#------------------------------------------------------------------------------
#$Date: 2016-03-23 20:26:43 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179412 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/09/4330957.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4330957
loop_
_publ_author_name
'Jian Lin'
'Justin N. Cross'
'Juan Diwu'
'Matthew J. Polinski'
'Eric M. Villa'
'Thomas E. Albrecht-Schmitt'
_publ_section_title
;
 Unusual Coordination for Plutonium(IV), Cerium(IV), and Zirconium(IV) in
 the Cationic Layered Materials [M2Te4O11]X2 (M = Pu, Ce, Zr; X = Cl, Br)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11949
_journal_page_last               11954
_journal_paper_doi               10.1021/ic301846g
_journal_volume                  51
_journal_year                    2012
_chemical_formula_moiety         '[Zr2Te4O11]Cl2'
_chemical_formula_sum            'Cl2 O11 Te4 Zr2'
_chemical_formula_weight         939.74
_chemical_name_common            'Zirconium tellurite chloride'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   none
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.031(2)
_cell_angle_beta                 107.958(2)
_cell_angle_gamma                98.476(2)
_cell_formula_units_Z            2
_cell_length_a                   7.7986(11)
_cell_length_b                   9.4173(13)
_cell_length_c                   10.3257(15)
_cell_measurement_reflns_used    2989
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.570
_cell_measurement_theta_min      1.083
_cell_volume                     644.28(16)
_computing_cell_refinement       'smart saint'
_computing_data_collection       smart
_computing_data_reduction        SAINT
_computing_molecular_graphics    'SHELXP-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXCIF-97 (Sheldrick, 2000)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'BRUKER apex II'
_diffrn_measurement_method       '0.5 wide w/ exposures'
_diffrn_radiation_monochromator  'Quazar optics'
_diffrn_radiation_source         'Imus microfocused'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0382
_diffrn_reflns_av_sigmaI/netI    0.0496
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            7683
_diffrn_reflns_theta_full        27.57
_diffrn_reflns_theta_max         27.57
_diffrn_reflns_theta_min         2.30
_exptl_absorpt_coefficient_mu    10.956
_exptl_absorpt_correction_T_max  0.947
_exptl_absorpt_correction_T_min  0.681
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   SHELTXPREP
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    4.844
_exptl_crystal_density_meas      ?
_exptl_crystal_description       Tablet
_exptl_crystal_F_000             820
_exptl_crystal_size_max          0.050
_exptl_crystal_size_mid          0.030
_exptl_crystal_size_min          0.005
_refine_diff_density_max         4.146
_refine_diff_density_min         -2.008
_refine_diff_density_rms         0.365
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     172
_refine_ls_number_reflns         2941
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.083
_refine_ls_R_factor_all          0.0589
