#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/23/4332328.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4332328
loop_
_publ_author_name
'Cametti, Massimo'
'Nissinen, Maija'
'Dalla Cort, Antonella'
'Rissanen, Kari'
'Mandolini, Luigi'
_publ_section_title
;
 Crystal Structure of a CsF−Uranyl−Salen Complex. An Unusual
 Cesium−Chlorine Coordination
;
_journal_issue                   16
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6099
_journal_page_last               6101
_journal_paper_doi               10.1021/ic060251u
_journal_volume                  45
_journal_year                    2006
_chemical_formula_moiety         'C30 H26 N2 O6 U1, CH4O, 0.5(C3H6O)'
_chemical_formula_sum            'C32.5 H33 N2 O7.5 U'
_chemical_formula_weight         809.64
_chemical_name_common            'Compound X'
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                103.338(2)
_cell_angle_beta                 95.853(2)
_cell_angle_gamma                104.600(3)
_cell_formula_units_Z            2
_cell_length_a                   10.0159(5)
_cell_length_b                   10.4519(4)
_cell_length_c                   15.2798(7)
_cell_measurement_reflns_used    3484
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      24.713
_cell_measurement_theta_min      0.407
_cell_volume                     1484.23(12)
_computing_cell_refinement       'HKL Scalepack (Otwinowski & Minor 1997)'
_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor 1997'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'CCD rotation images, thick slices'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0429
_diffrn_reflns_av_sigmaI/netI    0.0527
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            7938
_diffrn_reflns_theta_full        24.71
_diffrn_reflns_theta_max         24.71
_diffrn_reflns_theta_min         2.09
_exptl_absorpt_coefficient_mu    5.522
_exptl_absorpt_correction_T_max  0.2881
_exptl_absorpt_correction_T_min  0.2161
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.812
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             788
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.30
_refine_diff_density_max         2.292
_refine_diff_density_min         -2.937
_refine_diff_density_rms         0.247
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.142
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     399
_refine_ls_number_reflns         4987
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.142
_refine_ls_R_factor_all          0.0514
_refine_ls_R_factor_gt           0.0451
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0704P)²+6.7755P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1189
_refine_ls_wR_factor_ref         0.1225
_reflns_number_gt                4553
_reflns_number_total             4987
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic060251usup1.cif
_cod_data_source_block           ant044
_cod_original_cell_volume        1484.22(12)
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C32.50 H33 N2 O7.50 U'
_cod_database_code               4332328
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U1 U -0.27760(3) 0.31023(3) 0.244251(18) 0.01530(13) Uani 1 1 d .
C1 C -0.3278(11) 0.6317(9) 0.2869(6) 0.028(2) Uani 1 1 d .
H1A H -0.3910 0.6911 0.2948 0.034 Uiso 1 1 calc R
H1B H -0.2596 0.6648 0.2488 0.034 Uiso 1 1 calc R
C2 C -0.2523(9) 0.6360(8) 0.3783(6) 0.0237(19) Uani 1 1 d .
H2A H -0.1924 0.7303 0.4086 0.028 Uiso 1 1 calc R
H2B H -0.3210 0.6093 0.4178 0.028 Uiso 1 1 calc R
C8 C -0.5419(10) 0.4647(9) 0.2164(5) 0.0227(19) Uani 1 1 d .
H8 H -0.5790 0.5409 0.2290 0.027 Uiso 1 1 calc R
C9 C -0.6382(9) 0.3327(9) 0.1695(5) 0.0217(18) Uani 1 1 d .
C10 C -0.5941(8) 0.2200(8) 0.1260(5) 0.0180(17) Uani 1 1 d .
C11 C -0.6993(9) 0.0996(9) 0.0787(5) 0.0205(18) Uani 1 1 d .
C12 C -0.8392(9) 0.0900(10) 0.0772(6) 0.028(2) Uani 1 1 d .
H12 H -0.9070 0.0055 0.0466 0.033 Uiso 1 1 calc R
C13 C -0.8836(10) 0.2006(10) 0.1190(6) 0.030(2) Uani 1 1 d .
