#------------------------------------------------------------------------------
#$Date: 2016-03-23 20:45:00 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179422 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/19/4331999.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4331999
loop_
_publ_author_name
'Kennedy, Alan R.'
'Kirkhouse, Jennifer B. A.'
'Whyte, Lynda'
_publ_section_title
;
 Supramolecuar Motifs in s-Block Metal-Bound Sulfonated Monoazo
 Dyes:  The Case of Orange G
;
_journal_issue                   7
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2965
_journal_page_last               2971
_journal_paper_doi               10.1021/ic0520115
_journal_volume                  45
_journal_year                    2006
_chemical_formula_sum            'C16 H20 Ag2 N2 O12 S2'
_chemical_formula_weight         712.20
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.435(1)
_cell_angle_beta                 102.805(1)
_cell_angle_gamma                108.338(1)
_cell_formula_units_Z            2
_cell_length_a                   8.8702(9)
_cell_length_b                   10.6780(8)
_cell_length_c                   13.2722(9)
_cell_measurement_temperature    150(2)
_cell_volume                     1075.81(15)
_computing_data_collection       'Bruker software'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    Shelxs
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.936
_diffrn_measured_fraction_theta_max 0.875
_diffrn_measurement_device_type  'Bruker APEX'
_diffrn_measurement_method       'narrow frames'
_diffrn_radiation_monochromator  Si111
_diffrn_radiation_source         'Station 16.2, Daresbury SRS'
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.84660
_diffrn_reflns_av_R_equivalents  0.0226
_diffrn_reflns_av_sigmaI/netI    0.0344
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            7487
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         33.17
_diffrn_reflns_theta_min         4.06
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.131
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.199
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       chip
_exptl_crystal_F_000             704
_exptl_crystal_size_max          0.030
_exptl_crystal_size_mid          0.010
_exptl_crystal_size_min          0.005
_refine_diff_density_max         1.821
_refine_diff_density_min         -1.644
_refine_diff_density_rms         0.183
_refine_ls_extinction_coef       0.0075(17)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     320
_refine_ls_number_reflns         4262
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.031
_refine_ls_R_factor_all          0.0452
_refine_ls_R_factor_gt           0.0442
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0911P)²+1.5132P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1171
_refine_ls_wR_factor_ref         0.1185
_reflns_number_gt                4071
_reflns_number_total             4262
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ic0520115sup1.cif
_cod_data_source_block           sad
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4331999
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.50626(3) 0.49572(3) 0.83589(2) 0.01608(14) Uani 1 1 d .
Ag2 Ag 0.98401(3) 0.68379(3) 0.93296(2) 0.01276(14) Uani 1 1 d .
S1 S 0.22406(10) 0.23701(8) 0.90938(6) 0.00714(19) Uani 1 1 d .
S2 S 0.39169(9) -0.13735(8) 0.64572(6) 0.00491(18) Uani 1 1 d .
O1 O 0.5419(3) -0.0272(2) 0.73983(19) 0.0107(5) Uani 1 1 d .
O2 O 0.4123(3) -0.1406(3) 0.53993(19) 0.0105(5) Uani 1 1 d .
O1W O 0.4367(3) 0.7051(3) 0.8621(2) 0.0138(5) Uani 1 1 d .
H1W H 0.5503 0.7830 0.9106 0.021 Uiso 1 1 d R
H2W H 0.4134 0.7213 0.7849 0.021 Uiso 1 1 d R
O3 O 0.3451(3) -0.2743(2) 0.65832(19) 0.0093(5) Uani 1 1 d .
O2W O 0.7401(3) 0.4425(3) 0.8558(2) 0.0111(5) Uani 1 1 d .
O4 O 0.3937(3) 0.3391(2) 0.9332(2) 0.0132(5) Uani 1 1 d .
O3W O 1.1923(3) 0.5851(3) 0.9428(2) 0.0133(5) Uani 1 1 d .
H5W H 1.2731 0.6261 0.9214 0.020 Uiso 1 1 d R
H6W H 1.1871 0.5021 0.9213 0.020 Uiso 1 1 d R
O4W O 0.7045(3) 0.2108(3) 0.6891(2) 0.0173(5) Uani 1 1 d .
