#------------------------------------------------------------------------------
#$Date: 2016-03-23 20:37:02 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179415 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/12/4331259.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4331259
loop_
_publ_author_name
'Tommy Kenny'
'Simon Lamare'
'Shawkat M. Aly'
'Daniel Fortin'
'Gessie Brisard'
'Pierre D. Harvey'
_publ_section_title
;
 Reduced and Oxidized Forms of the Pt-Organometallic Version of
 Polyaniline
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              13081
_journal_page_last               13095
_journal_paper_doi               10.1021/ic300775n
_journal_volume                  51
_journal_year                    2012
_chemical_formula_sum            'C70 H118 Cl6 N2 P4 Pt2'
_chemical_formula_weight         1714.42
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_conform_dict_location     ftp://ftp.iucr.org/pub/cif_core.dic
_audit_conform_dict_name         cif_core.dic
_audit_conform_dict_version      2.3
_audit_creation_date             2010-04-19T15:20:23-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 98.48(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   14.294(5)
_cell_length_b                   12.545(5)
_cell_length_c                   23.197(9)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    193(2)
_cell_measurement_theta_max      12.5
_cell_measurement_theta_min      10
_cell_volume                     4114(3)
_computing_cell_refinement       Difrac
_computing_data_collection       Difrac
_computing_data_reduction        NRCVAX
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.95
_diffrn_measured_fraction_theta_max 0.95
_diffrn_measurement_device_type  CAD4
_diffrn_measurement_method       Omega
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_wavelength     0.7093
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_av_unetI/netI     0.3138
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            7306
_diffrn_reflns_theta_full        25.48
_diffrn_reflns_theta_max         25.48
_diffrn_reflns_theta_min         1.57
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 100
_diffrn_standards_number         1
_exptl_absorpt_coefficient_mu    3.706
_exptl_absorpt_correction_T_max  0.7082
_exptl_absorpt_correction_T_min  0.2146
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   empirical
_exptl_crystal_colour            Blue
_exptl_crystal_density_diffrn    1.384
_exptl_crystal_description       Needle
_exptl_crystal_F_000             1740
_exptl_crystal_size_max          0.6
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.951
_refine_diff_density_min         -1.656
_refine_diff_density_rms         0.19
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.83
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     187
_refine_ls_number_reflns         7306
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.83
_refine_ls_R_factor_all          0.2789
_refine_ls_R_factor_gt           0.0859
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0423P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1211
_refine_ls_wR_factor_ref         0.1551
_reflns_number_gt                2597
_reflns_number_total             7306
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic300775n_si_002_18.cif
_cod_data_source_block           9c
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Psi-Scan' changed to
'psi-scan' according to the built-in table from CIF Core dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_database_code               4331259
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C2 C 0.1814(13) 0.1439(15) 0.2532(8) 0.0698(14) Uani 1 1 d .
H2A H 0.174 0.1042 0.2891 0.084 Uiso 1 1 calc R
H2B H 0.1353 0.1123 0.2218 0.084 Uiso 1 1 calc R
C3 C 0.1462(11) 0.2510(18) 0.2619(7) 0.0698(14) Uani 1 1 d .
H3A H 0.1499 0.291 0.2255 0.084 Uiso 1 1 calc R
H3B H 0.1922 0.2846 0.2926 0.084 Uiso 1 1 calc R
C8 C 0.5531(12) 0.4545(15) 0.2977(7) 0.0698(14) Uani 1 1 d .
H8A H 0.5741 0.5178 0.3208 0.105 Uiso 1 1 calc R
H8B H 0.5243 0.4764 0.2585 0.105 Uiso 1 1 calc R
H8C H 0.6076 0.4084 0.2948 0.105 Uiso 1 1 calc R
C24 C 0.3080(10) 0.2424(17) -0.1591(6) 0.0698(14) Uani 1 1 d .
H24A H 0.3385 0.2089 -0.1897 0.105 Uiso 1 1 calc R
H24B H 0.3064 0.3199 -0.1648 0.105 Uiso 1 1 calc R
H24C H 0.2433 0.2154 -0.1612 0.105 Uiso 1 1 calc R
C1 C 0.2721(13) 0.1144(16) 0.2399(8) 0.0698(14) Uani 1 1 d .
