 24.91(13) . .
O1W La1 Mo1 97.97(15) . .
O2 La1 Mo1 148.22(12) . .
O3 La1 Mo1 148.44(13) . .
Se1 La1 Mo1 164.99(2) . .
O2 La1 La1 35.59(13) 2_765 2_765
O3 La1 La1 161.91(14) 2_755 2_765
O9 La1 La1 83.12(15) 1_655 2_765
O5 La1 La1 113.80(13) . 2_765
O8 La1 La1 111.48(14) . 2_765
O1W La1 La1 80.66(15) . 2_765
O2 La1 La1 33.37(12) . 2_765
O3 La1 La1 92.41(13) . 2_765
Se1 La1 La1 63.15(2) . 2_765
Mo1 La1 La1 116.40(2) . 2_765
O2 La1 La1 161.69(13) 2_765 2_755
O3 La1 La1 35.81(13) 2_755 2_755
O9 La1 La1 83.27(14) 1_655 2_755
O5 La1 La1 113.68(13) . 2_755
O8 La1 La1 111.11(13) . 2_755
O1W La1 La1 81.67(15) . 2_755
O2 La1 La1 92.73(12) . 2_755
O3 La1 La1 33.69(13) . 2_755
Se1 La1 La1 63.04(2) . 2_755
Mo1 La1 La1 116.26(2) . 2_755
La1 La1 La1 126.10(3) 2_765 2_755
O1 La2 O14 76.69(19) 2_755 .
O1 La2 O4 80.4(2) 2_755 1_545
O14 La2 O4 63.66(18) . 1_545
O1 La2 O6 81.01(19) 2_755 .
O14 La2 O6 64.11(18) . .
O4 La2 O6 127.22(18) 1_545 .
O1 La2 O17 131.7(2) 2_755 1_655
O14 La2 O17 122.4(2) . 1_655
O4 La2 O17 73.00(19) 1_545 1_655
O6 La2 O17 146.71(19) . 1_655
O1 La2 O13 71.23(19) 2_755 1_655
O14 La2 O13 134.38(18) . 1_655
O4 La2 O13 137.48(18) 1_545 1_655
O6 La2 O13 79.34(18) . 1_655
O17 La2 O13 103.17(19) 1_655 1_655
O1 La2 O22 133.5(2) 2_755 2_756
O14 La2 O22 123.01(18) . 2_756
O4 La2 O22 145.4(2) 1_545 2_756
O6 La2 O22 74.07(19) . 2_756
O17 La2 O22 76.82(19) 1_655 2_756
O13 La2 O22 65.99(19) 1_655 2_756
O1 La2 O15 71.01(19) 2_755 1_655
O14 La2 O15 134.23(17) . 1_655
O4 La2 O15 79.45(18) 1_545 1_655
O6 La2 O15 137.51(19) . 1_655
O17 La2 O15 65.02(19) 1_655 1_655
O13 La2 O15 61.89(18) 1_655 1_655
O22 La2 O15 102.75(18) 2_756 1_655
O1 La2 O21 151.47(19) 2_755 .
O14 La2 O21 74.79(18) . .
O4 La2 O21 87.46(19) 1_545 .
O6 La2 O21 86.15(19) . .
O17 La2 O21 67.00(19) 1_655 .
O13 La2 O21 131.13(18) 1_655 .
O22 La2 O21 65.17(19) 2_756 .
O15 La2 O21 132.02(19) 1_655 .
O9 Mo1 O8 104.2(3) . .
O9 Mo1 O11 100.5(3) . .
O8 Mo1 O11 103.5(3) . .
O9 Mo1 O7 99.9(3) . .
O8 Mo1 O7 103.3(3) . .
O11 Mo1 O7 140.9(2) . .
O9 Mo1 O10 92.3(3) . .
O8 Mo1 O10 163.5(2) . .
O11 Mo1 O10 73.2(2) . .
O7 Mo1 O10 73.0(2) . .
O9 Mo1 O5 176.1(2) . .
O8 Mo1 O5 79.7(2) . .
O11 Mo1 O5 78.8(2) . .
O7 Mo1 O5 78.6(2) . .
O10 Mo1 O5 83.9(2) . .
O9 Mo1 La1 141.9(2) . .
O8 Mo1 La1 37.74(18) . .
O11 Mo1 La1 92.29(18) . .
O7 Mo1 La1 91.81(17) . .
O10 Mo1 La1 125.80(14) . .
O5 Mo1 La1 41.93(14) . .
