#------------------------------------------------------------------------------
#$Date: 2016-03-23 20:48:37 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179425 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/22/4332222.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4332222
loop_
_publ_author_name
'Tretyakov, Eugene'
'Fokin, Sergei'
'Romanenko, Galina'
'Ikorskii, Vladimir'
'Vasilevsky, Sergei'
'Ovcharenko, Victor'
_publ_section_title
;
 2D and 3D Cu(hfac)2Complexes with Nitronyl Nitroxide Biradicals
;
_journal_issue                   9
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3671
_journal_page_last               3678
_journal_paper_doi               10.1021/ic060132e
_journal_volume                  45
_journal_year                    2006
_chemical_formula_sum            'C48 H48 Cu2 F24 N8 O13'
_chemical_formula_weight         1528.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.934(7)
_cell_angle_beta                 114.139(7)
_cell_angle_gamma                103.139(7)
_cell_formula_units_Z            1
_cell_length_a                   11.276(4)
_cell_length_b                   11.488(5)
_cell_length_c                   13.795(5)
_cell_measurement_reflns_used    3112
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      23.21
_cell_measurement_theta_min      2.26
_cell_volume                     1567.0(11)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      110(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0521
_diffrn_reflns_av_sigmaI/netI    0.0580
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            6759
_diffrn_reflns_theta_full        23.28
_diffrn_reflns_theta_max         23.28
_diffrn_reflns_theta_min         1.84
_exptl_absorpt_coefficient_mu    0.814
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    1.619
_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             770
_refine_diff_density_max         0.851
_refine_diff_density_min         -0.489
_refine_diff_density_rms         0.068
_refine_ls_extinction_coef       0.0000(8)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.809
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     537
_refine_ls_number_reflns         4469
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.809
_refine_ls_R_factor_all          0.0475
_refine_ls_R_factor_gt           0.0382
_refine_ls_shift/su_max          5.817
_refine_ls_shift/su_mean         0.028
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0850P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0987
_refine_ls_wR_factor_ref         0.1020
_reflns_number_gt                3452
_reflns_number_total             4469
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic060132esup1.cif
_cod_data_source_block           4_110
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4332222
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Cu1 Cu 0.5000 0.5000 1.0000 0.02861(19) Uani 1 2 d S
O1 O 0.3978(2) 0.53456(19) 1.07853(16) 0.0308(5) Uani 1 1 d .
C1 C 0.2272(3) 0.5878(3) 1.1111(3) 0.0418(9) Uani 1 1 d .
F1 F 0.1117(2) 0.6168(2) 1.06199(18) 0.0619(7) Uani 1 1 d .
F2 F 0.3160(2) 0.6864(2) 1.17625(18) 0.0630(7) Uani 1 1 d .
F3 F 0.2078(3) 0.5071(2) 1.1708(2) 0.0869(9) Uani 1 1 d .
C2 C 0.2763(3) 0.5389(3) 1.0330(3) 0.0286(7) Uani 1 1 d .
C3 C 0.1866(3) 0.5016(3) 0.9256(3) 0.0308(8) Uani 1 1 d .
H3A H 0.104(3) 0.504(3) 0.904(2) 0.021(8) Uiso 1 1 d .
C4 C 0.2248(3) 0.4534(3) 0.8516(2) 0.0263(7) Uani 1 1 d .
C5 C 0.1192(3) 0.4054(3) 0.7358(3) 0.0332(8) Uani 1 1 d .
F4 F -0.00580(17) 0.40940(16) 0.72026(15) 0.0375(5) Uani 1 1 d .
F5 F 0.1525(12) 0.4720(8) 0.6664(10) 0.024(3) Uani 0.50 1 d P
F6 F 0.122(3) 0.298(3) 0.7033(18) 0.030(3) Uani 0.50 1 d P
F51 F 0.1493(18) 0.4672(14) 0.6700(15) 0.074(5) Uani 0.50 1 d P
F61 F 0.100(3) 0.285(3) 0.711(2) 0.058(5) Uani 0.50 1 d P
O2 O 0.3381(2) 0.44122(18) 0.86652(16) 0.0291(5) Uani 1 1 d .