_refine_ls_R_factor_gt           0.0423
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0416P)²+1.2055P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0936
_refine_ls_wR_factor_ref         0.1023
_reflns_number_gt                2285
_reflns_number_total             2941
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic301846g_si_002_3.cif
_cod_data_source_block           '[Zr2Te4O11]Cl2'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'N/A' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               4330957
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
Zr1 Zr 0.37552(12) 0.11280(10) 0.11145(9) 0.0118(2) Uani 1 1 d
Zr2 Zr 0.11586(11) 0.38646(10) 0.38049(9) 0.0117(2) Uani 1 1 d
Te2 Te -0.25869(8) 0.49552(7) 0.21013(7) 0.01359(16) Uani 1 1 d
Te4 Te 0.00778(8) 0.26507(7) -0.00184(7) 0.01333(16) Uani 1 1 d
Te3 Te 0.21813(9) 0.02203(7) -0.26393(6) 0.01420(16) Uani 1 1 d
Te1 Te 0.52021(8) 0.23584(7) 0.52941(6) 0.01227(16) Uani 1 1 d
Cl2 Cl -0.1066(4) 0.1203(3) -0.3716(3) 0.0320(7) Uani 1 1 d
Cl1 Cl 0.3681(4) 0.6110(3) 0.1107(3) 0.0305(6) Uani 1 1 d
O3 O 0.4979(11) 0.1414(9) 0.3315(8) 0.037(2) Uani 1 1 d
O2 O 0.3286(10) 0.3314(9) 0.5145(9) 0.0332(19) Uani 1 1 d
O9 O 0.4100(8) 0.0070(8) -0.1075(7) 0.0205(16) Uani 1 1 d
O8 O 0.1738(9) 0.1346(8) -0.0820(7) 0.0189(15) Uani 1 1 d
O5 O -0.0726(9) 0.3889(8) 0.1685(7) 0.0234(16) Uani 1 1 d
O11 O 0.1810(9) 0.2583(8) 0.1763(7) 0.0185(15) Uani 1 1 d
O6 O -0.1102(8) 0.5052(8) 0.4003(7) 0.0194(15) Uani 1 1 d
O1 O 0.7108(9) 0.4141(7) 0.5890(7) 0.0215(15) Uani 1 1 d
O4 O -0.4470(8) 0.3224(7) 0.1600(7) 0.0178(15) Uani 1 1 d
O10 O -0.1778(8) 0.0855(7) -0.0614(7) 0.0177(14) Uani 1 1 d
O7 O 0.0620(8) -0.1750(7) -0.3278(7) 0.0167(14) Uani 1 1 d
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Te Te -0.5308 1.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zr Zr -2.9673 0.5597 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O10 Zr1 O4 174.3(2) 2 1_655
O10 Zr1 O3 90.3(3) 2 .
O4 Zr1 O3 91.6(3) 1_655 .
O10 Zr1 O9 93.1(2) 2 2_655
O4 Zr1 O9 92.6(2) 1_655 2_655
O3 Zr1 O9 76.3(3) . 2_655
O10 Zr1 O8 87.6(3) 2 .
O4 Zr1 O8 88.5(3) 1_655 .
O3 Zr1 O8 156.6(3) . .
O9 Zr1 O8 127.0(2) 2_655 .
O10 Zr1 O9 93.4(2) 2 .
O4 Zr1 O9 88.7(2) 1_655 .
O3 Zr1 O9 139.2(3) . .
O9 Zr1 O9 62.9(3) 2_655 .
O8 Zr1 O9 64.2(2) . .
O10 Zr1 O11 88.7(2) 2 .
O4 Zr1 O11 85.9(2) 1_655 .
O3 Zr1 O11 90.1(3) . .
O9 Zr1 O11 166.3(2) 2_655 .
O8 Zr1 O11 66.6(2) . .
O9 Zr1 O11 130.6(2) . .
O10 Zr1 Te3 88.62(18) 2 .
O4 Zr1 Te3 90.44(18) 1_655 .
O3 Zr1 Te3 170.2(2) . .
O9 Zr1 Te3 94.08(17) 2_655 .
O8 Zr1 Te3 32.96(15) . .
O9 Zr1 Te3 31.33(15) . .
O11 Zr1 Te3 99.59(16) . .
O1 Zr2 O7 174.2(2) 2_666 2
O1 Zr2 O2 93.7(3) 2_666 .
O7 Zr2 O2 88.4(3) 2 .
O1 Zr2 O6 92.7(3) 2_666 2_566
O7 Zr2 O6 93.0(2) 2 2_566
O2 Zr2 O6 76.3(3) . 2_566
O1 Zr2 O5 86.2(3) 2_666 .
O7 Zr2 O5 89.8(3) 2 .
O2 Zr2 O5 157.0(3) . .
O6 Zr2 O5 126.7(2) 2_566 .
O1 Zr2 O6 91.7(2) 2_666 .
O7 Zr2 O6 90.3(2) 2 .
O2 Zr2 O6 138.8(3) . .
O6 Zr2 O6 62.7(3) 2_566 .
O5 Zr2 O6 64.1(2) . .
O1 Zr2 O11 86.9(2) 2_666 .
O7 Zr2 O11 87.6(2) 2 .
O2 Zr2 O11 90.6(3) . .
O6 Zr2 O11 166.8(2) 2_566 .
O5 Zr2 O11 66.5(2) . .
