#------------------------------------------------------------------------------
#$Date: 2016-03-23 21:54:53 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179459 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/56/4335659.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4335659
loop_
_publ_author_name
'Ting Hu'
'Thomas C. W. Mak'
_publ_section_title
;
 Silver(I) Multiple Salts Assembled with Phosphonate,
 Perfluorocarboxylate, and the Multinuclear Silver-Ethynediide
 Supramolecular Synthon
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9066
_journal_page_last               9076
_journal_paper_doi               10.1021/ic401259r
_journal_volume                  52
_journal_year                    2013
_chemical_formula_sum            'C35 H27 Ag12 F30 O24 P2'
_chemical_formula_weight         2757.95
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 104.5080(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   25.1317(18)
_cell_length_b                   18.1550(13)
_cell_length_c                   28.2564(18)
_cell_measurement_reflns_used    62139
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.833
_cell_measurement_theta_min      2.188
_cell_volume                     12481.3(15)
_computing_cell_refinement       SAINT(Bruker,2001)
_computing_data_collection       APEX2(Bruker,2003)
_computing_data_reduction        APEX2(Bruker,2003)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1220
_diffrn_reflns_av_sigmaI/netI    0.1298
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            56049
_diffrn_reflns_theta_full        27.99
_diffrn_reflns_theta_max         27.99
_diffrn_reflns_theta_min         1.88
_exptl_absorpt_coefficient_mu    3.890
_exptl_absorpt_correction_T_max  0.6525
_exptl_absorpt_correction_T_min  0.4816
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.935
_exptl_crystal_description       plate-like
_exptl_crystal_F_000             10344
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.12
_refine_diff_density_max         3.314
_refine_diff_density_min         -1.840
_refine_diff_density_rms         0.444
_refine_ls_extinction_coef       0.00016(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.006
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     949
_refine_ls_number_reflns         14952
_refine_ls_number_restraints     50
_refine_ls_restrained_S_all      1.010
_refine_ls_R_factor_all          0.1065
_refine_ls_R_factor_gt           0.0904
_refine_ls_shift/su_max          0.030
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1538P)²+71.9956P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2271
_refine_ls_wR_factor_ref         0.2427
_reflns_number_gt                11793
_reflns_number_total             14952
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic401259r_si_002_7.cif
_cod_data_source_block           7
_cod_database_code               4335659
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.31225(4) 0.49460(5) -0.07507(3) 0.0380(2) Uani 1 1 d .
Ag2 Ag 0.38761(3) 0.58098(4) -0.11659(3) 0.0258(2) Uani 1 1 d .
Ag3 Ag 0.41366(4) 0.70605(5) -0.05013(3) 0.0354(2) Uani 1 1 d .
Ag4 Ag 0.45699(3) 0.62561(5) 0.04237(3) 0.0293(2) Uani 1 1 d .
Ag5 Ag 0.37652(3) 0.51811(4) 0.05212(3) 0.0276(2) Uani 1 1 d .
Ag6 Ag 0.43261(3) 0.49483(4) -0.03481(3) 0.02341(19) Uani 1 1 d .
Ag7 Ag 0.36143(3) 0.72135(5) 0.03162(3) 0.0322(2) Uani 1 1 d .
Ag8 Ag 0.27909(4) 0.61479(5) 0.00526(8) 0.0284(5) Uani 0.905(8) 1 d P
Ag9 Ag 0.42264(9) 0.27794(12) 0.21155(8) 0.0333(4) Uani 0.50 1 d P
Ag10 Ag 0.52420(3) 0.30432(4) 0.16956(3) 0.0253(2) Uani 1 1 d .
Ag11 Ag 0.44607(3) 0.41900(4) 0.16351(2) 0.0273(2) Uani 1 1 d .
Ag12 Ag 0.57050(3) 0.44135(4) 0.24026(3) 0.0272(2) Uani 1 1 d .
Ag8' Ag 0.2737(5) 0.6189(7) -0.0259(11) 0.047(6) Uani 0.095(8) 1 d P
Ag9' Ag 0.44755(14) 0.25048(16) 0.22386(8) 0.0523(7) Uani 0.50 1 d P
C1 C 0.3712(4) 0.5811(6) -0.0418(4) 0.026(2) Uani 1 1 d .
C2 C 0.3647(5) 0.6200(6) -0.0078(4) 0.027(2) Uani 1 1 d .
C3 C 0.4924(4) 0.3626(5) 0.2274(3) 0.0227(19) Uani 1 1 d .
C4 C 0.4232(4) 0.3048(6) 0.0350(3) 0.0234(19) Uani 1 1 d .
H4A H 0.3908 0.3248 0.0124 0.028 Uiso 1 1 calc R
H4B H 0.4401 0.2699 0.0172 0.028 Uiso 1 1 calc R
C5 C 0.4065(4) 0.2659(5) 0.0753(3) 0.0218(19) Uani 1 1 d .
C6 C 0.3629(5) 0.2909(7) 0.0929(4) 0.035(2) Uani 1 1 d .
H6 H 0.3443 0.3333 0.0796 0.042 Uiso 1 1 calc R
C7 C 0.3466(5) 0.2538(7) 0.1300(4) 0.036(3) Uani 1 1 d .
H7 H 0.3167 0.2714 0.1405 0.043 Uiso 1 1 calc R
C8 C 0.3733(5) 0.1929(6) 0.1513(4) 0.035(3) Uani 1 1 d .
H8 H 0.3621 0.1688 0.1762 0.042 Uiso 1 1 calc R
C9 C 0.4179(5) 0.1671(7) 0.1352(4) 0.037(3) Uani 1 1 d .
H9 H 0.4370 0.1256 0.1497 0.045 Uiso 1 1 calc R
C10 C 0.4341(5) 0.2026(6) 0.0978(4) 0.031(2) Uani 1 1 d .
H10 H 0.4637 0.1844 0.0873 0.037 Uiso 1 1 calc R
C11 C 0.5914(5) 0.6313(6) 0.1740(4) 0.032(2) Uani 1 1 d .
H11A H 0.5747 0.6787 0.1637 0.039 Uiso 1 1 calc R
H11B H 0.5995 0.6289 0.2094 0.039 Uiso 1 1 calc R
C12 C 0.6432(5) 0.6239(6) 0.1579(4) 0.038(3) Uani 1 1 d .
C13 C 0.6476(6) 0.6568(7) 0.1142(5) 0.039(3) Uani 1 1 d .
H13 H 0.6189 0.6852 0.0960 0.046 Uiso 1 1 calc R
C14 C 0.6944(6) 0.6468(7) 0.0986(5) 0.044(3) Uani 1 1 d .
H14 H 0.6974 0.6705 0.0703 0.053 Uiso 1 1 calc R
C15 C 0.7378(5) 0.6024(8) 0.1235(4) 0.042(3) Uani 1 1 d .
