#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/67/4336796.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4336796
loop_
_publ_author_name
'Bin Zhang'
'Ting Xiao'
'Chunmei Liu'
'Qian Li'
'Yanyan Zhu'
'Mingsheng Tang'
'Chenxia Du'
'Maoping Song'
_publ_section_title
;
 Systematic Study of the Luminescent Europium-Based Nonanuclear Clusters
 with Modified 2-Hydroxybenzophenone Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              13332
_journal_page_last               13340
_journal_paper_doi               10.1021/ic401191e
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         'C112 H88 Eu4.5 O29'
_chemical_formula_sum            'C112 H88 Eu4.5 O29'
_chemical_formula_weight         2581.64
_chemical_name_systematic
;
 ? 
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2012-11-28
_audit_creation_method
;
  Olex2 1.1
  (compiled 2011.11.01 svn.r2039, GUI svn.r3906)
;
_cell_angle_alpha                90.00
_cell_angle_beta                 107.0859(18)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   27.2191(5)
_cell_length_b                   28.5350(4)
_cell_length_c                   36.3189(6)
_cell_measurement_reflns_used    29652
_cell_measurement_temperature    291(2)
_cell_measurement_theta_max      26.3152
_cell_measurement_theta_min      2.8743
_cell_volume                     26963.8(8)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.39 (release 18-08-2010 CrysAlis171 .NET)
(compiled Aug 18 2010,17:42:00)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.39 (release 18-08-2010 CrysAlis171 .NET)
(compiled Aug 18 2010,17:42:00)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.39 (release 18-08-2010 CrysAlis171 .NET)
(compiled Aug 18 2010,17:42:00)
;
_computing_molecular_graphics
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_publication_material
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_structure_refinement
;
SHELXL, G.M. Sheldrick, Acta Cryst.
2008). A64, 112-122
;
_computing_structure_solution
;
SHELXS, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_diffrn_ambient_temperature      291.15
_diffrn_detector_area_resol_mean 16.2312
_diffrn_measured_fraction_theta_full 0.969
_diffrn_measured_fraction_theta_max 0.969
_diffrn_measurement_details
;
  1 omega  -32.00    7.00   0.5000   30.0000
omega____ theta____ kappa____ phi______ frames
    -      -17.1323   39.0000   37.0000 78

  2 omega  -28.00   -3.00   0.5000   30.0000
omega____ theta____ kappa____ phi______ frames
    -       19.9448  -39.0000  142.0000 50

  3 omega   36.00   63.00   0.5000   30.0000
omega____ theta____ kappa____ phi______ frames
    -       19.9448   77.0000 -150.0000 54

  4 omega   -7.00   89.00   0.5000   30.0000
omega____ theta____ kappa____ phi______ frames
    -       19.9448   77.0000 -180.0000 192

  5 omega  -49.00   47.00   0.5000   30.0000
omega____ theta____ kappa____ phi______ frames
    -       19.9448  -77.0000   60.0000 192
;
_diffrn_measurement_device_type  'Xcalibur, Eos, Gemini'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_UB_11      0.0029498000
_diffrn_orient_matrix_UB_12      -0.0223023000
_diffrn_orient_matrix_UB_13      -0.0077180000
_diffrn_orient_matrix_UB_21      0.0203946000
_diffrn_orient_matrix_UB_22      0.0088867000
_diffrn_orient_matrix_UB_23      -0.0064165000
_diffrn_orient_matrix_UB_31      0.0178383000
_diffrn_orient_matrix_UB_32      -0.0064664000
_diffrn_orient_matrix_UB_33      0.0177982000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.0387
_diffrn_reflns_av_unetI/netI     0.0556
_diffrn_reflns_limit_h_max       34
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -45
_diffrn_reflns_number            68745
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         2.89
_diffrn_source                   'Enhance (Mo) x-ray Source'
_exptl_absorpt_coefficient_mu    2.124
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.70112
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.39 (release 18-08-2010 CrysAlis171 .NET)
(compiled Aug 18 2010,17:42:00)
empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_density_diffrn    1.272
_exptl_crystal_F_000             10204
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.562
_refine_diff_density_min         -0.421
_refine_diff_density_rms         0.079
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.996
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1319
_refine_ls_number_reflns         26710
_refine_ls_number_restraints     260
_refine_ls_restrained_S_all      1.019
_refine_ls_R_factor_all          0.0549
_refine_ls_R_factor_gt           0.0356
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0570P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0953
_refine_ls_wR_factor_ref         0.1017
_reflns_number_gt                20096
_reflns_number_total             26710
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic401191e_si_003.cif
_cod_data_source_block           eu2
_cod_original_cell_volume        26963.8(7)
_cod_original_formula_sum        'C112 H88 Eu4.50 O29'
_cod_database_code               4336796
#BEGIN Tags that were not found in dictionaries:
_chemical_oxdiff_formula         C120H120O60Eu4.5
_reflns_odcompleteness_completeness 99.77
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
#END Tags that were not found in dictionaries
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x, y, -z+1/2'
3 'x+1/2, y+1/2, z'
4 '-x+1/2, y+1/2, -z+1/2'
5 '-x, -y, -z'
6 'x, -y, z-1/2'
7 '-x+1/2, -y+1/2, -z'
8 'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Eu1 Eu 0.099997(8) 0.074165(6) 0.233083(6) 0.03735(6) Uani 1 1 d .
Eu2 Eu -0.002520(8) 0.117129(7) 0.150362(5) 0.03787(6) Uani 1 1 d .
Eu3 Eu 0.032931(8) 0.237693(6) 0.181718(6) 0.03772(6) Uani 1 1 d .
Eu4 Eu -0.136253(7) 0.194897(6) 0.236378(6) 0.03690(6) Uani 1 1 d .
Eu5 Eu 0.0000 0.154961(8) 0.2500 0.03166(7) Uani 1 2 d S
O1 O 0.07486(11) 0.02658(9) 0.27513(8) 0.0503(7) Uani 1 1 d .
O2 O 0.17425(12) 0.04325(11) 0.27803(9) 0.0623(9) Uani 1 1 d .
O3 O 0.0422(2) -0.12466(15) 0.31569(16) 0.1201(17) Uani 1 1 d U
O4 O 0.11129(15) -0.00131(10) 0.20741(9) 0.0695(10) Uani 1 1 d .
O5 O 0.07968(11) 0.07640(9) 0.16410(8) 0.0473(7) Uani 1 1 d .
O6 O 0.1217(2) 0.0874(2) 0.04922(14) 0.139(2) Uani 1 1 d U
O7 O -0.01707(13) 0.04170(11) 0.12256(10) 0.0648(9) Uani 1 1 d .
O8 O -0.08542(11) 0.09586(10) 0.14479(8) 0.0486(7) Uani 1 1 d .
O9 O -0.26048(15) 0.07000(17) 0.07628(14) 0.1037(14) Uani 1 1 d .
O10 O -0.03879(14) 0.13078(12) 0.08248(8) 0.0674(10) Uani 1 1 d .
O11 O 0.03537(11) 0.18475(9) 0.12964(7) 0.0456(7) Uani 1 1 d .
O12 O 0.1445(2) 0.2637(2) 0.07386(16) 0.142(2) Uani 1 1 d U
O13 O -0.02274(14) 0.26861(11) 0.12340(8) 0.0630(9) Uani 1 1 d .
O14 O -0.02833(11) 0.28216(9) 0.19691(8) 0.0488(7) Uani 1 1 d .
O15 O -0.09339(19) 0.43044(14) 0.21923(14) 0.1021(15) Uani 1 1 d .
O16 O -0.13321(11) 0.20924(9) 0.17483(8) 0.0472(7) Uani 1 1 d .
O17 O -0.16930(12) 0.27123(9) 0.21716(8) 0.0537(8) Uani 1 1 d .
O18 O -0.22125(16) 0.20807(16) 0.04080(10) 0.0899(12) Uani 1 1 d .
O19 O -0.17085(11) 0.12902(9) 0.26272(8) 0.0466(7) Uani 1 1 d .
O20 O -0.22592(12) 0.18212(11) 0.20235(9) 0.0595(8) Uani 1 1 d .
O21 O -0.26398(17) 0.05200(15) 0.33307(12) 0.0957(13) Uani 1 1 d .
O22 O -0.12693(11) 0.23965(9) 0.29752(8) 0.0464(7) Uani 1 1 d .
O23 O -0.06351(14) 0.31515(10) 0.32261(11) 0.0696(10) Uani 1 1 d .
O24 O -0.30210(16) 0.27161(16) 0.28817(14) 0.1020(14) Uani 1 1 d .
O25 O -0.09034(10) 0.12996(8) 0.22248(7) 0.0359(6) Uani 1 1 d .
O26 O 0.05265(10) 0.22472(8) 0.24810(7) 0.0362(6) Uani 1 1 d .
O27 O -0.02842(10) 0.18001(8) 0.18237(7) 0.0355(6) Uani 1 1 d .
O28 O 0.01015(10) 0.08585(8) 0.21256(7) 0.0362(6) Uani 1 1 d .
O29 O 0.07260(9) 0.15704(8) 0.20417(7) 0.0362(6) Uani 1 1 d .
C1 C 0.09316(18) -0.01326(15) 0.29102(13) 0.0508(11) Uani 1 1 d .
C2 C 0.0585(2) -0.04645(16) 0.29723(15) 0.0672(14) Uani 1 1 d .
H2 H 0.0238 -0.0388 0.2912 0.081 Uiso 1 1 calc R
C3 C 0.0744(3) -0.0897(2) 0.31183(19) 0.0853(18) Uani 1 1 d .
C4 C 0.1257(3) -0.10233(19) 0.32150(18) 0.0893(19) Uani 1 1 d .
H4 H 0.1360 -0.1325 0.3300 0.107 Uiso 1 1 calc R
C5 C 0.1610(2) -0.06956(17) 0.31835(16) 0.0746(16) Uani 1 1 d .
H5 H 0.1958 -0.0772 0.3266 0.090 Uiso 1 1 calc R
C6 C 0.14644(18) -0.02453(14) 0.30298(13) 0.0522(11) Uani 1 1 d .
C7 C 0.18440(18) 0.00721(15) 0.29841(13) 0.0526(11) Uani 1 1 d .
C8 C 0.24017(19) -0.00175(16) 0.31695(15) 0.0596(13) Uani 1 1 d .
C9 C 0.2733(2) 0.00465(18) 0.29516(18) 0.0766(16) Uani 1 1 d .
H9 H 0.2600 0.0137 0.2696 0.092 Uiso 1 1 calc R
C10 C 0.3264(3) -0.0021(2) 0.3104(2) 0.099(2) Uani 1 1 d U
H10 H 0.3483 0.0018 0.2952 0.119 Uiso 1 1 calc R
C11 C 0.3448(3) -0.0146(2) 0.3481(3) 0.111(3) Uani 1 1 d U
H11 H 0.3800 -0.0194 0.3588 0.133 Uiso 1 1 calc R
C12 C 0.3133(3) -0.0201(3) 0.3704(2) 0.115(3) Uani 1 1 d U
H12 H 0.3267 -0.0282 0.3962 0.137 Uiso 1 1 calc R
C13 C 0.2611(2) -0.0137(2) 0.35460(18) 0.0894(19) Uani 1 1 d U
H13 H 0.2396 -0.0176 0.3701 0.107 Uiso 1 1 calc R
C14 C -0.0116(3) -0.1157(3) 0.3060(3) 0.160(4) Uani 1 1 d U
H14A H -0.0242 -0.1066 0.2794 0.240 Uiso 1 1 calc R
H14B H -0.0179 -0.0910 0.3219 0.240 Uiso 1 1 calc R
H14C H -0.0291 -0.1436 0.3100 0.240 Uiso 1 1 calc R
C15 C 0.09984(17) 0.05528(15) 0.13932(12) 0.0489(11) Uani 1 1 d .
C16 C 0.1008(2) 0.07845(17) 0.10671(13) 0.0627(13) Uani 1 1 d .
H16 H 0.0856 0.1079 0.1019 0.075 Uiso 1 1 calc R
C17 C 0.1235(3) 0.0598(2) 0.08055(16) 0.0832(18) Uani 1 1 d .
C18 C 0.1477(3) 0.0163(2) 0.08803(18) 0.0884(19) Uani 1 1 d .
H18 H 0.1656 0.0041 0.0720 0.106 Uiso 1 1 calc R
C19 C 0.1444(2) -0.00793(19) 0.11949(17) 0.0778(16) Uani 1 1 d .
H19 H 0.1593 -0.0375 0.1237 0.093 Uiso 1 1 calc R
C20 C 0.12009(18) 0.00859(15) 0.14604(13) 0.0537(11) Uani 1 1 d .
C21 C 0.11752(19) -0.01894(15) 0.17796(14) 0.0554(12) Uani 1 1 d .
C22 C 0.1204(2) -0.07117(16) 0.17787(16) 0.0672(14) Uani 1 1 d .
C23 C 0.1035(3) -0.09802(18) 0.14414(17) 0.088(2) Uani 1 1 d .
H23 H 0.0899 -0.0835 0.1204 0.106 Uiso 1 1 calc R
C24 C 0.1074(3) -0.1463(2) 0.1465(2) 0.113(3) Uani 1 1 d .
H24 H 0.0956 -0.1643 0.1244 0.136 Uiso 1 1 calc R
C25 C 0.1283(3) -0.1673(2) 0.1808(3) 0.116(3) Uani 1 1 d .
H25 H 0.1326 -0.1997 0.1817 0.140 Uiso 1 1 calc R
C26 C 0.1431(3) -0.1425(2) 0.2142(2) 0.102(2) Uani 1 1 d .
H26 H 0.1559 -0.1578 0.2377 0.122 Uiso 1 1 calc R
C27 C 0.1388(2) -0.09462(19) 0.21262(18) 0.0838(18) Uani 1 1 d .
H27 H 0.1484 -0.0775 0.2354 0.101 Uiso 1 1 calc R
C28 C 0.1380(5) 0.0693(4) 0.0204(3) 0.224(6) Uani 1 1 d U
H28A H 0.1338 0.0923 0.0004 0.335 Uiso 1 1 calc R
H28B H 0.1181 0.0420 0.0102 0.335 Uiso 1 1 calc R
H28C H 0.1736 0.0609 0.0302 0.335 Uiso 1 1 calc R
C29 C -0.11952(17) 0.07103(14) 0.11998(12) 0.0470(10) Uani 1 1 d .
C30 C -0.17166(19) 0.08230(17) 0.11380(14) 0.0602(13) Uani 1 1 d .
H30 H -0.1808 0.1054 0.1286 0.072 Uiso 1 1 calc R
C31 C -0.2094(2) 0.0590(2) 0.08565(17) 0.0720(15) Uani 1 1 d .
C32 C -0.1973(2) 0.0220(2) 0.06437(17) 0.0856(18) Uani 1 1 d .
H32 H -0.2230 0.0061 0.0460 0.103 Uiso 1 1 calc R
C33 C -0.1480(2) 0.00995(19) 0.07103(16) 0.0769(16) Uani 1 1 d .
H33 H -0.1400 -0.0144 0.0568 0.092 Uiso 1 1 calc R
C34 C -0.10695(18) 0.03313(15) 0.09930(13) 0.0548(12) Uani 1 1 d .
C35 C -0.0554(2) 0.01856(15) 0.10432(14) 0.0590(13) Uani 1 1 d .
C36 C -0.0428(2) -0.02505(19) 0.08637(17) 0.0774(16) Uani 1 1 d U
C37 C -0.0086(3) -0.0237(3) 0.0662(2) 0.113(2) Uani 1 1 d U
H37 H 0.0066 0.0048 0.0634 0.135 Uiso 1 1 calc R
C38 C 0.0050(4) -0.0644(4) 0.0491(3) 0.164(3) Uani 1 1 d U
H38 H 0.0245 -0.0630 0.0321 0.197 Uiso 1 1 calc R
C39 C -0.0122(5) -0.1054(4) 0.0591(3) 0.162(4) Uani 1 1 d DU
H39 H 0.0019 -0.1327 0.0526 0.195 Uiso 1 1 calc R
C40 C -0.0475(4) -0.1098(3) 0.0773(3) 0.150(3) Uani 1 1 d DU
H40 H -0.0617 -0.1388 0.0799 0.180 Uiso 1 1 calc R
C41 C -0.0630(3) -0.0686(2) 0.0930(2) 0.113(2) Uani 1 1 d U
H41 H -0.0861 -0.0704 0.1074 0.136 Uiso 1 1 calc R
C42 C -0.2758(3) 0.1064(3) 0.0967(3) 0.145(4) Uani 1 1 d .