Cu2 Cu 0.0000 0.0000 0.5000 0.01971(17) Uani 1 2 d S
O3 O -0.11643(19) 0.07139(17) 0.54404(15) 0.0211(5) Uani 1 1 d .
C6 C -0.2655(3) 0.1860(3) 0.5375(3) 0.0330(8) Uani 1 1 d .
F7 F -0.2796(19) 0.2939(12) 0.527(2) 0.037(3) Uani 0.50 1 d P
F8 F -0.249(4) 0.174(4) 0.633(3) 0.038(5) Uani 0.50 1 d P
F9 F -0.386(3) 0.108(3) 0.473(2) 0.041(4) Uani 0.50 1 d P
F71 F -0.291(2) 0.2959(17) 0.510(2) 0.068(6) Uani 0.50 1 d P
F81 F -0.226(4) 0.188(4) 0.646(3) 0.041(6) Uani 0.50 1 d P
F91 F -0.378(4) 0.098(3) 0.485(2) 0.063(8) Uani 0.50 1 d P
C7 C -0.1540(3) 0.1624(3) 0.5092(2) 0.0238(7) Uani 1 1 d .
C8 C -0.1096(3) 0.2369(3) 0.4488(3) 0.0294(8) Uani 1 1 d .
H8A H -0.140(3) 0.295(3) 0.432(2) 0.029(9) Uiso 1 1 d .
C9 C -0.0075(3) 0.2228(3) 0.4215(2) 0.0270(7) Uani 1 1 d .
C10 C 0.0383(4) 0.3169(3) 0.3589(3) 0.0419(9) Uani 1 1 d .
F10 F 0.0966(2) 0.42598(19) 0.41916(16) 0.0531(6) Uani 1 1 d .
F11 F -0.0674(2) 0.32520(18) 0.27129(15) 0.0528(6) Uani 1 1 d .
F12 F 0.1253(3) 0.2878(3) 0.3282(3) 0.0972(11) Uani 1 1 d .
O4 O 0.05531(19) 0.14359(17) 0.44177(15) 0.0228(5) Uani 1 1 d .
O01 O 0.5091(2) 0.29677(19) 1.03727(17) 0.0315(5) Uani 1 1 d .
N1 N 0.4161(3) 0.2139(2) 1.04691(19) 0.0280(6) Uani 1 1 d .
C01 C 0.4293(4) 0.1839(3) 1.1551(3) 0.0410(9) Uani 1 1 d .
C02 C 0.5281(6) 0.1053(4) 1.1868(3) 0.0718(16) Uani 1 1 d .
H02A H 0.5410 0.0834 1.2559 0.079(14) Uiso 1 1 calc R
H02B H 0.6131 0.1500 1.1903 0.10(2) Uiso 1 1 calc R
H02C H 0.4920 0.0333 1.1341 0.090(16) Uiso 1 1 calc R
C03 C 0.4852(5) 0.2985(3) 1.2360(3) 0.0518(11) Uani 1 1 d .
H03A H 0.4184 0.3427 1.2196 0.068(13) Uiso 1 1 calc R
H03B H 0.5644 0.3475 1.2329 0.086(16) Uiso 1 1 calc R
H03C H 0.5083 0.2783 1.3069 0.12(2) Uiso 1 1 calc R
C04 C 0.2804(4) 0.1128(3) 1.1238(3) 0.0502(11) Uani 1 1 d .
C05 C 0.2582(5) 0.0137(5) 1.1847(4) 0.0795(14) Uiso 1 1 d .
H05A H 0.3114 -0.0402 1.1832 0.000(6) Uiso 1 1 calc R
H05B H 0.1643 -0.0303 1.1522 0.039(9) Uiso 1 1 calc R
H05C H 0.2844 0.0475 1.2579 0.30(5) Uiso 1 1 calc R
C06 C 0.1898(5) 0.1963(4) 1.1220(4) 0.0678(13) Uani 1 1 d .
H06A H 0.0997 0.1478 1.1032 0.088(16) Uiso 1 1 calc R
H06B H 0.1881 0.2489 1.0699 0.063(13) Uiso 1 1 calc R
H06C H 0.2252 0.2441 1.1919 0.096(16) Uiso 1 1 calc R
N2 N 0.2368(3) 0.0641(2) 1.0074(2) 0.0339(7) Uani 1 1 d .