O12 Mo2 O13 100.1(3) . .
O12 Mo2 O10 97.8(3) . .
O13 Mo2 O10 98.4(3) . .
O12 Mo2 O14 97.8(3) . .
O13 Mo2 O14 98.4(3) . .
O10 Mo2 O14 154.6(2) . .
O12 Mo2 O11 167.1(3) . .
O13 Mo2 O11 91.6(2) . .
O10 Mo2 O11 74.9(2) . .
O14 Mo2 O11 85.8(2) . .
O12 Mo2 O6 86.4(2) . .
O13 Mo2 O6 173.3(2) . .
O10 Mo2 O6 81.8(2) . .
O14 Mo2 O6 79.4(2) . .
O11 Mo2 O6 82.0(2) . .
O16 Mo3 O15 101.4(3) . .
O16 Mo3 O10 96.2(3) . 1_545
O15 Mo3 O10 98.6(3) . 1_545
O16 Mo3 O14 98.3(3) . .
O15 Mo3 O14 97.6(3) . .
O10 Mo3 O14 155.7(2) 1_545 .
O16 Mo3 O7 165.5(2) . 1_545
O15 Mo3 O7 91.4(2) . 1_545
O10 Mo3 O7 74.8(2) 1_545 1_545
O14 Mo3 O7 86.8(2) . 1_545
O16 Mo3 O4 86.1(2) . 1_545
O15 Mo3 O4 172.2(3) . 1_545
O10 Mo3 O4 82.4(2) 1_545 1_545
O14 Mo3 O4 79.2(2) . 1_545
O7 Mo3 O4 81.4(2) 1_545 1_545
O18 Mo4 O17 101.3(3) . .
O18 Mo4 O19 100.5(3) . 2_646
O17 Mo4 O19 107.9(3) . 2_646
O18 Mo4 O20 101.8(3) . 2_656
O17 Mo4 O20 96.1(3) . 2_656
O19 Mo4 O20 143.1(3) 2_646 2_656
O18 Mo4 O19 103.9(3) . .
O17 Mo4 O19 153.5(3) . .
O19 Mo4 O19 75.3(3) 2_646 .
O20 Mo4 O19 71.0(2) 2_656 .
O18 Mo4 O16 175.4(3) . .
O17 Mo4 O16 82.8(3) . .
O19 Mo4 O16 76.1(2) 2_646 .
O20 Mo4 O16 79.7(2) 2_656 .
O19 Mo4 O16 72.4(2) . .
O21 Mo5 O22 105.6(3) . .
O21 Mo5 O19 101.5(3) . .
O22 Mo5 O19 106.1(3) . .
O21 Mo5 O20 101.7(3) . .
O22 Mo5 O20 94.1(3) . .
O19 Mo5 O20 143.7(3) . .
O21 Mo5 O20 98.2(3) . 2_656
O22 Mo5 O20 154.8(3) . 2_656
O19 Mo5 O20 76.7(3) . 2_656
O20 Mo5 O20 72.6(3) . 2_656
O21 Mo5 O12 172.9(2) . 2_656
O22 Mo5 O12 81.4(2) . 2_656
O19 Mo5 O12 74.9(2) . 2_656
O20 Mo5 O12 78.7(2) . 2_656
O20 Mo5 O12 75.1(2) 2_656 2_656
O1 Se1 O3 100.7(3) . .
O1 Se1 O2 101.2(3) . .
O3 Se1 O2 94.9(3) . .
O1 Se1 La1 100.6(2) . .
O3 Se1 La1 47.71(18) . .
O2 Se1 La1 47.68(19) . .
O5 Se2 O6 101.4(3) . .
O5 Se2 O4 100.8(3) . .
O6 Se2 O4 106.2(3) . .
Se1 O1 La2 147.3(3) . 2_755
Se1 O2 La1 146.0(3) . 2_765
Se1 O2 La1 102.5(2) . .
La1 O2 La1 111.0(2) 2_765 .
Se1 O3 La1 146.1(3) . 2_755
Se1 O3 La1 102.8(2) . .
La1 O3 La1 110.5(2) 2_755 .
Se2 O4 Mo3 128.2(3) . 1_565
Se2 O4 La2 125.9(3) . 1_565
Mo3 O4 La2 102.4(2) 1_565 1_565
Se2 O5 Mo1 123.4(3) . .
Se2 O5 La1 137.7(3) . .
Mo1 O5 La1 98.89(19) . .
Se2 O6 Mo2 128.2(3) . .