H42A H -0.3114 0.1136 0.0846 0.218 Uiso 1 1 calc R
H42B H -0.2553 0.1337 0.0966 0.218 Uiso 1 1 calc R
H42C H -0.2713 0.0966 0.1228 0.218 Uiso 1 1 calc R
C43 C 0.04568(19) 0.19676(15) 0.09715(12) 0.0507(11) Uani 1 1 d .
C44 C 0.0881(2) 0.2239(2) 0.09955(15) 0.0723(15) Uani 1 1 d .
H44 H 0.1080 0.2341 0.1236 0.087 Uiso 1 1 calc R
C45 C 0.1018(3) 0.2365(2) 0.06762(19) 0.101(2) Uani 1 1 d .
C46 C 0.0716(3) 0.2226(3) 0.03161(18) 0.113(3) Uani 1 1 d .
H46 H 0.0803 0.2316 0.0097 0.136 Uiso 1 1 calc R
C47 C 0.0301(3) 0.1962(2) 0.02843(15) 0.0864(19) Uani 1 1 d .
H47 H 0.0107 0.1865 0.0040 0.104 Uiso 1 1 calc R
C48 C 0.0143(2) 0.18249(17) 0.06050(12) 0.0572(12) Uani 1 1 d .
C49 C -0.0305(2) 0.15280(17) 0.05563(12) 0.0571(12) Uani 1 1 d .
C50 C -0.06991(19) 0.14686(17) 0.01719(12) 0.0568(12) Uani 1 1 d .
C51 C -0.0862(2) 0.1818(2) -0.00879(15) 0.0816(17) Uani 1 1 d .
H51 H -0.0721 0.2116 -0.0030 0.098 Uiso 1 1 calc R
C52 C -0.1233(3) 0.1745(3) -0.04370(18) 0.099(2) Uani 1 1 d U
H52 H -0.1336 0.1988 -0.0613 0.119 Uiso 1 1 calc R
C53 C -0.1442(3) 0.1320(3) -0.05176(17) 0.099(2) Uani 1 1 d U
H53 H -0.1688 0.1268 -0.0753 0.118 Uiso 1 1 calc R
C54 C -0.1303(2) 0.0964(2) -0.02620(17) 0.0885(18) Uani 1 1 d U
H54 H -0.1455 0.0671 -0.0320 0.106 Uiso 1 1 calc R
C55 C -0.0927(2) 0.10399(19) 0.00903(15) 0.0720(15) Uani 1 1 d .
H55 H -0.0833 0.0798 0.0269 0.086 Uiso 1 1 calc R
C56 C 0.1601(5) 0.2802(5) 0.0436(3) 0.226(6) Uani 1 1 d U
H56A H 0.1595 0.2551 0.0258 0.339 Uiso 1 1 calc R
H56B H 0.1945 0.2923 0.0531 0.339 Uiso 1 1 calc R
H56C H 0.1374 0.3047 0.0307 0.339 Uiso 1 1 calc R
C57 C -0.05088(16) 0.32156(14) 0.18267(13) 0.0471(10) Uani 1 1 d .
C58 C -0.06218(19) 0.35389(15) 0.20846(15) 0.0599(13) Uani 1 1 d .
H58 H -0.0552 0.3461 0.2343 0.072 Uiso 1 1 calc R
C59 C -0.0832(2) 0.39658(19) 0.19575(18) 0.0742(15) Uani 1 1 d .
C60 C -0.0949(2) 0.40910(18) 0.15663(17) 0.0788(17) Uani 1 1 d .
H60 H -0.1087 0.4384 0.1483 0.095 Uiso 1 1 calc R
C61 C -0.0858(2) 0.37771(16) 0.13108(16) 0.0670(14) Uani 1 1 d .
H61 H -0.0941 0.3858 0.1052 0.080 Uiso 1 1 calc R
C62 C -0.06392(17) 0.33306(14) 0.14286(13) 0.0490(11) Uani 1 1 d .
C63 C -0.05336(18) 0.30187(15) 0.11509(14) 0.0550(12) Uani 1 1 d .
C64 C -0.0789(2) 0.30861(16) 0.07270(14) 0.0615(13) Uani 1 1 d .
C65 C -0.1317(2) 0.3113(2) 0.05761(17) 0.0851(18) Uani 1 1 d .
H65 H -0.1522 0.3125 0.0741 0.102 Uiso 1 1 calc R
C66 C -0.1542(3) 0.3123(2) 0.0181(2) 0.106(2) Uani 1 1 d U
H66 H -0.1898 0.3118 0.0079 0.128 Uiso 1 1 calc R
C67 C -0.1244(4) 0.3140(2) -0.0050(2) 0.110(3) Uani 1 1 d U
H67 H -0.1400 0.3165 -0.0314 0.133 Uiso 1 1 calc R
C68 C -0.0722(3) 0.3122(2) 0.00814(19) 0.109(2) Uani 1 1 d U
H68 H -0.0523 0.3137 -0.0087 0.131 Uiso 1 1 calc R
C69 C -0.0494(3) 0.3080(2) 0.04826(16) 0.0847(18) Uani 1 1 d .
H69 H -0.0140 0.3047 0.0581 0.102 Uiso 1 1 calc R
C70 C -0.0850(3) 0.4180(3) 0.2584(2) 0.135(3) Uani 1 1 d .
H70A H -0.1048 0.3905 0.2599 0.202 Uiso 1 1 calc R
H70B H -0.0955 0.4434 0.2717 0.202 Uiso 1 1 calc R
H70C H -0.0492 0.4116 0.2701 0.202 Uiso 1 1 calc R
C72 C -0.17348(18) 0.20974(16) 0.10876(13) 0.0555(12) Uani 1 1 d .
H72 H -0.1503 0.1873 0.1055 0.067 Uiso 1 1 calc R
C73 C -0.2123(2) 0.22424(18) 0.07722(14) 0.0626(13) Uani 1 1 d .
C74 C -0.2458(2) 0.25966(19) 0.08086(15) 0.0711(15) Uani 1 1 d .
H74 H -0.2726 0.2692 0.0597 0.085 Uiso 1 1 calc R
C75 C -0.23889(19) 0.28028(18) 0.11615(15) 0.0654(14) Uani 1 1 d .
H75 H -0.2612 0.3041 0.1183 0.078 Uiso 1 1 calc R
C76 C -0.19906(17) 0.26674(14) 0.14951(12) 0.0472(10) Uani 1 1 d .
C77 C -0.16792(16) 0.22773(14) 0.14560(12) 0.0455(10) Uani 1 1 d .
C78 C -0.19125(17) 0.29041(14) 0.18544(13) 0.0495(11) Uani 1 1 d .
C79 C -0.20780(18) 0.34038(15) 0.18775(14) 0.0564(12) Uani 1 1 d .
C80 C -0.2178(2) 0.35449(16) 0.22080(17) 0.0724(15) Uani 1 1 d .
H80 H -0.2148 0.3332 0.2407 0.087 Uiso 1 1 calc R
C81 C -0.2323(3) 0.4002(2) 0.2248(2) 0.092(2) Uani 1 1 d .
H81 H -0.2395 0.4097 0.2471 0.110 Uiso 1 1 calc R
C82 C -0.2359(3) 0.4314(2) 0.1954(2) 0.102(2) Uani 1 1 d .
H82 H -0.2453 0.4622 0.1982 0.123 Uiso 1 1 calc R
C83 C -0.2263(3) 0.4185(2) 0.1624(2) 0.096(2) Uani 1 1 d .
H83 H -0.2298 0.4400 0.1425 0.116 Uiso 1 1 calc R
C84 C -0.2111(2) 0.37299(17) 0.15863(17) 0.0751(16) Uani 1 1 d .
H84 H -0.2030 0.3641 0.1365 0.090 Uiso 1 1 calc R
C86 C -0.1860(3) 0.1749(3) 0.03424(17) 0.124(3) Uani 1 1 d .
H86A H -0.1999 0.1612 0.0092 0.187 Uiso 1 1 calc R
H86B H -0.1802 0.1507 0.0534 0.187 Uiso 1 1 calc R
H86C H -0.1541 0.1901 0.0357 0.187 Uiso 1 1 calc R
C87 C -0.21693(17) 0.11707(14) 0.26544(13) 0.0484(10) Uani 1 1 d .
C88 C -0.22048(19) 0.09015(17) 0.29651(14) 0.0600(12) Uani 1 1 d .
H88 H -0.1903 0.0801 0.3144 0.072 Uiso 1 1 calc R
C89 C -0.2659(2) 0.07799(17) 0.30183(16) 0.0668(14) Uani 1 1 d .
C90 C -0.3118(2) 0.09258(19) 0.27531(17) 0.0741(15) Uani 1 1 d .
H90 H -0.3432 0.0851 0.2791 0.089 Uiso 1 1 calc R
C91 C -0.31008(19) 0.11801(18) 0.24367(16) 0.0686(14) Uani 1 1 d .
H91 H -0.3408 0.1272 0.2260 0.082 Uiso 1 1 calc R
C92 C -0.26363(17) 0.13064(16) 0.23717(13) 0.0531(11) Uani 1 1 d .
C93 C -0.26365(17) 0.15865(15) 0.20459(13) 0.0523(11) Uani 1 1 d .
C94 C -0.31094(18) 0.16289(18) 0.17117(14) 0.0619(13) Uani 1 1 d .
C95 C -0.3436(2) 0.1252(2) 0.15861(17) 0.094(2) Uani 1 1 d .
H95 H -0.3377 0.0966 0.1713 0.113 Uiso 1 1 calc R
C96 C -0.3869(3) 0.1321(3) 0.1253(2) 0.116(3) Uani 1 1 d U
H96 H -0.4081 0.1071 0.1144 0.140 Uiso 1 1 calc R
C97 C -0.3967(3) 0.1757(4) 0.1096(2) 0.121(3) Uani 1 1 d U
H97 H -0.4268 0.1807 0.0897 0.145 Uiso 1 1 calc R
C98 C -0.3650(3) 0.2111(3) 0.1216(2) 0.111(3) Uani 1 1 d .
H98 H -0.3718 0.2399 0.1093 0.133 Uiso 1 1 calc R
C99 C -0.3219(2) 0.2055(2) 0.15237(16) 0.0814(17) Uani 1 1 d .
H99 H -0.2997 0.2306 0.1607 0.098 Uiso 1 1 calc R
C100 C -0.3102(3) 0.0398(3) 0.3431(2) 0.130(3) Uani 1 1 d .
H10A H -0.3337 0.0239 0.3219 0.196 Uiso 1 1 calc R
H10B H -0.3260 0.0678 0.3489 0.196 Uiso 1 1 calc R
H10C H -0.3014 0.0196 0.3653 0.196 Uiso 1 1 calc R
C101 C -0.16229(17) 0.26825(14) 0.30360(12) 0.0476(10) Uani 1 1 d .
C102 C -0.21390(19) 0.25368(16) 0.29247(14) 0.0582(12) Uani 1 1 d .
H102 H -0.2226 0.2245 0.2809 0.070 Uiso 1 1 calc R
C103 C -0.2517(2) 0.2820(2) 0.29843(16) 0.0694(14) Uani 1 1 d .
C104 C -0.2397(2) 0.32593(19) 0.31591(17) 0.0772(16) Uani 1 1 d .
H104 H -0.2656 0.3453 0.3192 0.093 Uiso 1 1 calc R
C105 C -0.1905(2) 0.33962(18) 0.32781(16) 0.0726(15) Uani 1 1 d .
H105 H -0.1829 0.3685 0.3400 0.087 Uiso 1 1 calc R
C106 C -0.14945(18) 0.31263(15) 0.32287(13) 0.0545(11) Uani 1 1 d .
C107 C -0.0981(2) 0.32962(16) 0.33579(15) 0.0636(14) Uani 1 1 d .
C108 C -0.0819(2) 0.36546(19) 0.36693(18) 0.0765(17) Uani 1 1 d .
C109 C -0.0428(2) 0.39629(19) 0.36517(19) 0.092(2) Uani 1 1 d U
H109 H -0.0296 0.3951 0.3443 0.110 Uiso 1 1 calc R
C110 C -0.0232(3) 0.4288(3) 0.3946(3) 0.120(2) Uani 1 1 d U
H110 H 0.0019 0.4504 0.3936 0.145 Uiso 1 1 calc R
C111 C -0.0436(4) 0.4269(3) 0.4253(3) 0.131(3) Uani 1 1 d U
H111 H -0.0310 0.4481 0.4452 0.157 Uiso 1 1 calc R
C112 C -0.0807(3) 0.3964(3) 0.4288(2) 0.128(3) Uani 1 1 d U
H112 H -0.0923 0.3960 0.4504 0.153 Uiso 1 1 calc R
C113 C -0.0999(3) 0.3659(2) 0.3980(2) 0.100(2) Uani 1 1 d U
H113 H -0.1260 0.3451 0.3987 0.120 Uiso 1 1 calc R
C114 C -0.3177(3) 0.2294(3) 0.2693(3) 0.140(3) Uani 1 1 d .
H11A H -0.3103 0.2296 0.2450 0.209 Uiso 1 1 calc R
H11B H -0.3540 0.2255 0.2650 0.209 Uiso 1 1 calc R
H11C H -0.2996 0.2041 0.2849 0.209 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Eu2 Eu1 Eu4 90.350(6) . 2
Eu2 Eu1 Eu5 60.908(5) . .
Eu4 Eu1 Eu5 61.096(5) 2 .
O1 Eu1 Eu2 116.13(7) . .
O1 Eu1 Eu4 117.49(7) . 2
O1 Eu1 Eu5 83.23(7) . .
O1 Eu1 O2 71.39(11) . .
O1 Eu1 O4 79.91(11) . .
O1 Eu1 O5 133.46(10) . .
O1 Eu1 O19 136.00(10) . 2
O1 Eu1 O25 80.06(9) . 2
O1 Eu1 O28 79.04(9) . .
O1 Eu1 O29 134.40(9) . .
O2 Eu1 Eu2 169.40(9) . .
O2 Eu1 Eu4 92.42(8) . 2
O2 Eu1 Eu5 129.07(9) . .
O2 Eu1 O4 75.67(12) . .
O2 Eu1 O5 128.18(11) . .
O2 Eu1 O19 72.44(10) . 2
O2 Eu1 O29 134.61(9) . .
O4 Eu1 Eu2 97.78(8) . .
O4 Eu1 Eu4 155.03(9) . 2
O4 Eu1 Eu5 142.75(9) . .
O4 Eu1 O5 68.63(10) . .
O4 Eu1 O19 114.09(11) . 2
O4 Eu1 O29 135.34(9) . .
O5 Eu1 Eu2 41.28(7) . .
O5 Eu1 Eu4 104.46(6) . 2
O5 Eu1 Eu5 101.45(7) . .
O5 Eu1 O19 89.07(10) . 2
O5 Eu1 O29 66.72(8) . .
O19 Eu1 Eu2 103.48(6) 2 .
O19 Eu1 Eu4 40.94(6) 2 2
O19 Eu1 Eu5 101.10(6) 2 .
O19 Eu1 O29 64.71(8) 2 .
O25 Eu1 Eu2 97.21(6) 2 .
O25 Eu1 Eu4 39.21(6) 2 2
O25 Eu1 Eu5 40.01(6) 2 .
O25 Eu1 O2 91.38(10) 2 .
O25 Eu1 O4 158.80(10) 2 .
O25 Eu1 O5 131.61(9) 2 .
O25 Eu1 O19 76.60(9) 2 2
O25 Eu1 O28 78.79(8) 2 .
O25 Eu1 O29 65.35(8) 2 .
O28 Eu1 Eu2 39.14(6) . .
O28 Eu1 Eu4 97.16(6) . 2
O28 Eu1 Eu5 39.76(6) . .
O28 Eu1 O2 150.06(10) . .
O28 Eu1 O4 104.05(11) . .
O28 Eu1 O5 76.55(9) . .
O28 Eu1 O19 130.68(9) . 2
O28 Eu1 O29 66.26(8) . .
O29 Eu1 Eu2 46.07(5) . .
O29 Eu1 Eu4 44.65(5) . 2
O29 Eu1 Eu5 51.17(6) . .
Eu1 Eu2 Eu3 89.526(6) . .
Eu1 Eu2 Eu5 60.778(5) . .
Eu3 Eu2 Eu5 60.143(5) . .
O5 Eu2 Eu1 40.54(6) . .
O5 Eu2 Eu3 104.00(6) . .
O5 Eu2 Eu5 100.59(6) . .
O5 Eu2 O29 65.74(8) . .
O7 Eu2 Eu1 92.14(8) . .