H15 H 0.7692 0.5958 0.1121 0.050 Uiso 1 1 calc R
C16 C 0.7320(6) 0.5686(10) 0.1660(6) 0.058(4) Uani 1 1 d .
H16 H 0.7602 0.5388 0.1836 0.070 Uiso 1 1 calc R
C17 C 0.6854(5) 0.5782(9) 0.1827(5) 0.048(3) Uani 1 1 d .
H17 H 0.6822 0.5539 0.2108 0.058 Uiso 1 1 calc R
C18 C 0.3343(6) 0.6845(8) -0.2037(6) 0.049(3) Uani 1 1 d .
C19 C 0.2866(6) 0.7216(9) -0.2388(5) 0.047(3) Uani 1 1 d .
C20 C 0.2492(8) 0.6741(12) -0.2693(6) 0.069(5) Uani 1 1 d .
C21 C 0.3971(6) 0.7156(9) 0.1377(5) 0.054(4) Uani 1 1 d D
C22 C 0.4259(8) 0.7436(10) 0.1879(6) 0.086(6) Uani 1 1 d D
C23 C 0.3998(9) 0.8072(14) 0.2055(8) 0.118(10) Uani 1 1 d DU
C24 C 0.4747(5) 0.8034(7) 0.0484(5) 0.043(3) Uani 1 1 d D
C25 C 0.5191(6) 0.8579(9) 0.0778(7) 0.099(8) Uani 1 1 d DU
C26 C 0.5243(9) 0.9179(12) 0.0440(9) 0.117(8) Uani 1 1 d DU
C27 C 0.2545(5) 0.4487(6) 0.0127(4) 0.031(2) Uani 1 1 d .
C28 C 0.2125(6) 0.3844(7) 0.0023(4) 0.042(3) Uani 1 1 d .
C29 C 0.1913(5) 0.3606(7) 0.0440(4) 0.036(3) Uani 1 1 d .
C30 C 0.3501(5) 0.5215(6) 0.1708(4) 0.029(2) Uani 1 1 d .
C31 C 0.3041(5) 0.5806(8) 0.1556(4) 0.041(3) Uani 1 1 d .
C32 C 0.2466(6) 0.5541(10) 0.1602(5) 0.054(4) Uani 1 1 d .
C33 C 0.4331(5) 0.1462(7) 0.2993(5) 0.041(3) Uani 1 1 d .
C34 C 0.4218(10) 0.0666(10) 0.3116(8) 0.080(6) Uani 1 1 d .
C35 C 0.4003(11) 0.0140(9) 0.2723(9) 0.121(10) Uani 1 1 d DU
F1 F 0.3044(4) 0.7726(5) -0.2674(4) 0.068(3) Uani 1 1 d .
F2 F 0.2575(4) 0.7633(6) -0.2129(4) 0.071(3) Uani 1 1 d .
F3 F 0.2758(6) 0.6357(8) -0.2996(5) 0.108(5) Uani 1 1 d .
F4 F 0.2323(5) 0.6201(8) -0.2451(5) 0.105(4) Uani 1 1 d .
F5 F 0.2082(7) 0.7067(10) -0.3007(6) 0.142(7) Uani 1 1 d .
F6 F 0.4349(6) 0.6891(6) 0.2212(3) 0.086(4) Uani 1 1 d D
F7 F 0.4777(9) 0.7742(17) 0.1904(10) 0.221(13) Uani 1 1 d D
F8 F 0.3510(7) 0.7836(13) 0.2053(6) 0.154(8) Uani 1 1 d DU
F9 F 0.4292(11) 0.8211(11) 0.2514(6) 0.28(2) Uani 1 1 d D
F10 F 0.409(2) 0.8667(10) 0.1792(7) 0.40(4) Uani 1 1 d D
F11 F 0.5713(5) 0.8340(9) 0.0994(7) 0.136(6) Uani 1 1 d D
F12 F 0.5088(7) 0.8890(10) 0.1196(7) 0.157(9) Uani 1 1 d D
F13 F 0.5429(5) 0.8834(8) 0.0109(6) 0.117(6) Uani 1 1 d DU
F14 F 0.4778(4) 0.9457(8) 0.0308(7) 0.145(8) Uani 1 1 d D
F15 F 0.5618(6) 0.9683(9) 0.0651(6) 0.129(5) Uani 1 1 d DU
F16 F 0.1702(5) 0.4022(6) -0.0352(3) 0.081(4) Uani 1 1 d .
F17 F 0.2358(5) 0.3248(5) -0.0131(4) 0.076(3) Uani 1 1 d .
F18 F 0.2335(4) 0.3448(6) 0.0817(3) 0.069(3) Uani 1 1 d .
F19 F 0.1629(4) 0.4142(5) 0.0587(4) 0.063(2) Uani 1 1 d .
F20 F 0.1594(4) 0.3023(5) 0.0335(4) 0.059(2) Uani 1 1 d .
F21 F 0.3163(4) 0.6426(5) 0.1834(3) 0.062(3) Uani 1 1 d .
F22 F 0.2981(4) 0.6004(5) 0.1085(3) 0.052(2) Uani 1 1 d .
F23 F 0.2092(4) 0.6024(8) 0.1394(4) 0.097(4) Uani 1 1 d .
F24 F 0.2361(5) 0.4918(7) 0.1351(4) 0.085(3) Uani 1 1 d .
F25 F 0.2459(4) 0.5457(8) 0.2056(3) 0.082(3) Uani 1 1 d .
F26 F 0.4766(6) 0.0316(7) 0.3311(9) 0.174(10) Uani 1 1 d .
F27 F 0.3950(6) 0.0610(6) 0.3453(5) 0.089(4) Uani 1 1 d .
F28 F 0.4291(8) 0.0056(9) 0.2406(7) 0.159(9) Uani 1 1 d D
F29 F 0.3518(6) 0.0483(13) 0.2520(7) 0.188(10) Uani 1 1 d DU
F30 F 0.3892(7) -0.0495(7) 0.2898(7) 0.151(8) Uani 1 1 d D
O1 O 0.3288(5) 0.6699(6) -0.1631(4) 0.055(3) Uani 1 1 d .
O2 O 0.3749(4) 0.6736(6) -0.2208(4) 0.051(2) Uani 1 1 d .
O3 O 0.4222(5) 0.6615(8) 0.1260(4) 0.078(4) Uani 1 1 d .
O4 O 0.3587(4) 0.7524(6) 0.1107(3) 0.054(3) Uani 1 1 d .
O5 O 0.4946(5) 0.7455(6) 0.0401(6) 0.073(4) Uani 1 1 d .
O6 O 0.4251(4) 0.8183(5) 0.0487(4) 0.046(2) Uani 1 1 d .
O7 O 0.3014(3) 0.4372(5) 0.0101(3) 0.0377(19) Uani 1 1 d .