H1A H 0.2656 0.0441 0.2202 0.084 Uiso 1 1 calc R
H1B H 0.3147 0.1045 0.2772 0.084 Uiso 1 1 calc R
C4 C 0.0497(11) 0.2714(15) 0.2777(7) 0.0698(14) Uani 1 1 d .
H4A H 0.0378 0.3484 0.2776 0.105 Uiso 1 1 calc R
H4B H 0.0464 0.2426 0.3166 0.105 Uiso 1 1 calc R
H4C H 0.002 0.2367 0.2492 0.105 Uiso 1 1 calc R
C5 C 0.3780(13) 0.3177(15) 0.2364(8) 0.0698(14) Uani 1 1 d .
H5A H 0.414 0.3624 0.2122 0.084 Uiso 1 1 calc R
H5B H 0.3246 0.361 0.2462 0.084 Uiso 1 1 calc R
C6 C 0.4429(12) 0.2893(14) 0.2931(7) 0.0698(14) Uani 1 1 d .
H6A H 0.4958 0.2444 0.2841 0.084 Uiso 1 1 calc R
H6B H 0.4069 0.2483 0.3189 0.084 Uiso 1 1 calc R
C7 C 0.4840(13) 0.3966(16) 0.3257(7) 0.0698(14) Uani 1 1 d .
H7A H 0.4303 0.4449 0.3291 0.084 Uiso 1 1 calc R
H7B H 0.5135 0.3777 0.3657 0.084 Uiso 1 1 calc R
C9 C 0.4388(12) 0.1311(15) 0.1858(8) 0.0698(14) Uani 1 1 d .
H9A H 0.4745 0.1185 0.2251 0.084 Uiso 1 1 calc R
H9B H 0.4197 0.0605 0.1688 0.084 Uiso 1 1 calc R
C10 C 0.5018(13) 0.1794(15) 0.1505(8) 0.0698(14) Uani 1 1 d .
H10A H 0.5244 0.247 0.1697 0.084 Uiso 1 1 calc R
H10B H 0.4635 0.1987 0.1128 0.084 Uiso 1 1 calc R
C11 C 0.5855(13) 0.1220(16) 0.1370(8) 0.0698(14) Uani 1 1 d .
H11A H 0.6164 0.1643 0.109 0.084 Uiso 1 1 calc R
H11B H 0.5658 0.053 0.1183 0.084 Uiso 1 1 calc R
C12 C 0.6565(12) 0.1019(15) 0.1924(7) 0.0698(14) Uani 1 1 d .
H12A H 0.71 0.0603 0.1825 0.105 Uiso 1 1 calc R
H12B H 0.6254 0.0623 0.2206 0.105 Uiso 1 1 calc R
H12C H 0.6795 0.1703 0.2094 0.105 Uiso 1 1 calc R
C13 C 0.0552(12) 0.1710(15) 0.0096(8) 0.0698(14) Uani 1 1 d .
H13A H 0.0242 0.1683 -0.0315 0.084 Uiso 1 1 calc R
H13B H 0.0754 0.0976 0.021 0.084 Uiso 1 1 calc R
C14 C -0.0198(12) 0.2055(14) 0.0476(8) 0.0698(14) Uani 1 1 d .
H14A H 0.013 0.2269 0.0865 0.084 Uiso 1 1 calc R
H14B H -0.0536 0.2689 0.0296 0.084 Uiso 1 1 calc R
C15 C -0.0882(13) 0.1247(15) 0.0551(8) 0.0698(14) Uani 1 1 d .
H15A H -0.1192 0.1012 0.0162 0.084 Uiso 1 1 calc R
H15B H -0.0547 0.0625 0.0746 0.084 Uiso 1 1 calc R
C16 C -0.1593(12) 0.1585(15) 0.0883(7) 0.0698(14) Uani 1 1 d .
H16A H -0.2015 0.0986 0.0932 0.105 Uiso 1 1 calc R
H16B H -0.196 0.2167 0.0679 0.105 Uiso 1 1 calc R
H16C H -0.1294 0.1833 0.1267 0.105 Uiso 1 1 calc R
C17 C 0.1262(13) 0.3822(15) -0.0151(7) 0.0698(14) Uani 1 1 d .
