#------------------------------------------------------------------------------
#$Date: 2016-03-23 21:05:52 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179439 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/36/4333609.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4333609
loop_
_publ_author_name
'Eric M. Villa'
'Connor J. Marr'
'Juan Diwu'
'Evgeny V. Alekseev'
'Wulf Depmeier'
'Thomas E. Albrecht-Schmitt'
_publ_section_title
;
 From Order to Disorder and Back Again: In Situ Hydrothermal Redox
 Reactions of Uranium Phosphites and Phosphates
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              965
_journal_page_last               973
_journal_paper_doi               10.1021/ic302198w
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         Cs4[U6(PO4)8(HPO4)(HPO3)]
_chemical_formula_sum            'Cs4 H0 O39 P10 U6'
_chemical_formula_weight         2893.52
_chemical_name_common            'Cesium Uranium(IV) Phosphate-Phosphite'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           59
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ab 2a'
_symmetry_space_group_name_H-M   'P m m n :2'
_atom_sites_solution_hydrogens   none
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   6.9321(5)
_cell_length_b                   26.9350(19)
_cell_length_c                   10.9137(8)
_cell_measurement_reflns_used    2791
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.28
_cell_measurement_theta_min      0.76
_cell_volume                     2037.8(3)
_computing_cell_refinement       'smart saint'
_computing_data_collection       smart
_computing_data_reduction        SAINT
_computing_molecular_graphics    'SHELXP-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXCIF-97 (Sheldrick, 2000)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'BRUKER apex II'
_diffrn_measurement_method       '0.5 wide w/ exposures'
_diffrn_radiation_monochromator  'Quazar optics'
_diffrn_radiation_source         'Imus microfocused'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0437
_diffrn_reflns_av_sigmaI/netI    0.0129
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            75425
_diffrn_reflns_theta_full        28.28
_diffrn_reflns_theta_max         28.28
_diffrn_reflns_theta_min         0.76
_exptl_absorpt_coefficient_mu    27.784
_exptl_absorpt_correction_T_max  0.459
_exptl_absorpt_correction_T_min  0.206
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   SHELTXPREP
_exptl_crystal_colour            Green
_exptl_crystal_density_diffrn    4.716
_exptl_crystal_density_meas      ?
_exptl_crystal_description       Plate
_exptl_crystal_F_000             2468
_exptl_crystal_size_max          0.060
_exptl_crystal_size_mid          0.053
_exptl_crystal_size_min          0.028
_refine_diff_density_max         4.531
_refine_diff_density_min         -4.769
_refine_diff_density_rms         0.369
_refine_ls_extinction_coef       0.00009(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.089
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     223
_refine_ls_number_reflns         2791
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.089
_refine_ls_R_factor_all          0.0410
_refine_ls_R_factor_gt           0.0377
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0411P)²+83.4546P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0978
_refine_ls_wR_factor_ref         0.1003
_reflns_number_gt                2586
_reflns_number_total             2791
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic302198w_si_002_3.cif
_cod_data_source_block           Cs_U(IV)_PO4_HPO4_HPO3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'N/A' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      'P m m n'
_cod_database_code               4333609
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'-x, y+1/2, -z'
'x+1/2, -y, -z'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'x, -y-1/2, z'
'-x-1/2, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
U1 U 0.7500 0.127813(18) 0.72090(4) 0.01505(13) Uani 1 2 d S
U2 U 0.7500 0.040056(18) 1.15507(5) 0.01814(14) Uani 1 2 d S
U3 U 0.7500 0.2500 0.29125(6) 0.01047(15) Uani 1 4 d S
U4 U 0.2500 0.11427(3) 1.16500(8) 0.01347(19) Uani 0.50 2 d SP
Cs1 Cs 0.2500 0.12841(11) 1.3019(4) 0.0689(10) Uani 0.50 2 d SP
Cs2A Cs 0.2500 0.18981(9) 0.5419(2) 0.0276(4) Uani 0.44 2 d SP
Cs2B Cs 0.2500 0.1235(9) 0.541(2) 0.013(4) Uani 0.03 2 d SP
Cs2C Cs 0.2500 0.1593(12) 0.485(3) 0.031(7) Uani 0.03 2 d SP
Cs3A Cs 1.0382(4) 0.2500 0.9025(3) 0.0435(6) Uani 0.45 2 d SP
Cs3B Cs 0.7500 0.2500 0.899(3) 0.026(6) Uani 0.04 4 d SP
Cs4A Cs 0.980(8) -0.004(2) 0.488(3) 0.076(10) Uani 0.17 1 d P
Cs4B Cs 0.7500 -0.0342(8) 0.4910(15) 0.059(5) Uani 0.09 2 d SP
Cs4C Cs 0.897(7) -0.0313(11) 0.489(4) 0.122(16) Uani 0.06 1 d P
P1 P 0.7500 0.14973(11) 1.0553(3) 0.0114(6) Uani 1 2 d S
P2 P 0.2500 -0.00415(12) 1.1703(3) 0.0142(6) Uani 1 2 d S
P3 P 0.2500 0.2500 1.2071(7) 0.0327(13) Uani 1 4 d S
P4 P 0.7500 -0.09679(14) 1.1734(4) 0.0232(8) Uani 1 2 d S
P5 P 0.6478(8) 0.12195(17) 1.3904(4) 0.0200(10) Uani 0.50 1 d P
P6 P 0.7500 0.2500 0.6139(10) 0.064(2) Uani 1 4 d S
O1 O 0.7500 0.2001(3) 1.1154(9) 0.0204(19) Uani 1 2 d S
O2 O 0.7500 0.1562(4) 0.9168(8) 0.0182(18) Uani 1 2 d S
O3 O 0.7500 0.0760(4) 1.3383(9) 0.022(2) Uani 1 2 d S
O4 O 0.2500 -0.0431(4) 1.2688(10) 0.024(2) Uani 1 2 d S
O5 O 0.5792(10) 0.1169(2) 1.0961(6) 0.0193(13) Uani 1 1 d .
O6 O 0.4256(11) 0.0304(3) 1.1840(8) 0.0289(16) Uani 1 1 d .
O7 O 0.7500 0.1690(4) 1.3562(9) 0.029(2) Uani 1 2 d S
O8 O 0.5700(11) -0.1174(3) 1.2332(7) 0.0258(15) Uani 1 1 d .
O9 O 0.2500 -0.0293(5) 1.0455(10) 0.038(3) Uani 1 2 d S
O10 O 0.7500 -0.0400(5) 1.1925(17) 0.051(4) Uani 1 2 d S
O11 O 0.0728(17) 0.2500 1.2858(13) 0.040(3) Uani 1 2 d S
O12 O 0.7500 -0.1108(9) 1.0396(13) 0.078(7) Uani 1 2 d S
O13 O 0.2500 0.2964(9) 1.128(2) 0.092(8) Uani 1 2 d S
O14 O 0.443(3) 0.1221(8) 1.3396(14) 0.043(5) Uani 0.50 1 d P
O15 O 0.630(2) 0.1169(5) 1.5299(13) 0.028(3) Uiso 0.55 1 d P
O16 O 0.7500 0.2931(9) 0.683(2) 0.072(6) Uiso 0.79 2 d SP
O17 O 0.841(4) 0.2500 0.500(3) 0.064(7) Uiso 0.62 2 d SP
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O16 U1 O15 87.2(7) 2_655 1_554
O16 U1 O15 87.2(7) 2_655 8_754
O15 U1 O15 43.0(8) 1_554 8_754
O16 U1 O2 81.4(7) 2_655 .
O15 U1 O2 155.7(4) 1_554 .
O15 U1 O2 155.7(4) 8_754 .
O16 U1 O4 171.8(7) 2_655 5_657
O15 U1 O4 85.1(4) 1_554 5_657
O15 U1 O4 85.1(4) 8_754 5_657
O2 U1 O4 106.8(4) . 5_657
O16 U1 O8 99.3(2) 2_655 4_557
O15 U1 O8 122.7(4) 1_554 4_557
O15 U1 O8 80.2(4) 8_754 4_557
O2 U1 O8 80.5(2) . 4_557
O4 U1 O8 82.34(19) 5_657 4_557
O16 U1 O8 99.3(2) 2_655 5_657
O15 U1 O8 80.2(4) 1_554 5_657
O15 U1 O8 122.7(4) 8_754 5_657
O2 U1 O8 80.5(2) . 5_657
O4 U1 O8 82.34(19) 5_657 5_657
O8 U1 O8 151.0(4) 4_557 5_657
O16 U1 Cs3B 41.6(8) 2_655 .
O15 U1 Cs3B 125.5(5) 1_554 .
O15 U1 Cs3B 125.5(5) 8_754 .
O2 U1 Cs3B 39.7(5) . .
O4 U1 Cs3B 146.6(5) 5_657 .
O8 U1 Cs3B 89.7(2) 4_557 .
O8 U1 Cs3B 89.7(2) 5_657 .
O16 U1 Cs2B 86.2(5) 2_655 .
O15 U1 Cs2B 39.0(5) 1_554 .
O15 U1 Cs2B 82.0(5) 8_754 .
O2 U1 Cs2B 118.3(3) . .
O4 U1 Cs2B 89.7(4) 5_657 .
O8 U1 Cs2B 161.1(4) 4_557 .
O8 U1 Cs2B 42.4(3) 5_657 .
Cs3B U1 Cs2B 106.0(4) . .
O16 U1 Cs2B 86.2(5) 2_655 1_655
O15 U1 Cs2B 82.0(5) 1_554 1_655
O15 U1 Cs2B 39.0(5) 8_754 1_655
O2 U1 Cs2B 118.3(3) . 1_655
O4 U1 Cs2B 89.7(4) 5_657 1_655
O8 U1 Cs2B 42.4(3) 4_557 1_655
O8 U1 Cs2B 161.1(4) 5_657 1_655
Cs3B U1 Cs2B 106.0(4) . 1_655
Cs2B U1 Cs2B 120.8(6) . 1_655
O16 U1 Cs4C 119.9(7) 2_655 4_456
O15 U1 Cs4C 37.9(6) 1_554 4_456
O15 U1 Cs4C 68.6(7) 8_754 4_456
O2 U1 Cs4C 135.6(6) . 4_456
O4 U1 Cs4C 54.2(5) 5_657 4_456
O8 U1 Cs4C 127.0(6) 4_557 4_456
O8 U1 Cs4C 58.9(7) 5_657 4_456
Cs3B U1 Cs4C 143.3(6) . 4_456
Cs2B U1 Cs4C 38.2(6) . 4_456
Cs2B U1 Cs4C 102.6(7) 1_655 4_456
O16 U1 Cs4C 119.9(7) 2_655 5_756
O15 U1 Cs4C 68.6(7) 1_554 5_756
O15 U1 Cs4C 37.9(6) 8_754 5_756
O2 U1 Cs4C 135.6(6) . 5_756
O4 U1 Cs4C 54.2(5) 5_657 5_756
O8 U1 Cs4C 58.9(7) 4_557 5_756
O8 U1 Cs4C 127.0(6) 5_657 5_756
Cs3B U1 Cs4C 143.3(6) . 5_756
Cs2B U1 Cs4C 102.6(7) . 5_756
Cs2B U1 Cs4C 38.2(6) 1_655 5_756
Cs4C U1 Cs4C 70.5(12) 4_456 5_756
O10 U2 O9 93.2(6) . 5_657
O10 U2 O3 105.1(6) . .
O9 U2 O3 161.7(4) 5_657 .
O10 U2 O6 82.11(19) . 8_755
O9 U2 O6 97.0(2) 5_657 8_755
O3 U2 O6 85.7(2) . 8_755
O10 U2 O6 82.1(2) . .
O9 U2 O6 97.0(2) 5_657 .
O3 U2 O6 85.7(2) . .
O6 U2 O6 159.4(4) 8_755 .
O10 U2 O5 150.67(19) . 8_755
O9 U2 O5 81.5(3) 5_657 8_755
O3 U2 O5 82.5(3) . 8_755
O6 U2 O5 70.1(2) 8_755 8_755
O6 U2 O5 127.1(2) . 8_755
O10 U2 O5 150.67(19) . .
O9 U2 O5 81.5(3) 5_657 .
O3 U2 O5 82.5(3) . .
O6 U2 O5 127.1(2) 8_755 .
O6 U2 O5 70.1(2) . .
O5 U2 O5 57.3(3) 8_755 .
O10 U2 P1 170.5(5) . .
O9 U2 P1 77.3(3) 5_657 .
O3 U2 P1 84.4(3) . .
O6 U2 P1 98.87(19) 8_755 .
O6 U2 P1 98.87(19) . .
O5 U2 P1 28.79(15) 8_755 .
O5 U2 P1 28.79(15) . .
O10 U2 U4 119.05(7) . .
O9 U2 U4 95.32(17) 5_657 .
O3 U2 U4 75.99(12) . .
O6 U2 U4 154.81(19) 8_755 .
O6 U2 U4 36.96(19) . .
O5 U2 U4 90.22(15) 8_755 .
O5 U2 U4 34.24(15) . .
P1 U2 U4 62.664(18) . .
O10 U2 U4 119.05(7) . 1_655
O9 U2 U4 95.32(17) 5_657 1_655
O3 U2 U4 75.99(12) . 1_655
O6 U2 U4 36.96(19) 8_755 1_655
O6 U2 U4 154.80(19) . 1_655
O5 U2 U4 34.24(15) 8_755 1_655
O5 U2 U4 90.22(16) . 1_655
P1 U2 U4 62.663(18) . 1_655
U4 U2 U4 119.98(3) . 1_655
O10 U2 Cs4A 63.6(10) . 1_556
O9 U2 Cs4A 146.3(6) 5_657 1_556
O3 U2 Cs4A 48.3(7) . 1_556
O6 U2 Cs4A 57.9(9) 8_755 1_556
O6 U2 Cs4A 102.9(9) . 1_556
O5 U2 Cs4A 106.5(10) 8_755 1_556
O5 U2 Cs4A 130.8(7) . 1_556
P1 U2 Cs4A 124.9(9) . 1_556
U4 U2 Cs4A 116.9(7) . 1_556
U4 U2 Cs4A 77.7(10) 1_655 1_556
O10 U2 Cs4A 63.6(10) . 8_756
O9 U2 Cs4A 146.3(7) 5_657 8_756
O3 U2 Cs4A 48.3(7) . 8_756
O6 U2 Cs4A 102.9(9) 8_755 8_756
O6 U2 Cs4A 57.9(9) . 8_756
O5 U2 Cs4A 130.8(7) 8_755 8_756
O5 U2 Cs4A 106.5(10) . 8_756
P1 U2 Cs4A 124.9(9) . 8_756
U4 U2 Cs4A 77.7(10) . 8_756
U4 U2 Cs4A 116.9(7) 1_655 8_756
Cs4A U2 Cs4A 45.2(18) 1_556 8_756
O11 U3 O11 177.0(7) 2_554 1_654
O11 U3 O7 90.47(11) 2_554 2_654
O11 U3 O7 90.47(11) 1_654 2_654
O11 U3 O7 90.47(11) 2_554 1_554
O11 U3 O7 90.47(11) 1_654 1_554
O7 U3 O7 144.0(5) 2_654 1_554
O11 U3 O1 88.8(3) 2_554 1_554
O11 U3 O1 88.8(3) 1_654 1_554
O7 U3 O1 143.0(3) 2_654 1_554
O7 U3 O1 73.0(3) 1_554 1_554
O11 U3 O1 88.8(3) 2_554 2_654
O11 U3 O1 88.8(3) 1_654 2_654
O7 U3 O1 73.0(3) 2_654 2_654
O7 U3 O1 143.0(3) 1_554 2_654
O1 U3 O1 70.0(5) 1_554 2_654
O11 U3 O17 76.0(8) 2_554 2_655
O11 U3 O17 107.1(8) 1_654 2_655
O7 U3 O17 72.7(3) 2_654 2_655
O7 U3 O17 72.7(3) 1_554 2_655
O1 U3 O17 142.1(3) 1_554 2_655
O1 U3 O17 142.1(3) 2_654 2_655
O11 U3 O17 107.1(8) 2_554 .