O8 O 0.2350(4) 0.5093(5) 0.0227(4) 0.048(2) Uani 1 1 d .
O9 O 0.3683(3) 0.4950(5) 0.1392(3) 0.0339(18) Uani 1 1 d .
O10 O 0.3630(4) 0.5132(5) 0.2158(3) 0.042(2) Uani 1 1 d .
O11 O 0.4413(6) 0.1594(8) 0.2591(4) 0.075(4) Uani 1 1 d .
O12 O 0.4392(4) 0.1892(5) 0.3355(3) 0.0381(19) Uani 1 1 d .
O13 O 0.4856(3) 0.4152(4) 0.0134(2) 0.0181(13) Uani 1 1 d .
O14 O 0.4417(3) 0.4313(4) 0.0843(2) 0.0195(13) Uani 1 1 d .
O15 O 0.5223(3) 0.3436(3) 0.0919(2) 0.0187(13) Uani 1 1 d .
O16 O 0.5282(3) 0.5687(4) 0.0935(2) 0.0269(15) Uani 1 1 d .
O17 O 0.4940(3) 0.5643(5) 0.1710(3) 0.0317(16) Uani 1 1 d .
H17A H 0.5005 0.5947 0.1932 0.047 Uiso 1 1 calc R
O18 O 0.5716(3) 0.4861(4) 0.1652(2) 0.0263(15) Uani 1 1 d .
O1W O 0.2296(4) 0.5762(6) -0.0812(4) 0.058(3) Uani 1 1 d .
O2W O 0.2108(3) 0.6936(4) 0.0208(3) 0.0310(16) Uani 1 1 d .
O3W O 0.4198(6) 0.8203(6) -0.0737(4) 0.065(3) Uani 1 1 d .
O4W O 0.3595(4) 0.9158(5) 0.9698(4) 0.046(2) Uani 1 1 d .
O5W O 0.1218(5) 0.5577(8) 0.9219(6) 0.085(4) Uani 1 1 d .
O6W O 0.2471(4) 0.7805(5) 0.1048(3) 0.048(2) Uani 1 1 d .
P1 P 0.47068(9) 0.37813(12) 0.05760(7) 0.0147(4) Uani 1 1 d .
P2 P 0.54475(11) 0.55886(14) 0.14787(8) 0.0217(5) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Ag1 C15 166.7(4) . 5_665
C1 Ag1 O1W 93.7(4) . .
C15 Ag1 O1W 95.0(4) 5_665 .
C1 Ag1 C14 142.4(4) . 5_665
C15 Ag1 C14 31.7(5) 5_665 5_665
O1W Ag1 C14 123.6(4) . 5_665
C1 Ag1 Ag2 49.8(3) . .
C15 Ag1 Ag2 117.9(3) 5_665 .
O1W Ag1 Ag2 105.2(3) . .
C14 Ag1 Ag2 115.2(3) 5_665 .
C1 Ag1 Ag8' 61.1(3) . .
C15 Ag1 Ag8' 130.4(4) 5_665 .
O1W Ag1 Ag8' 38.5(5) . .
C14 Ag1 Ag8' 148.9(4) 5_665 .
Ag2 Ag1 Ag8' 95.8(4) . .
C1 Ag1 Ag6 47.1(3) . .
C15 Ag1 Ag6 124.4(4) 5_665 .
O1W Ag1 Ag6 140.6(3) . .
C14 Ag1 Ag6 95.3(3) 5_665 .
Ag2 Ag1 Ag6 56.59(3) . .
Ag8' Ag1 Ag6 104.1(3) . .
C1 Ag2 O18 141.9(3) . 5_665
C1 Ag2 O1 106.6(4) . .
O18 Ag2 O1 110.3(3) 5_665 .
C1 Ag2 O15 95.7(3) . 5_665
O18 Ag2 O15 87.1(2) 5_665 5_665
O1 Ag2 O15 99.9(3) . 5_665
C1 Ag2 Ag6 49.7(3) . .
O18 Ag2 Ag6 92.88(17) 5_665 .
O1 Ag2 Ag6 156.3(3) . .
O15 Ag2 Ag6 85.83(13) 5_665 .
C1 Ag2 Ag3 57.2(3) . .
O18 Ag2 Ag3 138.36(19) 5_665 .
O1 Ag2 Ag3 80.4(3) . .
O15 Ag2 Ag3 51.22(14) 5_665 .
Ag6 Ag2 Ag3 85.64(3) . .
C1 Ag2 Ag1 48.3(3) . .
O18 Ag2 Ag1 113.11(19) 5_665 .
O1 Ag2 Ag1 102.3(3) . .
O15 Ag2 Ag1 141.91(14) 5_665 .
Ag6 Ag2 Ag1 62.27(3) . .
Ag3 Ag2 Ag1 102.88(3) . .
O3W Ag3 O15 95.6(3) . 5_665
O3W Ag3 C2 145.6(4) . .
O15 Ag3 C2 118.5(3) 5_665 .
O3W Ag3 C1 159.0(4) . .
O15 Ag3 C1 93.4(3) 5_665 .
C2 Ag3 C1 28.5(3) . .
O3W Ag3 Ag2 124.2(3) . .
O15 Ag3 Ag2 57.34(15) 5_665 .
C2 Ag3 Ag2 76.2(2) . .
C1 Ag3 Ag2 48.2(2) . .
O3W Ag3 Ag7 103.2(3) . .
O15 Ag3 Ag7 155.31(15) 5_665 .
C2 Ag3 Ag7 46.1(2) . .
C1 Ag3 Ag7 74.4(2) . .
Ag2 Ag3 Ag7 120.47(4) . .
O3W Ag3 Ag4 134.2(3) . .
O15 Ag3 Ag4 96.06(14) 5_665 .
C2 Ag3 Ag4 51.5(2) . .
C1 Ag3 Ag4 63.1(2) . .
Ag2 Ag3 Ag4 99.12(3) . .
Ag7 Ag3 Ag4 59.33(3) . .
O16 Ag4 O5 100.3(4) . .
O16 Ag4 C2 148.9(3) . .
O5 Ag4 C2 110.8(4) . .
O16 Ag4 O13 77.1(2) . 5_665
O5 Ag4 O13 87.6(3) . 5_665
C2 Ag4 O13 103.9(3) . 5_665
O16 Ag4 Ag5 95.3(2) . .
O5 Ag4 Ag5 156.6(3) . .
C2 Ag4 Ag5 55.1(3) . .
O13 Ag4 Ag5 112.97(15) 5_665 .
O16 Ag4 Ag7 147.36(18) . .
O5 Ag4 Ag7 77.0(3) . .
C2 Ag4 Ag7 46.8(2) . .
O13 Ag4 Ag7 134.47(14) 5_665 .
Ag5 Ag4 Ag7 80.44(3) . .
O16 Ag4 Ag3 148.49(19) . .
O5 Ag4 Ag3 65.5(4) . .