O7 Eu2 Eu3 170.04(9) . .
O7 Eu2 Eu5 128.84(9) . .
O7 Eu2 O5 71.44(10) . .
O7 Eu2 O10 75.06(12) . .
O7 Eu2 O11 129.03(11) . .
O7 Eu2 O29 135.00(9) . .
O8 Eu2 Eu1 118.57(7) . .
O8 Eu2 Eu3 116.08(7) . .
O8 Eu2 Eu5 84.25(7) . .
O8 Eu2 O5 135.51(10) . .
O8 Eu2 O7 71.53(11) . .
O8 Eu2 O10 81.67(11) . .
O8 Eu2 O11 133.33(10) . .
O8 Eu2 O27 79.36(9) . .
O8 Eu2 O28 81.21(9) . .
O8 Eu2 O29 135.26(9) . .
O10 Eu2 Eu1 151.76(9) . .
O10 Eu2 Eu3 99.09(8) . .
O10 Eu2 Eu5 145.82(9) . .
O10 Eu2 O5 111.27(11) . .
O10 Eu2 O11 68.55(10) . .
O10 Eu2 O29 133.31(9) . .
O11 Eu2 Eu1 103.39(7) . .
O11 Eu2 Eu3 41.18(6) . .
O11 Eu2 Eu5 100.50(6) . .
O11 Eu2 O5 89.68(10) . .
O11 Eu2 O29 64.90(8) . .
O27 Eu2 Eu1 96.70(6) . .
O27 Eu2 Eu3 38.82(6) . .
O27 Eu2 Eu5 39.59(6) . .
O27 Eu2 O5 130.65(9) . .
O27 Eu2 O7 150.29(10) . .
O27 Eu2 O10 106.88(11) . .
O27 Eu2 O11 76.22(9) . .
O27 Eu2 O28 78.25(8) . .
O27 Eu2 O29 65.45(8) . .
O28 Eu2 Eu1 39.20(6) . .
O28 Eu2 Eu3 96.12(6) . .
O28 Eu2 Eu5 39.65(6) . .
O28 Eu2 O5 75.90(9) . .
O28 Eu2 O7 91.35(10) . .
O28 Eu2 O10 160.84(10) . .
O28 Eu2 O11 130.28(9) . .
O28 Eu2 O29 65.80(8) . .
O29 Eu2 Eu1 45.39(5) . .
O29 Eu2 Eu3 44.57(5) . .
O29 Eu2 Eu5 51.04(6) . .
Eu2 Eu3 Eu5 61.189(5) . .
Eu4 Eu3 Eu2 90.498(6) 2 .
Eu4 Eu3 Eu5 61.532(5) 2 .
O11 Eu3 Eu2 40.64(6) . .
O11 Eu3 Eu4 103.59(7) . 2
O11 Eu3 Eu5 101.01(6) . .
O11 Eu3 O22 89.36(10) . 2
O11 Eu3 O29 65.58(8) . .
O13 Eu3 Eu2 91.76(8) . .
O13 Eu3 Eu4 169.96(9) . 2
O13 Eu3 Eu5 127.80(9) . .
O13 Eu3 O11 72.23(10) . .
O13 Eu3 O22 126.88(11) . 2
O13 Eu3 O23 75.00(12) . 2
O13 Eu3 O29 135.38(9) . .
O14 Eu3 Eu2 116.86(7) . .
O14 Eu3 Eu4 115.49(7) . 2
O14 Eu3 Eu5 81.71(7) . .
O14 Eu3 O11 135.97(10) . .
O14 Eu3 O13 71.98(11) . .
O14 Eu3 O22 133.11(10) . 2
O14 Eu3 O23 78.17(11) . 2
O14 Eu3 O26 78.59(9) . .
O14 Eu3 O27 79.38(9) . .
O14 Eu3 O29 133.46(9) . .
O22 Eu3 Eu2 105.86(6) 2 .
O22 Eu3 Eu4 43.21(6) 2 2
O22 Eu3 Eu5 104.13(6) 2 .
O22 Eu3 O29 67.60(8) 2 .
O23 Eu3 Eu2 156.31(9) 2 .
O23 Eu3 Eu4 99.41(8) 2 2
O23 Eu3 Eu5 142.18(9) 2 .
O23 Eu3 O11 115.73(11) 2 .
O23 Eu3 O22 69.22(10) 2 2
O23 Eu3 O29 136.79(10) 2 .
O26 Eu3 Eu2 97.55(6) . .
O26 Eu3 Eu4 38.67(6) . 2
O26 Eu3 Eu5 40.53(6) . .
O26 Eu3 O11 130.64(9) . .
O26 Eu3 O13 150.22(10) . .
O26 Eu3 O22 77.50(9) . 2
O26 Eu3 O23 103.64(11) . 2
O26 Eu3 O27 80.07(8) . .
O26 Eu3 O29 65.40(8) . .
O27 Eu3 Eu2 38.94(6) . .
O27 Eu3 Eu4 97.88(6) . 2
O27 Eu3 Eu5 40.32(6) . .
O27 Eu3 O11 75.82(9) . .
O27 Eu3 O13 90.00(10) . .
O27 Eu3 O22 134.02(9) . 2
O27 Eu3 O23 155.96(10) . 2
O27 Eu3 O29 66.62(8) . .
O29 Eu3 Eu2 46.02(5) . .
O29 Eu3 Eu4 44.85(5) . 2
O29 Eu3 Eu5 51.78(6) . .
Eu1 Eu4 Eu5 60.604(6) 2 .
Eu3 Eu4 Eu1 89.619(6) 2 2
Eu3 Eu4 Eu5 60.118(5) 2 .
O16 Eu4 Eu1 112.23(7) . 2
O16 Eu4 Eu3 119.58(7) . 2
O16 Eu4 Eu5 82.32(7) . .
O16 Eu4 O17 70.76(10) . .
O16 Eu4 O19 130.68(10) . .
O16 Eu4 O20 81.32(11) . .
O16 Eu4 O22 138.35(9) . .
O16 Eu4 O25 76.12(9) . .
O16 Eu4 O26 81.89(9) . 2
O16 Eu4 O29 133.05(9) . 2
O17 Eu4 Eu1 173.44(8) . 2
O17 Eu4 Eu3 93.85(7) . 2
O17 Eu4 Eu5 125.95(8) . .
O17 Eu4 O19 131.95(10) . .
O17 Eu4 O20 75.55(10) . .
O17 Eu4 O22 74.05(9) . .
O17 Eu4 O29 137.10(9) . 2
O19 Eu4 Eu1 41.59(7) . 2
O19 Eu4 Eu3 103.51(6) . 2
O19 Eu4 Eu5 101.26(7) . .
O19 Eu4 O22 89.73(10) . .
O19 Eu4 O29 65.62(8) . 2
O20 Eu4 Eu1 98.89(7) . 2
O20 Eu4 Eu3 152.51(8) . 2
O20 Eu4 Eu5 145.87(8) . .
O20 Eu4 O19 68.50(9) . .
O20 Eu4 O22 110.71(11) . .
O20 Eu4 O29 134.01(9) . 2
O22 Eu4 Eu1 105.21(6) . 2
O22 Eu4 Eu3 41.87(7) . 2
O22 Eu4 Eu5 101.41(6) . .
O22 Eu4 O29 66.63(8) . 2
O25 Eu4 Eu1 38.53(6) . 2
O25 Eu4 Eu3 96.14(6) . 2
O25 Eu4 Eu5 39.84(6) . .
O25 Eu4 O17 146.07(10) . .
O25 Eu4 O19 76.58(9) . .
O25 Eu4 O20 106.82(10) . .
O25 Eu4 O22 131.58(8) . .
O25 Eu4 O29 65.40(8) . 2
O26 Eu4 Eu1 96.47(6) 2 2
O26 Eu4 Eu3 38.72(6) 2 2
O26 Eu4 Eu5 39.49(6) 2 .
O26 Eu4 O17 89.70(10) 2 .
O26 Eu4 O19 130.63(9) 2 .
O26 Eu4 O20 160.57(9) 2 .
O26 Eu4 O22 76.31(9) 2 .
O26 Eu4 O25 78.42(8) 2 .
O26 Eu4 O29 65.36(8) 2 2
O29 Eu4 Eu1 45.32(5) 2 2
O29 Eu4 Eu3 44.75(5) 2 2
O29 Eu4 Eu5 50.93(6) 2 .
Eu3 Eu5 Eu3 101.198(8) 2 .
O25 Eu5 Eu3 108.64(6) 2 2
O25 Eu5 Eu3 92.69(6) . 2
O25 Eu5 Eu3 92.68(6) 2 .
O25 Eu5 Eu3 108.64(6) . .
O25 Eu5 O25 146.45(11) 2 .
O25 Eu5 O29 122.15(7) . .
O25 Eu5 O29 122.15(7) 2 2
O25 Eu5 O29 58.64(7) . 2
O25 Eu5 O29 58.64(7) 2 .
O26 Eu5 Eu3 38.09(6) 2 2
O26 Eu5 Eu3 38.09(6) . .
O26 Eu5 Eu3 76.24(6) 2 .
O26 Eu5 Eu3 76.24(6) . 2
O26 Eu5 O25 74.15(8) . 2
O26 Eu5 O25 137.65(7) 2 2
O26 Eu5 O25 137.65(7) . .
O26 Eu5 O25 74.16(8) 2 .
O26 Eu5 O26 72.33(12) 2 .
O26 Eu5 O29 119.56(7) . 2
O26 Eu5 O29 58.27(7) 2 2
O26 Eu5 O29 58.26(7) . .
O26 Eu5 O29 119.56(7) 2 .
O27 Eu5 Eu3 114.55(6) 2 .
O27 Eu5 Eu3 38.26(6) . .
O27 Eu5 Eu3 38.26(6) 2 2
O27 Eu5 Eu3 114.55(6) . 2
O27 Eu5 O25 118.18(9) . 2
O27 Eu5 O25 72.30(8) 2 2
O27 Eu5 O25 118.18(9) 2 .
O27 Eu5 O25 72.30(8) . .
O27 Eu5 O26 77.17(8) . 2
O27 Eu5 O26 75.63(8) 2 2
O27 Eu5 O26 75.63(8) . .
O27 Eu5 O26 77.17(8) 2 .
O27 Eu5 O27 146.14(11) . 2
O27 Eu5 O28 74.55(8) . .
O27 Eu5 O28 137.22(8) 2 .
O27 Eu5 O28 74.55(8) 2 2
O27 Eu5 O28 137.22(8) . 2
O27 Eu5 O29 59.56(8) 2 2
O27 Eu5 O29 119.66(8) . 2
O27 Eu5 O29 59.56(8) . .
O27 Eu5 O29 119.66(8) 2 .
O28 Eu5 Eu3 165.22(6) . 2
O28 Eu5 Eu3 165.23(6) 2 .
O28 Eu5 Eu3 92.99(6) . .
O28 Eu5 Eu3 92.99(6) 2 2
O28 Eu5 O25 78.75(8) 2 2
O28 Eu5 O25 74.44(8) . 2
O28 Eu5 O25 78.74(8) . .
O28 Eu5 O25 74.44(8) 2 .
O28 Eu5 O26 145.53(8) 2 .
O28 Eu5 O26 118.15(9) . .
O28 Eu5 O26 118.15(9) 2 2
O28 Eu5 O26 145.53(8) . 2
O28 Eu5 O28 73.21(12) . 2
O28 Eu5 O29 59.89(7) 2 2
O28 Eu5 O29 122.29(7) 2 .
O28 Eu5 O29 59.89(7) . .
O28 Eu5 O29 122.29(8) . 2
O29 Eu5 Eu3 134.40(4) . 2
O29 Eu5 Eu3 43.50(4) . .
O29 Eu5 Eu3 134.40(4) 2 .
O29 Eu5 Eu3 43.50(4) 2 2
O29 Eu5 O29 177.68(9) 2 .
C1 O1 Eu1 131.3(3) . .
C7 O2 Eu1 135.4(3) . .
C3 O3 C14 119.3(5) . .
C21 O4 Eu1 139.9(3) . .
Eu1 O5 Eu2 98.18(10) . .
C15 O5 Eu1 132.8(3) . .
C15 O5 Eu2 127.9(3) . .
C28 O6 C17 118.9(7) . .
C35 O7 Eu2 135.9(3) . .
C29 O8 Eu2 133.8(3) . .
C31 O9 C42 118.4(5) . .
C49 O10 Eu2 141.0(3) . .
Eu2 O11 Eu3 98.17(10) . .
C43 O11 Eu2 134.6(2) . .
C43 O11 Eu3 126.0(2) . .
C45 O12 C56 120.9(7) . .
C63 O13 Eu3 134.9(3) . .
C57 O14 Eu3 132.1(3) . .
C59 O15 C70 116.4(5) . .
C77 O16 Eu4 129.6(3) . .
C78 O17 Eu4 134.7(3) . .
C73 O18 C86 117.1(4) . .
Eu4 O19 Eu1 97.46(10) . 2
C87 O19 Eu1 124.9(2) . 2
C87 O19 Eu4 135.4(2) . .
C93 O20 Eu4 140.7(3) . .
C89 O21 C100 121.6(5) . .
Eu3 O22 Eu4 94.92(10) 2 .
C101 O22 Eu3 134.9(3) . 2
C101 O22 Eu4 124.7(2) . .
C107 O23 Eu3 130.6(3) . 2
C103 O24 C114 117.8(5) . .
Eu1 O25 Eu4 102.25(10) 2 .
Eu1 O25 Eu5 102.58(9) 2 .
Eu4 O25 Eu5 102.25(9) . .
Eu3 O26 Eu5 101.37(9) . .
Eu4 O26 Eu3 102.62(10) 2 .
Eu4 O26 Eu5 103.41(9) 2 .
Eu2 O27 Eu5 102.70(9) . .
Eu3 O27 Eu2 102.24(10) . .
Eu3 O27 Eu5 101.42(9) . .
Eu1 O28 Eu5 102.31(9) . .
Eu2 O28 Eu1 101.67(10) . .
Eu2 O28 Eu5 102.58(9) . .
Eu1 O29 Eu2 88.54(7) . .
Eu1 O29 Eu5 85.06(7) . .
Eu2 O29 Eu5 84.66(7) . .
Eu3 O29 Eu1 169.72(11) . .
Eu3 O29 Eu2 89.41(7) . .
Eu3 O29 Eu4 90.39(7) . 2
Eu3 O29 Eu5 84.72(7) . .
Eu4 O29 Eu1 90.03(7) 2 .
Eu4 O29 Eu2 170.75(11) 2 .
Eu4 O29 Eu5 86.11(7) 2 .
O1 C1 C2 118.2(4) . .
O1 C1 C6 123.6(4) . .
C2 C1 C6 118.2(4) . .
C1 C2 H2 119.2 . .
C3 C2 C1 121.5(5) . .
C3 C2 H2 119.2 . .
O3 C3 C4 114.5(5) . .
C2 C3 O3 124.3(6) . .
C2 C3 C4 121.1(5) . .
C3 C4 H4 120.6 . .
C5 C4 C3 118.7(5) . .
C5 C4 H4 120.6 . .
C4 C5 H5 118.9 . .
C4 C5 C6 122.1(5) . .
C6 C5 H5 118.9 . .
C5 C6 C1 118.0(4) . .
C5 C6 C7 119.8(4) . .
C7 C6 C1 122.1(4) . .
O2 C7 C6 123.5(4) . .
O2 C7 C8 115.3(4) . .
C6 C7 C8 121.1(4) . .
C9 C8 C7 118.0(5) . .
C13 C8 C7 124.5(5) . .
C13 C8 C9 117.4(5) . .
C8 C9 H9 119.0 . .
C8 C9 C10 122.0(6) . .
C10 C9 H9 119.0 . .
C9 C10 H10 121.1 . .
C11 C10 C9 117.8(7) . .
C11 C10 H10 121.1 . .
C10 C11 H11 119.3 . .
C12 C11 C10 121.5(8) . .
C12 C11 H11 119.3 . .
C11 C12 H12 120.2 . .
C11 C12 C13 119.6(8) . .
C13 C12 H12 120.2 . .
C8 C13 C12 121.8(7) . .
C8 C13 H13 119.1 . .
C12 C13 H13 119.1 . .
O3 C14 H14A 109.5 . .
O3 C14 H14B 109.5 . .
O3 C14 H14C 109.5 . .
H14A C14 H14B 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
O5 C15 C16 119.0(4) . .
O5 C15 C20 121.4(4) . .
C16 C15 C20 119.6(4) . .
C15 C16 H16 118.8 . .
C15 C16 C17 122.5(5) . .