H7W H 0.6574 0.1837 0.6073 0.026 Uiso 1 1 d R
O5 O 0.2215(3) 0.1655(3) 0.9886(2) 0.0145(5) Uani 1 1 d .
O6 O 0.0980(3) 0.2982(3) 0.9019(2) 0.0138(5) Uani 1 1 d .
O7 O -0.2516(3) -0.4182(3) 0.3092(2) 0.0147(5) Uani 1 1 d .
O5W O 1.2379(10) 0.9152(5) 1.0289(6) 0.0175(19) Uiso 0.59(3) 1 d P
O6W O 1.1972(15) 0.9253(9) 1.0486(9) 0.022(3) Uiso 0.41(3) 1 d P
N1 N 0.0750(3) -0.3421(3) 0.4557(2) 0.0058(5) Uani 1 1 d .
N2 N 0.0080(3) -0.4613(3) 0.3695(2) 0.0072(5) Uani 1 1 d .
C1 C -0.0169(4) -0.2653(3) 0.4745(3) 0.0052(6) Uani 1 1 d .
C2 C -0.1864(4) -0.3075(3) 0.3985(3) 0.0076(6) Uani 1 1 d .
C3 C -0.2810(4) -0.2238(3) 0.4266(3) 0.0089(6) Uani 1 1 d .
H3 H -0.3913 -0.2504 0.3773 0.011 Uiso 1 1 calc R
C4 C -0.2143(4) -0.1081(3) 0.5222(3) 0.0082(6) Uani 1 1 d .
H4 H -0.2799 -0.0553 0.5395 0.010 Uiso 1 1 calc R
C4A C -0.0464(4) -0.0614(3) 0.5995(3) 0.0061(6) Uani 1 1 d .
C5 C 0.0062(4) 0.0567(3) 0.6987(3) 0.0070(6) Uani 1 1 d .
H5 H -0.0654 0.1049 0.7118 0.008 Uiso 1 1 calc R
C6 C 0.1621(4) 0.1020(3) 0.7768(2) 0.0057(6) Uani 1 1 d .
C7 C 0.2728(4) 0.0374(3) 0.7554(3) 0.0074(6) Uani 1 1 d .
H7 H 0.3823 0.0730 0.8090 0.009 Uiso 1 1 calc R
C8 C 0.2241(4) -0.0782(3) 0.6566(2) 0.0050(6) Uani 1 1 d .
C8A C 0.0581(4) -0.1354(3) 0.5763(2) 0.0036(5) Uani 1 1 d .
C9 C 0.0984(4) -0.5448(3) 0.3418(2) 0.0058(6) Uani 1 1 d .
C10 C 0.2731(4) -0.4950(3) 0.3928(3) 0.0092(6) Uani 1 1 d .
H10 H 0.3359 -0.4027 0.4502 0.011 Uiso 1 1 calc R
C11 C 0.3528(4) -0.5841(4) 0.3573(3) 0.0109(6) Uani 1 1 d .
H11 H 0.4716 -0.5514 0.3904 0.013 Uiso 1 1 calc R
C12 C 0.2617(4) -0.7195(4) 0.2746(3) 0.0104(6) Uani 1 1 d .
H12 H 0.3184 -0.7785 0.2517 0.013 Uiso 1 1 calc R
C13 C 0.0870(4) -0.7694(3) 0.2248(3) 0.0093(6) Uani 1 1 d .
H13 H 0.0248 -0.8623 0.1682 0.011 Uiso 1 1 calc R
C14 C 0.0038(4) -0.6819(3) 0.2585(3) 0.0066(6) Uani 1 1 d .
H14 H -0.1151 -0.7149 0.2255 0.008 Uiso 1 1 calc R
H1N H -0.103(7) -0.494(6) 0.329(4) 0.028(13) Uiso 1 1 d .
H4W H 0.738(6) 0.365(5) 0.804(4) 0.021(12) Uiso 1 1 d .
H3W H 0.759(8) 0.417(7) 0.921(6) 0.047(16) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.5420 1.5105 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1639 0.1757 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0161 0.0089 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0094 0.0049 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0050 0.0024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2W Ag1 O7 135.17(9) . 2_556
O2W Ag1 O1W 139.10(9) . .
O7 Ag1 O1W 74.77(8) 2_556 .
O2W Ag1 O4 90.68(9) . .