O02 O 0.1320(3) -0.0230(2) 0.95371(19) 0.0521(7) Uani 1 1 d .
C07 C 0.3119(3) 0.1337(3) 0.9673(2) 0.0242(7) Uani 1 1 d .
C08 C 0.2866(3) 0.1226(3) 0.8554(2) 0.0206(7) Uani 1 1 d .
C09 C 0.1725(3) 0.0513(3) 0.7662(2) 0.0226(7) Uani 1 1 d .
H09A H 0.096(3) 0.004(3) 0.766(2) 0.018(8) Uiso 1 1 d .
N3 N 0.1866(2) 0.0630(2) 0.67566(18) 0.0218(6) Uani 1 1 d .
N4 N 0.3102(2) 0.1417(2) 0.70746(18) 0.0201(6) Uani 1 1 d .
C041 C 0.3638(3) 0.1786(3) 0.6298(3) 0.0250(7) Uani 1 1 d .
H04A H 0.301(3) 0.136(3) 0.559(2) 0.024(8) Uiso 1 1 d .
H04B H 0.448(3) 0.159(2) 0.649(2) 0.021(8) Uiso 1 1 d .
C042 C 0.3809(4) 0.3114(3) 0.6219(3) 0.0249(7) Uani 1 1 d .
H04C H 0.433(3) 0.356(3) 0.692(2) 0.020(8) Uiso 1 1 d .
H04D H 0.300(3) 0.332(2) 0.599(2) 0.016(7) Uiso 1 1 d .
C043 C 0.4426(4) 0.3479(3) 0.5447(3) 0.0309(8) Uani 1 1 d .
H04E H 0.518(3) 0.328(3) 0.566(2) 0.029(9) Uiso 1 1 d .
H04F H 0.372(3) 0.300(3) 0.462(3) 0.033(8) Uiso 1 1 d .
C044 C 0.4726(4) 0.4818(3) 0.5402(3) 0.0307(8) Uani 1 1 d .
H04G H 0.541(3) 0.524(3) 0.611(2) 0.021(8) Uiso 1 1 d .
H04H H 0.403(3) 0.501(3) 0.529(2) 0.025(10) Uiso 1 1 d .
C010 C 0.3718(3) 0.1788(3) 0.8134(2) 0.0224(7) Uani 1 1 d .
H01A H 0.447(3) 0.227(3) 0.844(2) 0.011(8) Uiso 1 1 d .
O1W O 0.3173(12) -0.1826(11) 1.0055(10) 0.179(5) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 Cu1 O2 180.000(1) . 2_667
O2 Cu1 O1 92.35(9) . .
O2 Cu1 O1 87.65(9) 2_667 .
O2 Cu1 O1 87.65(9) . 2_667
O2 Cu1 O1 92.35(9) 2_667 2_667
O1 Cu1 O1 179.998(2) . 2_667
O2 Cu1 O01 93.07(8) . .
O2 Cu1 O01 86.93(8) 2_667 .
O1 Cu1 O01 99.59(8) . .
O1 Cu1 O01 80.41(8) 2_667 .
O2 Cu1 O01 86.93(8) . 2_667
O2 Cu1 O01 93.07(8) 2_667 2_667
O1 Cu1 O01 80.41(8) . 2_667
O1 Cu1 O01 99.59(8) 2_667 2_667
O01 Cu1 O01 179.999(1) . 2_667
C2 O1 Cu1 123.6(2) . .
F3 C1 F2 107.6(3) . .
F3 C1 F1 106.9(3) . .
F2 C1 F1 106.5(3) . .
F3 C1 C2 110.6(3) . .
F2 C1 C2 111.5(3) . .
F1 C1 C2 113.4(3) . .
O1 C2 C3 127.8(3) . .
O1 C2 C1 113.3(3) . .
C3 C2 C1 118.9(3) . .
O1 C2 Cu1 34.77(14) . .
C3 C2 Cu1 93.6(2) . .
C1 C2 Cu1 147.3(2) . .