C17 C16 H16 118.8 . .
O6 C17 C16 115.8(6) . .
O6 C17 C18 124.9(5) . .
C16 C17 C18 119.3(5) . .
C17 C18 H18 120.9 . .
C19 C18 C17 118.1(5) . .
C19 C18 H18 120.9 . .
C18 C19 H19 117.7 . .
C18 C19 C20 124.6(5) . .
C20 C19 H19 117.7 . .
C19 C20 C15 115.5(5) . .
C19 C20 C21 121.5(4) . .
C21 C20 C15 123.0(4) . .
O4 C21 C20 122.2(4) . .
O4 C21 C22 115.3(4) . .
C20 C21 C22 122.4(4) . .
C23 C22 C21 122.9(5) . .
C27 C22 C21 119.0(5) . .
C27 C22 C23 118.0(5) . .
C22 C23 H23 120.3 . .
C24 C23 C22 119.4(6) . .
C24 C23 H23 120.3 . .
C23 C24 H24 119.8 . .
C25 C24 C23 120.3(6) . .
C25 C24 H24 119.8 . .
C24 C25 H25 119.1 . .
C24 C25 C26 121.7(6) . .
C26 C25 H25 119.1 . .
C25 C26 H26 120.6 . .
C25 C26 C27 118.9(7) . .
C27 C26 H26 120.6 . .
C22 C27 H27 119.2 . .
C26 C27 C22 121.5(6) . .
C26 C27 H27 119.2 . .
O6 C28 H28A 109.5 . .
O6 C28 H28B 109.5 . .
O6 C28 H28C 109.5 . .
H28A C28 H28B 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
O8 C29 C30 117.9(4) . .
O8 C29 C34 123.4(4) . .
C30 C29 C34 118.7(4) . .
C29 C30 H30 120.0 . .
C31 C30 C29 120.1(5) . .
C31 C30 H30 120.0 . .
O9 C31 C30 123.4(5) . .
O9 C31 C32 115.0(5) . .
C30 C31 C32 121.6(5) . .
C31 C32 H32 120.7 . .
C33 C32 C31 118.6(5) . .
C33 C32 H32 120.7 . .
C32 C33 H33 118.6 . .
C32 C33 C34 122.7(5) . .
C34 C33 H33 118.6 . .
C29 C34 C33 118.1(5) . .
C29 C34 C35 122.6(4) . .
C35 C34 C33 119.2(4) . .
O7 C35 C34 123.5(4) . .
O7 C35 C36 114.2(5) . .
C34 C35 C36 122.2(4) . .
C37 C36 C35 119.9(6) . .
C37 C36 C41 119.1(6) . .
C41 C36 C35 120.8(6) . .
C36 C37 H37 119.2 . .
C36 C37 C38 121.7(8) . .
C38 C37 H37 119.2 . .
C37 C38 H38 121.9 . .
C39 C38 C37 116.1(10) . .
C39 C38 H38 121.9 . .
C38 C39 H39 117.4 . .
C40 C39 C38 125.3(11) . .
C40 C39 H39 117.4 . .
C39 C40 H40 121.2 . .
C39 C40 C41 117.7(10) . .
C41 C40 H40 121.2 . .
C36 C41 C40 119.1(8) . .
C36 C41 H41 120.5 . .
C40 C41 H41 120.5 . .
O9 C42 H42A 109.5 . .
O9 C42 H42B 109.5 . .
O9 C42 H42C 109.5 . .
H42A C42 H42B 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
O11 C43 C44 118.7(4) . .
O11 C43 C48 122.1(4) . .
C44 C43 C48 119.2(4) . .
C43 C44 H44 119.0 . .
C45 C44 C43 121.9(5) . .
C45 C44 H44 119.0 . .
O12 C45 C44 116.2(6) . .
O12 C45 C46 124.2(6) . .
C44 C45 C46 119.6(6) . .
C45 C46 H46 120.1 . .
C47 C46 C45 119.7(5) . .
C47 C46 H46 120.1 . .
C46 C47 H47 118.6 . .
C46 C47 C48 122.8(5) . .
C48 C47 H47 118.6 . .
C43 C48 C49 122.5(4) . .
C47 C48 C43 116.8(5) . .
C47 C48 C49 120.7(4) . .
O10 C49 C48 122.8(4) . .
O10 C49 C50 115.5(4) . .
C48 C49 C50 121.7(4) . .
C51 C50 C49 124.3(5) . .
C51 C50 C55 118.3(5) . .
C55 C50 C49 117.3(4) . .
C50 C51 H51 119.1 . .
C50 C51 C52 121.8(6) . .
C52 C51 H51 119.1 . .
C51 C52 H52 120.4 . .
C53 C52 C51 119.2(6) . .
C53 C52 H52 120.4 . .
C52 C53 H53 119.5 . .
C52 C53 C54 121.0(6) . .
C54 C53 H53 119.5 . .
C53 C54 H54 120.2 . .
C53 C54 C55 119.5(6) . .
C55 C54 H54 120.2 . .
C50 C55 C54 120.0(5) . .
C50 C55 H55 120.0 . .
C54 C55 H55 120.0 . .
O12 C56 H56A 109.5 . .
O12 C56 H56B 109.5 . .
O12 C56 H56C 109.5 . .
H56A C56 H56B 109.5 . .
H56A C56 H56C 109.5 . .
H56B C56 H56C 109.5 . .
O14 C57 C58 117.8(4) . .
O14 C57 C62 123.1(4) . .
C58 C57 C62 119.1(4) . .
C57 C58 H58 119.7 . .
C59 C58 C57 120.6(5) . .
C59 C58 H58 119.7 . .
O15 C59 C60 115.0(5) . .
C58 C59 O15 124.0(5) . .
C58 C59 C60 121.0(5) . .
C59 C60 H60 120.4 . .
C61 C60 C59 119.2(5) . .
C61 C60 H60 120.4 . .
C60 C61 H61 119.0 . .
C60 C61 C62 121.9(5) . .
C62 C61 H61 119.0 . .
C57 C62 C63 122.0(4) . .
C61 C62 C57 118.1(4) . .
C61 C62 C63 119.8(4) . .
O13 C63 C62 124.2(4) . .
O13 C63 C64 115.0(4) . .
C62 C63 C64 120.8(4) . .
C65 C64 C63 121.8(5) . .
C69 C64 C63 118.9(5) . .
C69 C64 C65 119.1(5) . .
C64 C65 H65 119.9 . .
C64 C65 C66 120.3(7) . .
C66 C65 H65 119.9 . .
C65 C66 H66 120.3 . .
C67 C66 C65 119.3(7) . .
C67 C66 H66 120.3 . .
C66 C67 H67 118.5 . .
C66 C67 C68 123.0(7) . .
C68 C67 H67 118.5 . .
C67 C68 H68 121.2 . .
C67 C68 C69 117.5(8) . .
C69 C68 H68 121.2 . .
C64 C69 C68 120.6(7) . .
C64 C69 H69 119.7 . .
C68 C69 H69 119.7 . .
O15 C70 H70A 109.5 . .
O15 C70 H70B 109.5 . .
O15 C70 H70C 109.5 . .
H70A C70 H70B 109.5 . .
H70A C70 H70C 109.5 . .
H70B C70 H70C 109.5 . .
C73 C72 H72 119.1 . .
C73 C72 C77 121.8(4) . .
C77 C72 H72 119.1 . .
O18 C73 C72 125.9(5) . .
O18 C73 C74 113.8(4) . .
C72 C73 C74 120.2(5) . .
C73 C74 H74 120.5 . .
C75 C74 C73 119.0(4) . .
C75 C74 H74 120.5 . .
C74 C75 H75 118.6 . .
C74 C75 C76 122.8(5) . .
C76 C75 H75 118.6 . .
C75 C76 C77 116.9(4) . .
C75 C76 C78 121.4(4) . .
C78 C76 C77 121.7(4) . .
O16 C77 C72 118.5(4) . .
O16 C77 C76 122.8(4) . .
C72 C77 C76 118.7(4) . .
O17 C78 C76 122.3(4) . .
O17 C78 C79 115.5(4) . .
C76 C78 C79 122.2(4) . .
C80 C79 C78 117.9(4) . .
C80 C79 C84 119.1(5) . .
C84 C79 C78 123.0(5) . .
C79 C80 H80 119.8 . .
C79 C80 C81 120.4(5) . .
C81 C80 H80 119.8 . .
C80 C81 H81 120.4 . .
C82 C81 C80 119.2(6) . .
C82 C81 H81 120.4 . .
C81 C82 H82 119.1 . .
C83 C82 C81 121.8(6) . .
C83 C82 H82 119.1 . .
C82 C83 H83 120.5 . .
C82 C83 C84 119.0(6) . .
C84 C83 H83 120.5 . .
C79 C84 H84 119.8 . .
C83 C84 C79 120.5(6) . .
C83 C84 H84 119.8 . .
O18 C86 H86A 109.5 . .
O18 C86 H86B 109.5 . .
O18 C86 H86C 109.5 . .
H86A C86 H86B 109.5 . .
H86A C86 H86C 109.5 . .
H86B C86 H86C 109.5 . .
O19 C87 C88 119.5(4) . .
O19 C87 C92 122.3(4) . .
C88 C87 C92 118.1(4) . .
C87 C88 H88 118.6 . .
C89 C88 C87 122.8(5) . .
C89 C88 H88 118.6 . .
O21 C89 C88 116.9(5) . .
O21 C89 C90 123.4(5) . .
C88 C89 C90 119.7(5) . .
C89 C90 H90 120.3 . .
C91 C90 C89 119.4(5) . .
C91 C90 H90 120.3 . .
C90 C91 H91 118.9 . .
C90 C91 C92 122.2(5) . .
C92 C91 H91 118.9 . .
C91 C92 C87 117.7(4) . .
C91 C92 C93 120.2(4) . .
C93 C92 C87 122.0(4) . .
O20 C93 C92 123.6(4) . .
O20 C93 C94 115.7(4) . .
C92 C93 C94 120.6(4) . .
C95 C94 C93 121.5(5) . .
C99 C94 C93 118.8(4) . .
C99 C94 C95 119.7(5) . .
C94 C95 H95 121.3 . .
C94 C95 C96 117.4(6) . .
C96 C95 H95 121.3 . .
C95 C96 H96 120.3 . .
C97 C96 C95 119.3(7) . .
C97 C96 H96 120.3 . .
C96 C97 H97 118.9 . .
C98 C97 C96 122.1(7) . .
C98 C97 H97 118.9 . .
C97 C98 H98 119.9 . .
C97 C98 C99 120.2(7) . .
C99 C98 H98 119.9 . .
C94 C99 H99 119.6 . .
C98 C99 C94 120.9(6) . .
C98 C99 H99 119.6 . .
O21 C100 H10A 109.5 . .
O21 C100 H10B 109.5 . .
O21 C100 H10C 109.5 . .
H10A C100 H10B 109.5 . .
H10A C100 H10C 109.5 . .
H10B C100 H10C 109.5 . .
O22 C101 C102 118.8(4) . .
O22 C101 C106 122.5(4) . .
C102 C101 C106 118.6(4) . .
C101 C102 H102 119.6 . .
C103 C102 C101 120.8(5) . .
C103 C102 H102 119.6 . .
O24 C103 C102 125.3(5) . .
O24 C103 C104 113.9(5) . .
C102 C103 C104 120.8(5) . .
C103 C104 H104 120.5 . .
C105 C104 C103 119.0(5) . .
C105 C104 H104 120.5 . .
C104 C105 H105 118.2 . .
C104 C105 C106 123.7(5) . .
C106 C105 H105 118.2 . .
C105 C106 C101 117.0(5) . .
C105 C106 C107 120.7(4) . .
C107 C106 C101 122.3(4) . .
O23 C107 C106 122.7(4) . .
O23 C107 C108 115.6(5) . .
C106 C107 C108 121.7(5) . .
C109 C108 C107 117.1(6) . .
C113 C108 C107 122.6(6) . .
C113 C108 C109 120.0(6) . .
C108 C109 H109 119.8 . .
C110 C109 C108 120.5(7) . .
C110 C109 H109 119.8 . .
C109 C110 H110 122.1 . .
C111 C110 C109 115.9(8) . .
C111 C110 H110 122.1 . .
C110 C111 H111 117.2 . .
C112 C111 C110 125.6(8) . .
C112 C111 H111 117.2 . .
C111 C112 H112 122.1 . .
C111 C112 C113 115.9(9) . .
C113 C112 H112 122.1 . .
C108 C113 C112 122.1(8) . .
C108 C113 H113 119.0 . .
C112 C113 H113 119.0 . .
O24 C114 H11A 109.5 . .
O24 C114 H11B 109.5 . .
O24 C114 H11C 109.5 . .
H11A C114 H11B 109.5 . .
H11A C114 H11C 109.5 . .
H11B C114 H11C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 Eu2 3.6591(3) .
Eu1 Eu4 3.6648(3) 2
Eu1 Eu5 3.7528(2) .
Eu1 O1 2.293(3) .
Eu1 O2 2.364(3) .
Eu1 O4 2.402(3) .
Eu1 O5 2.403(3) .
Eu1 O19 2.453(3) 2
Eu1 O25 2.336(2) 2
Eu1 O28 2.361(3) .
Eu1 O29 2.606(2) .
Eu2 Eu3 3.6630(3) .
Eu2 Eu5 3.7576(2) .
Eu2 O5 2.439(3) .
Eu2 O7 2.361(3) .
Eu2 O8 2.288(3) .
Eu2 O10 2.403(3) .
Eu2 O11 2.410(3) .
Eu2 O27 2.356(2) .
Eu2 O28 2.358(2) .
Eu2 O29 2.636(2) .
Eu3 Eu4 3.6515(3) 2
Eu3 Eu5 3.7193(3) .
Eu3 O11 2.437(3) .
Eu3 O13 2.382(3) .
Eu3 O14 2.288(3) .
Eu3 O22 2.446(3) 2
Eu3 O23 2.383(3) 2
Eu3 O26 2.340(2) .
Eu3 O27 2.350(2) .
Eu3 O29 2.571(2) .
Eu4 Eu1 3.6646(3) 2
Eu4 Eu3 3.6515(3) 2
Eu4 Eu5 3.7709(2) .
Eu4 O16 2.298(3) .
Eu4 O17 2.382(3) .
Eu4 O19 2.422(3) .
Eu4 O20 2.418(3) .
Eu4 O22 2.509(3) .
Eu4 O25 2.371(2) .
Eu4 O26 2.338(3) 2
Eu4 O29 2.575(2) 2
Eu5 Eu3 3.7192(2) 2
Eu5 O25 2.472(2) .
Eu5 O25 2.472(2) 2
Eu5 O26 2.466(2) 2
Eu5 O26 2.466(2) .
Eu5 O27 2.455(2) 2
Eu5 O27 2.455(2) .
Eu5 O28 2.457(2) 2
Eu5 O28 2.457(2) .
Eu5 O29 2.934(3) .
Eu5 O29 2.934(3) 2
O1 C1 1.306(5) .
O2 C7 1.250(5) .
O3 C3 1.363(7) .
O3 C14 1.426(9) .
O4 C21 1.238(5) .
O5 C15 1.328(5) .
O6 C17 1.372(7) .
O6 C28 1.353(10) .
O7 C35 1.248(5) .
O8 C29 1.298(5) .
O9 C31 1.368(6) .
O9 C42 1.407(8) .
O10 C49 1.236(5) .
O11 C43 1.335(5) .
O12 C45 1.361(7) .
O12 C56 1.373(9) .
O13 C63 1.240(5) .
O14 C57 1.312(5) .
O15 C59 1.369(6) .
O15 C70 1.418(8) .
O16 C77 1.307(4) .
O17 C78 1.257(5) .
O18 C73 1.354(6) .
O18 C86 1.417(8) .
O19 Eu1 2.454(3) 2
O19 C87 1.331(5) .
O20 C93 1.248(5) .
O21 C89 1.344(6) .
O21 C100 1.452(8) .
O22 Eu3 2.446(3) 2
O22 C101 1.329(5) .
O23 Eu3 2.383(3) 2
O23 C107 1.245(6) .
O24 C103 1.344(6) .
O24 C114 1.388(8) .
O25 Eu1 2.336(2) 2
O26 Eu4 2.338(3) 2
O29 Eu4 2.575(2) 2
C1 C2 1.401(6) .
C1 C6 1.423(6) .
C2 H2 0.9300 .
C2 C3 1.362(7) .
C3 C4 1.384(8) .
C4 H4 0.9300 .
C4 C5 1.370(8) .
C5 H5 0.9300 .
C5 C6 1.411(6) .