C2 Ag4 Ag3 53.9(3) . .
O13 Ag4 Ag3 74.44(14) 5_665 .
Ag5 Ag4 Ag3 107.97(3) . .
Ag7 Ag4 Ag3 60.14(3) . .
O16 Ag4 Ag6 94.76(19) . .
O5 Ag4 Ag6 132.4(3) . .
C2 Ag4 Ag6 64.6(2) . .
O13 Ag4 Ag6 52.31(15) 5_665 .
Ag5 Ag4 Ag6 62.54(3) . .
Ag7 Ag4 Ag6 111.19(3) . .
Ag3 Ag4 Ag6 78.30(3) . .
O14 Ag5 O7 99.7(3) . .
O14 Ag5 C2 137.5(3) . .
O7 Ag5 C2 99.8(3) . .
O14 Ag5 O9 74.2(2) . .
O7 Ag5 O9 97.5(3) . .
C2 Ag5 O9 139.2(3) . .
O14 Ag5 Ag4 93.13(18) . .
O7 Ag5 Ag4 146.7(2) . .
C2 Ag5 Ag4 52.6(3) . .
O9 Ag5 Ag4 115.6(2) . .
O14 Ag5 Ag8 171.88(18) . .
O7 Ag5 Ag8 72.3(2) . .
C2 Ag5 Ag8 47.4(3) . .
O9 Ag5 Ag8 105.32(16) . .
Ag4 Ag5 Ag8 94.34(3) . .
O14 Ag5 Ag6 78.58(16) . .
O7 Ag5 Ag6 89.0(2) . .
C2 Ag5 Ag6 64.4(2) . .
O9 Ag5 Ag6 152.66(16) . .
Ag4 Ag5 Ag6 63.47(3) . .
Ag8 Ag5 Ag6 101.95(4) . .
C1 Ag6 O13 146.9(3) . .
C1 Ag6 O16 133.1(3) . 5_665
O13 Ag6 O16 79.8(2) . 5_665
C1 Ag6 O13 94.1(3) . 5_665
O13 Ag6 O13 87.0(2) . 5_665
O16 Ag6 O13 91.4(2) 5_665 5_665
C1 Ag6 Ag2 52.3(3) . .
O13 Ag6 Ag2 160.55(17) . .
O16 Ag6 Ag2 81.37(16) 5_665 .
O13 Ag6 Ag2 88.45(13) 5_665 .
C1 Ag6 Ag1 48.0(3) . .
O13 Ag6 Ag1 129.96(18) . .
O16 Ag6 Ag1 106.77(17) 5_665 .
O13 Ag6 Ag1 140.49(14) 5_665 .
Ag2 Ag6 Ag1 61.14(3) . .
C1 Ag6 Ag5 61.8(3) . .
O13 Ag6 Ag5 85.66(17) . .
O16 Ag6 Ag5 159.24(18) 5_665 .
O13 Ag6 Ag5 102.64(14) 5_665 .
Ag2 Ag6 Ag5 113.79(3) . .
Ag1 Ag6 Ag5 71.66(3) . .
C1 Ag6 Ag4 62.2(3) . .
O13 Ag6 Ag4 94.77(17) . .
O16 Ag6 Ag4 141.64(19) 5_665 .
O13 Ag6 Ag4 50.22(14) 5_665 .
Ag2 Ag6 Ag4 96.79(3) . .
Ag1 Ag6 Ag4 105.55(3) . .
Ag5 Ag6 Ag4 53.98(3) . .
C2 Ag7 O4 135.7(4) . .
C2 Ag7 O6 129.2(4) . .
O4 Ag7 O6 78.6(4) . .
C2 Ag7 O2W 109.2(3) . 7_565
O4 Ag7 O2W 102.9(3) . 7_565
O6 Ag7 O2W 90.8(3) . 7_565
C2 Ag7 Ag8 52.8(3) . .
O4 Ag7 Ag8 103.1(3) . .
O6 Ag7 Ag8 174.7(3) . .
O2W Ag7 Ag8 83.87(18) 7_565 .
C2 Ag7 Ag4 53.9(3) . .
O4 Ag7 Ag4 105.4(3) . .
O6 Ag7 Ag4 85.6(2) . .
O2W Ag7 Ag4 150.10(19) 7_565 .
Ag8 Ag7 Ag4 98.66(4) . .
C2 Ag7 Ag3 55.5(3) . .
O4 Ag7 Ag3 154.8(3) . .
O6 Ag7 Ag3 79.4(3) . .
O2W Ag7 Ag3 89.62(19) 7_565 .
Ag8 Ag7 Ag3 99.88(5) . .
Ag4 Ag7 Ag3 60.53(3) . .
C2 Ag7 Ag8' 47.0(4) . .
O4 Ag7 Ag8' 118.2(6) . .
O6 Ag7 Ag8' 159.8(6) . .
O2W Ag7 Ag8' 75.2(4) 7_565 .
Ag8 Ag7 Ag8' 16.4(5) . .
Ag4 Ag7 Ag8' 99.2(2) . .
Ag3 Ag7 Ag8' 85.9(4) . .
Ag8' Ag8 C2 75.2(8) . .
Ag8' Ag8 O8 109.1(8) . .
C2 Ag8 O8 126.1(3) . .
Ag8' Ag8 O2W 101.6(8) . .
C2 Ag8 O2W 140.1(3) . .
O8 Ag8 O2W 93.0(3) . .
Ag8' Ag8 O1W 29.3(8) . .
C2 Ag8 O1W 96.4(4) . .
O8 Ag8 O1W 80.4(4) . .
O2W Ag8 O1W 98.2(3) . .
Ag8' Ag8 Ag7 97.4(7) . .
C2 Ag8 Ag7 49.2(3) . .
O8 Ag8 Ag7 150.9(3) . .
O2W Ag8 Ag7 93.19(19) . .
O1W Ag8 Ag7 126.7(3) . .
Ag8' Ag8 Ag5 113.7(8) . .
C2 Ag8 Ag5 53.3(3) . .
O8 Ag8 Ag5 78.8(3) . .
O2W Ag8 Ag5 144.6(2) . .
O1W Ag8 Ag5 114.0(3) . .
Ag7 Ag8 Ag5 79.72(4) . .
Ag9' Ag9 C3 81.8(3) . .
Ag9' Ag9 O11 38.9(4) . .
C3 Ag9 O11 116.0(4) . .
Ag9' Ag9 Ag11 119.9(3) . .
C3 Ag9 Ag11 45.1(2) . .
O11 Ag9 Ag11 158.8(3) . .
Ag9' Ag9 Ag10 68.8(2) . .
C3 Ag9 Ag10 46.3(3) . .
O11 Ag9 Ag10 105.9(3) . .
Ag11 Ag9 Ag10 55.09(4) . .