O11 U3 O17 76.0(8) 1_654 .
O7 U3 O17 72.7(3) 2_654 .
O7 U3 O17 72.7(3) 1_554 .
O1 U3 O17 142.1(3) 1_554 .
O1 U3 O17 142.1(3) 2_654 .
O17 U3 O17 31.1(14) 2_655 .
O11 U3 Cs3B 88.5(4) 2_554 1_554
O11 U3 Cs3B 88.5(4) 1_654 1_554
O7 U3 Cs3B 108.0(3) 2_654 1_554
O7 U3 Cs3B 108.0(3) 1_554 1_554
O1 U3 Cs3B 35.0(2) 1_554 1_554
O1 U3 Cs3B 35.0(2) 2_654 1_554
O17 U3 Cs3B 164.5(7) 2_655 1_554
O17 U3 Cs3B 164.5(7) . 1_554
O11 U3 Cs3A 63.3(4) 2_554 2_654
O11 U3 Cs3A 113.7(4) 1_654 2_654
O7 U3 Cs3A 106.2(2) 2_654 2_654
O7 U3 Cs3A 106.2(2) 1_554 2_654
O1 U3 Cs3A 42.17(18) 1_554 2_654
O1 U3 Cs3A 42.17(18) 2_654 2_654
O17 U3 Cs3A 139.2(7) 2_655 2_654
O17 U3 Cs3A 170.3(7) . 2_654
Cs3B U3 Cs3A 25.22(4) 1_554 2_654
O11 U3 Cs3A 113.7(4) 2_554 1_554
O11 U3 Cs3A 63.3(4) 1_654 1_554
O7 U3 Cs3A 106.2(2) 2_654 1_554
O7 U3 Cs3A 106.2(2) 1_554 1_554
O1 U3 Cs3A 42.17(18) 1_554 1_554
O1 U3 Cs3A 42.17(18) 2_654 1_554
O17 U3 Cs3A 170.3(7) 2_655 1_554
O17 U3 Cs3A 139.2(7) . 1_554
Cs3B U3 Cs3A 25.22(4) 1_554 1_554
Cs3A U3 Cs3A 50.44(8) 2_654 1_554
O11 U3 Cs2A 138.8(3) 2_554 2_655
O11 U3 Cs2A 43.9(3) 1_654 2_655
O7 U3 Cs2A 59.51(14) 2_654 2_655
O7 U3 Cs2A 98.52(17) 1_554 2_655
O1 U3 Cs2A 132.39(3) 1_554 2_655
O1 U3 Cs2A 106.19(15) 2_654 2_655
O17 U3 Cs2A 68.7(6) 2_655 2_655
O17 U3 Cs2A 40.7(6) . 2_655
Cs3B U3 Cs2A 125.56(2) 1_554 2_655
Cs3A U3 Cs2A 147.15(4) 2_654 2_655
Cs3A U3 Cs2A 102.25(4) 1_554 2_655
Cs1 U4 O12 168.1(7) . 5_657
Cs1 U4 O14 35.7(4) . .
O12 U4 O14 144.9(4) 5_657 .
Cs1 U4 O14 35.7(4) . 8_655
O12 U4 O14 144.9(4) 5_657 8_655
O14 U4 O14 69.7(8) . 8_655
Cs1 U4 O5 107.21(17) . .
O12 U4 O5 71.87(17) 5_657 .
O14 U4 O5 73.1(4) . .
O14 U4 O5 142.7(5) 8_655 .
Cs1 U4 O5 107.21(17) . 8_655
O12 U4 O5 71.87(17) 5_657 8_655
O14 U4 O5 142.7(5) . 8_655
O14 U4 O5 73.1(4) 8_655 8_655
O5 U4 O5 143.4(3) . 8_655
Cs1 U4 O13 85.3(5) . 2
O12 U4 O13 82.9(8) 5_657 2
O14 U4 O13 92.7(7) . 2
O14 U4 O13 92.7(7) 8_655 2
O5 U4 O13 85.4(2) . 2
O5 U4 O13 85.4(2) 8_655 2
Cs1 U4 O6 98.0(2) . .
O12 U4 O6 92.5(6) 5_657 .
O14 U4 O6 75.1(6) . .
O14 U4 O6 106.5(6) 8_655 .
O5 U4 O6 66.6(2) . .
O5 U4 O6 120.0(2) 8_655 .
O13 U4 O6 151.48(18) 2 .
Cs1 U4 O6 98.0(2) . 8_655
O12 U4 O6 92.5(6) 5_657 8_655
O14 U4 O6 106.5(6) . 8_655
O14 U4 O6 75.1(6) 8_655 8_655
O5 U4 O6 120.0(2) . 8_655
O5 U4 O6 66.6(2) 8_655 8_655
O13 U4 O6 151.48(18) 2 8_655
O6 U4 O6 56.4(3) . 8_655
Cs1 U4 P2 103.27(14) . .
O12 U4 P2 88.6(6) 5_657 .
O14 U4 P2 94.3(5) . .
O14 U4 P2 94.3(5) 8_655 .
O5 U4 P2 92.01(15) . .
O5 U4 P2 92.01(15) 8_655 .
O13 U4 P2 171.5(5) 2 .
O6 U4 P2 28.51(16) . .
O6 U4 P2 28.51(16) 8_655 .
Cs1 U4 Cs2C 4.8(6) . 1_556
O12 U4 Cs2C 163.3(8) 5_657 1_556
O14 U4 Cs2C 36.9(5) . 1_556
O14 U4 Cs2C 36.9(5) 8_655 1_556
O5 U4 Cs2C 106.61(18) . 1_556
O5 U4 Cs2C 106.61(18) 8_655 1_556
O13 U4 Cs2C 80.5(7) 2 1_556
O6 U4 Cs2C 102.2(5) . 1_556
O6 U4 Cs2C 102.2(5) 8_655 1_556
P2 U4 Cs2C 108.1(6) . 1_556
Cs1 U4 U2 98.61(6) . 1_455
O12 U4 U2 87.2(3) 5_657 1_455
O14 U4 U2 124.2(5) . 1_455
O14 U4 U2 64.7(5) 8_655 1_455
O5 U4 U2 145.93(16) . 1_455
O5 U4 U2 35.32(15) 8_655 1_455
O13 U4 U2 119.21(7) 2 1_455
O6 U4 U2 88.48(16) . 1_455
O6 U4 U2 32.27(16) 8_655 1_455
P2 U4 U2 60.078(13) . 1_455
Cs2C U4 U2 100.9(3) 1_556 1_455
O14 Cs1 O14 143.2(14) . 8_655
O14 Cs1 U4 104.7(7) . .
O14 Cs1 U4 104.7(7) 8_655 .
O14 Cs1 Cs2C 77.1(7) . 1_556
O14 Cs1 Cs2C 77.1(7) 8_655 1_556
U4 Cs1 Cs2C 171.8(10) . 1_556
O14 Cs1 Cs2B 72.7(7) . 1_556
O14 Cs1 Cs2B 72.7(7) 8_655 1_556
U4 Cs1 Cs2B 162.8(6) . 1_556
Cs2C Cs1 Cs2B 25.4(11) 1_556 1_556
O14 Cs1 O13 106.7(8) . 2
O14 Cs1 O13 106.7(8) 8_655 2
U4 Cs1 O13 61.1(4) . 2
Cs2C Cs1 O13 110.6(10) 1_556 2
Cs2B Cs1 O13 136.1(7) 1_556 2
O14 Cs1 P5 4.1(8) . .
O14 Cs1 P5 142.2(7) 8_655 .
U4 Cs1 P5 107.77(12) . .
Cs2C Cs1 P5 73.6(2) 1_556 .
Cs2B Cs1 P5 70.57(13) 1_556 .
O13 Cs1 P5 105.62(14) 2 .
O14 Cs1 P5 142.2(7) . 8_655
O14 Cs1 P5 4.1(8) 8_655 8_655
U4 Cs1 P5 107.77(12) . 8_655
Cs2C Cs1 P5 73.6(2) 1_556 8_655
Cs2B Cs1 P5 70.57(13) 1_556 8_655
O13 Cs1 P5 105.62(14) 2 8_655
P5 Cs1 P5 140.8(3) . 8_655
O14 Cs1 Cs2A 79.5(7) . 1_556
O14 Cs1 Cs2A 79.5(7) 8_655 1_556
U4 Cs1 Cs2A 162.0(2) . 1_556
Cs2C Cs1 Cs2A 9.7(9) 1_556 1_556
Cs2B Cs1 Cs2A 35.2(6) 1_556 1_556
O13 Cs1 Cs2A 100.9(3) 2 1_556
P5 Cs1 Cs2A 75.67(12) . 1_556
P5 Cs1 Cs2A 75.68(12) 8_655 1_556
O14 Cs1 O6 69.8(8) . .
O14 Cs1 O6 112.4(9) 8_655 .
U4 Cs1 O6 53.32(18) . .
Cs2C Cs1 O6 133.8(8) 1_556 .
Cs2B Cs1 O6 111.2(5) 1_556 .
O13 Cs1 O6 109.2(4) 2 .
P5 Cs1 O6 73.94(17) . .
P5 Cs1 O6 116.42(18) 8_655 .
Cs2A Cs1 O6 141.8(2) 1_556 .
O14 Cs1 O6 112.4(9) . 8_655
O14 Cs1 O6 69.8(8) 8_655 8_655
U4 Cs1 O6 53.32(18) . 8_655
Cs2C Cs1 O6 133.8(8) 1_556 8_655
Cs2B Cs1 O6 111.2(5) 1_556 8_655
O13 Cs1 O6 109.2(4) 2 8_655
P5 Cs1 O6 116.42(18) . 8_655
P5 Cs1 O6 73.94(17) 8_655 8_655
Cs2A Cs1 O6 141.8(2) 1_556 8_655
O6 Cs1 O6 45.0(3) . 8_655
O14 Cs1 O5 61.3(6) . .
O14 Cs1 O5 149.9(7) 8_655 .
U4 Cs1 O5 45.55(14) . .
Cs2C Cs1 O5 133.0(3) 1_556 .
Cs2B Cs1 O5 133.82(18) 1_556 .
O13 Cs1 O5 66.0(3) 2 .
P5 Cs1 O5 63.67(16) . .
P5 Cs1 O5 153.3(2) 8_655 .
Cs2A Cs1 O5 129.93(13) 1_556 .
O6 Cs1 O5 50.63(18) . .
O6 Cs1 O5 84.8(2) 8_655 .
Cs2C Cs2A Cs2B 37(2) . .
Cs2C Cs2A Cs1 21(2) . 1_554
Cs2B Cs2A Cs1 57.4(7) . 1_554
Cs2C Cs2A O14 28.2(10) . 8_654
Cs2B Cs2A O14 54.5(7) . 8_654
Cs1 Cs2A O14 26.0(3) 1_554 8_654
Cs2C Cs2A O14 28.2(10) . 1_554
Cs2B Cs2A O14 54.5(7) . 1_554
Cs1 Cs2A O14 26.0(3) 1_554 1_554
O14 Cs2A O14 50.0(7) 8_654 1_554
Cs2C Cs2A Cs2A 143(2) . 2
Cs2B Cs2A Cs2A 179.7(7) . 2
Cs1 Cs2A Cs2A 122.26(8) 1_554 2
O14 Cs2A Cs2A 125.2(4) 8_654 2
O14 Cs2A Cs2A 125.2(4) 1_554 2
Cs2C Cs2A O15 59.9(8) . 8_654
Cs2B Cs2A O15 53.3(3) . 8_654
Cs1 Cs2A O15 69.4(3) 1_554 8_654
O14 Cs2A O15 44.7(4) 8_654 8_654
O14 Cs2A O15 88.1(4) 1_554 8_654
Cs2A Cs2A O15 126.7(2) 2 8_654
Cs2C Cs2A O15 59.9(8) . 1_554
Cs2B Cs2A O15 53.3(3) . 1_554
Cs1 Cs2A O15 69.4(2) 1_554 1_554
O14 Cs2A O15 88.1(4) 8_654 1_554
O14 Cs2A O15 44.7(4) 1_554 1_554
Cs2A Cs2A O15 126.7(3) 2 1_554
O15 Cs2A O15 106.5(5) 8_654 1_554
Cs2C Cs2A O17 108.0(9) . 2_655
Cs2B Cs2A O17 119.4(3) . 2_655
Cs1 Cs2A O17 98.3(4) 1_554 2_655
O14 Cs2A O17 123.3(6) 8_654 2_655
O14 Cs2A O17 79.8(5) 1_554 2_655
Cs2A Cs2A O17 60.5(2) 2 2_655
O15 Cs2A O17 167.6(5) 8_654 2_655
O15 Cs2A O17 66.4(4) 1_554 2_655
Cs2C Cs2A O17 108.0(9) . 1_455
Cs2B Cs2A O17 119.4(3) . 1_455
Cs1 Cs2A O17 98.3(4) 1_554 1_455
O14 Cs2A O17 79.8(5) 8_654 1_455
O14 Cs2A O17 123.3(6) 1_554 1_455
Cs2A Cs2A O17 60.5(2) 2 1_455
O15 Cs2A O17 66.4(4) 8_654 1_455
O15 Cs2A O17 167.6(5) 1_554 1_455
O17 Cs2A O17 118.5(6) 2_655 1_455
Cs2C Cs2A O8 88.5(18) . 5_657
Cs2B Cs2A O8 55.0(6) . 5_657
Cs1 Cs2A O8 107.84(16) 1_554 5_657
O14 Cs2A O8 109.3(4) 8_654 5_657
O14 Cs2A O8 91.0(4) 1_554 5_657
Cs2A Cs2A O8 125.33(14) 2 5_657
O15 Cs2A O8 88.8(3) 8_654 5_657
O15 Cs2A O8 52.2(3) 1_554 5_657
O17 Cs2A O8 93.9(4) 2_655 5_657
O17 Cs2A O8 134.7(5) 1_455 5_657
Cs2C Cs2A O8 88.5(18) . 4_457
Cs2B Cs2A O8 55.0(6) . 4_457
Cs1 Cs2A O8 107.84(16) 1_554 4_457
O14 Cs2A O8 91.0(4) 8_654 4_457
O14 Cs2A O8 109.3(4) 1_554 4_457
Cs2A Cs2A O8 125.33(13) 2 4_457
O15 Cs2A O8 52.2(3) 8_654 4_457
O15 Cs2A O8 88.8(3) 1_554 4_457
O17 Cs2A O8 134.7(5) 2_655 4_457
O17 Cs2A O8 93.9(4) 1_455 4_457
O8 Cs2A O8 43.4(2) 5_657 4_457
Cs2C Cs2B Cs2A 32.6(16) . .