O6 Zr2 O11 130.5(2) . .
O1 Zr2 Te2 89.02(19) 2_666 .
O7 Zr2 Te2 89.87(17) 2 .
O2 Zr2 Te2 170.2(2) . .
O6 Zr2 Te2 94.19(17) 2_566 .
O5 Zr2 Te2 32.58(16) . .
O6 Zr2 Te2 31.51(15) . .
O11 Zr2 Te2 99.02(16) . .
O4 Te2 O6 95.4(3) . .
O4 Te2 O5 98.8(3) . .
O6 Te2 O5 76.1(3) . .
O4 Te2 Zr2 98.8(2) . .
O6 Te2 Zr2 37.92(19) . .
O5 Te2 Zr2 38.20(19) . .
O10 Te4 O11 97.7(3) . .
O10 Te4 O5 90.9(3) . .
O11 Te4 O5 76.1(3) . .
O10 Te4 O8 91.9(3) . .
O11 Te4 O8 76.2(2) . .
O5 Te4 O8 152.2(3) . .
O7 Te3 O9 94.8(3) . .
O7 Te3 O8 98.9(3) . .
O9 Te3 O8 75.8(3) . .
O7 Te3 Zr1 96.1(2) . .
O9 Te3 Zr1 37.83(19) . .
O8 Te3 Zr1 38.14(17) . .
O1 Te1 O2 96.5(3) . .
O1 Te1 O3 96.4(3) . .
O2 Te1 O3 102.5(4) . .
Te1 O3 Zr1 148.5(5) . .
Te1 O2 Zr2 148.1(5) . .
Te3 O9 Zr1 131.7(3) . 2_655
Te3 O9 Zr1 110.8(3) . .
Zr1 O9 Zr1 117.1(3) 2_655 .
Te3 O8 Te4 143.6(3) . .
Te3 O8 Zr1 108.9(3) . .
Te4 O8 Zr1 107.5(3) . .
Te2 O5 Te4 143.4(3) . .
Te2 O5 Zr2 109.2(3) . .
Te4 O5 Zr2 107.2(3) . .
Te4 O11 Zr2 110.2(3) . .
Te4 O11 Zr1 109.7(3) . .
Zr2 O11 Zr1 139.9(3) . .
Te2 O6 Zr2 132.1(3) . 2_566
Te2 O6 Zr2 110.6(3) . .
Zr2 O6 Zr2 117.3(3) 2_566 .
Te1 O1 Zr2 168.6(4) . 2_666
Te2 O4 Zr1 170.9(4) . 1_455
Te4 O10 Zr1 175.6(4) . 2
Te3 O7 Zr2 174.6(4) . 2
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Zr1 O10 2.025(6) 2
Zr1 O4 2.030(6) 1_655
Zr1 O3 2.072(7) .
Zr1 O9 2.154(6) 2_655
Zr1 O8 2.227(6) .
Zr1 O9 2.239(6) .
Zr1 O11 2.282(6) .
Zr1 Te3 3.4118(12) .
Zr2 O1 2.005(6) 2_666
Zr2 O7 2.032(6) 2
Zr2 O2 2.071(7) .
Zr2 O6 2.141(6) 2_566
Zr2 O5 2.240(6) .
Zr2 O6 2.245(6) .
Zr2 O11 2.274(6) .
Zr2 Te2 3.4197(11) .
Te2 O4 1.817(6) .
Te2 O6 1.909(6) .
Te2 O5 1.950(6) .
Te4 O10 1.821(6) .
Te4 O11 1.947(6) .
Te4 O5 2.066(6) .
Te4 O8 2.067(6) .
Te3 O7 1.822(6) .
Te3 O9 1.898(6) .
Te3 O8 1.962(6) .
Te1 O1 1.834(6) .
Te1 O2 1.849(7) .
Te1 O3 1.851(7) .
O9 Zr1 2.154(6) 2_655
O6 Zr2 2.141(6) 2_566
O1 Zr2 2.005(6) 2_666
O4 Zr1 2.030(6) 1_455
O10 Zr1 2.025(6) 2
O7 Zr2 2.032(6) 2
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 Zr2 Te2 O4 177.6(3) 2_666 .