H13 H -0.9804 0.1930 0.1169 0.036 Uiso 1 1 calc R
C14 C -0.7842(10) 0.3212(10) 0.1636(6) 0.028(2) Uani 1 1 d .
H14 H -0.8130 0.3988 0.1911 0.033 Uiso 1 1 calc R
C16 C -0.6037(9) -0.0885(9) 0.0794(6) 0.0247(19) Uani 1 1 d .
H16A H -0.5292 -0.0240 0.1289 0.030 Uiso 1 1 calc R
H16B H -0.5600 -0.1489 0.0393 0.030 Uiso 1 1 calc R
C17 C -0.7109(9) -0.1749(8) 0.1205(6) 0.0208(17) Uani 1 1 d .
C18 C -0.6806(11) -0.1742(9) 0.2110(6) 0.031(2) Uani 1 1 d .
H18 H -0.5943 -0.1168 0.2474 0.037 Uiso 1 1 calc R
C19 C -0.7755(12) -0.2569(11) 0.2485(7) 0.040(2) Uani 1 1 d .
H19 H -0.7531 -0.2570 0.3104 0.048 Uiso 1 1 calc R
C20 C -0.9004(11) -0.3381(10) 0.1981(7) 0.040(3) Uani 1 1 d .
H20 H -0.9664 -0.3929 0.2248 0.048 Uiso 1 1 calc R
C21 C -0.9297(12) -0.3396(12) 0.1086(8) 0.049(3) Uani 1 1 d .
H21 H -1.0163 -0.3972 0.0727 0.059 Uiso 1 1 calc R
C22 C -0.8349(11) -0.2585(11) 0.0691(7) 0.039(2) Uani 1 1 d .
H22 H -0.8564 -0.2612 0.0066 0.047 Uiso 1 1 calc R
C24 C -0.0388(9) 0.5852(8) 0.4075(5) 0.0212(18) Uani 1 1 d .
H24 H -0.0109 0.6761 0.4462 0.025 Uiso 1 1 calc R
C25 C 0.0670(9) 0.5113(8) 0.4030(5) 0.0189(17) Uani 1 1 d .
C26 C 0.0350(9) 0.3683(9) 0.3664(5) 0.0205(18) Uani 1 1 d .
C27 C 0.1433(9) 0.3061(8) 0.3667(5) 0.0183(17) Uani 1 1 d .
C28 C 0.2812(9) 0.3848(9) 0.3981(6) 0.0255(19) Uani 1 1 d .
H28 H 0.3547 0.3424 0.3936 0.031 Uiso 1 1 calc R
C29 C 0.3129(9) 0.5282(9) 0.4368(6) 0.027(2) Uani 1 1 d .
H29 H 0.4070 0.5818 0.4599 0.032 Uiso 1 1 calc R
C30 C 0.2071(9) 0.5887(9) 0.4407(6) 0.0228(18) Uani 1 1 d .
H30 H 0.2276 0.6841 0.4690 0.027 Uiso 1 1 calc R
C32 C 0.2060(10) 0.0936(9) 0.3246(6) 0.027(2) Uani 1 1 d .
H32A H 0.2883 0.1470 0.3049 0.032 Uiso 1 1 calc R
H32B H 0.1680 0.0040 0.2784 0.032 Uiso 1 1 calc R
C33 C 0.2511(9) 0.0703(9) 0.4158(6) 0.0237(19) Uani 1 1 d .
C34 C 0.1539(10) -0.0115(9) 0.4546(6) 0.028(2) Uani 1 1 d .
H34 H 0.0601 -0.0514 0.4234 0.034 Uiso 1 1 calc R
C35 C 0.1924(11) -0.0351(9) 0.5375(6) 0.030(2) Uani 1 1 d .
H35 H 0.1257 -0.0921 0.5624 0.036 Uiso 1 1 calc R
C36 C 0.3279(10) 0.0240(9) 0.5844(6) 0.029(2) Uani 1 1 d .
H36 H 0.3540 0.0087 0.6418 0.034 Uiso 1 1 calc R
C37 C 0.4257(9) 0.1057(9) 0.5472(6) 0.026(2) Uani 1 1 d .