C6 C7 1.420(6) .
C7 C8 1.491(6) .
C8 C9 1.375(7) .
C8 C13 1.361(7) .
C9 H9 0.9300 .
C9 C10 1.402(8) .
C10 H10 0.9300 .
C10 C11 1.360(9) .
C11 H11 0.9300 .
C11 C12 1.351(10) .
C12 H12 0.9300 .
C12 C13 1.380(9) .
C13 H13 0.9300 .
C14 H14A 0.9600 .
C14 H14B 0.9600 .
C14 H14C 0.9600 .
C15 C16 1.363(6) .
C15 C20 1.435(6) .
C16 H16 0.9300 .
C16 C17 1.383(7) .
C17 C18 1.395(8) .
C18 H18 0.9300 .
C18 C19 1.361(8) .
C19 H19 0.9300 .
C19 C20 1.401(7) .
C20 C21 1.419(6) .
C21 C22 1.492(6) .
C22 C23 1.403(7) .
C22 C27 1.386(7) .
C23 H23 0.9300 .
C23 C24 1.382(8) .
C24 H24 0.9300 .
C24 C25 1.349(10) .
C25 H25 0.9300 .
C25 C26 1.358(9) .
C26 H26 0.9300 .
C26 C27 1.372(7) .
C27 H27 0.9300 .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
C29 C30 1.407(6) .
C29 C34 1.415(6) .
C30 H30 0.9300 .
C30 C31 1.388(7) .
C31 C32 1.404(8) .
C32 H32 0.9300 .
C32 C33 1.334(8) .
C33 H33 0.9300 .
C33 C34 1.438(6) .
C34 C35 1.423(7) .
C35 C36 1.491(7) .
C36 C37 1.345(9) .
C36 C41 1.407(9) .
C37 H37 0.9300 .
C37 C38 1.416(11) .
C38 H38 0.9300 .
C38 C39 1.346(14) .
C39 H39 0.9300 .
C39 C40 1.324(11) .
C40 H40 0.9300 .
C40 C41 1.422(10) .
C41 H41 0.9300 .
C42 H42A 0.9600 .
C42 H42B 0.9600 .
C42 H42C 0.9600 .
C43 C44 1.371(6) .
C43 C48 1.414(6) .
C44 H44 0.9300 .
C44 C45 1.367(7) .
C45 C46 1.382(9) .
C46 H46 0.9300 .
C46 C47 1.336(8) .
C47 H47 0.9300 .
C47 C48 1.411(7) .
C48 C49 1.451(7) .
C49 C50 1.500(6) .
C50 C51 1.356(7) .
C50 C55 1.364(7) .
C51 H51 0.9300 .
C51 C52 1.385(8) .
C52 H52 0.9300 .
C52 C53 1.333(9) .
C53 H53 0.9300 .
C53 C54 1.354(9) .
C54 H54 0.9300 .
C54 C55 1.400(7) .
C55 H55 0.9300 .
C56 H56A 0.9600 .
C56 H56B 0.9600 .
C56 H56C 0.9600 .
C57 C58 1.411(6) .
C57 C62 1.422(6) .
C58 H58 0.9300 .
C58 C59 1.367(6) .
C59 C60 1.408(7) .
C60 H60 0.9300 .
C60 C61 1.364(7) .
C61 H61 0.9300 .
C61 C62 1.418(6) .
C62 C63 1.436(7) .
C63 C64 1.504(6) .
C64 C65 1.382(8) .
C64 C69 1.359(8) .
C65 H65 0.9300 .
C65 C66 1.384(8) .
C66 H66 0.9300 .
C66 C67 1.329(10) .
C67 H67 0.9300 .
C67 C68 1.360(10) .
C68 H68 0.9300 .
C68 C69 1.411(8) .
C69 H69 0.9300 .
C70 H70A 0.9600 .
C70 H70B 0.9600 .
C70 H70C 0.9600 .
C72 H72 0.9300 .
C72 C73 1.374(6) .
C72 C77 1.399(6) .
C73 C74 1.395(7) .
C74 H74 0.9300 .
C74 C75 1.372(7) .
C75 H75 0.9300 .
C75 C76 1.421(6) .
C76 C77 1.431(6) .
C76 C78 1.429(6) .
C78 C79 1.505(6) .
C79 C80 1.367(7) .
C79 C84 1.392(7) .
C80 H80 0.9300 .
C80 C81 1.382(7) .
C81 H81 0.9300 .
C81 C82 1.371(8) .
C82 H82 0.9300 .
C82 C83 1.349(9) .
C83 H83 0.9300 .
C83 C84 1.383(7) .
C84 H84 0.9300 .
C86 H86A 0.9600 .
C86 H86B 0.9600 .
C86 H86C 0.9600 .
C87 C88 1.392(6) .
C87 C92 1.433(6) .
C88 H88 0.9300 .
C88 C89 1.351(7) .
C89 C90 1.399(7) .
C90 H90 0.9300 .
C90 C91 1.372(7) .
C91 H91 0.9300 .
C91 C92 1.400(6) .
C92 C93 1.428(6) .
C93 C94 1.492(6) .
C94 C95 1.383(7) .
C94 C99 1.382(7) .
C95 H95 0.9300 .
C95 C96 1.434(9) .
C96 H96 0.9300 .
C96 C97 1.361(10) .
C97 H97 0.9300 .
C97 C98 1.316(10) .
C98 H98 0.9300 .
C98 C99 1.370(8) .
C99 H99 0.9300 .
C100 H10A 0.9600 .
C100 H10B 0.9600 .
C100 H10C 0.9600 .
C101 C102 1.406(6) .
C101 C106 1.440(6) .
C102 H102 0.9300 .
C102 C103 1.375(7) .
C103 C104 1.400(7) .
C104 H104 0.9300 .
C104 C105 1.340(8) .
C105 H105 0.9300 .
C105 C106 1.410(6) .
C106 C107 1.423(7) .
C107 C108 1.492(7) .
C108 C109 1.398(9) .
C108 C113 1.355(9) .
C109 H109 0.9300 .
C109 C110 1.397(8) .
C110 H110 0.9300 .
C110 C111 1.384(11) .
C111 H111 0.9300 .
C111 C112 1.367(12) .
C112 H112 0.9300 .
C112 C113 1.393(9) .
C113 H113 0.9300 .
C114 H11A 0.9600 .
C114 H11B 0.9600 .
C114 H11C 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
Eu1 Eu2 Eu3 Eu4 0.645(7) . 2
Eu1 Eu2 Eu3 Eu5 -56.070(5) . .
Eu1 Eu2 Eu3 O11 111.17(10) . .
Eu1 Eu2 Eu3 O13 170.86(9) . .
Eu1 Eu2 Eu3 O14 -118.49(8) . .
Eu1 Eu2 Eu3 O22 41.59(7) . 2
Eu1 Eu2 Eu3 O23 115.9(2) . 2
Eu1 Eu2 Eu3 O26 -37.50(6) . .
Eu1 Eu2 Eu3 O27 -101.33(9) . .
Eu1 Eu2 Eu3 O29 7.15(8) . .
Eu1 Eu2 O5 C15 169.3(4) . .
Eu1 Eu2 O7 C35 142.1(5) . .
Eu1 Eu2 O8 C29 -115.6(4) . .
Eu1 Eu2 O10 C49 -62.3(6) . .
Eu1 Eu2 O11 Eu3 -73.45(9) . .
Eu1 Eu2 O11 C43 119.5(4) . .
Eu1 Eu2 O27 Eu3 80.84(7) . .
Eu1 Eu2 O27 Eu5 -24.04(8) . .
Eu1 Eu2 O28 Eu5 105.61(11) . .
Eu1 Eu2 O29 Eu3 -169.93(11) . .
Eu1 Eu2 O29 Eu4 -81.1(6) . 2
Eu1 Eu2 O29 Eu5 -85.17(7) . .
Eu1 Eu4 O16 C77 129.2(3) 2 .
Eu1 Eu4 O17 C78 -90.6(7) 2 .
Eu1 Eu4 O19 C87 -162.9(4) 2 .
Eu1 Eu4 O20 C93 38.5(5) 2 .
Eu1 Eu4 O22 Eu3 71.72(8) 2 2
Eu1 Eu4 O22 C101 -131.1(3) 2 .
Eu1 Eu4 O25 Eu5 -105.97(11) 2 .
Eu1 O1 C1 C2 -145.0(4) . .
Eu1 O1 C1 C6 36.1(6) . .
Eu1 O2 C7 C6 -9.3(7) . .
Eu1 O2 C7 C8 168.4(3) . .
Eu1 O4 C21 C20 0.4(9) . .
Eu1 O4 C21 C22 -177.6(4) . .
Eu1 O5 C15 C16 -146.0(4) . .
Eu1 O5 C15 C20 34.6(6) . .
Eu1 O19 C87 C88 51.5(5) 2 .
Eu1 O19 C87 C92 -128.0(4) 2 .
Eu2 Eu1 O1 C1 133.5(3) . .
Eu2 Eu1 O2 C7 -110.5(5) . .
Eu2 Eu1 O4 C21 49.8(5) . .
Eu2 Eu1 O5 C15 -168.5(4) . .
Eu2 Eu1 O28 Eu5 -105.82(11) . .
Eu2 Eu1 O29 Eu3 78.5(6) . .
Eu2 Eu1 O29 Eu4 170.86(11) . 2
Eu2 Eu1 O29 Eu5 84.76(7) . .
Eu2 Eu3 Eu5 Eu3 -159.284(6) . 2
Eu2 Eu3 Eu5 O25 91.12(5) . 2
Eu2 Eu3 Eu5 O25 -62.55(6) . .
Eu2 Eu3 Eu5 O26 -130.27(6) . 2
Eu2 Eu3 Eu5 O26 150.93(10) . .
Eu2 Eu3 Eu5 O27 -43.62(9) . .
Eu2 Eu3 Eu5 O27 162.86(6) . 2
Eu2 Eu3 Eu5 O28 37.2(2) . 2
Eu2 Eu3 Eu5 O28 16.57(6) . .
Eu2 Eu3 Eu5 O29 54.86(6) . .
Eu2 Eu3 Eu5 O29 -126.55(6) . 2
Eu2 Eu3 O11 C43 168.6(4) . .
Eu2 Eu3 O13 C63 137.8(5) . .
Eu2 Eu3 O14 C57 -119.8(3) . .
Eu2 Eu3 O26 Eu4 81.28(7) . 2
Eu2 Eu3 O26 Eu5 -25.43(8) . .
Eu2 Eu3 O27 Eu5 105.87(12) . .
Eu2 Eu3 O29 Eu1 -78.4(6) . .
Eu2 Eu3 O29 Eu4 -170.75(11) . 2
Eu2 Eu3 O29 Eu5 -84.69(7) . .
Eu2 O5 C15 C16 48.5(5) . .
Eu2 O5 C15 C20 -130.9(4) . .
Eu2 O7 C35 C34 -8.5(8) . .
Eu2 O7 C35 C36 168.7(4) . .
Eu2 O8 C29 C30 -149.9(3) . .
Eu2 O8 C29 C34 30.8(6) . .
Eu2 O10 C49 C48 0.2(9) . .
Eu2 O10 C49 C50 -179.8(4) . .
Eu2 O11 C43 C44 -147.1(4) . .
Eu2 O11 C43 C48 33.1(6) . .
Eu3 Eu2 O5 Eu1 72.27(8) . .
Eu3 Eu2 O5 C15 -118.4(3) . .
Eu3 Eu2 O7 C35 -118.4(5) . .
Eu3 Eu2 O8 C29 139.6(3) . .
Eu3 Eu2 O10 C49 44.0(6) . .
Eu3 Eu2 O11 C43 -167.0(4) . .
Eu3 Eu2 O27 Eu5 -104.87(12) . .
Eu3 Eu2 O28 Eu1 -81.68(7) . .
Eu3 Eu2 O28 Eu5 23.93(8) . .
Eu3 Eu2 O29 Eu1 169.93(11) . .
Eu3 Eu2 O29 Eu4 88.8(6) . 2
Eu3 Eu2 O29 Eu5 84.76(7) . .
Eu3 Eu4 O16 C77 -127.9(3) 2 .
Eu3 Eu4 O17 C78 147.7(4) 2 .
Eu3 Eu4 O19 Eu1 -73.69(8) 2 2
Eu3 Eu4 O19 C87 123.4(4) 2 .
Eu3 Eu4 O20 C93 -68.2(6) 2 .
Eu3 Eu4 O22 C101 157.2(4) 2 .
Eu3 Eu4 O25 Eu1 81.62(7) 2 2
Eu3 Eu4 O25 Eu5 -24.35(8) 2 .
Eu3 Eu5 O25 Eu1 175.27(6) . 2
Eu3 Eu5 O25 Eu1 -81.96(8) 2 2
Eu3 Eu5 O25 Eu4 23.76(8) 2 .
Eu3 Eu5 O25 Eu4 -79.01(8) . .
Eu3 Eu5 O26 Eu3 -129.53(8) 2 .
Eu3 Eu5 O26 Eu4 124.38(8) 2 2
Eu3 Eu5 O26 Eu4 -106.08(13) . 2
Eu3 Eu5 O27 Eu2 105.50(12) . .
Eu3 Eu5 O27 Eu2 -178.06(5) 2 .
Eu3 Eu5 O27 Eu3 76.44(9) 2 .
Eu3 Eu5 O28 Eu1 -114.5(2) 2 .
Eu3 Eu5 O28 Eu1 81.68(7) . .
Eu3 Eu5 O28 Eu2 -23.43(8) . .
Eu3 Eu5 O28 Eu2 140.42(16) 2 .
Eu3 Eu5 O29 Eu1 -178.88(9) . .
Eu3 Eu5 O29 Eu1 130.70(4) 2 .
Eu3 Eu5 O29 Eu2 -89.89(7) . .
Eu3 Eu5 O29 Eu2 -140.31(3) 2 .
Eu3 Eu5 O29 Eu3 -50.41(8) 2 .
Eu3 Eu5 O29 Eu4 90.75(7) . 2
Eu3 Eu5 O29 Eu4 40.34(9) 2 2
Eu3 O11 C43 C44 48.8(6) . .
Eu3 O11 C43 C48 -131.0(4) . .
Eu3 O13 C63 C62 -1.0(8) . .
Eu3 O13 C63 C64 177.6(3) . .
Eu3 O14 C57 C58 -143.3(3) . .
Eu3 O14 C57 C62 36.3(6) . .
Eu3 O22 C101 C102 -168.4(3) 2 .
Eu3 O22 C101 C106 8.4(6) 2 .
Eu3 O23 C107 C106 -55.5(7) 2 .
Eu3 O23 C107 C108 123.1(4) 2 .
Eu4 Eu1 Eu2 Eu3 -0.642(6) 2 .
Eu4 Eu1 Eu2 Eu5 -56.183(6) 2 .
Eu4 Eu1 Eu2 O5 111.81(10) 2 .
Eu4 Eu1 Eu2 O7 169.54(9) 2 .
Eu4 Eu1 Eu2 O8 -120.38(8) 2 .
Eu4 Eu1 Eu2 O10 107.93(16) 2 .
Eu4 Eu1 Eu2 O11 38.50(7) 2 .
Eu4 Eu1 Eu2 O27 -38.88(6) 2 .
Eu4 Eu1 Eu2 O28 -100.95(9) 2 .
Eu4 Eu1 Eu2 O29 6.41(8) 2 .
Eu4 Eu1 O1 C1 -121.3(3) 2 .
Eu4 Eu1 O2 C7 144.4(4) 2 .
Eu4 Eu1 O4 C21 -58.2(6) 2 .
Eu4 Eu1 O5 Eu2 -73.50(8) 2 .
Eu4 Eu1 O5 C15 118.0(3) 2 .
Eu4 Eu1 O28 Eu2 81.69(7) 2 .
Eu4 Eu1 O28 Eu5 -24.13(8) 2 .
Eu4 Eu1 O29 Eu2 -170.86(11) 2 .
Eu4 Eu1 O29 Eu3 -92.3(6) 2 .
Eu4 Eu1 O29 Eu5 -86.10(7) 2 .
Eu4 Eu3 Eu5 Eu3 92.686(5) 2 2
Eu4 Eu3 Eu5 O25 -170.58(6) 2 .
Eu4 Eu3 Eu5 O25 -16.91(5) 2 2
Eu4 Eu3 Eu5 O26 121.70(6) 2 2
Eu4 Eu3 Eu5 O26 42.90(10) 2 .
Eu4 Eu3 Eu5 O27 -151.65(9) 2 .
Eu4 Eu3 Eu5 O27 54.83(6) 2 2
Eu4 Eu3 Eu5 O28 -91.46(6) 2 .