Se2 O6 La2 125.2(3) . .
Mo2 O6 La2 101.9(2) . .
Mo1 O7 Mo3 108.9(3) . 1_565
Mo1 O8 La1 117.3(3) . .
Mo1 O9 La1 155.1(3) . 1_455
Mo3 O10 Mo2 151.6(3) 1_565 .
Mo3 O10 Mo1 103.1(3) 1_565 .
Mo2 O10 Mo1 102.8(2) . .
Mo1 O11 Mo2 108.8(3) . .
Mo2 O12 Mo5 142.2(3) . 2_656
Mo2 O13 La2 146.6(3) . 1_455
Mo3 O14 Mo2 132.4(3) . .
Mo3 O14 La2 112.6(2) . .
Mo2 O14 La2 112.7(2) . .
Mo3 O15 La2 146.5(3) . 1_455
Mo3 O16 Mo4 139.3(3) . .
Mo4 O17 La2 146.2(4) . 1_455
Mo5 O19 Mo4 148.1(4) . 2_646
Mo5 O19 Mo4 103.8(3) . .
Mo4 O19 Mo4 104.7(3) 2_646 .
Mo5 O20 Mo4 138.8(3) . 2_656
Mo5 O20 Mo5 107.4(3) . 2_656
Mo4 O20 Mo5 108.5(3) 2_656 2_656
Mo5 O21 La2 177.1(3) . .
Mo5 O22 La2 147.7(3) . 2_756
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
La1 O2 2.429(6) 2_765
La1 O3 2.442(6) 2_755
La1 O9 2.476(6) 1_655
La1 O5 2.485(6) .
La1 O8 2.532(6) .
La1 O1W 2.532(6) .
La1 O2 2.570(6) .
La1 O3 2.575(6) .
La1 Se1 3.3942(13) .
La1 Mo1 3.6741(13) .
La1 La1 4.1213(15) 2_765
La1 La1 4.1227(15) 2_755
La2 O1 2.411(6) 2_755
La2 O14 2.554(6) .
La2 O4 2.561(6) 1_545
La2 O6 2.568(6) .
La2 O17 2.572(6) 1_655
La2 O13 2.599(6) 1_655
La2 O22 2.616(6) 2_756
La2 O15 2.618(6) 1_655
La2 O21 2.621(6) .
Mo1 O9 1.735(6) .
Mo1 O8 1.742(6) .
Mo1 O11 1.897(6) .
Mo1 O7 1.900(5) .
Mo1 O10 2.255(6) .
Mo1 O5 2.350(6) .
Mo2 O12 1.710(6) .
Mo2 O13 1.720(6) .
Mo2 O10 1.946(6) .
Mo2 O14 1.959(6) .
Mo2 O11 2.146(6) .
Mo2 O6 2.280(6) .
Mo3 O16 1.713(6) .
Mo3 O15 1.721(5) .
Mo3 O10 1.942(5) 1_545
Mo3 O14 1.954(6) .
Mo3 O7 2.144(6) 1_545
Mo3 O4 2.262(6) 1_545
Mo4 O18 1.695(8) .
Mo4 O17 1.740(6) .
Mo4 O19 1.939(6) 2_646
Mo4 O20 1.964(6) 2_656
Mo4 O19 2.316(7) .
Mo4 O16 2.389(6) .
Mo5 O21 1.724(6) .
Mo5 O22 1.729(6) .
Mo5 O19 1.891(6) .
Mo5 O20 1.954(6) .
Mo5 O20 2.126(6) 2_656
Mo5 O12 2.401(6) 2_656
Se1 O1 1.692(6) .
Se1 O3 1.712(6) .
Se1 O2 1.731(5) .
Se2 O5 1.708(5) .
Se2 O6 1.720(6) .
Se2 O4 1.725(5) .
O1 La2 2.411(6) 2_755
O2 La1 2.429(6) 2_765
O3 La1 2.442(6) 2_755
O4 Mo3 2.262(6) 1_565
O4 La2 2.561(6) 1_565
O7 Mo3 2.144(6) 1_565
O9 La1 2.476(6) 1_455
O10 Mo3 1.942(5) 1_565
O12 Mo5 2.401(6) 2_656
O13 La2 2.599(6) 1_455
O15 La2 2.618(6) 1_455
O17 La2 2.572(6) 1_455
O19 Mo4 1.939(6) 2_646
O20 Mo4 1.964(6) 2_656
O20 Mo5 2.126(6) 2_656
O22 La2 2.616(6) 2_756