H17A H 0.0831 0.413 0.0102 0.084 Uiso 1 1 calc R
H17B H 0.1834 0.4276 -0.0108 0.084 Uiso 1 1 calc R
C18 C 0.0768(13) 0.3924(14) -0.0791(7) 0.063(2) Uani 1 1 d .
H18A H 0.1167 0.3579 -0.1052 0.076 Uiso 1 1 calc R
H18B H 0.0155 0.3544 -0.0835 0.076 Uiso 1 1 calc R
C19 C 0.0599(13) 0.5082(14) -0.0974(7) 0.063(2) Uani 1 1 d .
H19A H 0.1202 0.5477 -0.0882 0.076 Uiso 1 1 calc R
H19B H 0.0145 0.5398 -0.0738 0.076 Uiso 1 1 calc R
C21 C 0.2237(12) 0.2003(14) -0.0428(7) 0.063(2) Uani 1 1 d .
H21A H 0.2355 0.1237 -0.0346 0.076 Uiso 1 1 calc R
H21B H 0.1817 0.2055 -0.0806 0.076 Uiso 1 1 calc R
C22 C 0.3134(11) 0.2501(19) -0.0492(6) 0.063(2) Uani 1 1 d .
H22A H 0.3569 0.2387 -0.0124 0.076 Uiso 1 1 calc R
H22B H 0.3023 0.3279 -0.0531 0.076 Uiso 1 1 calc R
C23 C 0.3647(12) 0.2159(13) -0.0987(6) 0.063(2) Uani 1 1 d .
H23A H 0.3763 0.1382 -0.096 0.076 Uiso 1 1 calc R
H23B H 0.4269 0.2522 -0.0947 0.076 Uiso 1 1 calc R
C25 C 0.2567(12) 0.0858(14) 0.0882(8) 0.055(4) Uani 1 1 d .
C26 C 0.2643(12) -0.0030(14) 0.0788(7) 0.055(4) Uani 1 1 d .
C27 C 0.2790(7) -0.1119(6) 0.0664(5) 0.0410(18) Uani 1 1 d G
C28 C 0.2186(5) -0.1904(9) 0.0817(4) 0.0410(18) Uani 1 1 d G
H28 H 0.1651 -0.1711 0.0994 0.049 Uiso 1 1 calc R
C29 C 0.2364(6) -0.2970(7) 0.0712(4) 0.0410(18) Uani 1 1 d G
H29 H 0.1951 -0.3507 0.0817 0.049 Uiso 1 1 calc R
C30 C 0.3146(7) -0.3252(6) 0.0454(4) 0.0410(18) Uani 1 1 d G
C31 C 0.3750(5) -0.2468(9) 0.0300(3) 0.0410(18) Uani 1 1 d G
H31 H 0.4285 -0.266 0.0124 0.049 Uiso 1 1 calc R
C32 C 0.3572(6) -0.1401(7) 0.0405(4) 0.0410(18) Uani 1 1 d G
H32 H 0.3985 -0.0865 0.03 0.049 Uiso 1 1 calc R
C33 C 0.4124(11) -0.4627(12) 0.0199(6) 0.034(2) Uani 1 1 d .
C34 C 0.4258(10) -0.4645(12) -0.0396(6) 0.034(2) Uani 1 1 d .
C35 C 0.4947(11) -0.5003(11) 0.0580(6) 0.034(2) Uani 1 1 d .
Cl1 Cl 0.2225(3) 0.4247(3) 0.12762(16) 0.0376(10) Uani 1 1 d .
Cl2 Cl 0.4861(3) -0.4974(4) 0.13198(16) 0.0521(12) Uani 1 1 d .
Cl3 Cl 0.3285(3) -0.4229(4) -0.08912(17) 0.0533(13) Uani 1 1 d .
N1 N 0.3322(8) -0.4334(10) 0.0389(5) 0.046(4) Uani 1 1 d .
H1 H 0.2914 -0.4815 0.0471 0.055 Uiso 1 1 calc R
P1 P 0.3312(3) 0.2053(3) 0.19416(18) 0.0395(12) Uani 1 1 d .
P2 P 0.1609(3) 0.2534(4) 0.01281(14) 0.0351(9) Uani 1 1 d .
Pt1 Pt 0.24307(5) 0.24369(6) 0.10529(3) 0.03532(19) Uani 1 1 d .