Eu4 Eu3 Eu5 O28 -70.9(2) 2 2
Eu4 Eu3 Eu5 O29 125.42(6) 2 2
Eu4 Eu3 Eu5 O29 -53.17(6) 2 .
Eu4 Eu3 O11 Eu2 74.46(9) 2 .
Eu4 Eu3 O11 C43 -116.9(3) 2 .
Eu4 Eu3 O13 C63 -119.3(5) 2 .
Eu4 Eu3 O14 C57 135.5(3) 2 .
Eu4 Eu3 O26 Eu5 -106.71(11) 2 .
Eu4 Eu3 O27 Eu2 -80.95(7) 2 .
Eu4 Eu3 O27 Eu5 24.92(8) 2 .
Eu4 Eu3 O29 Eu1 92.3(6) 2 .
Eu4 Eu3 O29 Eu2 170.75(11) 2 .
Eu4 Eu3 O29 Eu5 86.06(7) 2 .
Eu4 O16 C77 C72 -142.3(3) . .
Eu4 O16 C77 C76 40.1(6) . .
Eu4 O17 C78 C76 -4.0(7) . .
Eu4 O17 C78 C79 177.3(3) . .
Eu4 O19 C87 C88 -149.3(3) . .
Eu4 O19 C87 C92 31.2(6) . .
Eu4 O20 C93 C92 7.7(8) . .
Eu4 O20 C93 C94 -174.7(3) . .
Eu4 O22 C101 C102 44.6(5) . .
Eu4 O22 C101 C106 -138.5(3) . .
Eu5 Eu1 Eu2 Eu3 55.541(6) . .
Eu5 Eu1 Eu2 O5 167.99(10) . .
Eu5 Eu1 Eu2 O7 -134.28(9) . .
Eu5 Eu1 Eu2 O8 -64.20(8) . .
Eu5 Eu1 Eu2 O10 164.11(16) . .
Eu5 Eu1 Eu2 O11 94.68(7) . .
Eu5 Eu1 Eu2 O27 17.31(6) . .
Eu5 Eu1 Eu2 O28 -44.76(9) . .
Eu5 Eu1 Eu2 O29 62.59(8) . .
Eu5 Eu1 O1 C1 -173.7(4) . .
Eu5 Eu1 O2 C7 90.5(4) . .
Eu5 Eu1 O4 C21 100.6(5) . .
Eu5 Eu1 O5 Eu2 -10.69(9) . .
Eu5 Eu1 O5 C15 -179.1(3) . .
Eu5 Eu1 O28 Eu2 105.82(11) . .
Eu5 Eu1 O29 Eu2 -84.76(7) . .
Eu5 Eu1 O29 Eu3 -6.2(5) . .
Eu5 Eu1 O29 Eu4 86.10(7) . 2
Eu5 Eu2 Eu3 Eu4 56.714(5) . 2
Eu5 Eu2 Eu3 O11 167.24(10) . .
Eu5 Eu2 Eu3 O13 -133.07(9) . .
Eu5 Eu2 Eu3 O14 -62.42(8) . .
Eu5 Eu2 Eu3 O22 97.66(7) . 2
Eu5 Eu2 Eu3 O23 172.0(2) . 2
Eu5 Eu2 Eu3 O26 18.57(6) . .
Eu5 Eu2 Eu3 O27 -45.26(9) . .
Eu5 Eu2 Eu3 O29 63.22(8) . .
Eu5 Eu2 O5 Eu1 10.65(9) . .
Eu5 Eu2 O5 C15 179.9(3) . .
Eu5 Eu2 O7 C35 88.8(5) . .
Eu5 Eu2 O8 C29 -167.7(4) . .
Eu5 Eu2 O10 C49 92.5(6) . .
Eu5 Eu2 O11 Eu3 -11.24(9) . .
Eu5 Eu2 O11 C43 -178.3(4) . .
Eu5 Eu2 O27 Eu3 104.87(12) . .
Eu5 Eu2 O28 Eu1 -105.61(11) . .
Eu5 Eu2 O29 Eu1 85.17(7) . .
Eu5 Eu2 O29 Eu3 -84.76(7) . .
Eu5 Eu2 O29 Eu4 4.0(6) . 2
Eu5 Eu3 O11 Eu2 11.37(9) . .
Eu5 Eu3 O11 C43 180.0(3) . .
Eu5 Eu3 O13 C63 83.7(5) . .
Eu5 Eu3 O14 C57 -171.5(3) . .
Eu5 Eu3 O26 Eu4 106.71(11) . 2
Eu5 Eu3 O27 Eu2 -105.87(12) . .
Eu5 Eu3 O29 Eu1 6.2(5) . .
Eu5 Eu3 O29 Eu2 84.69(7) . .
Eu5 Eu3 O29 Eu4 -86.06(7) . 2
Eu5 Eu4 O16 C77 -177.0(3) . .
Eu5 Eu4 O17 C78 92.3(4) . .
Eu5 Eu4 O19 Eu1 -12.02(9) . 2
Eu5 Eu4 O19 C87 -174.9(4) . .
Eu5 Eu4 O20 C93 87.6(5) . .
Eu5 Eu4 O22 Eu3 9.37(8) . 2
Eu5 Eu4 O22 C101 166.5(3) . .
Eu5 Eu4 O25 Eu1 105.97(11) . 2
O1 Eu1 Eu2 Eu3 120.50(8) . .
O1 Eu1 Eu2 Eu5 64.96(8) . .
O1 Eu1 Eu2 O5 -127.05(13) . .
O1 Eu1 Eu2 O7 -69.32(12) . .
O1 Eu1 Eu2 O8 0.76(11) . .
O1 Eu1 Eu2 O10 -130.93(18) . .
O1 Eu1 Eu2 O11 159.64(10) . .
O1 Eu1 Eu2 O27 82.27(10) . .
O1 Eu1 Eu2 O28 20.19(12) . .
O1 Eu1 Eu2 O29 127.55(11) . .
O1 Eu1 O2 C7 26.2(4) . .
O1 Eu1 O4 C21 165.1(6) . .
O1 Eu1 O5 Eu2 80.81(14) . .
O1 Eu1 O5 C15 -87.6(4) . .
O1 Eu1 O28 Eu2 -161.60(11) . .
O1 Eu1 O28 Eu5 92.58(10) . .
O1 Eu1 O29 Eu2 -84.99(13) . .
O1 Eu1 O29 Eu3 -6.5(6) . .
O1 Eu1 O29 Eu4 85.87(13) . 2
O1 Eu1 O29 Eu5 -0.22(14) . .
O1 C1 C2 C3 176.6(5) . .
O1 C1 C6 C5 -177.5(4) . .
O1 C1 C6 C7 -0.1(7) . .
O2 Eu1 Eu2 Eu3 -105.9(4) . .
O2 Eu1 Eu2 Eu5 -161.4(4) . .
O2 Eu1 Eu2 O5 6.6(4) . .
O2 Eu1 Eu2 O7 64.3(4) . .
O2 Eu1 Eu2 O8 134.4(4) . .
O2 Eu1 Eu2 O10 2.7(4) . .
O2 Eu1 Eu2 O11 -66.7(4) . .
O2 Eu1 Eu2 O27 -144.1(4) . .
O2 Eu1 Eu2 O28 153.8(4) . .
O2 Eu1 Eu2 O29 -98.8(4) . .
O2 Eu1 O1 C1 -38.5(4) . .
O2 Eu1 O4 C21 -121.7(6) . .
O2 Eu1 O5 Eu2 -178.47(10) . .
O2 Eu1 O5 C15 13.1(4) . .
O2 Eu1 O28 Eu2 -170.64(16) . .
O2 Eu1 O28 Eu5 83.5(2) . .
O2 Eu1 O29 Eu2 165.21(12) . .
O2 Eu1 O29 Eu3 -116.3(6) . .
O2 Eu1 O29 Eu4 -23.93(17) . 2
O2 Eu1 O29 Eu5 -110.02(14) . .
O2 C7 C8 C9 -43.1(6) . .
O2 C7 C8 C13 133.6(5) . .
O3 C3 C4 C5 179.6(6) . .
O4 Eu1 Eu2 Eu3 -156.97(9) . .
O4 Eu1 Eu2 Eu5 147.49(9) . .
O4 Eu1 Eu2 O5 -44.52(14) . .
O4 Eu1 Eu2 O7 13.22(12) . .
O4 Eu1 Eu2 O8 83.30(12) . .
O4 Eu1 Eu2 O10 -48.39(18) . .
O4 Eu1 Eu2 O11 -117.83(11) . .
O4 Eu1 Eu2 O27 164.80(11) . .
O4 Eu1 Eu2 O28 102.73(13) . .
O4 Eu1 Eu2 O29 -149.91(12) . .
O4 Eu1 O1 C1 39.7(4) . .
O4 Eu1 O2 C7 -57.8(4) . .
O4 Eu1 O5 Eu2 131.76(14) . .
O4 Eu1 O5 C15 -36.7(3) . .
O4 Eu1 O28 Eu2 -85.04(11) . .
O4 Eu1 O28 Eu5 169.14(10) . .
O4 Eu1 O29 Eu2 44.97(17) . .
O4 Eu1 O29 Eu3 123.5(6) . .
O4 Eu1 O29 Eu4 -144.17(14) . 2
O4 Eu1 O29 Eu5 129.73(14) . .
O4 C21 C22 C23 149.1(6) . .
O4 C21 C22 C27 -28.5(8) . .
O5 Eu1 Eu2 Eu3 -112.45(10) . .
O5 Eu1 Eu2 Eu5 -167.99(10) . .
O5 Eu1 Eu2 O7 57.74(13) . .
O5 Eu1 Eu2 O8 127.82(13) . .
O5 Eu1 Eu2 O10 -3.87(18) . .
O5 Eu1 Eu2 O11 -73.31(12) . .
O5 Eu1 Eu2 O27 -150.68(12) . .
O5 Eu1 Eu2 O28 147.25(14) . .
O5 Eu1 Eu2 O29 -105.40(13) . .
O5 Eu1 O1 C1 86.9(4) . .
O5 Eu1 O2 C7 -105.0(4) . .
O5 Eu1 O4 C21 20.0(5) . .
O5 Eu1 O28 Eu2 -21.53(9) . .
O5 Eu1 O28 Eu5 -127.35(10) . .
O5 Eu1 O29 Eu2 43.83(9) . .
O5 Eu1 O29 Eu3 122.4(6) . .
O5 Eu1 O29 Eu4 -145.31(11) . 2
O5 Eu1 O29 Eu5 128.59(10) . .
O5 Eu2 Eu3 Eu4 -37.60(7) . 2
O5 Eu2 Eu3 Eu5 -94.32(7) . .
O5 Eu2 Eu3 O11 72.92(12) . .
O5 Eu2 Eu3 O13 132.61(11) . .
O5 Eu2 Eu3 O14 -156.74(10) . .
O5 Eu2 Eu3 O22 3.34(10) . 2
O5 Eu2 Eu3 O23 77.7(2) . 2
O5 Eu2 Eu3 O26 -75.74(9) . .
O5 Eu2 Eu3 O27 -139.57(12) . .
O5 Eu2 Eu3 O29 -31.09(11) . .
O5 Eu2 O7 C35 177.6(5) . .
O5 Eu2 O8 C29 -68.5(4) . .
O5 Eu2 O10 C49 -65.0(6) . .
O5 Eu2 O11 Eu3 -111.95(10) . .
O5 Eu2 O11 C43 81.0(4) . .
O5 Eu2 O27 Eu3 56.03(14) . .
O5 Eu2 O27 Eu5 -48.84(15) . .
O5 Eu2 O28 Eu1 21.26(9) . .
O5 Eu2 O28 Eu5 126.86(11) . .
O5 Eu2 O29 Eu1 -43.42(8) . .
O5 Eu2 O29 Eu3 146.66(11) . .
O5 Eu2 O29 Eu4 -124.6(6) . 2
O5 Eu2 O29 Eu5 -128.59(9) . .
O5 C15 C16 C17 176.6(5) . .
O5 C15 C20 C19 -174.5(4) . .
O5 C15 C20 C21 3.6(7) . .
O6 C17 C18 C19 -177.3(6) . .
O7 Eu2 Eu3 Eu4 -99.1(5) . 2
O7 Eu2 Eu3 Eu5 -155.8(5) . .
O7 Eu2 Eu3 O11 11.4(5) . .
O7 Eu2 Eu3 O13 71.1(5) . .
O7 Eu2 Eu3 O14 141.8(5) . .
O7 Eu2 Eu3 O22 -58.1(5) . 2
O7 Eu2 Eu3 O23 16.2(5) . 2
O7 Eu2 Eu3 O26 -137.2(5) . .
O7 Eu2 Eu3 O27 158.9(5) . .
O7 Eu2 Eu3 O29 -92.6(5) . .
O7 Eu2 O5 Eu1 -116.96(13) . .
O7 Eu2 O5 C15 52.3(3) . .
O7 Eu2 O8 C29 -33.4(4) . .
O7 Eu2 O10 C49 -127.8(6) . .
O7 Eu2 O11 Eu3 -177.47(11) . .
O7 Eu2 O11 C43 15.5(4) . .
O7 Eu2 O27 Eu3 -172.80(18) . .
O7 Eu2 O27 Eu5 82.3(2) . .
O7 Eu2 O28 Eu1 91.73(11) . .
O7 Eu2 O28 Eu5 -162.66(11) . .
O7 Eu2 O29 Eu1 -24.21(17) . .
O7 Eu2 O29 Eu3 165.86(13) . .
O7 Eu2 O29 Eu4 -105.4(6) . 2
O7 Eu2 O29 Eu5 -109.38(14) . .
O7 C35 C36 C37 -47.3(8) . .
O7 C35 C36 C41 127.2(6) . .
O8 Eu2 Eu3 Eu4 122.54(8) . 2
O8 Eu2 Eu3 Eu5 65.82(8) . .
O8 Eu2 Eu3 O11 -126.94(13) . .
O8 Eu2 Eu3 O13 -67.25(12) . .
O8 Eu2 Eu3 O14 3.41(11) . .
O8 Eu2 Eu3 O22 163.49(10) . 2
O8 Eu2 Eu3 O23 -122.2(2) . 2
O8 Eu2 Eu3 O26 84.40(10) . .
O8 Eu2 Eu3 O27 20.57(12) . .
O8 Eu2 Eu3 O29 129.05(11) . .
O8 Eu2 O5 Eu1 -81.92(14) . .
O8 Eu2 O5 C15 87.4(3) . .
O8 Eu2 O7 C35 22.7(5) . .
O8 Eu2 O10 C49 159.2(6) . .
O8 Eu2 O11 Eu3 80.76(14) . .
O8 Eu2 O11 C43 -86.3(4) . .
O8 Eu2 O27 Eu3 -161.27(11) . .
O8 Eu2 O27 Eu5 93.86(10) . .
O8 Eu2 O28 Eu1 162.80(11) . .
O8 Eu2 O28 Eu5 -91.59(10) . .
O8 Eu2 O29 Eu1 87.65(13) . .
O8 Eu2 O29 Eu3 -82.28(13) . .
O8 Eu2 O29 Eu4 6.5(7) . 2
O8 Eu2 O29 Eu5 2.48(13) . .
O8 C29 C30 C31 175.5(4) . .
O8 C29 C34 C33 -176.6(4) . .
O8 C29 C34 C35 0.7(7) . .
O9 C31 C32 C33 178.1(6) . .
O10 Eu2 Eu3 Eu4 -152.34(9) . 2
O10 Eu2 Eu3 Eu5 150.94(9) . .
O10 Eu2 Eu3 O11 -41.82(14) . .
O10 Eu2 Eu3 O13 17.87(13) . .
O10 Eu2 Eu3 O14 88.52(12) . .
O10 Eu2 Eu3 O22 -111.40(11) . 2
O10 Eu2 Eu3 O23 -37.1(2) . 2
O10 Eu2 Eu3 O26 169.52(11) . .
O10 Eu2 Eu3 O27 105.69(13) . .
O10 Eu2 Eu3 O29 -145.83(12) . .
O10 Eu2 O5 Eu1 178.03(9) . .
O10 Eu2 O5 C15 -12.7(3) . .
O10 Eu2 O7 C35 -63.4(5) . .
O10 Eu2 O8 C29 43.5(4) . .
O10 Eu2 O11 Eu3 134.97(14) . .
O10 Eu2 O11 C43 -32.1(4) . .
O10 Eu2 O27 Eu3 -83.46(11) . .
O10 Eu2 O27 Eu5 171.67(10) . .