O7 Zr2 Te2 O4 3.2(3) 2 .
O2 Zr2 Te2 O4 -76.5(12) . .
O6 Zr2 Te2 O4 -89.8(3) 2_566 .
O5 Zr2 Te2 O4 93.1(4) . .
O6 Zr2 Te2 O4 -87.6(4) . .
O11 Zr2 Te2 O4 90.8(3) . .
O1 Zr2 Te2 O6 -94.8(4) 2_666 .
O7 Zr2 Te2 O6 90.8(4) 2 .
O2 Zr2 Te2 O6 11.1(13) . .
O6 Zr2 Te2 O6 -2.2(5) 2_566 .
O5 Zr2 Te2 O6 -179.3(5) . .
O11 Zr2 Te2 O6 178.4(4) . .
O1 Zr2 Te2 O5 84.5(4) 2_666 .
O7 Zr2 Te2 O5 -89.9(4) 2 .
O2 Zr2 Te2 O5 -169.6(12) . .
O6 Zr2 Te2 O5 177.1(4) 2_566 .
O6 Zr2 Te2 O5 179.3(5) . .
O11 Zr2 Te2 O5 -2.3(4) . .
O10 Zr1 Te3 O7 -8.9(3) 2 .
O4 Zr1 Te3 O7 176.8(3) 1_655 .
O3 Zr1 Te3 O7 74.7(13) . .
O9 Zr1 Te3 O7 84.1(3) 2_655 .
O8 Zr1 Te3 O7 -96.6(4) . .
O9 Zr1 Te3 O7 90.0(4) . .
O11 Zr1 Te3 O7 -97.3(3) . .
O10 Zr1 Te3 O9 -98.9(4) 2 .
O4 Zr1 Te3 O9 86.8(4) 1_655 .
O3 Zr1 Te3 O9 -15.3(13) . .
O9 Zr1 Te3 O9 -5.8(5) 2_655 .
O8 Zr1 Te3 O9 173.4(4) . .
O11 Zr1 Te3 O9 172.7(4) . .
O10 Zr1 Te3 O8 87.8(4) 2 .
O4 Zr1 Te3 O8 -86.6(4) 1_655 .
O3 Zr1 Te3 O8 171.3(13) . .
O9 Zr1 Te3 O8 -179.2(4) 2_655 .
O9 Zr1 Te3 O8 -173.4(4) . .
O11 Zr1 Te3 O8 -0.7(4) . .
O1 Te1 O3 Zr1 -89.0(8) . .
O2 Te1 O3 Zr1 9.2(9) . .
O10 Zr1 O3 Te1 -95.5(8) 2 .
O4 Zr1 O3 Te1 79.1(8) 1_655 .
O9 Zr1 O3 Te1 171.4(9) 2_655 .
O8 Zr1 O3 Te1 -10.9(13) . .
O9 Zr1 O3 Te1 169.0(6) . .
O11 Zr1 O3 Te1 -6.8(8) . .
Te3 Zr1 O3 Te1 -178.9(5) . .
O1 Te1 O2 Zr2 93.3(8) . .
O3 Te1 O2 Zr2 -4.7(9) . .
O1 Zr2 O2 Te1 -86.1(8) 2_666 .
O7 Zr2 O2 Te1 88.5(8) 2 .
O6 Zr2 O2 Te1 -178.0(8) 2_566 .
O5 Zr2 O2 Te1 2.8(13) . .
O6 Zr2 O2 Te1 177.2(6) . .
O11 Zr2 O2 Te1 0.9(8) . .
Te2 Zr2 O2 Te1 168.4(5) . .
O7 Te3 O9 Zr1 78.4(5) . 2_655
O8 Te3 O9 Zr1 176.4(5) . 2_655
Zr1 Te3 O9 Zr1 172.2(7) . 2_655
O7 Te3 O9 Zr1 -93.8(3) . .
O8 Te3 O9 Zr1 4.2(3) . .