C20 C 0.0215(12) 0.5241(14) -0.1622(6) 0.063(2) Uani 1 1 d .
H20A H 0.0081 0.5998 -0.1698 0.095 Uiso 1 1 calc R
H20B H -0.0368 0.4827 -0.1722 0.095 Uiso 1 1 calc R
H20C H 0.0687 0.4997 -0.1859 0.095 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
C1 C2 C3 127.8(18) .
C2 C3 C4 122.6(18) .
C2 C1 P1 118.1(14) .
C6 C5 P1 114.6(12) .
C5 C6 C7 109.9(14) .
C8 C7 C6 115.6(16) .
C10 C9 P1 116.9(14) .
C9 C10 C11 120.9(17) .
C10 C11 C12 111.1(15) .
C14 C13 P2 117.3(13) .
C15 C14 C13 114.4(16) .
C16 C15 C14 114.1(18) .
C18 C17 P2 119.0(13) .
C19 C18 C17 112.1(14) .
C18 C19 C20 114.5(14) .
C22 C21 P2 117.0(12) .
C21 C22 C23 119.4(16) .
C22 C23 C24 112.2(13) .
C26 C25 Pt1 180(2) .
C25 C26 C27 177(2) .
C28 C27 C32 120 .
C28 C27 C26 120.9(11) .
C32 C27 C26 119.0(11) .
C27 C28 C29 120 .
C30 C29 C28 120 .
C31 C30 C29 120 .
C31 C30 N1 122.2(10) .
C29 C30 N1 117.7(10) .
C30 C31 C32 120 .
C31 C32 C27 120 .
N1 C33 C34 124.6(15) .
N1 C33 C35 123.4(14) .
C34 C33 C35 112.0(13) .
C35 C34 C33 123.6(14) 3_645
C35 C34 Cl3 121.2(12) 3_645
C33 C34 Cl3 115.2(12) .
C34 C35 C33 124.5(14) 3_645
C34 C35 Cl2 120.3(12) 3_645
C33 C35 Cl2 115.2(12) .
C33 N1 C30 118.8(12) .
C5 P1 C9 101.9(9) .
C5 P1 C1 109.8(9) .
C9 P1 C1 102.1(8) .
C5 P1 Pt1 115.9(6) .
C9 P1 Pt1 111.6(6) .
C1 P1 Pt1 114.0(6) .
C17 P2 C21 102.5(9) .
C17 P2 C13 108.3(9) .
C21 P2 C13 105.0(8) .
C17 P2 Pt1 117.7(6) .
C21 P2 Pt1 114.2(6) .
C13 P2 Pt1 108.4(6) .
C25 Pt1 P2 85.4(5) .
C25 Pt1 P1 85.2(5) .
P2 Pt1 P1 170.49(18) .
C25 Pt1 Cl1 177.6(6) .
P2 Pt1 Cl1 95.22(16) .
P1 Pt1 Cl1 94.25(13) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C2 C1 1.42(2) .
C2 C3 1.46(3) .
C3 C4 1.501(19) .
C8 C7 1.45(2) .
C24 C23 1.550(18) .
C1 P1 1.845(18) .
C5 C6 1.53(2) .
C5 P1 1.790(18) .
C6 C7 1.61(2) .
C9 C10 1.44(2) .
C9 P1 1.833(18) .
C10 C11 1.47(2) .
C11 C12 1.54(2) .
C13 C14 1.55(2) .
C13 P2 1.824(18) .
C14 C15 1.44(2) .
C15 C16 1.43(2) .
C17 C18 1.55(2) .
C17 P2 1.784(19) .
C18 C19 1.52(2) .
C19 C20 1.535(18) .
C21 C22 1.45(2) .
C21 P2 1.804(17) .
C22 C23 1.512(19) .
C25 C26 1.14(2) .
C25 Pt1 2.035(17) .
C26 C27 1.419(17) .
C27 C28 1.39 .
C27 C32 1.39 .
C28 C29 1.39 .
C29 C30 1.39 .
C30 C31 1.39 .
C30 N1 1.392(14) .
C31 C32 1.39 .
C33 N1 1.337(17) .
C33 C34 1.423(19) .
C33 C35 1.442(19) .
C34 C35 1.345(18) 3_645
C34 Cl3 1.747(14) .