O10 Eu2 O28 Eu1 135.9(3) . .
O10 Eu2 O28 Eu5 -118.5(3) . .
O10 Eu2 O29 Eu1 -140.43(13) . .
O10 Eu2 O29 Eu3 49.65(16) . .
O10 Eu2 O29 Eu4 138.4(6) . 2
O10 Eu2 O29 Eu5 134.40(13) . .
O10 C49 C50 C51 141.4(5) . .
O10 C49 C50 C55 -34.8(7) . .
O11 Eu2 Eu3 Eu4 -110.52(10) . 2
O11 Eu2 Eu3 Eu5 -167.24(10) . .
O11 Eu2 Eu3 O13 59.69(14) . .
O11 Eu2 Eu3 O14 130.34(13) . .
O11 Eu2 Eu3 O22 -69.58(12) . 2
O11 Eu2 Eu3 O23 4.8(2) . 2
O11 Eu2 Eu3 O26 -148.66(12) . .
O11 Eu2 Eu3 O27 147.51(14) . .
O11 Eu2 Eu3 O29 -104.01(13) . .
O11 Eu2 O5 Eu1 111.28(10) . .
O11 Eu2 O5 C15 -79.4(3) . .
O11 Eu2 O7 C35 -108.7(5) . .
O11 Eu2 O8 C29 93.3(4) . .
O11 Eu2 O10 C49 15.8(5) . .
O11 Eu2 O27 Eu3 -21.36(9) . .
O11 Eu2 O27 Eu5 -126.23(11) . .
O11 Eu2 O28 Eu1 -56.01(14) . .
O11 Eu2 O28 Eu5 49.60(15) . .
O11 Eu2 O29 Eu1 -145.20(11) . .
O11 Eu2 O29 Eu3 44.87(9) . .
O11 Eu2 O29 Eu4 133.7(6) . 2
O11 Eu2 O29 Eu5 129.63(10) . .
O11 Eu3 Eu5 Eu3 -167.71(7) . 2
O11 Eu3 Eu5 O25 82.69(9) . 2
O11 Eu3 Eu5 O25 -70.98(9) . .
O11 Eu3 Eu5 O26 -138.70(9) . 2
O11 Eu3 Eu5 O26 142.50(12) . .
O11 Eu3 Eu5 O27 154.43(10) . 2
O11 Eu3 Eu5 O27 -52.05(12) . .
O11 Eu3 Eu5 O28 8.14(9) . .
O11 Eu3 Eu5 O28 28.7(2) . 2
O11 Eu3 Eu5 O29 -134.98(9) . 2
O11 Eu3 Eu5 O29 46.43(9) . .
O11 Eu3 O13 C63 174.0(5) . .
O11 Eu3 O14 C57 -74.3(4) . .
O11 Eu3 O26 Eu4 54.76(14) . 2
O11 Eu3 O26 Eu5 -51.95(15) . .
O11 Eu3 O27 Eu2 21.16(9) . .
O11 Eu3 O27 Eu5 127.02(10) . .
O11 Eu3 O29 Eu1 -122.4(6) . .
O11 Eu3 O29 Eu2 -43.95(8) . .
O11 Eu3 O29 Eu4 145.30(11) . 2
O11 Eu3 O29 Eu5 -128.64(9) . .
O11 C43 C44 C45 178.1(6) . .
O11 C43 C48 C47 -178.1(5) . .
O11 C43 C48 C49 -1.8(7) . .
O12 C45 C46 C47 -179.3(8) . .
O13 Eu3 Eu5 Eu3 -91.76(10) . 2
O13 Eu3 Eu5 O25 158.65(11) . 2
O13 Eu3 Eu5 O25 4.97(11) . .
O13 Eu3 Eu5 O26 -141.54(14) . .
O13 Eu3 Eu5 O26 -62.74(11) . 2
O13 Eu3 Eu5 O27 -129.61(12) . 2
O13 Eu3 Eu5 O27 23.90(14) . .
O13 Eu3 Eu5 O28 84.10(11) . .
O13 Eu3 Eu5 O28 104.7(2) . 2
O13 Eu3 Eu5 O29 -59.02(12) . 2
O13 Eu3 Eu5 O29 122.39(12) . .
O13 Eu3 O11 Eu2 -115.02(13) . .
O13 Eu3 O11 C43 53.6(3) . .
O13 Eu3 O14 C57 -37.2(3) . .
O13 Eu3 O26 Eu4 -171.61(17) . 2
O13 Eu3 O26 Eu5 81.7(2) . .
O13 Eu3 O27 Eu2 92.81(11) . .
O13 Eu3 O27 Eu5 -161.33(11) . .
O13 Eu3 O29 Eu1 -102.0(6) . .
O13 Eu3 O29 Eu2 -23.53(17) . .
O13 Eu3 O29 Eu4 165.72(13) . 2
O13 Eu3 O29 Eu5 -108.22(14) . .
O13 C63 C64 C65 127.0(5) . .
O13 C63 C64 C69 -47.3(7) . .
O14 Eu3 Eu5 Eu3 -32.33(7) . 2
O14 Eu3 Eu5 O25 64.40(9) . .
O14 Eu3 Eu5 O25 -141.93(9) . 2
O14 Eu3 Eu5 O26 -82.12(12) . .
O14 Eu3 Eu5 O26 -3.31(9) . 2
O14 Eu3 Eu5 O27 83.33(12) . .
O14 Eu3 Eu5 O27 -70.18(9) . 2
O14 Eu3 Eu5 O28 143.52(9) . .
O14 Eu3 Eu5 O28 164.1(2) . 2
O14 Eu3 Eu5 O29 0.41(10) . 2
O14 Eu3 Eu5 O29 -178.19(10) . .
O14 Eu3 O11 Eu2 -78.04(15) . .
O14 Eu3 O11 C43 90.6(4) . .
O14 Eu3 O13 C63 20.1(4) . .
O14 Eu3 O26 Eu4 -162.74(11) . 2
O14 Eu3 O26 Eu5 90.55(10) . .
O14 Eu3 O27 Eu2 164.46(11) . .
O14 Eu3 O27 Eu5 -89.67(10) . .
O14 Eu3 O29 Eu1 8.7(6) . .
O14 Eu3 O29 Eu2 87.16(12) . .
O14 Eu3 O29 Eu4 -83.59(13) . 2
O14 Eu3 O29 Eu5 2.47(13) . .
O14 C57 C58 C59 176.6(4) . .
O14 C57 C62 C61 -176.7(4) . .
O14 C57 C62 C63 0.2(7) . .
O15 C59 C60 C61 179.6(5) . .
O16 Eu4 O17 C78 27.6(4) . .
O16 Eu4 O19 Eu1 77.48(14) . 2
O16 Eu4 O19 C87 -85.4(4) . .
O16 Eu4 O20 C93 149.8(5) . .
O16 Eu4 O22 Eu3 -81.87(14) . 2
O16 Eu4 O22 C101 75.3(3) . .
O16 Eu4 O25 Eu1 -159.37(12) . 2
O16 Eu4 O25 Eu5 94.66(10) . .
O17 Eu4 O16 C77 -44.6(3) . .
O17 Eu4 O19 Eu1 178.33(9) . 2
O17 Eu4 O19 C87 15.4(4) . .
O17 Eu4 O20 C93 -138.0(5) . .
O17 Eu4 O22 Eu3 -115.04(12) . 2
O17 Eu4 O22 C101 42.1(3) . .
O17 Eu4 O25 Eu1 -172.08(13) . 2
O17 Eu4 O25 Eu5 81.95(18) . .
O17 C78 C79 C80 -26.3(7) . .
O17 C78 C79 C84 150.7(5) . .
O18 C73 C74 C75 -177.0(5) . .
O19 Eu1 Eu2 Eu3 -39.81(7) 2 .
O19 Eu1 Eu2 Eu5 -95.35(7) 2 .
O19 Eu1 Eu2 O5 72.64(12) 2 .
O19 Eu1 Eu2 O7 130.37(11) 2 .
O19 Eu1 Eu2 O8 -159.55(10) 2 .
O19 Eu1 Eu2 O10 68.76(17) 2 .
O19 Eu1 Eu2 O11 -0.67(9) 2 .
O19 Eu1 Eu2 O27 -78.04(9) 2 .
O19 Eu1 Eu2 O28 -140.11(11) 2 .
O19 Eu1 Eu2 O29 -32.76(10) 2 .
O19 Eu1 O1 C1 -74.7(4) 2 .
O19 Eu1 O2 C7 -179.3(5) 2 .
O19 Eu1 O4 C21 -58.8(6) 2 .
O19 Eu1 O5 Eu2 -111.84(10) 2 .
O19 Eu1 O5 C15 79.7(4) 2 .
O19 Eu1 O28 Eu2 55.31(14) 2 .
O19 Eu1 O28 Eu5 -50.51(14) 2 .
O19 Eu1 O29 Eu2 144.41(11) 2 .
O19 Eu1 O29 Eu3 -137.1(6) 2 .
O19 Eu1 O29 Eu4 -44.73(8) 2 2
O19 Eu1 O29 Eu5 -130.82(9) 2 .
O19 Eu4 O16 C77 84.7(3) . .
O19 Eu4 O17 C78 -100.3(4) . .
O19 Eu4 O20 C93 9.5(5) . .
O19 Eu4 O22 Eu3 110.80(9) . 2
O19 Eu4 O22 C101 -92.0(3) . .
O19 Eu4 O25 Eu1 -20.85(9) . 2
O19 Eu4 O25 Eu5 -126.82(10) . .
O19 C87 C88 C89 177.8(4) . .
O19 C87 C92 C91 -177.2(4) . .
O19 C87 C92 C93 -1.2(7) . .
O20 Eu4 O16 C77 33.0(3) . .
O20 Eu4 O17 C78 -58.0(4) . .
O20 Eu4 O19 Eu1 133.95(13) . 2
O20 Eu4 O19 C87 -29.0(4) . .
O20 Eu4 O22 Eu3 177.63(9) . 2
O20 Eu4 O22 C101 -25.2(3) . .
O20 Eu4 O25 Eu1 -83.09(11) . 2
O20 Eu4 O25 Eu5 170.94(9) . .
O20 C93 C94 C95 145.0(6) . .
O20 C93 C94 C99 -34.5(7) . .
O21 C89 C90 C91 -178.3(5) . .
O22 Eu3 Eu5 Eu3 100.16(7) 2 2
O22 Eu3 Eu5 O25 -163.11(9) 2 .
O22 Eu3 Eu5 O25 -9.44(8) 2 2
O22 Eu3 Eu5 O26 129.17(9) 2 2
O22 Eu3 Eu5 O26 50.37(12) 2 .
O22 Eu3 Eu5 O27 -144.18(12) 2 .
O22 Eu3 Eu5 O27 62.30(9) 2 2
O22 Eu3 Eu5 O28 -63.4(2) 2 2
O22 Eu3 Eu5 O28 -83.99(9) 2 .
O22 Eu3 Eu5 O29 -45.70(9) 2 .
O22 Eu3 Eu5 O29 132.89(9) 2 2
O22 Eu3 O11 Eu2 115.64(10) 2 .
O22 Eu3 O11 C43 -75.8(3) 2 .
O22 Eu3 O13 C63 -110.8(5) 2 .
O22 Eu3 O14 C57 86.8(4) 2 .
O22 Eu3 O26 Eu4 -23.38(9) 2 2
O22 Eu3 O26 Eu5 -130.09(10) 2 .
O22 Eu3 O27 Eu2 -53.76(15) 2 .
O22 Eu3 O27 Eu5 52.11(15) 2 .
O22 Eu3 O29 Eu1 137.6(6) 2 .
O22 Eu3 O29 Eu2 -143.96(10) 2 .
O22 Eu3 O29 Eu4 45.29(8) 2 2
O22 Eu3 O29 Eu5 131.35(9) 2 .
O22 Eu4 O16 C77 -78.5(4) . .
O22 Eu4 O17 C78 -175.0(4) . .
O22 Eu4 O19 Eu1 -113.60(9) . 2
O22 Eu4 O19 C87 83.5(4) . .
O22 Eu4 O20 C93 -71.6(5) . .
O22 Eu4 O25 Eu1 56.56(14) . 2
O22 Eu4 O25 Eu5 -49.42(15) . .
O22 C101 C102 C103 179.6(4) . .
O22 C101 C106 C105 -179.5(4) . .
O22 C101 C106 C107 1.9(7) . .
O23 Eu3 Eu5 Eu3 25.96(14) 2 2
O23 Eu3 Eu5 O25 122.68(15) 2 .
O23 Eu3 Eu5 O25 -83.64(15) 2 2
O23 Eu3 Eu5 O26 54.97(15) 2 2
O23 Eu3 Eu5 O26 -23.83(17) 2 .
O23 Eu3 Eu5 O27 141.61(17) 2 .
O23 Eu3 Eu5 O27 -11.90(15) 2 2
O23 Eu3 Eu5 O28 -137.6(3) 2 2
O23 Eu3 Eu5 O28 -158.19(15) 2 .
O23 Eu3 Eu5 O29 58.69(15) 2 2
O23 Eu3 Eu5 O29 -119.90(15) 2 .
O23 Eu3 O11 Eu2 -177.88(10) 2 .
O23 Eu3 O11 C43 -9.3(4) 2 .
O23 Eu3 O13 C63 -62.1(5) 2 .
O23 Eu3 O14 C57 40.7(3) 2 .
O23 Eu3 O26 Eu4 -88.06(11) 2 2
O23 Eu3 O26 Eu5 165.23(11) 2 .
O23 Eu3 O27 Eu2 143.3(2) 2 .
O23 Eu3 O27 Eu5 -110.8(3) 2 .
O23 Eu3 O29 Eu1 135.3(6) 2 .
O23 Eu3 O29 Eu2 -146.25(14) 2 .
O23 Eu3 O29 Eu4 43.00(18) 2 2
O23 Eu3 O29 Eu5 129.06(15) 2 .
O23 C107 C108 C109 32.4(7) . .
O23 C107 C108 C113 -140.8(6) . .
O24 C103 C104 C105 179.1(6) . .
O25 Eu1 Eu2 Eu3 38.07(6) 2 .
O25 Eu1 Eu2 Eu5 -17.47(6) 2 .
O25 Eu1 Eu2 O5 150.52(12) 2 .
O25 Eu1 Eu2 O7 -151.74(11) 2 .
O25 Eu1 Eu2 O8 -81.66(10) 2 .
O25 Eu1 Eu2 O10 146.65(17) 2 .
O25 Eu1 Eu2 O11 77.21(9) 2 .
O25 Eu1 Eu2 O27 -0.16(9) 2 .
O25 Eu1 Eu2 O28 -62.23(11) 2 .
O25 Eu1 Eu2 O29 45.13(10) 2 .
O25 Eu1 O1 C1 -133.3(4) 2 .
O25 Eu1 O2 C7 105.2(4) 2 .
O25 Eu1 O4 C21 -175.6(4) 2 .
O25 Eu1 O5 Eu2 -40.77(15) 2 .
O25 Eu1 O5 C15 150.8(3) 2 .
O25 Eu1 O28 Eu2 116.50(10) 2 .
O25 Eu1 O28 Eu5 10.68(9) 2 .
O25 Eu1 O29 Eu2 -129.33(10) 2 .
O25 Eu1 O29 Eu3 -50.8(6) 2 .
O25 Eu1 O29 Eu4 41.53(8) 2 2
O25 Eu1 O29 Eu5 -44.56(7) 2 .
O25 Eu4 O16 C77 142.9(3) . .
O25 Eu4 O17 C78 40.7(5) . .
O25 Eu4 O19 Eu1 19.51(8) . 2
O25 Eu4 O19 C87 -143.4(4) . .
O25 Eu4 O20 C93 77.2(5) . .
O25 Eu4 O22 Eu3 39.13(15) . 2
O25 Eu4 O22 C101 -163.7(3) . .
O25 Eu5 O25 Eu1 48.55(6) 2 2
O25 Eu5 O25 Eu4 154.27(9) 2 .
O25 Eu5 O26 Eu3 -50.90(15) . .
O25 Eu5 O26 Eu3 116.16(10) 2 .
O25 Eu5 O26 Eu4 10.08(9) 2 2
O25 Eu5 O26 Eu4 -156.98(9) . 2
O25 Eu5 O27 Eu2 51.91(11) 2 .
O25 Eu5 O27 Eu2 -93.32(9) . .
O25 Eu5 O27 Eu3 161.17(11) . .
O25 Eu5 O27 Eu3 -53.60(11) 2 .
O25 Eu5 O28 Eu1 -10.27(9) 2 .