Cs2C Cs2B Cs4B 140(2) . 5_656
Cs2A Cs2B Cs4B 172.1(13) . 5_656
Cs2C Cs2B O14 63.7(15) . 8_654
Cs2A Cs2B O14 91.1(10) . 8_654
Cs4B Cs2B O14 82.1(9) 5_656 8_654
Cs2C Cs2B O14 63.7(15) . 1_554
Cs2A Cs2B O14 91.1(10) . 1_554
Cs4B Cs2B O14 82.1(9) 5_656 1_554
O14 Cs2B O14 62.6(9) 8_654 1_554
Cs2C Cs2B Cs1 54.9(17) . 1_554
Cs2A Cs2B Cs1 87.5(9) . 1_554
Cs4B Cs2B Cs1 84.6(8) 5_656 1_554
O14 Cs2B Cs1 31.5(5) 8_654 1_554
O14 Cs2B Cs1 31.5(5) 1_554 1_554
Cs2C Cs2B O15 91.9(6) . 8_654
Cs2A Cs2B O15 93.9(6) . 8_654
Cs4B Cs2B O15 85.8(6) 5_656 8_654
O14 Cs2B O15 56.1(6) 8_654 8_654
O14 Cs2B O15 118.5(9) 1_554 8_654
Cs1 Cs2B O15 87.6(6) 1_554 8_654
Cs2C Cs2B O15 91.9(6) . 1_554
Cs2A Cs2B O15 93.9(6) . 1_554
Cs4B Cs2B O15 85.8(6) 5_656 1_554
O14 Cs2B O15 118.5(9) 8_654 1_554
O14 Cs2B O15 56.1(6) 1_554 1_554
Cs1 Cs2B O15 87.6(6) 1_554 1_554
O15 Cs2B O15 170.6(12) 8_654 1_554
Cs2C Cs2B Cs4C 135(2) . 5_656
Cs2A Cs2B Cs4C 156.9(11) . 5_656
Cs4B Cs2B Cs4C 22.1(11) 5_656 5_656
O14 Cs2B Cs4C 71.8(12) 8_654 5_656
O14 Cs2B Cs4C 94.4(13) 1_554 5_656
Cs1 Cs2B Cs4C 85.7(11) 1_554 5_656
O15 Cs2B Cs4C 63.8(12) 8_654 5_656
O15 Cs2B Cs4C 107.8(14) 1_554 5_656
Cs2C Cs2B Cs4C 135(2) . 4_456
Cs2A Cs2B Cs4C 156.9(12) . 4_456
Cs4B Cs2B Cs4C 22.1(11) 5_656 4_456
O14 Cs2B Cs4C 94.4(13) 8_654 4_456
O14 Cs2B Cs4C 71.8(12) 1_554 4_456
Cs1 Cs2B Cs4C 85.7(11) 1_554 4_456
O15 Cs2B Cs4C 107.8(14) 8_654 4_456
O15 Cs2B Cs4C 63.8(12) 1_554 4_456
Cs4C Cs2B Cs4C 44(2) 5_656 4_456
Cs2C Cs2B O8 121.7(18) . 5_657
Cs2A Cs2B O8 93.1(9) . 5_657
Cs4B Cs2B O8 93.9(8) 5_656 5_657
O14 Cs2B O8 173.8(10) 8_654 5_657
O14 Cs2B O8 121.7(4) 1_554 5_657
Cs1 Cs2B O8 153.2(3) 1_554 5_657
O15 Cs2B O8 119.1(8) 8_654 5_657
O15 Cs2B O8 65.6(5) 1_554 5_657
Cs4C Cs2B O8 102.9(12) 5_656 5_657
Cs4C Cs2B O8 83.3(11) 4_456 5_657
Cs2C Cs2B O8 121.7(18) . 4_457
Cs2A Cs2B O8 93.1(9) . 4_457
Cs4B Cs2B O8 93.9(8) 5_656 4_457
O14 Cs2B O8 121.7(4) 8_654 4_457
O14 Cs2B O8 173.8(10) 1_554 4_457
Cs1 Cs2B O8 153.2(3) 1_554 4_457
O15 Cs2B O8 65.6(5) 8_654 4_457
O15 Cs2B O8 119.1(8) 1_554 4_457
Cs4C Cs2B O8 83.3(11) 5_656 4_457
Cs4C Cs2B O8 102.9(12) 4_456 4_457
O8 Cs2B O8 53.6(5) 5_657 4_457
Cs2A Cs2C Cs2B 111(3) . .
Cs2A Cs2C Cs1 149(3) . 1_554
Cs2B Cs2C Cs1 100(2) . 1_554
Cs2A Cs2C O14 139.6(14) . 8_654
Cs2B Cs2C O14 90.1(18) . 8_654
Cs1 Cs2C O14 36.5(6) 1_554 8_654
Cs2A Cs2C O14 139.6(14) . 1_554
Cs2B Cs2C O14 90.1(18) . 1_554
Cs1 Cs2C O14 36.5(6) 1_554 1_554
O14 Cs2C O14 70.8(12) 8_654 1_554
Cs2A Cs2C O15 102.3(9) . 8_654
Cs2B Cs2C O15 65.1(7) . 8_654
Cs1 Cs2C O15 90.2(7) 1_554 8_654
O14 Cs2C O15 54.6(6) 8_654 8_654
O14 Cs2C O15 118.0(12) 1_554 8_654
Cs2A Cs2C O15 102.3(9) . 1_554
Cs2B Cs2C O15 65.1(7) . 1_554
Cs1 Cs2C O15 90.2(7) 1_554 1_554
O14 Cs2C O15 118.0(12) 8_654 1_554
O14 Cs2C O15 54.6(6) 1_554 1_554
O15 Cs2C O15 129.6(14) 8_654 1_554
Cs2A Cs2C P5 117.3(5) . 8_654
Cs2B Cs2C P5 84.5(10) . 8_654
Cs1 Cs2C P5 64.5(5) 1_554 8_654
O14 Cs2C P5 28.0(4) 8_654 8_654
O14 Cs2C P5 98.3(10) 1_554 8_654
O15 Cs2C P5 29.2(3) 8_654 8_654
O15 Cs2C P5 136.9(11) 1_554 8_654
Cs2A Cs2C P5 117.3(5) . 1_554
Cs2B Cs2C P5 84.5(10) . 1_554
Cs1 Cs2C P5 64.5(5) 1_554 1_554
O14 Cs2C P5 98.3(10) 8_654 1_554
O14 Cs2C P5 28.0(4) 1_554 1_554
O15 Cs2C P5 136.9(11) 8_654 1_554
O15 Cs2C P5 29.2(3) 1_554 1_554
P5 Cs2C P5 124.8(9) 8_654 1_554
Cs2A Cs2C Cs4B 139(2) . 5_656
Cs2B Cs2C Cs4B 27.9(15) . 5_656
Cs1 Cs2C Cs4B 71.8(9) 1_554 5_656
O14 Cs2C Cs4B 67.7(9) 8_654 5_656
O14 Cs2C Cs4B 67.7(9) 1_554 5_656
O15 Cs2C Cs4B 66.2(7) 8_654 5_656
O15 Cs2C Cs4B 66.2(7) 1_554 5_656
P5 Cs2C Cs4B 72.8(6) 8_654 5_656
P5 Cs2C Cs4B 72.8(6) 1_554 5_656
Cs2A Cs2C O11 79.3(19) . 2_554
Cs2B Cs2C O11 157.5(9) . 2_554
Cs1 Cs2C O11 72.1(9) 1_554 2_554
O14 Cs2C O11 94.4(12) 8_654 2_554
O14 Cs2C O11 70.7(9) 1_554 2_554
O15 Cs2C O11 134.1(9) 8_654 2_554
O15 Cs2C O11 93.5(5) 1_554 2_554
P5 Cs2C O11 109.2(9) 8_654 2_554
P5 Cs2C O11 73.0(5) 1_554 2_554
Cs4B Cs2C O11 138.1(8) 5_656 2_554
Cs2A Cs2C O11 79.3(19) . 1_554
Cs2B Cs2C O11 157.5(9) . 1_554
Cs1 Cs2C O11 72.1(9) 1_554 1_554
O14 Cs2C O11 70.7(9) 8_654 1_554
O14 Cs2C O11 94.4(12) 1_554 1_554
O15 Cs2C O11 93.5(5) 8_654 1_554
O15 Cs2C O11 134.1(9) 1_554 1_554
P5 Cs2C O11 73.0(5) 8_654 1_554
P5 Cs2C O11 109.2(9) 1_554 1_554
Cs4B Cs2C O11 138.1(8) 5_656 1_554
O11 Cs2C O11 41.1(6) 2_554 1_554
Cs3B Cs3A Cs3A 179.0(9) . 2_755
Cs3B Cs3A O13 118.9(9) . 1_655
Cs3A Cs3A O13 62.0(2) 2_755 1_655
Cs3B Cs3A O13 118.9(9) . 2_655
Cs3A Cs3A O13 62.0(2) 2_755 2_655
O13 Cs3A O13 47.1(7) 1_655 2_655
Cs3B Cs3A O2 51.80(14) . .
Cs3A Cs3A O2 128.27(11) 2_755 .
O13 Cs3A O2 124.5(3) 1_655 .
O13 Cs3A O2 86.5(4) 2_655 .
Cs3B Cs3A O2 51.80(14) . 2_655
Cs3A Cs3A O2 128.27(11) 2_755 2_655
O13 Cs3A O2 86.5(4) 1_655 2_655
O13 Cs3A O2 124.5(3) 2_655 2_655
O2 Cs3A O2 103.2(2) . 2_655
Cs3B Cs3A O16 52.2(9) . 2_655
Cs3A Cs3A O16 126.9(3) 2_755 2_655
O13 Cs3A O16 171.1(4) 1_655 2_655
O13 Cs3A O16 135.1(6) 2_655 2_655
O2 Cs3A O16 52.4(4) . 2_655
O2 Cs3A O16 86.4(4) 2_655 2_655
Cs3B Cs3A O16 52.2(9) . .
Cs3A Cs3A O16 126.9(3) 2_755 .
O13 Cs3A O16 135.1(6) 1_655 .
O13 Cs3A O16 171.1(4) 2_655 .
O2 Cs3A O16 86.4(4) . .
O2 Cs3A O16 52.4(4) 2_655 .
O16 Cs3A O16 40.8(8) 2_655 .
Cs3B Cs3A O1 54.2(8) . .
Cs3A Cs3A O1 126.67(11) 2_755 .
O13 Cs3A O1 84.0(3) 1_655 .
O13 Cs3A O1 64.8(3) 2_655 .
O2 Cs3A O1 44.1(2) . .
O2 Cs3A O1 84.9(2) 2_655 .
O16 Cs3A O1 90.1(4) 2_655 .
O16 Cs3A O1 106.4(3) . .
Cs3B Cs3A O1 54.2(8) . 2_655
Cs3A Cs3A O1 126.67(11) 2_755 2_655
O13 Cs3A O1 64.8(3) 1_655 2_655
O13 Cs3A O1 84.0(3) 2_655 2_655
O2 Cs3A O1 84.9(2) . 2_655
O2 Cs3A O1 44.1(2) 2_655 2_655
O16 Cs3A O1 106.4(3) 2_655 2_655
O16 Cs3A O1 90.1(4) . 2_655
O1 Cs3A O1 47.3(3) . 2_655
Cs3B Cs3A P3 114.8(9) . 1_655
Cs3A Cs3A P3 66.18(7) 2_755 1_655
O13 Cs3A P3 24.5(3) 1_655 1_655
O13 Cs3A P3 24.5(3) 2_655 1_655
O2 Cs3A P3 101.88(16) . 1_655
O2 Cs3A P3 101.88(16) 2_655 1_655
O16 Cs3A P3 154.3(4) 2_655 1_655
O16 Cs3A P3 154.3(4) . 1_655
O1 Cs3A P3 66.79(14) . 1_655
O1 Cs3A P3 66.79(13) 2_655 1_655
Cs3B Cs3A P6 56.6(9) . .
Cs3A Cs3A P6 122.39(10) 2_755 .
O13 Cs3A P6 156.4(3) 1_655 .
O13 Cs3A P6 156.4(3) 2_655 .
O2 Cs3A P6 73.09(17) . .
O2 Cs3A P6 73.09(17) 2_655 .
O16 Cs3A P6 21.7(4) 2_655 .
O16 Cs3A P6 21.7(4) . .
O1 Cs3A P6 105.46(16) . .
O1 Cs3A P6 105.46(16) 2_655 .
P3 Cs3A P6 171.44(14) 1_655 .
Cs3A Cs3B Cs3A 178.0(19) . 2_655
Cs3A Cs3B O2 89.92(8) . .
Cs3A Cs3B O2 89.92(8) 2_655 .
Cs3A Cs3B O2 89.92(8) . 2_655
Cs3A Cs3B O2 89.92(8) 2_655 2_655
O2 Cs3B O2 171.3(15) . 2_655
Cs3A Cs3B O16 90.9(8) . 2_655
Cs3A Cs3B O16 90.9(8) 2_655 2_655
O2 Cs3B O16 68.1(7) . 2_655
O2 Cs3B O16 120.5(12) 2_655 2_655
Cs3A Cs3B O16 90.9(8) . .
Cs3A Cs3B O16 90.9(8) 2_655 .
O2 Cs3B O16 120.5(12) . .
O2 Cs3B O16 68.1(7) 2_655 .
O16 Cs3B O16 52.4(12) 2_655 .
Cs3A Cs3B O1 89.1(8) . .
Cs3A Cs3B O1 89.1(8) 2_655 .
O2 Cs3B O1 56.0(5) . .
O2 Cs3B O1 115.3(11) 2_655 .
O16 Cs3B O1 124.1(6) 2_655 .
O16 Cs3B O1 176.5(9) . .
Cs3A Cs3B O1 89.1(8) . 2_655
Cs3A Cs3B O1 89.1(8) 2_655 2_655
O2 Cs3B O1 115.3(11) . 2_655
O2 Cs3B O1 56.0(5) 2_655 2_655
O16 Cs3B O1 176.5(9) 2_655 2_655
O16 Cs3B O1 124.1(6) . 2_655
O1 Cs3B O1 59.3(8) . 2_655
Cs3A Cs3B P6 91.0(9) . .