C2 C3 C4 121.3(3) . .
C2 C3 Cu1 61.34(18) . .
C4 C3 Cu1 60.27(18) . .
O2 C4 C3 128.6(3) . .
O2 C4 C5 112.2(3) . .
C3 C4 C5 119.2(3) . .
O2 C4 Cu1 34.21(13) . .
C3 C4 Cu1 94.5(2) . .
C5 C4 Cu1 146.3(2) . .
F51 C5 F6 101.5(12) . .
F51 C5 F61 113.2(12) . .
F6 C5 F61 13.6(16) . .
F51 C5 F4 107.2(8) . .
F6 C5 F4 112.5(11) . .
F61 C5 F4 101.4(11) . .
F51 C5 F5 0.6(13) . .
F6 C5 F5 101.7(10) . .
F61 C5 F5 113.5(10) . .
F4 C5 F5 107.5(5) . .
F51 C5 C4 111.0(8) . .
F6 C5 C4 111.1(12) . .
F61 C5 C4 110.8(12) . .
F4 C5 C4 112.9(3) . .
F5 C5 C4 110.4(6) . .
F61 F6 C5 92(10) . .
F6 F61 C5 74(10) . .
C4 O2 Cu1 124.5(2) . .
O4 Cu2 O4 180.0 2_556 .
O4 Cu2 O3 92.71(8) 2_556 2_556
O4 Cu2 O3 87.29(8) . 2_556
O4 Cu2 O3 87.29(8) 2_556 .
O4 Cu2 O3 92.71(8) . .
O3 Cu2 O3 180.0 2_556 .
O4 Cu2 N3 95.27(8) 2_556 2_556
O4 Cu2 N3 84.73(8) . 2_556
O3 Cu2 N3 92.66(8) 2_556 2_556
O3 Cu2 N3 87.34(8) . 2_556
O4 Cu2 N3 84.73(8) 2_556 .
O4 Cu2 N3 95.27(8) . .
O3 Cu2 N3 87.34(8) 2_556 .
O3 Cu2 N3 92.66(8) . .
N3 Cu2 N3 180.0 2_556 .
C7 O3 Cu2 122.98(18) . .
F8 C6 F91 98(2) . .
F8 C6 F71 113.0(19) . .
F91 C6 F71 109(2) . .
F8 C6 F7 105.5(19) . .
F91 C6 F7 114.7(19) . .
F71 C6 F7 8(2) . .
F8 C6 F9 105(2) . .
F91 C6 F9 9(3) . .
F71 C6 F9 100.5(18) . .
F7 C6 F9 106.8(19) . .
F8 C6 F81 10(4) . .
F91 C6 F81 108(2) . .
F71 C6 F81 109.4(19) . .
F7 C6 F81 101.4(19) . .
F9 C6 F81 115(2) . .
F8 C6 C7 114.7(16) . .
F91 C6 C7 109.8(15) . .
F71 C6 C7 111.3(9) . .
F7 C6 C7 113.0(8) . .
F9 C6 C7 110.9(13) . .
F81 C6 C7 109.1(15) . .
C6 F8 F91 41.7(16) . .
C6 F91 F8 40.0(14) . .
O3 C7 C8 127.9(3) . .
O3 C7 C6 113.2(3) . .
C8 C7 C6 118.9(3) . .
O3 C7 Cu2 35.27(12) . .
C8 C7 Cu2 93.0(2) . .
C6 C7 Cu2 147.3(2) . .
C7 C8 C9 122.4(3) . .
C7 C8 Cu2 61.83(17) . .
C9 C8 Cu2 61.12(17) . .
O4 C9 C8 128.6(3) . .
O4 C9 C10 114.2(3) . .
C8 C9 C10 117.2(3) . .
O4 C9 Cu2 35.57(13) . .
C8 C9 Cu2 93.49(19) . .
C10 C9 Cu2 148.9(2) . .
F12 C10 F11 108.0(3) . .
F12 C10 F10 107.8(3) . .
F11 C10 F10 107.8(3) . .
F12 C10 C9 111.7(3) . .
F11 C10 C9 110.4(3) . .
F10 C10 C9 111.0(3) . .