Ag9' Ag9 Ag12 115.4(3) . 2_655
C3 Ag9 Ag12 49.3(3) . 2_655
O11 Ag9 Ag12 125.0(2) . 2_655
Ag11 Ag9 Ag12 54.51(4) . 2_655
Ag10 Ag9 Ag12 93.26(6) . 2_655
Ag9' Ag9 Ag10 65.3(2) . 2_655
C3 Ag9 Ag10 67.1(2) . 2_655
O11 Ag9 Ag10 67.1(2) . 2_655
Ag11 Ag9 Ag10 104.91(6) . 2_655
Ag10 Ag9 Ag10 101.70(6) . 2_655
Ag12 Ag9 Ag10 58.63(4) 2_655 2_655
Ag9' Ag9 Ag9' 29.6(2) . 2_655
C3 Ag9 Ag9' 53.2(3) . 2_655
O11 Ag9 Ag9' 63.7(3) . 2_655
Ag11 Ag9 Ag9' 95.62(8) . 2_655
Ag10 Ag9 Ag9' 56.69(6) . 2_655
Ag12 Ag9 Ag9' 88.01(8) 2_655 2_655
Ag10 Ag9 Ag9' 51.78(5) 2_655 2_655
C3 Ag10 O12 133.7(3) . 2_655
C3 Ag10 O15 128.4(3) . .
O12 Ag10 O15 97.8(2) 2_655 .
C3 Ag10 Ag11 48.2(2) . .
O12 Ag10 Ag11 160.7(2) 2_655 .
O15 Ag10 Ag11 82.32(15) . .
C3 Ag10 Ag9' 51.3(3) . .
O12 Ag10 Ag9' 93.2(2) 2_655 .
O15 Ag10 Ag9' 138.46(17) . .
Ag11 Ag10 Ag9' 74.88(8) . .
C3 Ag10 Ag9' 58.4(2) . 2_655
O12 Ag10 Ag9' 76.96(19) 2_655 2_655
O15 Ag10 Ag9' 168.21(17) . 2_655
Ag11 Ag10 Ag9' 106.19(5) . 2_655
Ag9' Ag10 Ag9' 53.06(12) . 2_655
C3 Ag10 Ag9 47.3(3) . .
O12 Ag10 Ag9 105.3(2) 2_655 .
O15 Ag10 Ag9 126.14(16) . .
Ag11 Ag10 Ag9 60.94(5) . .
Ag9' Ag10 Ag9 14.96(6) . .
Ag9' Ag10 Ag9 65.65(10) 2_655 .
C3 Ag10 Ag12 47.7(3) . .
O12 Ag10 Ag12 130.7(2) 2_655 .
O15 Ag10 Ag12 105.72(16) . .
Ag11 Ag10 Ag12 66.89(3) . .
Ag9' Ag10 Ag12 96.68(5) . .
Ag9' Ag10 Ag12 71.28(7) 2_655 .
Ag9 Ag10 Ag12 94.93(4) . .
C3 Ag10 Ag9 57.4(2) . 2_655
O12 Ag10 Ag9 82.30(19) 2_655 2_655
O15 Ag10 Ag9 156.54(17) . 2_655
Ag11 Ag10 Ag9 105.28(4) . 2_655
Ag9' Ag10 Ag9 64.61(8) . 2_655
Ag9' Ag10 Ag9 13.80(6) 2_655 2_655
Ag9 Ag10 Ag9 75.68(7) . 2_655
Ag12 Ag10 Ag9 59.54(4) . 2_655
C3 Ag11 O14 140.6(3) . .
C3 Ag11 O9 139.6(3) . .
O14 Ag11 O9 79.6(2) . .
C3 Ag11 Ag10 51.5(3) . .
O14 Ag11 Ag10 89.60(16) . .
O9 Ag11 Ag10 163.87(19) . .
C3 Ag11 Ag12 56.6(3) . 2_655
O14 Ag11 Ag12 162.41(16) . 2_655
O9 Ag11 Ag12 83.50(18) . 2_655
Ag10 Ag11 Ag12 107.93(3) . 2_655
C3 Ag11 Ag9 49.0(3) . .
O14 Ag11 Ag9 124.80(18) . .
O9 Ag11 Ag9 112.8(2) . .
Ag10 Ag11 Ag9 63.98(5) . .
Ag12 Ag11 Ag9 66.75(5) 2_655 .
C3 Ag11 Ag12 45.0(3) . .
O14 Ag11 Ag12 116.17(18) . .
O9 Ag11 Ag12 133.7(2) . .
Ag10 Ag11 Ag12 62.01(3) . .
Ag12 Ag11 Ag12 72.81(3) 2_655 .
Ag9 Ag11 Ag12 93.84(5) . .
O10 Ag12 O18 97.3(3) 2_655 .
O10 Ag12 C3 155.2(3) 2_655 .
O18 Ag12 C3 105.9(3) . .
O10 Ag12 C3 126.2(3) 2_655 2_655
O18 Ag12 C3 135.2(3) . 2_655
C3 Ag12 C3 29.5(4) . 2_655
O10 Ag12 Ag11 79.8(2) 2_655 2_655
O18 Ag12 Ag11 165.35(19) . 2_655
C3 Ag12 Ag11 75.6(2) . 2_655
C3 Ag12 Ag11 46.5(2) 2_655 2_655
O10 Ag12 Ag10 154.0(3) 2_655 .
O18 Ag12 Ag10 77.57(18) . .
C3 Ag12 Ag10 44.4(2) . .
C3 Ag12 Ag10 67.5(2) 2_655 .
Ag11 Ag12 Ag10 111.20(3) 2_655 .
O10 Ag12 Ag9 110.2(2) 2_655 2_655
O18 Ag12 Ag9 134.73(19) . 2_655
C3 Ag12 Ag9 58.1(2) . 2_655
C3 Ag12 Ag9 44.6(2) 2_655 2_655
Ag11 Ag12 Ag9 58.74(4) 2_655 2_655
Ag10 Ag12 Ag9 61.83(5) . 2_655
O10 Ag12 Ag11 151.2(3) 2_655 .
O18 Ag12 Ag11 70.62(19) . .
C3 Ag12 Ag11 39.6(2) . .
C3 Ag12 Ag11 65.8(2) 2_655 .
Ag11 Ag12 Ag11 105.16(3) 2_655 .
Ag10 Ag12 Ag11 51.09(2) . .
Ag9 Ag12 Ag11 95.94(5) 2_655 .
Ag8 Ag8' O1W 137.6(14) . .
Ag8 Ag8' C2 82.8(11) . .
O1W Ag8' C2 124.4(10) . .
Ag8 Ag8' C1 103.3(11) . .
O1W Ag8' C1 97.5(8) . .
C2 Ag8' C1 27.0(4) . .
Ag8 Ag8' Ag1 115.5(12) . .
O1W Ag8' Ag1 58.4(5) . .