Cs3A Cs3B P6 91.0(9) 2_655 .
O2 Cs3B P6 94.3(7) . .
O2 Cs3B P6 94.3(7) 2_655 .
O16 Cs3B P6 26.2(6) 2_655 .
O16 Cs3B P6 26.2(6) . .
O1 Cs3B P6 150.3(4) . .
O1 Cs3B P6 150.3(4) 2_655 .
Cs3A Cs3B P1 89.5(5) . .
Cs3A Cs3B P1 89.5(5) 2_655 .
O2 Cs3B P1 27.9(3) . .
O2 Cs3B P1 143.4(12) 2_655 .
O16 Cs3B P1 96.0(6) 2_655 .
O16 Cs3B P1 148.4(10) . .
O1 Cs3B P1 28.1(2) . .
O1 Cs3B P1 87.4(8) 2_655 .
P6 Cs3B P1 122.2(5) . .
Cs3A Cs3B P1 89.5(5) . 2_655
Cs3A Cs3B P1 89.5(5) 2_655 2_655
O2 Cs3B P1 143.4(12) . 2_655
O2 Cs3B P1 27.9(3) 2_655 2_655
O16 Cs3B P1 148.4(10) 2_655 2_655
O16 Cs3B P1 96.0(6) . 2_655
O1 Cs3B P1 87.4(8) . 2_655
O1 Cs3B P1 28.1(2) 2_655 2_655
P6 Cs3B P1 122.2(5) . 2_655
P1 Cs3B P1 115.6(10) . 2_655
Cs3A Cs3B U1 90.5(5) . .
Cs3A Cs3B U1 90.5(5) 2_655 .
O2 Cs3B U1 34.9(4) . .
O2 Cs3B U1 153.7(11) 2_655 .
O16 Cs3B U1 33.2(6) 2_655 .
O16 Cs3B U1 85.6(9) . .
O1 Cs3B U1 90.9(2) . .
O1 Cs3B U1 150.3(8) 2_655 .
P6 Cs3B U1 59.4(4) . .
P1 Cs3B U1 62.83(9) . .
P1 Cs3B U1 178.4(9) 2_655 .
Cs4A Cs4A Cs4C 141(10) 5_756 .
Cs4A Cs4A Cs4C 27(10) 5_756 5_756
Cs4C Cs4A Cs4C 168(4) . 5_756
Cs4A Cs4A Cs4B 142(10) 5_756 .
Cs4C Cs4A Cs4B 25(3) . .
Cs4C Cs4A Cs4B 156(4) 5_756 .
Cs4A Cs4A Cs4B 31(10) 5_756 5_756
Cs4C Cs4A Cs4B 156(5) . 5_756
Cs4C Cs4A Cs4B 20(3) 5_756 5_756
Cs4B Cs4A Cs4B 172.7(18) . 5_756
Cs4A Cs4A Cs4C 138(10) 5_756 8_755
Cs4C Cs4A Cs4C 36(3) . 8_755
Cs4C Cs4A Cs4C 146(4) 5_756 8_755
Cs4B Cs4A Cs4C 11.3(12) . 8_755
Cs4B Cs4A Cs4C 165(2) 5_756 8_755
Cs4A Cs4A Cs4C 36(10) 5_756 4_556
Cs4C Cs4A Cs4C 146(4) . 4_556
Cs4C Cs4A Cs4C 30(3) 5_756 4_556
Cs4B Cs4A Cs4C 169(3) . 4_556
Cs4B Cs4A Cs4C 10.6(9) 5_756 4_556
Cs4C Cs4A Cs4C 174.5(12) 8_755 4_556
Cs4A Cs4A O3 107(10) 5_756 1_554
Cs4C Cs4A O3 104(3) . 1_554
Cs4C Cs4A O3 86(3) 5_756 1_554
Cs4B Cs4A O3 82.5(15) . 1_554
Cs4B Cs4A O3 100(2) 5_756 1_554
Cs4C Cs4A O3 72.6(11) 8_755 1_554
Cs4C Cs4A O3 108(2) 4_556 1_554
Cs4A Cs4A Cs4A 130(10) 5_756 8_755
Cs4C Cs4A Cs4A 52(4) . 8_755
Cs4C Cs4A Cs4A 131(3) 5_756 8_755
Cs4B Cs4A Cs4A 27.0(17) . 8_755
Cs4B Cs4A Cs4A 150.7(14) 5_756 8_755
Cs4C Cs4A Cs4A 15.7(13) 8_755 8_755
Cs4C Cs4A Cs4A 161.2(12) 4_556 8_755
O3 Cs4A Cs4A 59.5(13) 1_554 8_755
Cs4A Cs4A O4 103(10) 5_756 1_654
Cs4C Cs4A O4 96(3) . 1_654
Cs4C Cs4A O4 90(3) 5_756 1_654
Cs4B Cs4A O4 112.6(18) . 1_654
Cs4B Cs4A O4 74.2(16) 5_756 1_654
Cs4C Cs4A O4 118.4(13) 8_755 1_654
Cs4C Cs4A O4 67.1(13) 4_556 1_654
O3 Cs4A O4 97.6(11) 1_554 1_654
Cs4A Cs4A O4 125.7(8) 8_755 1_654
Cs4A Cs4A O15 107(10) 5_756 4_557
Cs4C Cs4A O15 57(4) . 4_557
Cs4C Cs4A O15 119(3) 5_756 4_557
Cs4B Cs4A O15 82(2) . 4_557
Cs4B Cs4A O15 100.1(16) 5_756 4_557
Cs4C Cs4A O15 93(2) 8_755 4_557
Cs4C Cs4A O15 89.5(13) 4_556 4_557
O3 Cs4A O15 141.4(10) 1_554 4_557
Cs4A Cs4A O15 108.9(12) 8_755 4_557
O4 Cs4A O15 57.1(8) 1_654 4_557
Cs4A Cs4A O3 66(10) 5_756 5_757
Cs4C Cs4A O3 83(4) . 5_757
Cs4C Cs4A O3 87(3) 5_756 5_757
Cs4B Cs4A O3 103(3) . 5_757
Cs4B Cs4A O3 74.0(11) 5_756 5_757
Cs4C Cs4A O3 113(2) 8_755 5_757
Cs4C Cs4A O3 66.3(11) 4_556 5_757
O3 Cs4A O3 173(2) 1_554 5_757
Cs4A Cs4A O3 124.7(12) 8_755 5_757
O4 Cs4A O3 84.5(11) 1_654 5_757
O15 Cs4A O3 45.2(7) 4_557 5_757
Cs4C Cs4B Cs4C 171(5) . 8_755
Cs4C Cs4B Cs4A 148(4) . 8_755
Cs4C Cs4B Cs4A 23(3) 8_755 8_755
Cs4C Cs4B Cs4A 23(3) . .
Cs4C Cs4B Cs4A 148(3) 8_755 .
Cs4A Cs4B Cs4A 126(3) 8_755 .
Cs4C Cs4B Cs4A 25(3) . 5_756
Cs4C Cs4B Cs4A 147(3) 8_755 5_756
Cs4A Cs4B Cs4A 124.1(12) 8_755 5_756
Cs4A Cs4B Cs4A 7.3(18) . 5_756
Cs4C Cs4B Cs4A 147(3) . 4_456
Cs4C Cs4B Cs4A 25(3) 8_755 4_456
Cs4A Cs4B Cs4A 7.3(18) 8_755 4_456
Cs4A Cs4B Cs4A 124.1(12) . 4_456
Cs4A Cs4B Cs4A 121(3) 5_756 4_456
Cs4C Cs4B Cs2B 94(3) . 5_656
Cs4C Cs4B Cs2B 94(3) 8_755 5_656
Cs4A Cs4B Cs2B 116.5(17) 8_755 5_656
Cs4A Cs4B Cs2B 116.6(17) . 5_656
Cs4A Cs4B Cs2B 119.3(14) 5_756 5_656
Cs4A Cs4B Cs2B 119.3(14) 4_456 5_656
Cs4C Cs4B Cs4C 32(3) . 5_756
Cs4C Cs4B Cs4C 140(2) 8_755 5_756
Cs4A Cs4B Cs4C 117.3(18) 8_755 5_756
Cs4A Cs4B Cs4C 10.1(18) . 5_756
Cs4A Cs4B Cs4C 7.2(16) 5_756 5_756
Cs4A Cs4B Cs4C 114.8(16) 4_456 5_756
Cs2B Cs4B Cs4C 125.9(8) 5_656 5_756
Cs4C Cs4B Cs4C 140(2) . 4_456
Cs4C Cs4B Cs4C 32(3) 8_755 4_456
Cs4A Cs4B Cs4C 10.1(18) 8_755 4_456
Cs4A Cs4B Cs4C 117.3(18) . 4_456
Cs4A Cs4B Cs4C 114.8(16) 5_756 4_456
Cs4A Cs4B Cs4C 7.2(16) 4_456 4_456
Cs2B Cs4B Cs4C 125.9(8) 5_656 4_456
Cs4C Cs4B Cs4C 108.1(15) 5_756 4_456
Cs4C Cs4B O10 89(3) . 1_554
Cs4C Cs4B O10 89(3) 8_755 1_554
Cs4A Cs4B O10 90.2(10) 8_755 1_554
Cs4A Cs4B O10 90.2(10) . 1_554
Cs4A Cs4B O10 97.4(10) 5_756 1_554
Cs4A Cs4B O10 97.4(10) 4_456 1_554
Cs2B Cs4B O10 79.0(7) 5_656 1_554
Cs4C Cs4B O10 95.7(8) 5_756 1_554
Cs4C Cs4B O10 95.7(8) 4_456 1_554
Cs4C Cs4B O14 118(3) . 5_657
Cs4C Cs4B O14 70(2) 8_755 5_657
Cs4A Cs4B O14 88.6(16) 8_755 5_657
Cs4A Cs4B O14 134.4(15) . 5_657
Cs4A Cs4B O14 129.7(13) 5_756 5_657
Cs4A Cs4B O14 86.0(14) 4_456 5_657
Cs2B Cs4B O14 50.8(7) 5_656 5_657
Cs4C Cs4B O14 135.1(8) 5_756 5_657
Cs4C Cs4B O14 92.9(8) 4_456 5_657
O10 Cs4B O14 121.8(7) 1_554 5_657
Cs4C Cs4B O14 70(2) . 4_557
Cs4C Cs4B O14 118(3) 8_755 4_557
Cs4A Cs4B O14 134.4(15) 8_755 4_557
Cs4A Cs4B O14 88.6(16) . 4_557
Cs4A Cs4B O14 86.0(14) 5_756 4_557
Cs4A Cs4B O14 129.7(13) 4_456 4_557
Cs2B Cs4B O14 50.8(7) 5_656 4_557
Cs4C Cs4B O14 92.9(8) 5_756 4_557
Cs4C Cs4B O14 135.1(8) 4_456 4_557
O10 Cs4B O14 121.8(7) 1_554 4_557
O14 Cs4B O14 47.9(7) 5_657 4_557
Cs4A Cs4C Cs4B 133(5) . .
Cs4A Cs4C Cs4A 12(3) . 5_756
Cs4B Cs4C Cs4A 135(5) . 5_756
Cs4A Cs4C Cs4C 128(4) . 8_755
Cs4B Cs4C Cs4C 5(3) . 8_755
Cs4A Cs4C Cs4C 131(3) 5_756 8_755
Cs4A Cs4C Cs4C 7.2(18) . 5_756
Cs4B Cs4C Cs4C 134(5) . 5_756
Cs4A Cs4C Cs4C 5.2(18) 5_756 5_756
Cs4C Cs4C Cs4C 130(2) 8_755 5_756
Cs4A Cs4C Cs2B 162(4) . 5_656
Cs4B Cs4C Cs2B 64(2) . 5_656
Cs4A Cs4C Cs2B 160(4) 5_756 5_656
Cs4C Cs4C Cs2B 67.9(11) 8_755 5_656
Cs4C Cs4C Cs2B 162(4) 5_756 5_656
Cs4A Cs4C Cs4A 112(4) . 8_755
Cs4B Cs4C Cs4A 20(2) . 8_755
Cs4A Cs4C Cs4A 116(3) 5_756 8_755
Cs4C Cs4C Cs4A 15.7(13) 8_755 8_755
Cs4C Cs4C Cs4A 115(3) 5_756 8_755
Cs2B Cs4C Cs4A 83.5(16) 5_656 8_755
Cs4A Cs4C O15 107(4) . 4_557
Cs4B Cs4C O15 121(3) . 4_557
Cs4A Cs4C O15 103(4) 5_756 4_557
Cs4C Cs4C O15 125.0(9) 8_755 4_557
Cs4C Cs4C O15 105(3) 5_756 4_557
Cs2B Cs4C O15 57.1(7) 5_656 4_557
Cs4A Cs4C O15 140.6(16) 8_755 4_557
Cs4A Cs4C Cs4B 17(3) . 5_756
Cs4B Cs4C Cs4B 148(3) . 5_756
Cs4A Cs4C Cs4B 14(3) 5_756 5_756
Cs4C Cs4C Cs4B 144.1(8) 8_755 5_756
Cs4C Cs4C Cs4B 13.9(18) 5_756 5_756
Cs2B Cs4C Cs4B 148.0(18) 5_656 5_756
Cs4A Cs4C Cs4B 128.5(15) 8_755 5_756
O15 Cs4C Cs4B 90.9(14) 4_557 5_756
Cs4A Cs4C Cs4A 110(3) . 4_456
Cs4B Cs4C Cs4A 23(2) . 4_456
Cs4A Cs4C Cs4A 112(4) 5_756 4_456
Cs4C Cs4C Cs4A 18.8(12) 8_755 4_456
Cs4C Cs4C Cs4A 111(3) 5_756 4_456
Cs2B Cs4C Cs4A 86.6(17) 5_656 4_456
Cs4A Cs4C Cs4A 5.5(12) 8_755 4_456
O15 Cs4C Cs4A 143.4(17) 4_557 4_456
Cs4B Cs4C Cs4A 125.4(15) 5_756 4_456
Cs4A Cs4C O14 124(4) . 4_557
Cs4B Cs4C O14 92(2) . 4_557
Cs4A Cs4C O14 113(3) 5_756 4_557
Cs4C Cs4C O14 95.9(10) 8_755 4_557
Cs4C Cs4C O14 118(3) 5_756 4_557
Cs2B Cs4C O14 52.1(7) 5_656 4_557
Cs4A Cs4C O14 108.4(18) 8_755 4_557
O15 Cs4C O14 48.7(7) 4_557 4_557
Cs4B Cs4C O14 109.5(15) 5_756 4_557
Cs4A Cs4C O14 107.1(16) 4_456 4_557
Cs4A Cs4C P5 105(4) . 4_557
Cs4B Cs4C P5 118(3) . 4_557
Cs4A Cs4C P5 97(3) 5_756 4_557
Cs4C Cs4C P5 122.1(8) 8_755 4_557
Cs4C Cs4C P5 100(3) 5_756 4_557
Cs2B Cs4C P5 64.1(8) 5_656 4_557
Cs4A Cs4C P5 135.7(18) 8_755 4_557
O15 Cs4C P5 27.9(5) 4_557 4_557
Cs4B Cs4C P5 88.6(13) 5_756 4_557
Cs4A Cs4C P5 134.7(15) 4_456 4_557
O14 Cs4C P5 27.5(5) 4_557 4_557
O1 P1 O2 109.3(6) . .