H37 H 0.5188 0.1467 0.5794 0.031 Uiso 1 1 calc R
C38 C 0.3882(9) 0.1278(8) 0.4629(6) 0.0227(18) Uani 1 1 d .
H38 H 0.4562 0.1822 0.4373 0.027 Uiso 1 1 calc R
N7 N -0.4094(8) 0.4877(7) 0.2427(4) 0.0211(15) Uani 1 1 d .
N23 N -0.1655(8) 0.5406(6) 0.3649(5) 0.0202(15) Uani 1 1 d .
O1 O -0.3912(7) 0.2409(6) 0.3145(4) 0.0257(13) Uani 1 1 d .
O2 O -0.1686(6) 0.3840(6) 0.1733(4) 0.0238(13) Uani 1 1 d .
O10 O -0.4609(6) 0.2283(6) 0.1269(4) 0.0218(12) Uani 1 1 d .
O15 O -0.6633(6) -0.0113(6) 0.0270(4) 0.0219(13) Uani 1 1 d .
O26 O -0.0963(6) 0.2912(5) 0.3348(4) 0.0193(12) Uani 1 1 d .
O31 O 0.1007(6) 0.1663(6) 0.3297(4) 0.0240(13) Uani 1 1 d .
O100 O -0.2559(7) 0.0852(6) 0.1576(4) 0.0247(13) Uani 1 1 d .
H100 H -0.2811 0.0634 0.1007 0.037 Uiso 1 1 calc R
C101 C -0.2038(12) -0.0223(8) 0.1836(7) 0.037(2) Uani 1 1 d .
H10A H -0.1459 -0.0534 0.1399 0.055 Uiso 1 1 calc R
H10B H -0.2832 -0.0998 0.1832 0.055 Uiso 1 1 calc R
H10C H -0.1475 0.0144 0.2449 0.055 Uiso 1 1 calc R
C102 C -0.6278(16) -0.4965(16) -0.0084(9) 0.066(4) Uani 1 1 d .
H10D H -0.7194 -0.5558 -0.0421 0.099 Uiso 1 1 calc R
H10E H -0.6072 -0.4094 -0.0252 0.099 Uiso 1 1 calc R
H10F H -0.6292 -0.4788 0.0573 0.099 Uiso 1 1 calc R
O103 O -0.557(2) -0.6754(17) -0.0861(12) 0.058(5) Uani 0.50 1 d P
C104 C -0.523(2) -0.562(2) -0.0303(13) 0.038(5) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O1 U1 O2 177.6(2) .
O1 U1 O26 88.8(3) .
O2 U1 O26 93.1(2) .
O1 U1 O10 88.4(3) .
O2 U1 O10 90.4(2) .
O26 U1 O10 153.5(2) .
O1 U1 N7 88.7(3) .
O2 U1 N7 88.9(3) .
O26 U1 N7 136.3(2) .
O10 U1 N7 70.0(2) .
O1 U1 N23 94.3(3) .
O2 U1 N23 85.0(2) .
O26 U1 N23 71.0(2) .
O10 U1 N23 135.5(2) .
N7 U1 N23 65.6(2) .
N7 C1 C2 107.6(7) .
N23 C2 C1 109.0(7) .
N7 C8 C9 125.3(8) .
C10 C9 C14 119.9(8) .
C10 C9 C8 122.9(8) .
C14 C9 C8 117.1(8) .
O10 C10 C11 121.3(7) .
O10 C10 C9 121.7(8) .
C11 C10 C9 117.0(8) .
C12 C11 O15 118.2(8) .
C12 C11 C10 121.7(8) .
O15 C11 C10 119.9(7) .
C11 C12 C13 121.6(9) .
C14 C13 C12 118.3(9) .
C13 C14 C9 121.3(8) .
O15 C16 C17 112.7(7) .
C22 C17 C18 119.2(9) .
C22 C17 C16 121.2(8) .
C18 C17 C16 119.4(8) .
C19 C18 C17 120.1(9) .
C20 C19 C18 120.9(10) .
C19 C20 C21 119.0(9) .
C20 C21 C22 121.1(10) .
C17 C22 C21 119.7(10) .
N23 C24 C25 127.0(8) .