O7 Ag1 O4 96.74(9) 2_556 .
O1W Ag1 O4 116.15(8) . .
O3W Ag2 O6 108.44(8) . 2_667
O3W Ag2 O6W 92.1(3) . .
O6 Ag2 O6W 84.2(4) 2_667 .
O3W Ag2 O5W 83.0(2) . .
O6 Ag2 O5W 94.1(2) 2_667 .
O6W Ag2 O5W 11.8(2) . .
O3W Ag2 O2W 93.44(8) . .
O6 Ag2 O2W 81.45(8) 2_667 .
O6W Ag2 O2W 165.6(4) . .
O5W Ag2 O2W 173.11(13) . .
O3W Ag2 C13 118.66(9) . 2_656
O6 Ag2 C13 132.58(9) 2_667 2_656
O6W Ag2 C13 88.7(2) . 2_656
O5W Ag2 C13 86.62(14) . 2_656
O2W Ag2 C13 100.27(9) . 2_656
O3W Ag2 C14 87.97(9) . 2_656
O6 Ag2 C14 163.33(9) 2_667 2_656
O6W Ag2 C14 98.5(3) . 2_656
O5W Ag2 C14 90.8(2) . 2_656
O2W Ag2 C14 94.95(9) . 2_656
C13 Ag2 C14 31.83(10) 2_656 2_656
O4 S1 O6 113.42(15) . .
O4 S1 O5 111.18(15) . .
O6 S1 O5 111.93(15) . .
O4 S1 C6 107.87(14) . .
O6 S1 C6 105.98(15) . .
O5 S1 C6 105.96(14) . .
O2 S2 O3 115.09(14) . .
O2 S2 O1 110.91(14) . .
O3 S2 O1 111.04(13) . .
O2 S2 C8 107.02(14) . .
O3 S2 C8 107.44(14) . .
O1 S2 C8 104.67(14) . .
Ag1 O1W H1W 100.2 . .
Ag1 O1W H2W 108.6 . .
H1W O1W H2W 103.8 . .
Ag1 O2W Ag2 103.70(9) . .
Ag1 O2W H4W 121(3) . .
Ag2 O2W H4W 122(3) . .
Ag1 O2W H3W 108(3) . .
Ag2 O2W H3W 99(4) . .
H4W O2W H3W 100(5) . .
S1 O4 Ag1 131.30(14) . .
Ag2 O3W H5W 112.8 . .
Ag2 O3W H6W 133.6 . .
H5W O3W H6W 100.1 . .
S1 O6 Ag2 107.43(13) . 2_667
C2 O7 Ag1 127.7(2) . 2_556
O6W O5W Ag2 78.3(12) . .
O5W O6W Ag2 89.9(12) . .
N2 N1 C1 118.8(3) . .
N1 N2 C9 122.1(3) . .
N1 N2 H1N 119(3) . .
C9 N2 H1N 119(3) . .
N1 C1 C2 122.3(3) . .
N1 C1 C8A 117.7(3) . .
C2 C1 C8A 120.1(3) . .
O7 C2 C3 120.0(3) . .
O7 C2 C1 120.7(3) . .
C3 C2 C1 119.3(3) . .
C4 C3 C2 120.4(3) . .
C4 C3 H3 119.8 . .
C2 C3 H3 119.8 . .
C3 C4 C4A 122.2(3) . .
C3 C4 H4 118.9 . .
C4A C4 H4 118.9 . .
C5 C4A C8A 122.0(3) . .
C5 C4A C4 117.0(3) . .
C8A C4A C4 121.0(3) . .
C6 C5 C4A 119.3(3) . .
C6 C5 H5 120.4 . .
C4A C5 H5 120.4 . .
C5 C6 C7 120.8(3) . .
C5 C6 S1 120.9(2) . .
C7 C6 S1 118.3(2) . .
C8 C7 C6 120.6(3) . .
C8 C7 H7 119.7 . .
C6 C7 H7 119.7 . .
C7 C8 C8A 120.4(3) . .
C7 C8 S2 112.3(2) . .
C8A C8 S2 127.3(2) . .
C4A C8A C8 116.7(3) . .
C4A C8A C1 116.8(3) . .
C8 C8A C1 126.4(3) . .
C10 C9 C14 121.4(3) . .
C10 C9 N2 122.4(3) . .