O1 P1 O5 113.0(3) . .
O2 P1 O5 110.6(4) . .
O1 P1 O5 113.0(3) . 8_755
O2 P1 O5 110.6(4) . 8_755
O5 P1 O5 100.2(5) . 8_755
O1 P1 U2 134.0(4) . .
O2 P1 U2 116.8(4) . .
O5 P1 U2 50.4(3) . .
O5 P1 U2 50.4(3) 8_755 .
O1 P1 Cs3B 58.0(6) . .
O2 P1 Cs3B 51.2(6) . .
O5 P1 Cs3B 129.7(3) . .
O5 P1 Cs3B 129.7(3) 8_755 .
U2 P1 Cs3B 168.0(5) . .
O1 P1 Cs3A 62.9(3) . .
O2 P1 Cs3A 58.4(3) . .
O5 P1 Cs3A 161.7(3) . .
O5 P1 Cs3A 97.6(3) 8_755 .
U2 P1 Cs3A 146.04(5) . .
Cs3B P1 Cs3A 32.19(5) . .
O1 P1 Cs3A 62.9(3) . 2_655
O2 P1 Cs3A 58.4(3) . 2_655
O5 P1 Cs3A 97.6(3) . 2_655
O5 P1 Cs3A 161.7(3) 8_755 2_655
U2 P1 Cs3A 146.04(5) . 2_655
Cs3B P1 Cs3A 32.19(5) . 2_655
Cs3A P1 Cs3A 64.38(10) . 2_655
O4 P2 O9 109.3(7) . .
O4 P2 O6 110.6(4) . 8_655
O9 P2 O6 110.9(4) . 8_655
O4 P2 O6 110.6(4) . .
O9 P2 O6 110.9(4) . .
O6 P2 O6 104.4(6) 8_655 .
O4 P2 U4 135.3(5) . .
O9 P2 U4 115.4(5) . .
O6 P2 U4 52.9(3) 8_655 .
O6 P2 U4 52.9(3) . .
O4 P2 Cs4B 59.9(5) . 5_657
O9 P2 Cs4B 169.2(6) . 5_657
O6 P2 Cs4B 75.1(4) 8_655 5_657
O6 P2 Cs4B 75.1(4) . 5_657
U4 P2 Cs4B 75.4(3) . 5_657
O4 P2 Cs1 112.4(5) . .
O9 P2 Cs1 138.3(5) . .
O6 P2 Cs1 53.3(3) 8_655 .
O6 P2 Cs1 53.3(3) . .
U4 P2 Cs1 22.95(7) . .
Cs4B P2 Cs1 52.5(3) 5_657 .
O4 P2 Cs4A 51.0(8) . 8_756
O9 P2 Cs4A 142.0(10) . 8_756
O6 P2 Cs4A 106.9(10) 8_655 8_756
O6 P2 Cs4A 62.5(7) . 8_756
U4 P2 Cs4A 90.9(9) . 8_756
Cs4B P2 Cs4A 32.1(9) 5_657 8_756
Cs1 P2 Cs4A 70.8(10) . 8_756
O4 P2 Cs4A 51.0(8) . 1_456
O9 P2 Cs4A 142.0(10) . 1_456
O6 P2 Cs4A 62.5(7) 8_655 1_456
O6 P2 Cs4A 106.9(10) . 1_456
U4 P2 Cs4A 90.9(9) . 1_456
Cs4B P2 Cs4A 32.1(9) 5_657 1_456
Cs1 P2 Cs4A 70.8(10) . 1_456
Cs4A P2 Cs4A 56.8(13) 8_756 1_456
O4 P2 Cs4C 59.8(6) . 4_457
O9 P2 Cs4C 161.0(6) . 4_457
O6 P2 Cs4C 88.0(7) 8_655 4_457
O6 P2 Cs4C 64.0(8) . 4_457
U4 P2 Cs4C 77.1(4) . 4_457
Cs4B P2 Cs4C 14.9(7) 5_657 4_457
Cs1 P2 Cs4C 55.1(4) . 4_457
Cs4A P2 Cs4C 19.0(12) 8_756 4_457
Cs4A P2 Cs4C 45.4(9) 1_456 4_457
O4 P2 Cs4C 59.8(6) . 5_657
O9 P2 Cs4C 161.0(7) . 5_657
O6 P2 Cs4C 64.0(8) 8_655 5_657
O6 P2 Cs4C 88.0(7) . 5_657
U4 P2 Cs4C 77.1(4) . 5_657
Cs4B P2 Cs4C 14.9(7) 5_657 5_657
Cs1 P2 Cs4C 55.1(4) . 5_657
Cs4A P2 Cs4C 45.4(9) 8_756 5_657
Cs4A P2 Cs4C 19.0(12) 1_456 5_657
Cs4C P2 Cs4C 29.7(15) 4_457 5_657
O4 P2 Cs4A 51.7(9) . 4_457
O9 P2 Cs4A 147.9(10) . 4_457
O6 P2 Cs4A 100.8(10) 8_655 4_457
O6 P2 Cs4A 64.4(7) . 4_457
U4 P2 Cs4A 87.8(9) . 4_457
Cs4B P2 Cs4A 25.9(9) 5_657 4_457
Cs1 P2 Cs4A 66.9(9) . 4_457
Cs4A P2 Cs4A 6.1(17) 8_756 4_457
Cs4A P2 Cs4A 51.57(10) 1_456 4_457
Cs4C P2 Cs4A 13.3(10) 4_457 4_457
Cs4C P2 Cs4A 39.4(12) 5_657 4_457
O11 P3 O11 110.1(11) 2 .
O11 P3 O13 109.0(6) 2 2
O11 P3 O13 109.0(6) . 2
O11 P3 O13 109.0(6) 2 .
O11 P3 O13 109.0(6) . .
O13 P3 O13 111(2) 2 .
O11 P3 Cs1 80.07(18) 2 2
O11 P3 Cs1 80.07(18) . 2
O13 P3 Cs1 162.8(11) 2 2
O13 P3 Cs1 52.2(11) . 2
O11 P3 Cs1 80.07(18) 2 .
O11 P3 Cs1 80.07(18) . .
O13 P3 Cs1 52.2(11) 2 .
O13 P3 Cs1 162.8(11) . .
Cs1 P3 Cs1 145.0(3) 2 .
O11 P3 Cs3A 148.8(6) 2 1_455
O11 P3 Cs3A 101.1(5) . 1_455
O13 P3 Cs3A 58.6(10) 2 1_455
O13 P3 Cs3A 58.6(10) . 1_455
Cs1 P3 Cs3A 105.99(11) 2 1_455
Cs1 P3 Cs3A 105.99(11) . 1_455
O11 P3 Cs3A 101.1(5) 2 2_655
O11 P3 Cs3A 148.8(6) . 2_655
O13 P3 Cs3A 58.6(10) 2 2_655
O13 P3 Cs3A 58.6(10) . 2_655
Cs1 P3 Cs3A 105.99(11) 2 2_655
Cs1 P3 Cs3A 105.99(11) . 2_655
Cs3A P3 Cs3A 47.65(13) 1_455 2_655
O11 P3 Cs2C 63.5(4) 2 2_556
O11 P3 Cs2C 63.5(4) . 2_556
O13 P3 Cs2C 163.6(12) 2 2_556
O13 P3 Cs2C 85.9(12) . 2_556
Cs1 P3 Cs2C 33.6(4) 2 2_556
Cs1 P3 Cs2C 111.3(5) . 2_556
Cs3A P3 Cs2C 135.4(3) 1_455 2_556
Cs3A P3 Cs2C 135.4(3) 2_655 2_556
O11 P3 Cs2C 63.5(4) 2 1_556
O11 P3 Cs2C 63.5(4) . 1_556
O13 P3 Cs2C 85.9(12) 2 1_556
O13 P3 Cs2C 163.6(12) . 1_556
Cs1 P3 Cs2C 111.3(5) 2 1_556
Cs1 P3 Cs2C 33.6(4) . 1_556
Cs3A P3 Cs2C 135.4(3) 1_455 1_556
Cs3A P3 Cs2C 135.4(3) 2_655 1_556
Cs2C P3 Cs2C 77.7(8) 2_556 1_556
O11 P3 Cs2A 58.4(5) 2 2_556
O11 P3 Cs2A 58.4(5) . 2_556
O13 P3 Cs2A 148.6(11) 2 2_556
O13 P3 Cs2A 100.8(11) . 2_556
Cs1 P3 Cs2A 48.55(10) 2 2_556
Cs1 P3 Cs2A 96.41(17) . 2_556
Cs3A P3 Cs2A 146.74(4) 1_455 2_556
Cs3A P3 Cs2A 146.74(4) 2_655 2_556
Cs2C P3 Cs2A 14.9(4) 2_556 2_556
Cs2C P3 Cs2A 62.8(4) 1_556 2_556
O11 P3 Cs2A 58.4(5) 2 1_556
O11 P3 Cs2A 58.4(5) . 1_556
O13 P3 Cs2A 100.8(11) 2 1_556
O13 P3 Cs2A 148.6(11) . 1_556
Cs1 P3 Cs2A 96.40(17) 2 1_556
Cs1 P3 Cs2A 48.55(10) . 1_556
Cs3A P3 Cs2A 146.74(4) 1_455 1_556
Cs3A P3 Cs2A 146.74(4) 2_655 1_556
Cs2C P3 Cs2A 62.8(4) 2_556 1_556
Cs2C P3 Cs2A 14.9(4) 1_556 1_556
Cs2A P3 Cs2A 47.85(11) 2_556 1_556
O12 P4 O8 109.1(6) . 8_755
O12 P4 O8 109.1(6) . .
O8 P4 O8 111.0(6) 8_755 .
O12 P4 O10 112.2(12) . .
O8 P4 O10 107.7(5) 8_755 .
O8 P4 O10 107.7(5) . .
O12 P4 Cs2B 152.5(11) . 5_657
O8 P4 Cs2B 59.8(3) 8_755 5_657
O8 P4 Cs2B 59.8(3) . 5_657
O10 P4 Cs2B 95.2(8) . 5_657
O12 P4 Cs4B 168.5(10) . 1_556
O8 P4 Cs4B 76.8(4) 8_755 1_556
O8 P4 Cs4B 76.8(4) . 1_556
O10 P4 Cs4B 56.3(8) . 1_556
Cs2B P4 Cs4B 38.9(6) 5_657 1_556
O12 P4 Cs2A 126.7(10) . 5_657
O8 P4 Cs2A 55.5(3) 8_755 5_657
O8 P4 Cs2A 55.5(3) . 5_657
O10 P4 Cs2A 121.1(7) . 5_657
Cs2B P4 Cs2A 25.9(5) 5_657 5_657
Cs4B P4 Cs2A 64.8(3) 1_556 5_657
O12 P4 Cs4C 160.7(9) . 1_556
O8 P4 Cs4C 65.2(8) 8_755 1_556
O8 P4 Cs4C 90.0(7) . 1_556
O10 P4 Cs4C 56.4(8) . 1_556
Cs2B P4 Cs4C 42.3(6) 5_657 1_556
Cs4B P4 Cs4C 14.7(7) 1_556 1_556
Cs2A P4 Cs4C 66.8(4) 5_657 1_556
O12 P4 Cs4C 160.7(9) . 8_756
O8 P4 Cs4C 90.0(7) 8_755 8_756
O8 P4 Cs4C 65.2(8) . 8_756
O10 P4 Cs4C 56.4(8) . 8_756
Cs2B P4 Cs4C 42.3(6) 5_657 8_756
Cs4B P4 Cs4C 14.7(7) 1_556 8_756
Cs2A P4 Cs4C 66.8(4) 5_657 8_756
Cs4C P4 Cs4C 29.4(15) 1_556 8_756
O12 P4 Cs2C 141.2(10) . 5_657
O8 P4 Cs2C 57.0(3) 8_755 5_657
O8 P4 Cs2C 57.0(3) . 5_657
O10 P4 Cs2C 106.5(8) . 5_657
Cs2B P4 Cs2C 11.3(6) 5_657 5_657
Cs4B P4 Cs2C 50.3(5) 1_556 5_657
Cs2A P4 Cs2C 14.6(4) 5_657 5_657
Cs4C P4 Cs2C 52.9(6) 1_556 5_657
Cs4C P4 Cs2C 52.9(6) 8_756 5_657
P5 P5 O7 61.8(3) 8_755 .
P5 P5 O14 158.7(6) 8_755 .
O7 P5 O14 110.3(9) . .
P5 P5 O15 94.6(6) 8_755 .
O7 P5 O15 111.1(7) . .
O14 P5 O15 106.7(9) . .
P5 P5 O3 62.5(3) 8_755 .
O7 P5 O3 111.8(5) . .
O14 P5 O3 107.3(8) . .
O15 P5 O3 109.4(7) . .
P5 P5 O15 44.8(4) 8_755 8_755
O7 P5 O15 83.9(5) . 8_755
O14 P5 O15 156.4(8) . 8_755
O15 P5 O15 49.7(9) . 8_755
O3 P5 O15 83.2(5) . 8_755
P5 P5 Cs1 160.40(13) 8_755 .
O7 P5 Cs1 108.2(3) . .
O14 P5 Cs1 3.8(8) . .
O15 P5 Cs1 105.0(6) . .
O3 P5 Cs1 111.1(3) . .
O15 P5 Cs1 154.7(4) 8_755 .