C35 C34 1.345(18) 3_645
C35 Cl2 1.740(15) .
Cl1 Pt1 2.357(4) .
P1 Pt1 2.303(4) .
P2 Pt1 2.292(3) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_4
C1 C2 C3 C4 -178.0(17) .
C3 C2 C1 P1 -33(3) .
P1 C5 C6 C7 177.5(12) .
C5 C6 C7 C8 -71(2) .
P1 C9 C10 C11 -174.6(14) .
C9 C10 C11 C12 -65(2) .
P2 C13 C14 C15 -164.6(13) .
C13 C14 C15 C16 -177.7(15) .
P2 C17 C18 C19 -175.0(14) .
C17 C18 C19 C20 173.5(15) .
P2 C21 C22 C23 -174.4(12) .
C21 C22 C23 C24 64(2) .
Pt1 C25 C26 C27 -13E1(10) .
C25 C26 C27 C28 17E1(4) .
C25 C26 C27 C32 -1E1(4) .
C32 C27 C28 C29 0 .
C26 C27 C28 C29 -177.4(12) .
C27 C28 C29 C30 0 .
C28 C29 C30 C31 0 .
C28 C29 C30 N1 176.4(10) .
C29 C30 C31 C32 0 .
N1 C30 C31 C32 -176.2(10) .
C30 C31 C32 C27 0 .
C28 C27 C32 C31 0 .
C26 C27 C32 C31 177.5(12) .
N1 C33 C34 C35 -176.4(14) 3_645
C35 C33 C34 C35 1(2) 3_645
N1 C33 C34 Cl3 1(2) .
C35 C33 C34 Cl3 178.7(10) .
N1 C33 C35 C34 176.4(14) 3_645
C34 C33 C35 C34 -1(2) 3_645
N1 C33 C35 Cl2 -4(2) .
C34 C33 C35 Cl2 178.2(10) .
C34 C33 N1 C30 -82.0(18) .
C35 C33 N1 C30 100.4(17) .
C31 C30 N1 C33 3.4(16) .
C29 C30 N1 C33 -172.9(10) .
C6 C5 P1 C9 -54.0(16) .
C6 C5 P1 C1 53.7(16) .
C6 C5 P1 Pt1 -175.3(11) .
C10 C9 P1 C5 -67.9(16) .
C10 C9 P1 C1 178.6(15) .
C10 C9 P1 Pt1 56.4(16) .
C2 C1 P1 C5 75.7(17) .
C2 C1 P1 C9 -176.7(15) .
C2 C1 P1 Pt1 -56.2(17) .
C18 C17 P2 C21 49.5(17) .
C18 C17 P2 C13 -61.1(17) .
C18 C17 P2 Pt1 175.7(12) .
C22 C21 P2 C17 68.3(16) .
C22 C21 P2 C13 -178.7(14) .
C22 C21 P2 Pt1 -60.1(16) .
C14 C13 P2 C17 -64.0(15) .
C14 C13 P2 C21 -172.9(13) .
C14 C13 P2 Pt1 64.7(14) .
C26 C25 Pt1 P2 -13E1(10) .
C26 C25 Pt1 P1 5E1(10) .
C26 C25 Pt1 Cl1 -3E1(10) .
C17 P2 Pt1 C25 -173.9(9) .
C21 P2 Pt1 C25 -53.7(9) .
C13 P2 Pt1 C25 62.9(8) .
C17 P2 Pt1 P1 -166.2(11) .
C21 P2 Pt1 P1 -45.9(13) .
C13 P2 Pt1 P1 70.6(12) .
C17 P2 Pt1 Cl1 8.4(8) .
C21 P2 Pt1 Cl1 128.6(7) .
C13 P2 Pt1 Cl1 -114.8(7) .
C5 P1 Pt1 C25 166.4(9) .
C9 P1 Pt1 C25 50.4(9) .
C1 P1 Pt1 C25 -64.6(9) .
C5 P1 Pt1 P2 158.7(11) .
C9 P1 Pt1 P2 42.6(13) .
C1 P1 Pt1 P2 -72.4(13) .
C5 P1 Pt1 Cl1 -15.9(7) .
C9 P1 Pt1 Cl1 -131.9(7) .
C1 P1 Pt1 Cl1 113.0(7) .