C14 C9 N2 116.2(3) . .
C11 C10 C9 118.3(3) . .
C11 C10 H10 120.8 . .
C9 C10 H10 120.8 . .
C12 C11 C10 121.2(3) . .
C12 C11 H11 119.4 . .
C10 C11 H11 119.4 . .
C11 C12 C13 120.3(3) . .
C11 C12 H12 119.8 . .
C13 C12 H12 119.8 . .
C12 C13 C14 119.7(3) . .
C12 C13 Ag2 110.7(2) . 2_656
C14 C13 Ag2 74.78(18) . 2_656
C12 C13 H13 120.2 . .
C14 C13 H13 120.2 . .
Ag2 C13 H13 84.8 2_656 .
C13 C14 C9 119.1(3) . .
C13 C14 Ag2 73.38(18) . 2_656
C9 C14 Ag2 111.0(2) . 2_656
C13 C14 H14 120.4 . .
C9 C14 H14 120.4 . .
Ag2 C14 H14 85.9 2_656 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O2W 2.298(2) .
Ag1 O7 2.343(2) 2_556
Ag1 O1W 2.455(3) .
Ag1 O4 2.492(2) .
Ag2 O3W 2.396(2) .
Ag2 O6 2.435(2) 2_667
Ag2 O6W 2.447(8) .
Ag2 O5W 2.499(5) .
Ag2 O2W 2.526(3) .
Ag2 C13 2.545(3) 2_656
Ag2 C14 2.562(3) 2_656
S1 O4 1.454(3) .
S1 O6 1.460(2) .
S1 O5 1.464(2) .
S1 C6 1.764(3) .
S2 O2 1.448(2) .
S2 O3 1.458(2) .
S2 O1 1.471(2) .
S2 C8 1.807(3) .
O1W H1W 1.0018 .
O1W H2W 1.0729 .
O2W H4W 0.91(5) .
O2W H3W 0.97(7) .
O3W H5W 0.8659 .
O3W H6W 0.8334 .
O4W H7W 0.9916 .
O6 Ag2 2.435(2) 2_667
O7 C2 1.269(4) .
O7 Ag1 2.343(2) 2_556
O5W O6W 0.510(9) .
N1 N2 1.297(4) .
N1 C1 1.340(4) .
N2 C9 1.403(4) .
N2 H1N 0.91(5) .
C1 C2 1.458(4) .
C1 C8A 1.467(4) .
C2 C3 1.436(4) .
C3 C4 1.344(5) .
C3 H3 0.9500 .
C4 C4A 1.444(4) .
C4 H4 0.9500 .
C4A C5 1.400(4) .
C4A C8A 1.423(4) .
C5 C6 1.372(4) .
C5 H5 0.9500 .
C6 C7 1.400(4) .
C7 C8 1.388(4) .
C7 H7 0.9500 .
C8 C8A 1.431(4) .
C9 C10 1.398(4) .
C9 C14 1.403(4) .
C10 C11 1.394(4) .
C10 H10 0.9500 .
C11 C12 1.386(5) .
C11 H11 0.9500 .
C12 C13 1.396(5) .
C12 H12 0.9500 .
C13 C14 1.401(4) .
C13 Ag2 2.545(3) 2_656
C13 H13 0.9500 .
C14 Ag2 2.562(3) 2_656
C14 H14 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O7 Ag1 O2W Ag2 128.48(11) 2_556 .
O1W Ag1 O2W Ag2 2.15(17) . .
O4 Ag1 O2W Ag2 -131.24(9) . .
O3W Ag2 O2W Ag1 179.42(9) . .
O6 Ag2 O2W Ag1 71.28(10) 2_667 .
O6W Ag2 O2W Ag1 66.9(10) . .
O5W Ag2 O2W Ag1 121(2) . .
C13 Ag2 O2W Ag1 -60.64(11) 2_656 .
C14 Ag2 O2W Ag1 -92.32(10) 2_656 .
O6 S1 O4 Ag1 -55.2(2) . .
O5 S1 O4 Ag1 177.63(16) . .
C6 S1 O4 Ag1 61.9(2) . .
O2W Ag1 O4 S1 -137.63(19) . .
O7 Ag1 O4 S1 -1.93(19) 2_556 .
O1W Ag1 O4 S1 74.4(2) . .