P5 P5 Cs2C 152.4(5) 8_755 1_556
O7 P5 Cs2C 103.2(7) . 1_556
O14 P5 Cs2C 45.1(8) . 1_556
O15 P5 Cs2C 68.2(8) . 1_556
O3 P5 Cs2C 142.4(6) . 1_556
O15 P5 Cs2C 114.5(7) 8_755 1_556
Cs1 P5 Cs2C 41.9(5) . 1_556
P5 P5 Cs2B 149.2(4) 8_755 1_556
O7 P5 Cs2B 121.5(6) . 1_556
O14 P5 Cs2B 52.1(7) . 1_556
O15 P5 Cs2B 54.9(7) . 1_556
O3 P5 Cs2B 126.6(6) . 1_556
O15 P5 Cs2B 104.5(5) 8_755 1_556
Cs1 P5 Cs2B 50.1(4) . 1_556
Cs2C P5 Cs2B 20.7(8) 1_556 1_556
P5 P5 Cs4C 122.1(8) 8_755 4_457
O7 P5 Cs4C 169.0(8) . 4_457
O14 P5 Cs4C 69.7(11) . 4_457
O15 P5 Cs4C 59.5(10) . 4_457
O3 P5 Cs4C 78.1(8) . 4_457
O15 P5 Cs4C 92.8(9) 8_755 4_457
Cs1 P5 Cs4C 71.1(8) . 4_457
Cs2C P5 Cs4C 68.7(10) 1_556 4_457
Cs2B P5 Cs4C 49.3(8) 1_556 4_457
P5 P5 Cs4A 108.7(11) 8_755 4_457
O7 P5 Cs4A 169.0(11) . 4_457
O14 P5 Cs4A 80.6(13) . 4_457
O15 P5 Cs4A 62.2(7) . 4_457
O3 P5 Cs4A 65.1(9) . 4_457
O15 P5 Cs4A 85.2(10) 8_755 4_457
Cs1 P5 Cs4A 82.5(11) . 4_457
Cs2C P5 Cs4A 82.9(12) 1_556 4_457
Cs2B P5 Cs4A 63.2(10) 1_556 4_457
Cs4C P5 Cs4A 14.3(11) 4_457 4_457
P5 P5 Cs4A 103.9(10) 8_755 8_756
O7 P5 Cs4A 165.7(11) . 8_756
O14 P5 Cs4A 83.3(13) . 8_756
O15 P5 Cs4A 67.0(7) . 8_756
O3 P5 Cs4A 58.2(8) . 8_756
O15 P5 Cs4A 84.7(10) 8_755 8_756
Cs1 P5 Cs4A 85.6(10) . 8_756
Cs2C P5 Cs4A 89.4(11) 1_556 8_756
Cs2B P5 Cs4A 69.9(10) 1_556 8_756
Cs4C P5 Cs4A 20.7(12) 4_457 8_756
Cs4A P5 Cs4A 6.9(15) 4_457 8_756
O16 P6 O16 114(2) 2_655 .
O16 P6 O17 119.0(10) 2_655 .
O16 P6 O17 119.0(10) . .
O16 P6 O17 119.0(10) 2_655 2_655
O16 P6 O17 119.0(10) . 2_655
O17 P6 O17 54(2) . 2_655
O16 P6 Cs3B 57.0(11) 2_655 .
O16 P6 Cs3B 57.0(11) . .
O17 P6 Cs3B 153.1(12) . .
O17 P6 Cs3B 153.1(12) 2_655 .
O16 P6 Cs3A 62.6(9) 2_655 .
O16 P6 Cs3A 62.6(9) . .
O17 P6 Cs3A 120.7(12) . .
O17 P6 Cs3A 174.5(12) 2_655 .
Cs3B P6 Cs3A 32.39(10) . .
O16 P6 Cs3A 62.6(9) 2_655 2_655
O16 P6 Cs3A 62.6(9) . 2_655
O17 P6 Cs3A 174.5(12) . 2_655
O17 P6 Cs3A 120.7(12) 2_655 2_655
Cs3B P6 Cs3A 32.39(10) . 2_655
Cs3A P6 Cs3A 64.8(2) . 2_655
O16 P6 Cs2A 117.23(13) 2_655 2_655
O16 P6 Cs2A 76.2(4) . 2_655
O17 P6 Cs2A 54.5(10) . 2_655
O17 P6 Cs2A 102.9(11) 2_655 2_655
Cs3B P6 Cs2A 101.60(16) . 2_655
Cs3A P6 Cs2A 72.21(9) . 2_655
Cs3A P6 Cs2A 130.2(2) 2_655 2_655
O16 P6 Cs2A 117.23(13) 2_655 2
O16 P6 Cs2A 76.2(4) . 2
O17 P6 Cs2A 102.9(11) . 2
O17 P6 Cs2A 54.5(10) 2_655 2
Cs3B P6 Cs2A 101.60(16) . 2
Cs3A P6 Cs2A 130.2(2) . 2
Cs3A P6 Cs2A 72.21(9) 2_655 2
Cs2A P6 Cs2A 125.08(14) 2_655 2
O16 P6 Cs2A 76.2(4) 2_655 1_655
O16 P6 Cs2A 117.23(13) . 1_655
O17 P6 Cs2A 54.5(10) . 1_655
O17 P6 Cs2A 102.9(11) 2_655 1_655
Cs3B P6 Cs2A 101.60(16) . 1_655
Cs3A P6 Cs2A 72.21(9) . 1_655
Cs3A P6 Cs2A 130.2(2) 2_655 1_655
Cs2A P6 Cs2A 49.04(7) 2_655 1_655
Cs2A P6 Cs2A 156.8(3) 2 1_655
O16 P6 Cs2A 76.2(4) 2_655 .
O16 P6 Cs2A 117.23(13) . .
O17 P6 Cs2A 102.9(11) . .
O17 P6 Cs2A 54.5(10) 2_655 .
Cs3B P6 Cs2A 101.60(16) . .
Cs3A P6 Cs2A 130.2(2) . .
Cs3A P6 Cs2A 72.21(9) 2_655 .
Cs2A P6 Cs2A 156.8(3) 2_655 .
Cs2A P6 Cs2A 49.04(7) 2 .
Cs2A P6 Cs2A 125.08(14) 1_655 .
P1 O1 U3 150.8(6) . 1_556
P1 O1 Cs3B 93.9(6) . .
U3 O1 Cs3B 115.3(5) 1_556 .
P1 O1 Cs3A 93.4(4) . .
U3 O1 Cs3A 109.8(3) 1_556 .
Cs3B O1 Cs3A 36.67(11) . .
P1 O1 Cs3A 93.4(4) . 2_655
U3 O1 Cs3A 109.8(3) 1_556 2_655
Cs3B O1 Cs3A 36.67(11) . 2_655
Cs3A O1 Cs3A 73.3(2) . 2_655
P1 O2 U1 153.8(6) . .
P1 O2 Cs3B 100.9(9) . .
U1 O2 Cs3B 105.3(8) . .
P1 O2 Cs3A 97.9(4) . .
U1 O2 Cs3A 102.6(3) . .
Cs3B O2 Cs3A 38.28(11) . .
P1 O2 Cs3A 97.9(4) . 2_655
U1 O2 Cs3A 102.6(3) . 2_655
Cs3B O2 Cs3A 38.28(11) . 2_655
Cs3A O2 Cs3A 76.5(2) . 2_655
P5 O3 P5 54.9(5) 8_755 .
P5 O3 U2 133.2(5) 8_755 .
P5 O3 U2 133.2(5) . .
P5 O3 Cs4A 126.5(8) 8_755 8_756
P5 O3 Cs4A 97.3(11) . 8_756
U2 O3 Cs4A 99.7(7) . 8_756
P5 O3 Cs4A 97.3(11) 8_755 1_556
P5 O3 Cs4A 126.5(8) . 1_556
U2 O3 Cs4A 99.7(7) . 1_556
Cs4A O3 Cs4A 61(3) 8_756 1_556
P5 O3 Cs4A 89.9(11) 8_755 5_757
P5 O3 Cs4A 121.5(8) . 5_757
U2 O3 Cs4A 105.1(7) . 5_757
Cs4A O3 Cs4A 65.5(2) 8_756 5_757
Cs4A O3 Cs4A 7(2) 1_556 5_757
P5 O3 Cs4A 121.5(8) 8_755 4_457
P5 O3 Cs4A 89.9(11) . 4_457
U2 O3 Cs4A 105.1(7) . 4_457
Cs4A O3 Cs4A 7(2) 8_756 4_457
Cs4A O3 Cs4A 65.5(2) 1_556 4_457
Cs4A O3 Cs4A 69(3) 5_757 4_457
P5 O3 Cs4C 75.0(6) 8_755 5_757
P5 O3 Cs4C 115.0(8) . 5_757
U2 O3 Cs4C 110.6(8) . 5_757
Cs4A O3 Cs4C 80.2(14) 8_756 5_757
Cs4A O3 Cs4C 23.1(14) 1_556 5_757
Cs4A O3 Cs4C 16.2(13) 5_757 5_757
Cs4A O3 Cs4C 83.1(14) 4_457 5_757
P5 O3 Cs4C 115.0(8) 8_755 4_457
P5 O3 Cs4C 75.0(6) . 4_457
U2 O3 Cs4C 110.6(8) . 4_457
Cs4A O3 Cs4C 23.1(14) 8_756 4_457
Cs4A O3 Cs4C 80.2(14) 1_556 4_457
Cs4A O3 Cs4C 83.1(14) 5_757 4_457
Cs4A O3 Cs4C 16.2(13) 4_457 4_457
Cs4C O3 Cs4C 95.2(15) 5_757 4_457
P5 O3 Cs4B 121.4(5) 8_755 1_556
P5 O3 Cs4B 121.4(5) . 1_556
U2 O3 Cs4B 93.5(4) . 1_556
Cs4A O3 Cs4B 31.4(13) 8_756 1_556
Cs4A O3 Cs4B 31.4(13) 1_556 1_556
Cs4A O3 Cs4B 37.4(13) 5_757 1_556
Cs4A O3 Cs4B 37.4(13) 4_457 1_556
Cs4C O3 Cs4B 53.5(6) 5_757 1_556
Cs4C O3 Cs4B 53.5(6) 4_457 1_556
P5 O3 Cs4C 129.0(9) 8_755 8_756
P5 O3 Cs4C 111.0(8) . 8_756
U2 O3 Cs4C 93.7(8) . 8_756
Cs4A O3 Cs4C 15.1(13) 8_756 8_756
Cs4A O3 Cs4C 48.0(16) 1_556 8_756
Cs4A O3 Cs4C 53.5(15) 5_757 8_756
Cs4A O3 Cs4C 22.0(16) 4_457 8_756
Cs4C O3 Cs4C 69.2(5) 5_757 8_756
Cs4C O3 Cs4C 38.1(12) 4_457 8_756
Cs4B O3 Cs4C 17.0(8) 1_556 8_756
P5 O3 Cs4C 111.0(8) 8_755 1_556
P5 O3 Cs4C 129.0(9) . 1_556
U2 O3 Cs4C 93.7(8) . 1_556
Cs4A O3 Cs4C 48.0(16) 8_756 1_556
Cs4A O3 Cs4C 15.1(13) 1_556 1_556
Cs4A O3 Cs4C 22.0(16) 5_757 1_556
Cs4A O3 Cs4C 53.5(15) 4_457 1_556
Cs4C O3 Cs4C 38.1(12) 5_757 1_556
Cs4C O3 Cs4C 69.2(5) 4_457 1_556
Cs4B O3 Cs4C 17.0(8) 1_556 1_556
Cs4C O3 Cs4C 34.0(16) 8_756 1_556
P2 O4 U1 137.1(7) . 5_657
P2 O4 Cs4A 107.7(11) . 8_756
U1 O4 Cs4A 106.8(13) 5_657 8_756
P2 O4 Cs4A 107.7(11) . 1_456
U1 O4 Cs4A 106.8(13) 5_657 1_456
Cs4A O4 Cs4A 71.3(17) 8_756 1_456
P2 O4 Cs4A 107.7(11) . 4_457
U1 O4 Cs4A 109.9(12) 5_657 4_457
Cs4A O4 Cs4A 7(2) 8_756 4_457
Cs4A O4 Cs4A 64.1(2) 1_456 4_457
P2 O4 Cs4A 107.7(11) . 5_657
U1 O4 Cs4A 109.9(12) 5_657 5_657
Cs4A O4 Cs4A 64.1(2) 8_756 5_657
Cs4A O4 Cs4A 7(2) 1_456 5_657
Cs4A O4 Cs4A 56.8(17) 4_457 5_657
P2 O4 Cs4B 97.3(6) . 5_657
U1 O4 Cs4B 125.6(5) 5_657 5_657
Cs4A O4 Cs4B 38.2(11) 8_756 5_657
Cs4A O4 Cs4B 38.2(11) 1_456 5_657
Cs4A O4 Cs4B 31.0(11) 4_457 5_657
Cs4A O4 Cs4B 31.0(11) 5_657 5_657
P2 O4 Cs4C 115.8(7) . 8_756
U1 O4 Cs4C 93.3(5) 5_657 8_756
Cs4A O4 Cs4C 15.6(13) 8_756 8_756
Cs4A O4 Cs4C 82.3(12) 1_456 8_756
Cs4A O4 Cs4C 22.1(15) 4_457 8_756
Cs4A O4 Cs4C 75.5(9) 5_657 8_756
Cs4B O4 Cs4C 52.9(7) 5_657 8_756
P2 O4 Cs4C 115.8(7) . 1_456
U1 O4 Cs4C 93.3(5) 5_657 1_456
Cs4A O4 Cs4C 82.3(12) 8_756 1_456
Cs4A O4 Cs4C 15.6(13) 1_456 1_456
Cs4A O4 Cs4C 75.5(9) 4_457 1_456
Cs4A O4 Cs4C 22.1(15) 5_657 1_456
Cs4B O4 Cs4C 52.9(7) 5_657 1_456
Cs4C O4 Cs4C 90.6(16) 8_756 1_456
P2 O4 Cs4C 98.2(7) . 4_457
U1 O4 Cs4C 122.6(6) 5_657 4_457
Cs4A O4 Cs4C 22.1(15) 8_756 4_457
Cs4A O4 Cs4C 54.2(11) 1_456 4_457
Cs4A O4 Cs4C 15.6(14) 4_457 4_457
Cs4A O4 Cs4C 46.8(15) 5_657 4_457
Cs4B O4 Cs4C 17.1(8) 5_657 4_457
Cs4C O4 Cs4C 37.5(11) 8_756 4_457
Cs4C O4 Cs4C 67.9(5) 1_456 4_457
P2 O4 Cs4C 98.2(7) . 5_657
U1 O4 Cs4C 122.6(6) 5_657 5_657
Cs4A O4 Cs4C 54.2(11) 8_756 5_657
Cs4A O4 Cs4C 22.1(15) 1_456 5_657
Cs4A O4 Cs4C 46.8(15) 4_457 5_657
Cs4A O4 Cs4C 15.6(14) 5_657 5_657
Cs4B O4 Cs4C 17.1(8) 5_657 5_657
Cs4C O4 Cs4C 67.9(5) 8_756 5_657
Cs4C O4 Cs4C 37.5(11) 1_456 5_657
Cs4C O4 Cs4C 34.1(16) 4_457 5_657
P1 O5 U4 146.7(4) . .
P1 O5 U2 100.8(3) . .
U4 O5 U2 110.4(2) . .
P1 O5 Cs1 133.7(4) . .
U4 O5 Cs1 27.25(9) . .
U2 O5 Cs1 103.8(2) . .
P2 O6 U2 146.4(5) . .
P2 O6 U4 98.6(4) . .
U2 O6 U4 110.8(3) . .
P2 O6 Cs1 103.8(4) . .
U2 O6 Cs1 109.8(3) . .
U4 O6 Cs1 28.71(12) . .