O10 Zr1 O9 Te3 81.7(3) 2 .
O4 Zr1 O9 Te3 -93.0(3) 1_655 .
O3 Zr1 O9 Te3 176.1(3) . .
O9 Zr1 O9 Te3 173.5(6) 2_655 .
O8 Zr1 O9 Te3 -4.0(3) . .
O11 Zr1 O9 Te3 -9.5(5) . .
O10 Zr1 O9 Zr1 -91.7(3) 2 2_655
O4 Zr1 O9 Zr1 93.6(3) 1_655 2_655
O3 Zr1 O9 Zr1 2.6(6) . 2_655
O9 Zr1 O9 Zr1 0.0 2_655 2_655
O8 Zr1 O9 Zr1 -177.4(4) . 2_655
O11 Zr1 O9 Zr1 177.1(2) . 2_655
Te3 Zr1 O9 Zr1 -173.5(6) . 2_655
O7 Te3 O8 Te4 -90.6(6) . .
O9 Te3 O8 Te4 176.6(7) . .
Zr1 Te3 O8 Te4 -179.2(8) . .
O7 Te3 O8 Zr1 88.6(3) . .
O9 Te3 O8 Zr1 -4.2(3) . .
O10 Te4 O8 Te3 83.1(6) . .
O11 Te4 O8 Te3 -179.4(7) . .
O5 Te4 O8 Te3 178.7(5) . .
O10 Te4 O8 Zr1 -96.1(3) . .
O11 Te4 O8 Zr1 1.4(3) . .
O5 Te4 O8 Zr1 -0.5(8) . .
O10 Zr1 O8 Te3 -91.1(3) 2 .
O4 Zr1 O8 Te3 93.1(3) 1_655 .
O3 Zr1 O8 Te3 -176.3(5) . .
O9 Zr1 O8 Te3 1.0(5) 2_655 .
O9 Zr1 O8 Te3 3.8(3) . .
O11 Zr1 O8 Te3 179.3(4) . .
O10 Zr1 O8 Te4 88.4(3) 2 .
O4 Zr1 O8 Te4 -87.4(3) 1_655 .
O3 Zr1 O8 Te4 3.2(8) . .
O9 Zr1 O8 Te4 -179.5(2) 2_655 .
O9 Zr1 O8 Te4 -176.7(4) . .
O11 Zr1 O8 Te4 -1.2(2) . .
Te3 Zr1 O8 Te4 179.5(5) . .
O4 Te2 O5 Te4 82.0(7) . .
O6 Te2 O5 Te4 175.5(7) . .
Zr2 Te2 O5 Te4 175.0(9) . .
O4 Te2 O5 Zr2 -93.0(3) . .
O6 Te2 O5 Zr2 0.5(3) . .
O10 Te4 O5 Te2 -78.1(7) . .
O11 Te4 O5 Te2 -175.8(7) . .
O8 Te4 O5 Te2 -173.9(4) . .
O10 Te4 O5 Zr2 97.0(3) . .
O11 Te4 O5 Zr2 -0.7(3) . .
O8 Te4 O5 Zr2 1.1(8) . .
O1 Zr2 O5 Te2 -94.1(3) 2_666 .
O7 Zr2 O5 Te2 90.0(3) 2 .
O2 Zr2 O5 Te2 175.5(5) . .
O6 Zr2 O5 Te2 -3.6(5) 2_566 .
O6 Zr2 O5 Te2 -0.4(3) . .
O11 Zr2 O5 Te2 177.5(4) . .
O1 Zr2 O5 Te4 89.0(3) 2_666 .
O7 Zr2 O5 Te4 -86.9(3) 2 .
O2 Zr2 O5 Te4 -1.4(9) . .
O6 Zr2 O5 Te4 179.5(2) 2_566 .
O6 Zr2 O5 Te4 -177.3(4) . .
O11 Zr2 O5 Te4 0.7(3) . .
Te2 Zr2 O5 Te4 -176.9(6) . .
O10 Te4 O11 Zr2 -88.3(3) . .
O5 Te4 O11 Zr2 0.7(3) . .