C2 Ag8' Ag1 70.8(4) . .
C1 Ag8' Ag1 45.8(3) . .
Ag8 Ag8' Ag7 66.2(7) . .
O1W Ag8' Ag7 156.2(13) . .
C2 Ag8' Ag7 45.5(4) . .
C1 Ag8' Ag7 71.0(3) . .
Ag1 Ag8' Ag7 116.3(4) . .
Ag9 Ag9' O11 126.0(5) . .
Ag9 Ag9' C3 78.0(3) . .
O11 Ag9' C3 145.2(4) . .
Ag9 Ag9' Ag9' 141.9(2) . 2_655
O11 Ag9' Ag9' 85.0(4) . 2_655
C3 Ag9' Ag9' 64.9(3) . 2_655
Ag9 Ag9' C3 91.6(3) . 2_655
O11 Ag9' C3 119.0(4) . 2_655
C3 Ag9' C3 27.3(4) . 2_655
Ag9' Ag9' C3 51.0(2) 2_655 2_655
Ag9 Ag9' Ag10 96.3(3) . .
O11 Ag9' Ag10 134.3(4) . .
C3 Ag9' Ag10 49.4(3) . .
Ag9' Ag9' Ag10 66.52(11) 2_655 .
C3 Ag9' Ag10 69.9(2) 2_655 .
Ag9 Ag9' Ag10 100.9(3) . 2_655
O11 Ag9' Ag10 78.4(3) . 2_655
C3 Ag9' Ag10 71.8(2) . 2_655
Ag9' Ag9' Ag10 60.41(8) 2_655 2_655
C3 Ag9' Ag10 45.4(2) 2_655 2_655
Ag10 Ag9' Ag10 112.82(8) . 2_655
Ag9 Ag9' Ag9 133.3(3) . 2_655
O11 Ag9' Ag9 92.3(4) . 2_655
C3 Ag9' Ag9 56.6(2) . 2_655
Ag9' Ag9' Ag9 8.55(6) 2_655 2_655
C3 Ag9' Ag9 42.8(2) 2_655 2_655
Ag10 Ag9' Ag9 63.61(7) . 2_655
Ag10 Ag9' Ag9 57.67(6) 2_655 2_655
C2 C1 Ag6 124.8(8) . .
C2 C1 Ag1 122.3(9) . .
Ag6 C1 Ag1 84.9(4) . .
C2 C1 Ag2 145.2(9) . .
Ag6 C1 Ag2 78.0(3) . .
Ag1 C1 Ag2 82.0(3) . .
C2 C1 Ag3 72.7(7) . .
Ag6 C1 Ag3 110.3(4) . .
Ag1 C1 Ag3 148.2(5) . .
Ag2 C1 Ag3 74.6(3) . .
C2 C1 Ag8' 54.6(8) . .
Ag6 C1 Ag8' 145.6(7) . .
Ag1 C1 Ag8' 73.1(4) . .
Ag2 C1 Ag8' 123.1(7) . .
Ag3 C1 Ag8' 102.1(5) . .
C1 C2 Ag7 156.3(9) . .
C1 C2 Ag8' 98.4(9) . .
Ag7 C2 Ag8' 87.5(5) . .
C1 C2 Ag8 114.6(8) . .
Ag7 C2 Ag8 78.0(3) . .
Ag8' C2 Ag8 22.0(7) . .
C1 C2 Ag4 100.8(8) . .
Ag7 C2 Ag4 79.4(3) . .
Ag8' C2 Ag4 157.9(9) . .
Ag8 C2 Ag4 136.1(5) . .
C1 C2 Ag3 78.8(7) . .
Ag7 C2 Ag3 78.4(3) . .
Ag8' C2 Ag3 120.2(8) . .
Ag8 C2 Ag3 135.2(5) . .
Ag4 C2 Ag3 74.6(3) . .
C1 C2 Ag5 95.1(7) . .
Ag7 C2 Ag5 107.3(4) . .
Ag8' C2 Ag5 95.3(8) . .
Ag8 C2 Ag5 79.3(3) . .
Ag4 C2 Ag5 72.3(3) . .
Ag3 C2 Ag5 144.5(5) . .
C3 C3 Ag11 146.0(7) 2_655 .
C3 C3 Ag10 132.4(9) 2_655 .
Ag11 C3 Ag10 80.2(3) . .
C3 C3 Ag9 103.0(8) 2_655 .
Ag11 C3 Ag9 85.9(3) . .
Ag10 C3 Ag9 86.4(3) . .
C3 C3 Ag9' 93.7(5) 2_655 .
Ag11 C3 Ag9' 103.1(4) . .
Ag10 C3 Ag9' 79.3(3) . .
Ag9 C3 Ag9' 20.19(12) . .
C3 C3 Ag12 79.2(7) 2_655 .
Ag11 C3 Ag12 95.4(4) . .
Ag10 C3 Ag12 87.9(4) . .
Ag9 C3 Ag12 173.9(5) . .
Ag9' C3 Ag12 155.2(5) . .
C3 C3 Ag12 71.3(7) 2_655 2_655
Ag11 C3 Ag12 76.8(3) . 2_655
Ag10 C3 Ag12 156.3(4) . 2_655
Ag9 C3 Ag12 86.1(3) . 2_655
Ag9' C3 Ag12 100.1(4) . 2_655
Ag12 C3 Ag12 100.1(4) . 2_655
C3 C3 Ag9' 59.0(4) 2_655 2_655
Ag11 C3 Ag9' 154.9(5) . 2_655
Ag10 C3 Ag9' 76.2(3) . 2_655
Ag9 C3 Ag9' 84.1(3) . 2_655
Ag9' C3 Ag9' 64.1(3) . 2_655
Ag12 C3 Ag9' 92.3(3) . 2_655
Ag12 C3 Ag9' 125.2(4) 2_655 2_655
C5 C4 P1 111.7(6) . .
C10 C5 C6 116.7(9) . .
C10 C5 C4 122.1(9) . .
C6 C5 C4 121.2(10) . .
C7 C6 C5 121.3(11) . .
C8 C7 C6 121.6(12) . .
C7 C8 C9 118.6(11) . .
C10 C9 C8 120.5(11) . .
C9 C10 C5 121.3(11) . .
C12 C11 P2 109.9(7) . .
C17 C12 C13 118.8(13) . .
C17 C12 C11 121.0(11) . .
C13 C12 C11 119.9(12) . .
C14 C13 C12 119.4(13) . .
C13 C14 C15 122.8(12) . .
C13 C14 Ag1 101.8(8) . 5_665
C15 C14 Ag1 63.8(7) . 5_665
C16 C15 C14 116.8(13) . .
C16 C15 Ag1 90.8(9) . 5_665
C14 C15 Ag1 84.5(7) . 5_665
C15 C16 C17 121.5(15) . .
C12 C17 C16 120.6(13) . .
O1 C18 O2 128.8(12) . .