P2 O6 Cs4A 94.6(8) . 8_756
U2 O6 Cs4A 88.6(9) . 8_756
U4 O6 Cs4A 113.4(11) . 8_756
Cs1 O6 Cs4A 84.8(10) . 8_756
P2 O6 Cs4C 93.2(9) . 4_457
U2 O6 Cs4C 101.1(9) . 4_457
U4 O6 Cs4C 92.8(6) . 4_457
Cs1 O6 Cs4C 64.5(5) . 4_457
Cs4A O6 Cs4C 21.2(13) 8_756 4_457
P2 O6 Cs4A 93.3(8) . 4_457
U2 O6 Cs4A 93.2(9) . 4_457
U4 O6 Cs4A 107.3(11) . 4_457
Cs1 O6 Cs4A 78.8(11) . 4_457
Cs4A O6 Cs4A 7(2) 8_756 4_457
Cs4C O6 Cs4A 14.7(11) 4_457 4_457
P2 O6 Cs4B 81.5(4) . 5_657
U2 O6 Cs4B 116.6(3) . 5_657
U4 O6 Cs4B 84.2(4) . 5_657
Cs1 O6 Cs4B 58.1(4) . 5_657
Cs4A O6 Cs4B 34.3(10) 8_756 5_657
Cs4C O6 Cs4B 15.8(8) 4_457 5_657
Cs4A O6 Cs4B 27.8(10) 4_457 5_657
P5 O7 P5 56.4(6) . 8_755
P5 O7 U3 151.8(3) . 1_556
P5 O7 U3 151.8(3) 8_755 1_556
P5 O7 Cs1 103.5(4) . 1_655
P5 O7 Cs1 49.0(2) 8_755 1_655
U3 O7 Cs1 103.45(18) 1_556 1_655
P5 O7 Cs1 49.0(2) . .
P5 O7 Cs1 103.5(4) 8_755 .
U3 O7 Cs1 103.45(18) 1_556 .
Cs1 O7 Cs1 140.5(3) 1_655 .
P5 O7 Cs2C 106.5(7) . 1_656
P5 O7 Cs2C 53.9(6) 8_755 1_656
U3 O7 Cs2C 100.5(6) 1_556 1_656
Cs1 O7 Cs2C 33.9(4) 1_655 1_656
Cs1 O7 Cs2C 155.4(6) . 1_656
P5 O7 Cs2C 53.9(6) . 1_556
P5 O7 Cs2C 106.5(7) 8_755 1_556
U3 O7 Cs2C 100.5(6) 1_556 1_556
Cs1 O7 Cs2C 155.4(6) 1_655 1_556
Cs1 O7 Cs2C 33.9(4) . 1_556
Cs2C O7 Cs2C 135.1(9) 1_656 1_556
P4 O8 U1 159.6(5) . 5_657
P4 O8 Cs2B 92.0(4) . 5_657
U1 O8 Cs2B 103.6(3) 5_657 5_657
P4 O8 Cs2A 102.8(4) . 5_657
U1 O8 Cs2A 97.4(2) 5_657 5_657
Cs2B O8 Cs2A 31.9(5) 5_657 5_657
P4 O8 Cs2C 101.7(4) . 5_657
U1 O8 Cs2C 96.5(3) 5_657 5_657
Cs2B O8 Cs2C 16.0(7) 5_657 5_657
Cs2A O8 Cs2C 17.1(5) 5_657 5_657
P4 O8 Cs4C 92.6(9) . 8_756
U1 O8 Cs4C 88.4(8) 5_657 8_756
Cs2B O8 Cs4C 47.6(8) 5_657 8_756
Cs2A O8 Cs4C 77.7(5) 5_657 8_756
Cs2C O8 Cs4C 60.6(7) 5_657 8_756
P4 O8 Cs4B 80.4(4) . 1_556
U1 O8 Cs4B 103.2(3) 5_657 1_556
Cs2B O8 Cs4B 39.6(6) 5_657 1_556
Cs2A O8 Cs4B 71.4(3) 5_657 1_556
Cs2C O8 Cs4B 54.9(6) 5_657 1_556
Cs4C O8 Cs4B 15.5(8) 8_756 1_556
P2 O9 U2 161.2(8) . 5_657
P4 O10 U2 161.5(12) . .
P4 O10 Cs4B 100.5(8) . 1_556
U2 O10 Cs4B 98.0(7) . 1_556
P4 O10 Cs4C 101.4(9) . 1_556
U2 O10 Cs4C 96.3(7) . 1_556
Cs4B O10 Cs4C 17.4(8) 1_556 1_556
P4 O10 Cs4C 101.4(9) . 8_756
U2 O10 Cs4C 96.3(7) . 8_756
Cs4B O10 Cs4C 17.4(8) 1_556 8_756
Cs4C O10 Cs4C 34.8(17) 1_556 8_756
P4 O10 Cs2B 60.0(7) . 5_657
U2 O10 Cs2B 138.5(8) . 5_657
Cs4B O10 Cs2B 40.5(6) 1_556 5_657
Cs4C O10 Cs2B 44.7(6) 1_556 5_657
Cs4C O10 Cs2B 44.7(6) 8_756 5_657
P4 O10 Cs4A 112.0(11) . 1_556
U2 O10 Cs4A 84.6(11) . 1_556
Cs4B O10 Cs4A 28.7(11) 1_556 1_556
Cs4C O10 Cs4A 14.1(12) 1_556 1_556
Cs4C O10 Cs4A 44.4(14) 8_756 1_556
Cs2B O10 Cs4A 58.3(12) 5_657 1_556
P4 O10 Cs4A 112.0(11) . 8_756
U2 O10 Cs4A 84.6(11) . 8_756
Cs4B O10 Cs4A 28.7(11) 1_556 8_756
Cs4C O10 Cs4A 44.4(14) 1_556 8_756
Cs4C O10 Cs4A 14.1(12) 8_756 8_756
Cs2B O10 Cs4A 58.3(12) 5_657 8_756
Cs4A O10 Cs4A 50.6(18) 1_556 8_756
P3 O11 U3 146.6(9) . 1_456
P3 O11 Cs2A 99.9(5) . 2_556
U3 O11 Cs2A 109.5(4) 1_456 2_556
P3 O11 Cs2A 99.9(5) . 1_556
U3 O11 Cs2A 109.5(4) 1_456 1_556
Cs2A O11 Cs2A 55.9(2) 2_556 1_556
P3 O11 Cs2C 94.0(5) . 2_556
U3 O11 Cs2C 109.5(4) 1_456 2_556
Cs2A O11 Cs2C 17.0(5) 2_556 2_556
Cs2A O11 Cs2C 72.5(5) 1_556 2_556
P3 O11 Cs2C 94.0(5) . 1_556
U3 O11 Cs2C 109.5(4) 1_456 1_556
Cs2A O11 Cs2C 72.5(5) 2_556 1_556
Cs2A O11 Cs2C 17.0(5) 1_556 1_556
Cs2C O11 Cs2C 88.7(9) 2_556 1_556
P3 O11 Cs1 75.0(2) . 2
U3 O11 Cs1 110.44(18) 1_456 2
Cs2A O11 Cs1 52.87(14) 2_556 2
Cs2A O11 Cs1 105.9(3) 1_556 2
Cs2C O11 Cs1 36.1(5) 2_556 2
Cs2C O11 Cs1 120.0(5) 1_556 2
P3 O11 Cs1 75.0(2) . .
U3 O11 Cs1 110.44(18) 1_456 .
Cs2A O11 Cs1 105.9(3) 2_556 .
Cs2A O11 Cs1 52.87(14) 1_556 .
Cs2C O11 Cs1 120.0(5) 2_556 .
Cs2C O11 Cs1 36.1(5) 1_556 .
Cs1 O11 Cs1 138.5(4) 2 .
P4 O12 U4 168.0(16) . 5_657
P4 O12 Cs1 172.8(13) . 5_657
U4 O12 Cs1 4.8(3) 5_657 5_657
P3 O13 U4 135.7(15) . 2
P3 O13 Cs1 102.1(12) . 2
U4 O13 Cs1 33.6(4) 2 2
P3 O13 Cs3A 96.9(11) . 1_455
U4 O13 Cs3A 121.7(5) 2 1_455
Cs1 O13 Cs3A 146.1(4) 2 1_455
P3 O13 Cs3A 96.9(11) . 2_655
U4 O13 Cs3A 121.7(5) 2 2_655
Cs1 O13 Cs3A 146.1(4) 2 2_655
Cs3A O13 Cs3A 56.0(5) 1_455 2_655
Cs1 O14 P5 172.0(16) . .
Cs1 O14 Cs2C 66.4(8) . 1_556
P5 O14 Cs2C 106.9(9) . 1_556
Cs1 O14 U4 39.7(5) . .
P5 O14 U4 146.0(10) . .
Cs2C O14 U4 105.7(9) 1_556 .
Cs1 O14 Cs2B 75.8(8) . 1_556
P5 O14 Cs2B 100.0(8) . 1_556
Cs2C O14 Cs2B 26.3(11) 1_556 1_556
U4 O14 Cs2B 113.7(7) . 1_556
Cs1 O14 Cs4C 100.0(14) . 4_457
P5 O14 Cs4C 82.8(12) . 4_457
Cs2C O14 Cs4C 82.3(13) 1_556 4_457
U4 O14 Cs4C 111.2(12) . 4_457
Cs2B O14 Cs4C 56.1(10) 1_556 4_457
Cs1 O14 Cs2A 74.6(7) . 1_556
P5 O14 Cs2A 98.1(8) . 1_556
Cs2C O14 Cs2A 12.2(6) 1_556 1_556
U4 O14 Cs2A 112.4(7) . 1_556
Cs2B O14 Cs2A 34.4(6) 1_556 1_556
Cs4C O14 Cs2A 89.5(9) 4_457 1_556
Cs1 O14 Cs4B 82.3(9) . 5_657
P5 O14 Cs4B 99.9(9) . 5_657
Cs2C O14 Cs4B 71.9(10) 1_556 5_657
U4 O14 Cs4B 99.3(7) . 5_657
Cs2B O14 Cs4B 47.1(7) 1_556 5_657
Cs4C O14 Cs4B 18.0(9) 4_457 5_657
Cs2A O14 Cs4B 81.4(5) 1_556 5_657
Cs1 O14 Cs4A 108.5(13) . 4_457
P5 O14 Cs4A 75.4(11) . 4_457
Cs2C O14 Cs4A 93.6(12) 1_556 4_457
U4 O14 Cs4A 112.1(10) . 4_457
Cs2B O14 Cs4A 67.3(9) 1_556 4_457
Cs4C O14 Cs4A 12.0(9) 4_457 4_457
Cs2A O14 Cs4A 99.8(7) 1_556 4_457
Cs4B O14 Cs4A 28.8(8) 5_657 4_457
Cs1 O14 Cs4A 111.5(13) . 8_756
P5 O14 Cs4A 73.2(11) . 8_756
Cs2C O14 Cs4A 100.1(12) 1_556 8_756
U4 O14 Cs4A 110.4(10) . 8_756
Cs2B O14 Cs4A 73.9(9) 1_556 8_756
Cs4C O14 Cs4A 18.4(12) 4_457 8_756
Cs2A O14 Cs4A 106.1(6) 1_556 8_756
Cs4B O14 Cs4A 34.4(8) 5_657 8_756
Cs4A O14 Cs4A 6.6(12) 4_457 8_756
P5 O15 O15 85.4(6) . 8_755
P5 O15 P5 40.6(5) . 8_755
O15 O15 P5 44.8(4) 8_755 8_755
P5 O15 U1 150.9(9) . 1_556
O15 O15 U1 68.5(4) 8_755 1_556
P5 O15 U1 112.2(6) 8_755 1_556
P5 O15 Cs2B 96.8(9) . 1_556
O15 O15 Cs2B 175.3(6) 8_755 1_556
P5 O15 Cs2B 137.3(8) 8_755 1_556
U1 O15 Cs2B 108.4(8) 1_556 1_556
P5 O15 Cs4C 92.6(11) . 4_457
O15 O15 Cs4C 125.0(9) 8_755 4_457
P5 O15 Cs4C 114.0(10) 8_755 4_457
U1 O15 Cs4C 112.6(10) 1_556 4_457
Cs2B O15 Cs4C 59.2(11) 1_556 4_457
P5 O15 Cs2C 82.6(9) . 1_556
O15 O15 Cs2C 154.8(7) 8_755 1_556
P5 O15 Cs2C 120.0(8) 8_755 1_556
U1 O15 Cs2C 115.8(8) 1_556 1_556
Cs2B O15 Cs2C 23.0(9) 1_556 1_556
Cs4C O15 Cs2C 77.8(11) 4_457 1_556
P5 O15 Cs4A 92.8(8) . 4_457
O15 O15 Cs4A 108.9(12) 8_755 4_457
P5 O15 Cs4A 104.3(8) 8_755 4_457
U1 O15 Cs4A 107.4(10) 1_556 4_457
Cs2B O15 Cs4A 75.1(13) 1_556 4_457
Cs4C O15 Cs4A 16.1(13) 4_457 4_457
Cs2C O15 Cs4A 93.8(14) 1_556 4_457
P5 O15 Cs2A 92.9(6) . 1_556
O15 O15 Cs2A 143.2(2) 8_755 1_556
P5 O15 Cs2A 123.9(6) 8_755 1_556
U1 O15 Cs2A 100.3(5) 1_556 1_556
Cs2B O15 Cs2A 32.8(6) 1_556 1_556
Cs4C O15 Cs2A 91.8(10) 4_457 1_556
Cs2C O15 Cs2A 17.8(6) 1_556 1_556
Cs4A O15 Cs2A 107.8(12) 4_457 1_556
P5 O15 Cs4A 88.3(8) . 8_756
O15 O15 Cs4A 103.0(11) 8_755 8_756
P5 O15 Cs4A 97.2(7) 8_755 8_756
U1 O15 Cs4A 109.5(10) 1_556 8_756
Cs2B O15 Cs4A 81.2(13) 1_556 8_756
Cs4C O15 Cs4A 22.1(15) 4_457 8_756
Cs2C O15 Cs4A 98.7(14) 1_556 8_756
Cs4A O15 Cs4A 7.2(15) 4_457 8_756
Cs2A O15 Cs4A 113.6(12) 1_556 8_756
P5 O15 Cs4B 93.0(7) . 5_657
O15 O15 Cs4B 139.7(4) 8_755 5_657
P5 O15 Cs4B 122.3(6) 8_755 5_657
U1 O15 Cs4B 115.1(6) 1_556 5_657
Cs2B O15 Cs4B 44.5(7) 1_556 5_657
Cs4C O15 Cs4B 14.7(9) 4_457 5_657
Cs2C O15 Cs4B 63.4(7) 1_556 5_657
Cs4A O15 Cs4B 30.8(12) 4_457 5_657
Cs2A O15 Cs4B 77.1(4) 1_556 5_657
Cs4A O15 Cs4B 36.7(11) 8_756 5_657
P5 O15 Cs1 51.0(5) . .
O15 O15 Cs1 136.4(2) 8_755 .
P5 O15 Cs1 91.6(5) 8_755 .
U1 O15 Cs1 152.2(6) 1_556 .
Cs2B O15 Cs1 45.8(5) 1_556 .
Cs4C O15 Cs1 66.7(9) 4_457 .
Cs2C O15 Cs1 36.6(6) 1_556 .
Cs4A O15 Cs1 78.7(12) 4_457 .