O4 S1 O6 Ag2 -108.52(14) . 2_667
O5 S1 O6 Ag2 18.26(17) . 2_667
C6 S1 O6 Ag2 133.32(13) . 2_667
O3W Ag2 O5W O6W -140.8(12) . .
O6 Ag2 O5W O6W -32.7(12) 2_667 .
O2W Ag2 O5W O6W -82(2) . .
C13 Ag2 O5W O6W 99.7(12) 2_656 .
C14 Ag2 O5W O6W 131.3(12) 2_656 .
O3W Ag2 O6W O5W 38.9(12) . .
O6 Ag2 O6W O5W 147.2(12) 2_667 .
O2W Ag2 O6W O5W 151.5(10) . .
C13 Ag2 O6W O5W -79.8(12) 2_656 .
C14 Ag2 O6W O5W -49.4(12) 2_656 .
C1 N1 N2 C9 177.4(3) . .
N2 N1 C1 C2 -3.0(4) . .
N2 N1 C1 C8A 176.3(3) . .
Ag1 O7 C2 C3 8.5(4) 2_556 .
Ag1 O7 C2 C1 -172.6(2) 2_556 .
N1 C1 C2 O7 -1.9(5) . .
C8A C1 C2 O7 178.8(3) . .
N1 C1 C2 C3 177.0(3) . .
C8A C1 C2 C3 -2.3(4) . .
O7 C2 C3 C4 178.6(3) . .
C1 C2 C3 C4 -0.4(5) . .
C2 C3 C4 C4A 1.0(5) . .
C3 C4 C4A C5 -177.1(3) . .
C3 C4 C4A C8A 1.2(5) . .
C8A C4A C5 C6 -0.7(5) . .
C4 C4A C5 C6 177.5(3) . .
C4A C5 C6 C7 4.0(5) . .
C4A C5 C6 S1 -172.8(2) . .
O4 S1 C6 C5 -133.1(3) . .
O6 S1 C6 C5 -11.3(3) . .
O5 S1 C6 C5 107.7(3) . .
O4 S1 C6 C7 50.0(3) . .
O6 S1 C6 C7 171.8(2) . .
O5 S1 C6 C7 -69.1(3) . .
C5 C6 C7 C8 -2.9(5) . .
S1 C6 C7 C8 174.0(2) . .
C6 C7 C8 C8A -1.7(5) . .
C6 C7 C8 S2 177.3(2) . .
O2 S2 C8 C7 -126.7(2) . .
O3 S2 C8 C7 109.2(2) . .
O1 S2 C8 C7 -9.0(3) . .
O2 S2 C8 C8A 52.2(3) . .
O3 S2 C8 C8A -71.9(3) . .
O1 S2 C8 C8A 169.9(3) . .
C5 C4A C8A C8 -3.6(4) . .
C4 C4A C8A C8 178.2(3) . .
C5 C4A C8A C1 174.5(3) . .
C4 C4A C8A C1 -3.7(4) . .
C7 C8 C8A C4A 4.7(4) . .
S2 C8 C8A C4A -174.1(2) . .
C7 C8 C8A C1 -173.2(3) . .
S2 C8 C8A C1 8.0(5) . .
N1 C1 C8A C4A -175.1(3) . .
C2 C1 C8A C4A 4.2(4) . .
N1 C1 C8A C8 2.8(5) . .
C2 C1 C8A C8 -177.9(3) . .
N1 N2 C9 C10 -11.2(5) . .
N1 N2 C9 C14 169.5(3) . .
C14 C9 C10 C11 1.3(5) . .
N2 C9 C10 C11 -178.0(3) . .
C9 C10 C11 C12 -0.8(5) . .
C10 C11 C12 C13 0.1(5) . .
C11 C12 C13 C14 0.1(5) . .
C11 C12 C13 Ag2 84.0(3) . 2_656
C12 C13 C14 C9 0.3(4) . .
Ag2 C13 C14 C9 -105.2(3) 2_656 .
C12 C13 C14 Ag2 105.5(3) . 2_656
C10 C9 C14 C13 -1.0(5) . .
N2 C9 C14 C13 178.3(3) . .
C10 C9 C14 Ag2 -83.2(3) . 2_656
N2 C9 C14 Ag2 96.2(3) . 2_656