O1 C18 C19 117.1(13) . .
O2 C18 C19 114.0(13) . .
F1 C19 F2 103.6(12) . .
F1 C19 C20 108.7(13) . .
F2 C19 C20 107.5(14) . .
F1 C19 C18 111.3(12) . .
F2 C19 C18 109.6(12) . .
C20 C19 C18 115.5(14) . .
F5 C20 F4 112.5(19) . .
F5 C20 C19 115.3(18) . .
F4 C20 C19 112.9(15) . .
F5 C20 F3 103.0(16) . .
F4 C20 F3 102.3(18) . .
C19 C20 F3 109.5(16) . .
O4 C21 O3 127.7(14) . .
O4 C21 C22 120.3(15) . .
O3 C21 C22 111.0(13) . .
F6 C22 F7 105.5(17) . .
F6 C22 C23 110.5(17) . .
F7 C22 C23 99(2) . .
F6 C22 C21 111.5(14) . .
F7 C22 C21 113.7(19) . .
C23 C22 C21 115.6(15) . .
F8 C23 F9 111(2) . .
F8 C23 F10 124(3) . .
F9 C23 F10 104.3(19) . .
F8 C23 C22 103.9(18) . .
F9 C23 C22 106.8(19) . .
F10 C23 C22 106(2) . .
O5 C24 O6 129.5(12) . .
O5 C24 C25 112.2(12) . .
O6 C24 C25 115.4(11) . .
F11 C25 F12 96.4(16) . .
F11 C25 C26 106.9(16) . .
F12 C25 C26 108.4(16) . .
F11 C25 C24 120.7(13) . .
F12 C25 C24 116.7(13) . .
C26 C25 C24 106.8(14) . .
F14 C26 F13 117(2) . .
F14 C26 F15 111.1(18) . .
F13 C26 F15 107.9(17) . .
F14 C26 C25 105.3(17) . .
F13 C26 C25 102.5(18) . .
F15 C26 C25 112(2) . .
O7 C27 O8 126.8(11) . .
O7 C27 C28 118.8(10) . .
O8 C27 C28 114.4(11) . .
F16 C28 F17 105.1(11) . .
F16 C28 C29 109.2(12) . .
F17 C28 C29 107.1(11) . .
F16 C28 C27 109.6(10) . .
F17 C28 C27 109.5(12) . .
C29 C28 C27 115.7(10) . .
F20 C29 F19 108.2(10) . .
F20 C29 F18 109.0(10) . .
F19 C29 F18 106.9(11) . .
F20 C29 C28 112.2(10) . .
F19 C29 C28 111.3(11) . .
F18 C29 C28 109.1(10) . .
O9 C30 O10 131.5(10) . .
O9 C30 C31 117.7(9) . .
O10 C30 C31 110.7(9) . .
F21 C31 F22 107.5(12) . .
F21 C31 C30 111.5(10) . .
F22 C31 C30 110.4(9) . .
F21 C31 C32 106.6(11) . .
F22 C31 C32 106.7(10) . .
C30 C31 C32 113.7(12) . .
F25 C32 F24 112.4(15) . .
F25 C32 F23 109.6(13) . .
F24 C32 F23 107.8(13) . .
F25 C32 C31 111.2(12) . .
F24 C32 C31 106.4(12) . .
F23 C32 C31 109.3(14) . .
O11 C33 O12 127.8(13) . .
O11 C33 C34 118.6(13) . .
O12 C33 C34 113.0(13) . .
F27 C34 C35 110.1(16) . .
F27 C34 F26 107(2) . .
C35 C34 F26 97.7(17) . .
F27 C34 C33 113.6(14) . .
C35 C34 C33 119.9(19) . .
F26 C34 C33 106.2(14) . .
F28 C35 F30 111.4(16) . .
F28 C35 F29 111(2) . .
F30 C35 F29 108(2) . .
F28 C35 C34 116(2) . .
F30 C35 C34 111(2) . .
F29 C35 C34 98.3(17) . .
C18 O1 Ag2 118.1(9) . .
C21 O4 Ag7 104.6(9) . .
C24 O5 Ag4 127.0(9) . .
C24 O6 Ag7 117.1(8) . .
C27 O7 Ag5 120.5(7) . .
C27 O8 Ag8 115.8(8) . .
C30 O9 Ag11 117.5(6) . .
C30 O9 Ag5 142.0(7) . .
Ag11 O9 Ag5 96.7(3) . .
C30 O10 Ag12 127.5(7) . 2_655
C33 O11 Ag9' 133.5(10) . .
C33 O11 Ag9 127.5(10) . .
Ag9' O11 Ag9 15.04(15) . .
C33 O12 Ag10 118.6(8) . 2_655
P1 O13 Ag6 123.9(4) . .
P1 O13 Ag4 132.5(4) . 5_665
Ag6 O13 Ag4 99.2(2) . 5_665
P1 O13 Ag6 115.3(3) . 5_665
Ag6 O13 Ag6 93.0(2) . 5_665
Ag4 O13 Ag6 77.47(19) 5_665 5_665
P1 O14 Ag11 121.8(3) . .
P1 O14 Ag5 128.6(3) . .
Ag11 O14 Ag5 108.6(3) . .
P1 O15 Ag10 122.6(4) . .
P1 O15 Ag3 114.0(3) . 5_665
Ag10 O15 Ag3 119.9(2) . 5_665
P1 O15 Ag2 119.7(3) . 5_665
Ag10 O15 Ag2 95.7(2) . 5_665
Ag3 O15 Ag2 71.44(18) 5_665 5_665
P2 O16 Ag4 133.2(4) . .
P2 O16 Ag6 126.1(4) . 5_665
Ag4 O16 Ag6 100.0(2) . 5_665
P2 O18 Ag2 120.5(4) . 5_665
P2 O18 Ag12 120.4(4) . .
Ag2 O18 Ag12 119.1(3) 5_665 .
Ag8' O1W Ag1 83.1(5) . .
Ag8' O1W Ag8 13.2(7) . .
Ag1 O1W Ag8 84.2(3) . .
Ag8 O2W Ag7 134.6(4) . 7_565
O14 P1 O15 112.2(3) . .
O14 P1 O13 111.6(4) . .
O15 P1 O13 110.4(4) . .
O14 P1 C4 106.8(5) . .
O15 P1 C4 107.5(4) . .
O13 P1 C4 108.1(4) . .
O16 P2 O18 115.1(4) . .
O16 P2 O17 111.9(4) . .
O18 P2 O17 105.2(4) . .
O16 P2 C11 108.6(5) . .
O18 P2 C11 108.4(5) . .
O17 P2 C11 107.3(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C1 2.202(10) .
Ag1 C15 2.386(11) 5_665
Ag1 O1W 2.522(11) .
Ag1 C14 2.646(12) 5_665
Ag1 Ag2 2.9217(12) .