Cs2A O15 Cs1 52.8(2) 1_556 .
Cs4A O15 Cs1 80.0(11) 8_756 .
Cs4B O15 Cs1 57.2(4) 5_657 .
P6 O16 U1 158.1(17) . 2_655
P6 O16 Cs3B 96.8(13) . .
U1 O16 Cs3B 105.2(10) 2_655 .
P6 O16 Cs3A 95.7(10) . .
U1 O16 Cs3A 101.8(7) 2_655 .
Cs3B O16 Cs3A 36.9(3) . .
P6 O16 Cs3A 95.7(10) . 2_655
U1 O16 Cs3A 101.8(7) 2_655 2_655
Cs3B O16 Cs3A 36.9(3) . 2_655
Cs3A O16 Cs3A 73.8(5) . 2_655
O17 O17 P6 63.1(12) 2_655 .
O17 O17 U3 74.5(7) 2_655 .
P6 O17 U3 137.5(17) . .
O17 O17 Cs2A 149.3(3) 2_655 2_655
P6 O17 Cs2A 105.4(12) . 2_655
U3 O17 Cs2A 111.4(9) . 2_655
O17 O17 Cs2A 149.3(3) 2_655 1_655
P6 O17 Cs2A 105.4(12) . 1_655
U3 O17 Cs2A 111.4(9) . 1_655
Cs2A O17 Cs2A 58.9(5) 2_655 1_655
O17 O17 Cs2C 139.2(5) 2_655 2_655
P6 O17 Cs2C 112.3(11) . 2_655
U3 O17 Cs2C 99.3(8) . 2_655
Cs2A O17 Cs2C 15.2(4) 2_655 2_655
Cs2A O17 Cs2C 71.1(6) 1_655 2_655
O17 O17 Cs2C 139.2(5) 2_655 1_655
P6 O17 Cs2C 112.3(11) . 1_655
U3 O17 Cs2C 99.3(8) . 1_655
Cs2A O17 Cs2C 71.1(6) 2_655 1_655
Cs2A O17 Cs2C 15.2(4) 1_655 1_655
Cs2C O17 Cs2C 81.5(10) 2_655 1_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
U1 O16 2.17(3) 2_655
U1 O15 2.262(14) 1_554
U1 O15 2.262(14) 8_754
U1 O2 2.271(9) .
U1 O4 2.286(10) 5_657
U1 O8 2.291(7) 4_557
U1 O8 2.291(7) 5_657
U1 Cs3B 3.824(16) .
U1 Cs2B 3.986(11) .
U1 Cs2B 3.986(11) 1_655
U1 Cs4C 4.25(5) 4_456
U1 Cs4C 4.25(5) 5_756
U2 O10 2.194(13) .
U2 O9 2.208(11) 5_657
U2 O3 2.221(10) .
U2 O6 2.286(7) 8_755
U2 O6 2.286(7) .
U2 O5 2.470(7) 8_755
U2 O5 2.470(6) .
U2 P1 3.148(3) .
U2 U4 4.0026(6) .
U2 U4 4.0027(6) 1_655
U2 Cs4A 4.14(3) 1_556
U2 Cs4A 4.14(3) 8_756
U3 O11 2.239(12) 2_554
U3 O11 2.239(12) 1_654
U3 O7 2.294(10) 2_654
U3 O7 2.294(10) 1_554
U3 O1 2.343(9) 1_554
U3 O1 2.343(9) 2_654
U3 O17 2.36(3) 2_655
U3 O17 2.36(3) .
U3 Cs3B 4.28(3) 1_554
U3 Cs3A 4.689(3) 2_654
U3 Cs3A 4.689(3) 1_554
U3 Cs2A 4.7039(16) 2_655
U4 Cs1 1.542(4) .
U4 O12 2.235(14) 5_657
U4 O14 2.336(16) .
U4 O14 2.336(16) 8_655
U4 O5 2.403(7) .
U4 O5 2.403(7) 8_655
U4 O13 2.44(3) 2
U4 O6 2.574(8) .
U4 O6 2.574(8) 8_655
U4 P2 3.190(3) .
U4 Cs2C 3.70(3) 1_556
U4 U2 4.0026(6) 1_455
Cs1 O14 1.408(18) .
Cs1 O14 1.408(18) 8_655
Cs1 Cs2C 2.17(3) 1_556
Cs1 Cs2B 2.61(2) 1_556
Cs1 O13 2.78(3) 2
Cs1 P5 2.928(6) .
Cs1 P5 2.928(6) 8_655
Cs1 Cs2A 3.098(4) 1_556
Cs1 O6 3.178(8) .
Cs1 O6 3.178(8) 8_655
Cs1 O5 3.216(7) .
Cs2A Cs2C 1.03(3) .
Cs2A Cs2B 1.79(3) .
Cs2A Cs1 3.098(4) 1_554
Cs2A O14 3.160(18) 8_654
Cs2A O14 3.160(18) 1_554
Cs2A Cs2A 3.242(5) 2
Cs2A O15 3.290(15) 8_654
Cs2A O15 3.290(15) 1_554
Cs2A O17 3.30(2) 2_655
Cs2A O17 3.30(2) 1_455
Cs2A O8 3.374(8) 5_657
Cs2A O8 3.374(8) 4_457
Cs2B Cs2C 1.14(4) .
Cs2B Cs4B 2.43(3) 5_656
Cs2B O14 2.57(2) 8_654
Cs2B O14 2.57(2) 1_554
Cs2B Cs1 2.61(2) 1_554
Cs2B O15 2.645(15) 8_654
Cs2B O15 2.645(15) 1_554
Cs2B Cs4C 2.71(4) 5_656
Cs2B Cs4C 2.71(4) 4_456
Cs2B O8 2.77(2) 5_657
Cs2B O8 2.77(2) 4_457
Cs2C Cs1 2.17(3) 1_554
Cs2C O14 2.31(3) 8_654
Cs2C O14 2.31(3) 1_554
Cs2C O15 2.91(2) 8_654
Cs2C O15 2.91(2) 1_554
Cs2C P5 3.113(14) 8_654
Cs2C P5 3.113(14) 1_554
Cs2C Cs4B 3.38(4) 5_656
Cs2C O11 3.50(3) 2_554
Cs2C O11 3.50(3) 1_554
Cs3A Cs3B 1.998(3) .
Cs3A Cs3A 2.936(6) 2_755
Cs3A O13 3.12(2) 1_655
Cs3A O13 3.12(2) 2_655
Cs3A O2 3.226(8) .
Cs3A O2 3.226(8) 2_655
Cs3A O16 3.33(2) 2_655
Cs3A O16 3.33(2) .
Cs3A O1 3.346(8) .
Cs3A O1 3.346(8) 2_655
Cs3A P3 3.634(7) 1_655
Cs3A P6 3.730(10) .
Cs3B Cs3A 1.998(3) 2_655
Cs3B O2 2.535(10) .
Cs3B O2 2.535(10) 2_655
Cs3B O16 2.63(4) 2_655
Cs3B O16 2.63(4) .
Cs3B O1 2.71(3) .
Cs3B O1 2.71(3) 2_655
Cs3B P6 3.11(3) .
Cs3B P1 3.192(17) .
Cs3B P1 3.193(17) 2_655
Cs4A Cs4A 0.44(10) 5_756
Cs4A Cs4C 0.93(8) .
Cs4A Cs4C 1.31(8) 5_756
Cs4A Cs4B 1.79(7) .
Cs4A Cs4B 2.15(7) 5_756
Cs4A Cs4C 2.71(9) 8_755
Cs4A Cs4C 3.05(8) 4_556
Cs4A O3 3.14(4) 1_554
Cs4A Cs4A 3.18(11) 8_755
Cs4A O4 3.22(4) 1_654
Cs4A O15 3.22(5) 4_557
Cs4A O3 3.30(4) 5_757
Cs4B Cs4C 1.02(5) .
Cs4B Cs4C 1.02(5) 8_755
Cs4B Cs4A 1.79(7) 8_755
Cs4B Cs4A 2.15(7) 5_756
Cs4B Cs4A 2.15(7) 4_456
Cs4B Cs2B 2.43(3) 5_656
Cs4B Cs4C 3.03(4) 5_756
Cs4B Cs4C 3.03(4) 4_456
Cs4B O10 3.26(2) 1_554
Cs4B O14 3.29(3) 5_657
Cs4B O14 3.29(3) 4_557
Cs4C Cs4A 1.31(8) 5_756
Cs4C Cs4C 2.03(10) 8_755
Cs4C Cs4C 2.22(7) 5_756
Cs4C Cs2B 2.71(4) 5_656
Cs4C Cs4A 2.71(9) 8_755
Cs4C O15 2.83(5) 4_557
Cs4C Cs4B 3.03(4) 5_756
Cs4C Cs4A 3.05(8) 4_456
Cs4C O14 3.10(4) 4_557
Cs4C P5 3.28(4) 4_557
P1 O1 1.508(9) .
P1 O2 1.521(9) .
P1 O5 1.544(7) .
P1 O5 1.544(7) 8_755
P1 Cs3A 3.750(3) 2_655
P2 O4 1.501(10) .
P2 O9 1.521(12) .
P2 O6 1.540(7) 8_655
P2 O6 1.540(7) .
P2 Cs4B 3.837(17) 5_657
P2 Cs4A 3.94(5) 8_756
P2 Cs4A 3.94(5) 1_456
P2 Cs4C 3.97(4) 4_457
P2 Cs4C 3.97(4) 5_657
P2 Cs4A 4.06(4) 4_457
P3 O11 1.498(13) 2
P3 O11 1.498(13) .
P3 O13 1.520(17) 2
P3 O13 1.520(17) .
P3 Cs1 3.434(4) 2
P3 Cs3A 3.634(7) 1_455
P3 Cs3A 3.634(7) 2_655
P3 Cs2C 3.90(4) 2_556
P3 Cs2C 3.90(4) 1_556
P3 Cs2A 3.997(7) 2_556
P3 Cs2A 3.997(7) 1_556
P4 O12 1.508(15) .
P4 O8 1.514(7) 8_755
P4 O8 1.514(7) .
P4 O10 1.545(14) .
P4 Cs2B 3.20(2) 5_657
P4 Cs4B 3.855(18) 1_556
P4 Cs2A 3.991(4) 5_657
P4 Cs4C 4.00(4) 1_556
P4 Cs4C 4.00(4) 8_756
P4 Cs2C 4.09(3) 5_657
P5 P5 1.416(11) 8_755
P5 O7 1.499(10) .
P5 O14 1.527(18) .
P5 O15 1.534(15) .
P5 O3 1.535(10) .
P5 O15 2.169(15) 8_755
P5 Cs2C 3.113(14) 1_556
P5 Cs2B 3.210(13) 1_556
P5 Cs4C 3.28(4) 4_457
P5 Cs4A 3.63(5) 4_457
P5 Cs4A 3.66(6) 8_756
P6 O16 1.38(3) 2_655
P6 O16 1.38(3) .
P6 O17 1.40(3) .
P6 O17 1.40(3) 2_655
P6 Cs3A 3.730(10) 2_655
P6 Cs2A 3.906(2) 2_655
P6 Cs2A 3.906(2) 2
P6 Cs2A 3.906(2) 1_655
O1 U3 2.343(9) 1_556
O1 Cs3A 3.346(8) 2_655
O2 Cs3A 3.226(8) 2_655
O3 P5 1.535(10) 8_755
O3 Cs4A 3.14(4) 8_756
O3 Cs4A 3.14(4) 1_556
O3 Cs4A 3.30(4) 5_757
O3 Cs4A 3.30(4) 4_457
O3 Cs4C 3.32(5) 5_757
O3 Cs4C 3.32(5) 4_457
O3 Cs4B 3.40(2) 1_556
O3 Cs4C 3.48(4) 8_756
O3 Cs4C 3.48(4) 1_556
O4 U1 2.286(10) 5_657
O4 Cs4A 3.22(4) 8_756
O4 Cs4A 3.22(4) 1_456
O4 Cs4A 3.34(4) 4_457
O4 Cs4A 3.34(4) 5_657
O4 Cs4B 3.35(2) 5_657
O4 Cs4C 3.45(5) 8_756
O4 Cs4C 3.45(5) 1_456
O4 Cs4C 3.47(4) 4_457
O4 Cs4C 3.47(4) 5_657
O6 Cs4A 3.51(5) 8_756
O6 Cs4C 3.57(4) 4_457
O6 Cs4A 3.67(4) 4_457
O6 Cs4B 3.750(17) 5_657
O7 P5 1.499(10) 8_755
O7 U3 2.294(10) 1_556
O7 Cs1 3.682(4) 1_655
O7 Cs2C 3.751(13) 1_656
O7 Cs2C 3.751(13) 1_556
O8 U1 2.291(7) 5_657
O8 Cs2B 2.77(2) 5_657
O8 Cs2A 3.374(8) 5_657
O8 Cs2C 3.50(3) 5_657
O8 Cs4C 3.64(4) 8_756
O8 Cs4B 3.81(2) 1_556
O9 U2 2.208(11) 5_657
O10 Cs4B 3.26(2) 1_556
O10 Cs4C 3.40(5) 1_556
O10 Cs4C 3.40(5) 8_756
O10 Cs2B 3.68(3) 5_657
O10 Cs4A 3.72(3) 1_556
O10 Cs4A 3.72(3) 8_756
O11 U3 2.239(12) 1_456
O11 Cs2A 3.457(12) 2_556
O11 Cs2A 3.457(12) 1_556
O11 Cs2C 3.50(3) 2_556
O11 Cs2C 3.50(3) 1_556
O11 Cs1 3.502(5) 2
O12 U4 2.235(14) 5_657
O12 Cs1 3.757(14) 5_657
O13 U4 2.44(3) 2
O13 Cs1 2.78(3) 2
O13 Cs3A 3.12(2) 1_455
O13 Cs3A 3.12(2) 2_655
O14 Cs2C 2.31(3) 1_556
O14 Cs2B 2.57(2) 1_556
O14 Cs4C 3.10(4) 4_457
O14 Cs2A 3.160(18) 1_556
O14 Cs4B 3.29(3) 5_657
O14 Cs4A 3.70(7) 4_457
O14 Cs4A 3.80(7) 8_756
O15 O15 1.66(3) 8_755
O15 P5 2.169(15) 8_755
O15 U1 2.263(14) 1_556
O15 Cs2B 2.645(15) 1_556
O15 Cs4C 2.83(5) 4_457
O15 Cs2C 2.91(2) 1_556
O15 Cs4A 3.22(5) 4_457
O15 Cs2A 3.290(15) 1_556
O15 Cs4A 3.38(6) 8_756
O15 Cs4B 3.46(2) 5_657
O16 U1 2.17(3) 2_655
O16 Cs3A 3.33(2) 2_655
O17 O17 1.27(6) 2_655
O17 Cs2A 3.30(2) 2_655
O17 Cs2A 3.30(2) 1_655
O17 Cs2C 3.75(3) 2_655
O17 Cs2C 3.75(3) 1_655