O8 Te4 O11 Zr2 -178.4(4) . .
O10 Te4 O11 Zr1 88.7(3) . .
O5 Te4 O11 Zr1 177.8(4) . .
O8 Te4 O11 Zr1 -1.3(3) . .
O1 Zr2 O11 Te4 -87.9(3) 2_666 .
O7 Zr2 O11 Te4 90.1(3) 2 .
O2 Zr2 O11 Te4 178.5(3) . .
O6 Zr2 O11 Te4 -176.7(9) 2_566 .
O5 Zr2 O11 Te4 -0.7(3) . .
O6 Zr2 O11 Te4 1.7(5) . .
Te2 Zr2 O11 Te4 0.6(3) . .
O1 Zr2 O11 Zr1 96.4(5) 2_666 .
O7 Zr2 O11 Zr1 -85.6(5) 2 .
O2 Zr2 O11 Zr1 2.8(5) . .
O6 Zr2 O11 Zr1 7.6(13) 2_566 .
O5 Zr2 O11 Zr1 -176.4(6) . .
O6 Zr2 O11 Zr1 -174.0(4) . .
Te2 Zr2 O11 Zr1 -175.1(4) . .
O10 Zr1 O11 Te4 -86.7(3) 2 .
O4 Zr1 O11 Te4 91.5(3) 1_655 .
O3 Zr1 O11 Te4 -176.9(3) . .
O9 Zr1 O11 Te4 175.7(8) 2_655 .
O8 Zr1 O11 Te4 1.3(3) . .
O9 Zr1 O11 Te4 6.7(5) . .
Te3 Zr1 O11 Te4 1.7(3) . .
O10 Zr1 O11 Zr2 89.0(5) 2 .
O4 Zr1 O11 Zr2 -92.8(5) 1_655 .
O3 Zr1 O11 Zr2 -1.2(5) . .
O9 Zr1 O11 Zr2 -8.6(13) 2_655 .
O8 Zr1 O11 Zr2 177.0(6) . .
O9 Zr1 O11 Zr2 -177.6(4) . .
Te3 Zr1 O11 Zr2 177.4(4) . .
O4 Te2 O6 Zr2 -85.6(5) . 2_566
O5 Te2 O6 Zr2 176.6(5) . 2_566
Zr2 Te2 O6 Zr2 177.1(7) . 2_566
O4 Te2 O6 Zr2 97.3(3) . .
O5 Te2 O6 Zr2 -0.5(3) . .
O1 Zr2 O6 Te2 85.4(3) 2_666 .
O7 Zr2 O6 Te2 -89.2(3) 2 .
O2 Zr2 O6 Te2 -177.1(3) . .
O6 Zr2 O6 Te2 177.6(5) 2_566 .
O5 Zr2 O6 Te2 0.4(3) . .
O11 Zr2 O6 Te2 -2.0(5) . .
O1 Zr2 O6 Zr2 -92.2(3) 2_666 2_566
O7 Zr2 O6 Zr2 93.2(3) 2 2_566
O2 Zr2 O6 Zr2 5.3(6) . 2_566
O6 Zr2 O6 Zr2 0.0 2_566 2_566
O5 Zr2 O6 Zr2 -177.1(4) . 2_566
O11 Zr2 O6 Zr2 -179.6(3) . 2_566
Te2 Zr2 O6 Zr2 -177.6(5) . 2_566
O2 Te1 O1 Zr2 -48.9(19) . 2_666
O3 Te1 O1 Zr2 54.4(19) . 2_666
O6 Te2 O4 Zr1 -52(2) . 1_455
O5 Te2 O4 Zr1 25(2) . 1_455
Zr2 Te2 O4 Zr1 -14(2) . 1_455
O11 Te4 O10 Zr1 19(5) . 2
O5 Te4 O10 Zr1 -57(5) . 2
O8 Te4 O10 Zr1 95(5) . 2
O9 Te3 O7 Zr2 69(4) . 2
O8 Te3 O7 Zr2 -7(4) . 2
Zr1 Te3 O7 Zr2 31(4) . 2