C26 C25 C30 119.7(8) .
C26 C25 C24 123.2(8) .
C30 C25 C24 117.1(7) .
O26 C26 C27 119.6(7) .
O26 C26 C25 121.3(8) .
C27 C26 C25 119.0(8) .
O31 C27 C28 125.0(7) .
O31 C27 C26 114.3(7) .
C28 C27 C26 120.6(8) .
C27 C28 C29 120.2(8) .
C30 C29 C28 119.5(8) .
C29 C30 C25 120.8(8) .
O31 C32 C33 111.4(7) .
C38 C33 C34 118.5(8) .
C38 C33 C32 121.8(8) .
C34 C33 C32 119.7(8) .
C35 C34 C33 120.9(9) .
C36 C35 C34 120.2(9) .
C35 C36 C37 119.7(8) .
C36 C37 C38 120.3(8) .
C37 C38 C33 120.3(8) .
C8 N7 C1 116.9(7) .
C8 N7 U1 127.0(6) .
C1 N7 U1 115.7(5) .
C24 N23 C2 117.2(7) .
C24 N23 U1 126.7(6) .
C2 N23 U1 115.8(5) .
C10 O10 U1 130.5(5) .
C11 O15 C16 115.0(6) .
C26 O26 U1 134.2(5) .
C27 O31 C32 118.3(7) .
O103 C104 C102 119(2) .
O103 C104 C102 116.3(19) 2_445
C102 C104 C102 124.7(16) 2_445
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 O1 1.778(6) .
U1 O2 1.779(6) .
U1 O26 2.247(5) .
U1 O10 2.268(6) .
U1 N7 2.536(7) .
U1 N23 2.574(6) .
C1 N7 1.479(11) .
C1 C2 1.504(12) .
C2 N23 1.473(11) .
C8 N7 1.291(11) .
C8 C9 1.441(13) .
C9 C10 1.409(12) .
C9 C14 1.428(12) .
C10 O10 1.314(10) .
C10 C11 1.405(12) .
C11 C12 1.377(12) .
C11 O15 1.394(10) .
C12 C13 1.385(14) .
C13 C14 1.370(14) .
C16 O15 1.446(10) .
C16 C17 1.508(12) .
C17 C22 1.363(13) .
C17 C18 1.383(13) .
C18 C19 1.380(14) .
C19 C20 1.358(15) .
C20 C21 1.365(16) .
C21 C22 1.390(15) .
C24 N23 1.282(11) .
C24 C25 1.459(12) .
C25 C26 1.409(12) .
C25 C30 1.415(12) .
C26 O26 1.330(10) .
C26 C27 1.398(12) .
C27 O31 1.376(10) .
C27 C28 1.387(12) .
C28 C29 1.418(13) .
C29 C30 1.364(13) .
C32 O31 1.445(10) .
C32 C33 1.513(12) .
C33 C38 1.395(12) .
C33 C34 1.401(13) .
C34 C35 1.382(13) .
C35 C36 1.382(14) .
C36 C37 1.389(13) .
C37 C38 1.391(12) .
O100 C101 1.467(11) .
C102 C104 1.42(3) .
O103 C104 1.23(3) .