C9 O4 Cu2 122.61(19) . .
N1 O01 Cu1 126.93(17) . .
O01 N1 C07 126.5(2) . .
O01 N1 C01 121.6(2) . .
C07 N1 C01 111.1(3) . .
C03 C01 N1 110.1(3) . .
C03 C01 C04 116.3(3) . .
N1 C01 C04 99.6(2) . .
C03 C01 C02 110.3(3) . .
N1 C01 C02 105.6(3) . .
C04 C01 C02 113.9(4) . .
C05 C04 N2 111.3(3) . .
C05 C04 C01 117.0(4) . .
N2 C04 C01 99.8(3) . .
C05 C04 C06 109.4(4) . .
N2 C04 C06 105.3(3) . .
C01 C04 C06 113.1(3) . .
O02 N2 C07 125.8(3) . .
O02 N2 C04 122.9(3) . .
C07 N2 C04 110.9(3) . .
N1 C07 N2 109.6(3) . .
N1 C07 C08 125.0(3) . .
N2 C07 C08 125.4(3) . .
C010 C08 C09 104.7(3) . .
C010 C08 C07 127.0(3) . .
C09 C08 C07 128.3(3) . .
N3 C09 C08 111.1(3) . .
C09 N3 N4 104.7(2) . .
C09 N3 Cu2 122.87(19) . .
N4 N3 Cu2 130.14(17) . .
C010 N4 N3 112.2(2) . .
C010 N4 C041 126.3(3) . .
N3 N4 C041 121.5(2) . .
N4 C041 C042 112.5(2) . .
C041 C042 C043 111.2(3) . .
C044 C043 C042 113.6(3) . .
C043 C044 C044 114.2(4) . 2_666
N4 C010 C08 107.3(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cu1 O2 1.934(2) .
Cu1 O2 1.934(2) 2_667
Cu1 O1 1.961(2) .
Cu1 O1 1.961(2) 2_667
Cu1 O01 2.432(2) .
Cu1 O01 2.432(2) 2_667
O1 C2 1.266(4) .
C1 F3 1.312(4) .
C1 F2 1.318(4) .
C1 F1 1.329(4) .
C1 C2 1.533(5) .
C2 C3 1.383(5) .
C3 C4 1.394(5) .
C4 O2 1.251(4) .
C4 C5 1.527(5) .
C5 F51 1.285(17) .
C5 F6 1.30(3) .
C5 F61 1.35(3) .
C5 F4 1.348(4) .
C5 F5 1.371(13) .
F6 F61 0.32(4) .
Cu2 O4 1.9578(19) 2_556
Cu2 O4 1.9579(19) .
Cu2 O3 1.9637(19) 2_556
Cu2 O3 1.9638(19) .
Cu2 N3 2.405(2) 2_556
Cu2 N3 2.405(2) .
O3 C7 1.260(3) .
C6 F8 1.28(3) .
C6 F91 1.32(3) .
C6 F71 1.39(2) .
C6 F7 1.293(18) .
C6 F9 1.34(3) .
C6 F81 1.38(4) .
C6 C7 1.534(4) .
F8 F91 1.97(5) .
C7 C8 1.377(4) .
C8 C9 1.388(4) .
C9 O4 1.251(4) .
C9 C10 1.545(5) .
C10 F12 1.314(4) .
C10 F11 1.332(4) .
C10 F10 1.328(4) .
O01 N1 1.303(3) .
N1 C07 1.336(4) .
N1 C01 1.504(4) .
C01 C03 1.508(5) .
C01 C04 1.556(5) .
C01 C02 1.532(5) .
C04 C05 1.485(6) .
C04 N2 1.507(4) .
C04 C06 1.547(6) .
N2 O02 1.272(3) .
N2 C07 1.336(4) .
C07 C08 1.443(4) .
C08 C010 1.374(4) .
C08 C09 1.401(4) .
C09 N3 1.331(4) .
N3 N4 1.355(3) .
N4 C010 1.331(4) .
N4 C041 1.467(4) .
C041 C042 1.510(4) .
C042 C043 1.521(4) .
C043 C044 1.508(5) .
C044 C044 1.510(6) 2_666