Ag1 Ag8' 2.940(12) .
Ag1 Ag6 2.9530(12) .
Ag2 C1 2.253(11) .
Ag2 O18 2.264(8) 5_665
Ag2 O1 2.354(9) .
Ag2 O15 2.588(6) 5_665
Ag2 Ag6 2.7850(10) .
Ag2 Ag3 2.9147(12) .
Ag3 O3W 2.195(10) .
Ag3 O15 2.397(6) 5_665
Ag3 C2 2.475(11) .
Ag3 C1 2.543(11) .
Ag3 Ag7 2.9421(12) .
Ag3 Ag4 2.9536(12) .
Ag4 O16 2.249(7) .
Ag4 O5 2.381(10) .
Ag4 C2 2.398(11) .
Ag4 O13 2.502(6) 5_665
Ag4 Ag5 2.8730(12) .
Ag4 Ag7 2.9181(11) .
Ag4 Ag6 3.1780(11) .
Ag5 O14 2.291(6) .
Ag5 O7 2.451(8) .
Ag5 C2 2.474(10) .
Ag5 O9 2.555(8) .
Ag5 Ag8 3.0338(12) .
Ag5 Ag6 3.1519(11) .
Ag6 C1 2.173(10) .
Ag6 O13 2.193(6) .
Ag6 O16 2.422(7) 5_665
Ag6 O13 2.576(7) 5_665
Ag7 C2 2.163(10) .
Ag7 O4 2.322(9) .
Ag7 O6 2.346(9) .
Ag7 O2W 2.555(7) 7_565
Ag7 Ag8 2.7941(13) .
Ag7 Ag8' 3.028(13) .
Ag8 Ag8' 0.86(3) .
Ag8 C2 2.274(11) .
Ag8 O8 2.327(9) .
Ag8 O2W 2.359(8) .
Ag8 O1W 2.547(12) .
Ag9 Ag9' 0.808(3) .
Ag9 C3 2.290(10) .
Ag9 O11 2.518(14) .
Ag9 Ag11 3.025(2) .
Ag9 Ag10 3.109(2) .
Ag9 Ag12 3.251(2) 2_655
Ag9 Ag10 3.324(2) 2_655
Ag9 Ag9' 3.353(5) 2_655
Ag10 C3 2.254(10) .
Ag10 O12 2.302(8) 2_655
Ag10 O15 2.297(6) .
Ag10 Ag11 2.8375(11) .
Ag10 Ag9' 2.916(3) .
Ag10 Ag9' 3.075(2) 2_655
Ag10 Ag12 3.2201(11) .
Ag10 Ag9 3.324(2) 2_655
Ag11 C3 2.147(9) .
Ag11 O14 2.224(6) .
Ag11 O9 2.350(7) .
Ag11 Ag12 2.8809(10) 2_655
Ag11 Ag12 3.3540(11) .
Ag12 O10 2.236(8) 2_655
Ag12 O18 2.277(7) .
Ag12 C3 2.382(10) .
Ag12 C3 2.471(10) 2_655
Ag12 Ag11 2.8809(10) 2_655
Ag12 Ag9 3.251(2) 2_655
Ag8' O1W 1.85(2) .
Ag8' C2 2.216(16) .
Ag8' C1 2.690(16) .
Ag9' O11 1.957(15) .
Ag9' C3 2.316(10) .
Ag9' Ag9' 2.680(7) 2_655
Ag9' C3 2.697(10) 2_655
Ag9' Ag10 3.075(2) 2_655
Ag9' Ag9 3.353(5) 2_655
C1 C2 1.235(14) .
C3 C3 1.239(19) 2_655
C3 Ag12 2.471(10) 2_655
C3 Ag9' 2.697(10) 2_655
C4 C5 1.488(13) .
C4 P1 1.795(9) .
C5 C10 1.408(15) .
C5 C6 1.387(16) .
C6 C7 1.393(16) .
C7 C8 1.354(18) .
C8 C9 1.394(19) .
C9 C10 1.383(16) .
C11 C12 1.489(18) .
C11 P2 1.794(11) .
C12 C17 1.39(2) .
C12 C13 1.399(16) .
C13 C14 1.368(19) .
C14 C15 1.40(2) .
C14 Ag1 2.646(12) 5_665
C15 C16 1.39(2) .
C15 Ag1 2.386(11) 5_665
C16 C17 1.38(2) .
C18 O1 1.219(18) .
C18 O2 1.249(18) .
C18 C19 1.511(16) .
C19 F1 1.375(17) .
C19 F2 1.382(16) .
C19 C20 1.40(2) .
C20 F5 1.32(2) .
C20 F4 1.33(2) .
C20 F3 1.40(2) .
C21 O4 1.262(17) .
C21 O3 1.26(2) .
C21 C22 1.508(19) .
C22 F6 1.345(18) .
C22 F7 1.40(2) .
C22 C23 1.48(2) .
C23 F8 1.30(2) .
C23 F9 1.35(2) .
C23 F10 1.37(2) .
C24 O5 1.211(17) .
C24 O6 1.278(16) .
C24 C25 1.564(17) .
C25 F11 1.371(16) .
C25 F12 1.390(17) .
C25 C26 1.48(2) .
C26 F14 1.24(2) .
C26 F13 1.31(2) .
C26 F15 1.34(2) .
C27 O7 1.218(14) .
C27 O8 1.265(14) .
C27 C28 1.552(16) .
C28 F16 1.339(15) .
C28 F17 1.353(17) .
C28 C29 1.475(18) .
C29 F20 1.316(14) .
C29 F19 1.335(15) .
C29 F18 1.332(14) .
C30 O9 1.203(13) .
C30 O10 1.238(13) .
C30 C31 1.556(15) .
C31 F21 1.362(16) .
C31 F22 1.351(15) .
C31 C32 1.56(2) .
C32 F25 1.294(17) .
C32 F24 1.33(2) .
C32 F23 1.313(17) .
C33 O11 1.229(18) .
C33 O12 1.265(15) .
C33 C34 1.53(2) .
C34 F27 1.30(2) .
C34 C35 1.46(3) .
C34 F26 1.49(3) .
C35 F28 1.29(2) .
C35 F30 1.31(2) .
C35 F29 1.36(2) .
O10 Ag12 2.236(7) 2_655
O12 Ag10 2.302(8) 2_655
O13 P1 1.544(6) .
O13 Ag4 2.502(6) 5_665
O13 Ag6 2.576(7) 5_665
O14 P1 1.519(7) .
O15 P1 1.544(6) .
O15 Ag3 2.397(6) 5_665
O15 Ag2 2.588(6) 5_665
O16 P2 1.500(7) .
O16 Ag6 2.422(7) 5_665
O17 P2 1.575(8) .
O18 P2 1.509(8) .
O18 Ag2 2.264(8) 5_665
O2W Ag7 2.555(7) 7_565