C104 C102 1.48(3) 2_445
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O100 H100 O15 0.84 1.88 2.724(8) 178.8 2_455
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
N7 C1 C2 N23 56.5(10)
N7 C8 C9 C10 -17.0(13)
N7 C8 C9 C14 166.6(8)
C14 C9 C10 O10 177.3(7)
C8 C9 C10 O10 1.0(12)
C14 C9 C10 C11 -0.4(12)
C8 C9 C10 C11 -176.6(7)
O10 C10 C11 C12 -179.8(8)
C9 C10 C11 C12 -2.1(12)
O10 C10 C11 O15 -3.8(11)
C9 C10 C11 O15 173.9(7)
O15 C11 C12 C13 -173.3(8)
C10 C11 C12 C13 2.8(13)
C11 C12 C13 C14 -0.7(13)
C12 C13 C14 C9 -1.8(13)
C10 C9 C14 C13 2.4(13)
C8 C9 C14 C13 178.9(8)
O15 C16 C17 C22 49.2(12)
O15 C16 C17 C18 -133.8(8)
C22 C17 C18 C19 -0.4(14)
C16 C17 C18 C19 -177.5(8)
C17 C18 C19 C20 -1.1(15)
C18 C19 C20 C21 1.7(16)
C19 C20 C21 C22 -0.9(18)
C18 C17 C22 C21 1.1(15)
C16 C17 C22 C21 178.2(10)
C20 C21 C22 C17 -0.5(18)
N23 C24 C25 C26 -14.9(13)
N23 C24 C25 C30 167.4(8)
C30 C25 C26 O26 176.4(7)
C24 C25 C26 O26 -1.2(12)
C30 C25 C26 C27 -1.1(11)
C24 C25 C26 C27 -178.7(7)
O26 C26 C27 O31 2.3(11)
C25 C26 C27 O31 179.8(7)
O26 C26 C27 C28 179.0(7)
C25 C26 C27 C28 -3.4(12)
O31 C27 C28 C29 -178.7(8)
C26 C27 C28 C29 4.9(12)
C27 C28 C29 C30 -1.8(13)
C28 C29 C30 C25 -2.7(13)
C26 C25 C30 C29 4.2(12)
C24 C25 C30 C29 -178.1(8)
O31 C32 C33 C38 -116.9(9)
O31 C32 C33 C34 63.5(10)
C38 C33 C34 C35 0.0(13)
C32 C33 C34 C35 179.6(8)
C33 C34 C35 C36 1.0(13)
C34 C35 C36 C37 -0.9(13)
C35 C36 C37 C38 -0.3(13)
C36 C37 C38 C33 1.3(13)
C34 C33 C38 C37 -1.2(12)
C32 C33 C38 C37 179.2(8)
C9 C8 N7 C1 177.9(8)
C9 C8 N7 U1 -10.1(12)
C2 C1 N7 C8 125.0(8)
C2 C1 N7 U1 -48.0(8)
O1 U1 N7 C8 -56.9(7)
O2 U1 N7 C8 122.7(7)
O26 U1 N7 C8 -143.9(6)
O10 U1 N7 C8 31.9(6)
N23 U1 N7 C8 -152.2(7)
O1 U1 N7 C1 115.3(6)
O2 U1 N7 C1 -65.1(6)
O26 U1 N7 C1 28.3(7)
O10 U1 N7 C1 -155.9(6)
N23 U1 N7 C1 19.9(5)
C25 C24 N23 C2 -178.2(8)
C25 C24 N23 U1 -5.5(12)
C1 C2 N23 C24 133.2(8)
C1 C2 N23 U1 -40.3(9)
O1 U1 N23 C24 112.1(7)
O2 U1 N23 C24 -70.3(7)
O26 U1 N23 C24 24.8(6)
O10 U1 N23 C24 -155.8(6)
N7 U1 N23 C24 -161.3(7)
O1 U1 N23 C2 -75.1(6)
O2 U1 N23 C2 102.6(6)
O26 U1 N23 C2 -162.4(6)
O10 U1 N23 C2 17.1(7)
N7 U1 N23 C2 11.5(5)
C11 C10 O10 U1 -133.8(6)
C9 C10 O10 U1 48.6(10)
O1 U1 O10 C10 36.9(7)
O2 U1 O10 C10 -141.0(7)
O26 U1 O10 C10 121.2(7)
N7 U1 O10 C10 -52.3(7)
N23 U1 O10 C10 -57.7(8)
C12 C11 O15 C16 -109.0(8)
C10 C11 O15 C16 74.9(9)
C17 C16 O15 C11 72.9(9)
C27 C26 O26 U1 -136.9(6)
C25 C26 O26 U1 45.7(11)
O1 U1 O26 C26 -141.8(7)
O2 U1 O26 C26 36.9(7)
O10 U1 O26 C26 134.1(7)
N7 U1 O26 C26 -54.8(8)
N23 U1 O26 C26 -46.8(7)
C28 C27 O31 C32 1.6(11)
C26 C27 O31 C32 178.2(7)
C33 C32 O31 C27 79.2(9)