O25 Eu5 O28 Eu1 -169.91(10) . .
O25 Eu5 O28 Eu2 84.98(9) . .
O25 Eu5 O28 Eu2 -115.39(10) 2 .
O25 Eu5 O29 Eu1 44.90(7) 2 .
O25 Eu5 O29 Eu1 -95.43(8) . .
O25 Eu5 O29 Eu2 133.89(9) 2 .
O25 Eu5 O29 Eu2 -6.44(9) . .
O25 Eu5 O29 Eu3 -136.22(9) 2 .
O25 Eu5 O29 Eu3 83.46(8) . .
O25 Eu5 O29 Eu4 -45.47(7) 2 2
O25 Eu5 O29 Eu4 174.21(7) . 2
O26 Eu3 Eu5 Eu3 49.79(10) . 2
O26 Eu3 Eu5 O25 146.52(11) . .
O26 Eu3 Eu5 O25 -59.81(11) . 2
O26 Eu3 Eu5 O26 78.80(14) . 2
O26 Eu3 Eu5 O27 165.45(14) . .
O26 Eu3 Eu5 O27 11.93(11) . 2
O26 Eu3 Eu5 O28 -113.8(2) . 2
O26 Eu3 Eu5 O28 -134.36(11) . .
O26 Eu3 Eu5 O29 82.52(11) . 2
O26 Eu3 Eu5 O29 -96.07(12) . .
O26 Eu3 O11 Eu2 42.80(15) . .
O26 Eu3 O11 C43 -148.6(3) . .
O26 Eu3 O13 C63 29.2(6) . .
O26 Eu3 O14 C57 147.4(4) . .
O26 Eu3 O27 Eu2 -115.41(10) . .
O26 Eu3 O27 Eu5 -9.54(9) . .
O26 Eu3 O29 Eu1 51.5(6) . .
O26 Eu3 O29 Eu2 129.99(10) . .
O26 Eu3 O29 Eu4 -40.76(8) . 2
O26 Eu3 O29 Eu5 45.30(7) . .
O26 Eu4 O16 C77 -137.1(3) 2 .
O26 Eu4 O17 C78 109.2(4) 2 .
O26 Eu4 O19 Eu1 -42.02(15) 2 2
O26 Eu4 O19 C87 155.1(3) 2 .
O26 Eu4 O20 C93 -179.7(4) 2 .
O26 Eu4 O22 Eu3 -21.37(8) 2 2
O26 Eu4 O22 C101 135.8(3) 2 .
O26 Eu4 O25 Eu1 116.23(10) 2 2
O26 Eu4 O25 Eu5 10.26(9) 2 .
O26 Eu5 O25 Eu1 -115.62(10) 2 2
O26 Eu5 O25 Eu1 -154.38(9) . 2
O26 Eu5 O25 Eu4 -9.90(9) 2 .
O26 Eu5 O25 Eu4 -48.66(15) . .
O26 Eu5 O26 Eu3 -90.10(10) 2 .
O26 Eu5 O26 Eu4 163.82(15) 2 2
O26 Eu5 O27 Eu2 114.71(10) . .
O26 Eu5 O27 Eu2 -170.54(11) 2 .
O26 Eu5 O27 Eu3 83.96(9) 2 .
O26 Eu5 O27 Eu3 9.21(9) . .
O26 Eu5 O28 Eu1 51.66(11) . .
O26 Eu5 O28 Eu1 151.51(11) 2 .
O26 Eu5 O28 Eu2 -53.45(12) . .
O26 Eu5 O28 Eu2 46.39(18) 2 .
O26 Eu5 O29 Eu1 134.95(9) . .
O26 Eu5 O29 Eu1 175.39(7) 2 .
O26 Eu5 O29 Eu2 -136.06(9) . .
O26 Eu5 O29 Eu2 -95.62(8) 2 .
O26 Eu5 O29 Eu3 -5.73(10) 2 .
O26 Eu5 O29 Eu3 -46.16(7) . .
O26 Eu5 O29 Eu4 44.59(7) . 2
O26 Eu5 O29 Eu4 85.03(8) 2 2
O27 Eu2 Eu3 Eu4 101.97(9) . 2
O27 Eu2 Eu3 Eu5 45.26(9) . .
O27 Eu2 Eu3 O11 -147.51(14) . .
O27 Eu2 Eu3 O13 -87.82(13) . .
O27 Eu2 Eu3 O14 -17.16(12) . .
O27 Eu2 Eu3 O22 142.92(12) . 2
O27 Eu2 Eu3 O23 -142.8(2) . 2
O27 Eu2 Eu3 O26 63.83(11) . .
O27 Eu2 Eu3 O29 108.48(12) . .
O27 Eu2 O5 Eu1 39.87(15) . .
O27 Eu2 O5 C15 -150.8(3) . .
O27 Eu2 O7 C35 34.6(6) . .
O27 Eu2 O8 C29 152.6(4) . .
O27 Eu2 O10 C49 83.1(6) . .
O27 Eu2 O11 Eu3 20.29(9) . .
O27 Eu2 O11 C43 -146.8(4) . .
O27 Eu2 O28 Eu1 -116.33(10) . .
O27 Eu2 O28 Eu5 -10.72(9) . .
O27 Eu2 O29 Eu1 129.11(10) . .
O27 Eu2 O29 Eu3 -40.82(8) . .
O27 Eu2 O29 Eu4 48.0(6) . 2
O27 Eu2 O29 Eu5 43.94(7) . .
O27 Eu3 Eu5 Eu3 -115.66(9) . 2
O27 Eu3 Eu5 O25 -18.93(11) . .
O27 Eu3 Eu5 O25 134.74(11) . 2
O27 Eu3 Eu5 O26 -86.64(11) . 2
O27 Eu3 Eu5 O26 -165.45(14) . .
O27 Eu3 Eu5 O27 -153.51(9) . 2
O27 Eu3 Eu5 O28 60.20(11) . .
O27 Eu3 Eu5 O28 80.8(2) . 2
O27 Eu3 Eu5 O29 -82.92(11) . 2
O27 Eu3 Eu5 O29 98.48(11) . .
O27 Eu3 O11 Eu2 -20.38(9) . .
O27 Eu3 O11 C43 148.2(3) . .
O27 Eu3 O13 C63 98.9(5) . .
O27 Eu3 O14 C57 -130.7(4) . .
O27 Eu3 O26 Eu4 116.21(10) . 2
O27 Eu3 O26 Eu5 9.50(9) . .
O27 Eu3 O29 Eu1 -38.0(6) . .
O27 Eu3 O29 Eu2 40.49(7) . .
O27 Eu3 O29 Eu4 -130.26(10) . 2
O27 Eu3 O29 Eu5 -44.20(7) . .
O27 Eu5 O25 Eu1 -52.03(11) 2 2
O27 Eu5 O25 Eu1 163.10(11) . 2
O27 Eu5 O25 Eu4 -91.18(9) . .
O27 Eu5 O25 Eu4 53.69(11) 2 .
O27 Eu5 O26 Eu3 -168.88(11) 2 .
O27 Eu5 O26 Eu3 -9.24(9) . .
O27 Eu5 O26 Eu4 -115.33(10) . 2
O27 Eu5 O26 Eu4 85.04(9) 2 2
O27 Eu5 O27 Eu2 152.23(9) 2 .
O27 Eu5 O27 Eu3 46.73(6) 2 .
O27 Eu5 O28 Eu1 -50.31(15) 2 .
O27 Eu5 O28 Eu1 115.56(10) . .
O27 Eu5 O28 Eu2 10.45(9) . .
O27 Eu5 O28 Eu2 -155.43(9) 2 .
O27 Eu5 O29 Eu1 -133.61(9) . .
O27 Eu5 O29 Eu1 85.70(8) 2 .
O27 Eu5 O29 Eu2 -44.63(7) . .
O27 Eu5 O29 Eu2 174.68(7) 2 .
O27 Eu5 O29 Eu3 -95.42(8) 2 .
O27 Eu5 O29 Eu3 45.27(7) . .
O27 Eu5 O29 Eu4 136.02(9) . 2
O27 Eu5 O29 Eu4 -4.67(9) 2 2
O28 Eu1 Eu2 Eu3 100.31(9) . .
O28 Eu1 Eu2 Eu5 44.76(9) . .
O28 Eu1 Eu2 O5 -147.25(14) . .
O28 Eu1 Eu2 O7 -89.51(12) . .
O28 Eu1 Eu2 O8 -19.43(12) . .
O28 Eu1 Eu2 O10 -151.12(18) . .
O28 Eu1 Eu2 O11 139.44(11) . .
O28 Eu1 Eu2 O27 62.07(11) . .
O28 Eu1 Eu2 O29 107.36(12) . .
O28 Eu1 O1 C1 146.3(4) . .
O28 Eu1 O2 C7 35.6(6) . .
O28 Eu1 O4 C21 89.2(5) . .
O28 Eu1 O5 Eu2 20.55(9) . .
O28 Eu1 O5 C15 -147.9(4) . .
O28 Eu1 O29 Eu2 -41.15(8) . .
O28 Eu1 O29 Eu3 37.4(6) . .
O28 Eu1 O29 Eu4 129.71(10) . 2
O28 Eu1 O29 Eu5 43.61(7) . .
O28 Eu2 Eu3 Eu4 39.35(6) . 2
O28 Eu2 Eu3 Eu5 -17.36(6) . .
O28 Eu2 Eu3 O11 149.88(12) . .
O28 Eu2 Eu3 O13 -150.43(11) . .
O28 Eu2 Eu3 O14 -79.78(10) . .
O28 Eu2 Eu3 O22 80.30(9) . 2
O28 Eu2 Eu3 O23 154.6(2) . 2
O28 Eu2 Eu3 O26 1.21(9) . .
O28 Eu2 Eu3 O27 -62.62(11) . .
O28 Eu2 Eu3 O29 45.86(10) . .
O28 Eu2 O5 Eu1 -20.64(9) . .
O28 Eu2 O5 C15 148.6(3) . .
O28 Eu2 O7 C35 102.9(5) . .
O28 Eu2 O8 C29 -127.8(4) . .
O28 Eu2 O10 C49 -173.9(4) . .
O28 Eu2 O11 Eu3 -40.85(15) . .
O28 Eu2 O11 C43 152.1(4) . .
O28 Eu2 O27 Eu3 115.61(10) . .
O28 Eu2 O27 Eu5 10.73(9) . .
O28 Eu2 O29 Eu1 41.40(8) . .
O28 Eu2 O29 Eu3 -128.52(10) . .
O28 Eu2 O29 Eu4 -39.7(6) . 2
O28 Eu2 O29 Eu5 -43.77(7) . .
O28 Eu5 O25 Eu1 85.90(9) . 2
O28 Eu5 O25 Eu1 10.40(9) 2 2
O28 Eu5 O25 Eu4 -168.38(10) . .
O28 Eu5 O25 Eu4 116.12(10) 2 .
O28 Eu5 O26 Eu3 54.07(11) . .
O28 Eu5 O26 Eu3 155.65(11) 2 .
O28 Eu5 O26 Eu4 49.57(18) 2 2
O28 Eu5 O26 Eu4 -52.01(11) . 2
O28 Eu5 O27 Eu2 -52.74(16) 2 .
O28 Eu5 O27 Eu2 -10.46(9) . .
O28 Eu5 O27 Eu3 -158.25(9) 2 .
O28 Eu5 O27 Eu3 -115.97(10) . .
O28 Eu5 O28 Eu1 -92.94(11) 2 .
O28 Eu5 O28 Eu2 161.94(15) 2 .
O28 Eu5 O29 Eu1 -44.55(7) . .
O28 Eu5 O29 Eu1 -4.14(10) 2 .
O28 Eu5 O29 Eu2 44.44(7) . .
O28 Eu5 O29 Eu2 84.84(9) 2 .
O28 Eu5 O29 Eu3 134.33(9) . .
O28 Eu5 O29 Eu3 174.74(7) 2 .
O28 Eu5 O29 Eu4 -94.51(8) 2 2
O28 Eu5 O29 Eu4 -134.91(9) . 2
O29 Eu1 Eu2 Eu3 -7.05(8) . .
O29 Eu1 Eu2 Eu5 -62.59(8) . .
O29 Eu1 Eu2 O5 105.40(13) . .
O29 Eu1 Eu2 O7 163.13(12) . .
O29 Eu1 Eu2 O8 -126.79(11) . .
O29 Eu1 Eu2 O10 101.52(18) . .
O29 Eu1 Eu2 O11 32.09(10) . .
O29 Eu1 Eu2 O27 -45.29(10) . .
O29 Eu1 Eu2 O28 -107.36(12) . .
O29 Eu1 O1 C1 -173.5(3) . .
O29 Eu1 O2 C7 161.0(4) . .
O29 Eu1 O4 C21 18.9(6) . .
O29 Eu1 O5 Eu2 -49.10(8) . .
O29 Eu1 O5 C15 142.4(4) . .
O29 Eu1 O28 Eu2 48.67(8) . .
O29 Eu1 O28 Eu5 -57.15(8) . .
O29 Eu2 Eu3 Eu4 -6.51(8) . 2
O29 Eu2 Eu3 Eu5 -63.22(8) . .
O29 Eu2 Eu3 O11 104.01(13) . .
O29 Eu2 Eu3 O13 163.70(12) . .
O29 Eu2 Eu3 O14 -125.64(11) . .
O29 Eu2 Eu3 O22 34.44(11) . 2
O29 Eu2 Eu3 O23 108.8(2) . 2
O29 Eu2 Eu3 O26 -44.65(10) . .
O29 Eu2 Eu3 O27 -108.48(12) . .
O29 Eu2 O5 Eu1 48.84(8) . .
O29 Eu2 O5 C15 -141.9(3) . .
O29 Eu2 O7 C35 159.1(4) . .
O29 Eu2 O8 C29 -169.7(3) . .
O29 Eu2 O10 C49 11.2(6) . .
O29 Eu2 O11 Eu3 -48.76(8) . .
O29 Eu2 O11 C43 144.2(4) . .
O29 Eu2 O27 Eu3 47.04(8) . .
O29 Eu2 O27 Eu5 -57.83(9) . .
O29 Eu2 O28 Eu1 -48.16(8) . .
O29 Eu2 O28 Eu5 57.45(8) . .
O29 Eu3 Eu5 Eu3 145.86(6) . 2
O29 Eu3 Eu5 O25 36.26(8) . 2
O29 Eu3 Eu5 O25 -117.41(9) . .
O29 Eu3 Eu5 O26 174.87(9) . 2
O29 Eu3 Eu5 O26 96.07(12) . .
O29 Eu3 Eu5 O27 -98.48(11) . .
O29 Eu3 Eu5 O27 108.00(9) . 2
O29 Eu3 Eu5 O28 -17.7(2) . 2
O29 Eu3 Eu5 O28 -38.29(9) . .
O29 Eu3 Eu5 O29 178.59(5) . 2
O29 Eu3 O11 Eu2 50.06(9) . .
O29 Eu3 O11 C43 -141.3(3) . .
O29 Eu3 O13 C63 154.5(4) . .
O29 Eu3 O14 C57 -173.5(3) . .
O29 Eu3 O26 Eu4 47.48(8) . 2
O29 Eu3 O26 Eu5 -59.23(9) . .
O29 Eu3 O27 Eu2 -48.03(8) . .
O29 Eu3 O27 Eu5 57.83(8) . .
O29 Eu4 O16 C77 178.0(3) 2 .
O29 Eu4 O17 C78 161.0(4) 2 .
O29 Eu4 O19 Eu1 -49.29(8) 2 2
O29 Eu4 O19 C87 147.8(4) 2 .
O29 Eu4 O20 C93 5.4(6) 2 .
O29 Eu4 O22 Eu3 47.40(8) 2 2
O29 Eu4 O22 C101 -155.4(3) 2 .
O29 Eu4 O25 Eu1 48.21(8) 2 2
O29 Eu4 O25 Eu5 -57.77(8) 2 .
O29 Eu5 O25 Eu1 129.08(8) . 2
O29 Eu5 O25 Eu1 -53.49(8) 2 2
O29 Eu5 O25 Eu4 52.24(8) 2 .
O29 Eu5 O25 Eu4 -125.20(8) . .
O29 Eu5 O26 Eu3 -125.48(8) 2 .
O29 Eu5 O26 Eu3 53.59(8) . .
O29 Eu5 O26 Eu4 -52.49(8) . 2
O29 Eu5 O26 Eu4 128.44(8) 2 2
O29 Eu5 O27 Eu2 53.35(8) . .
O29 Eu5 O27 Eu2 -129.17(8) 2 .
O29 Eu5 O27 Eu3 -52.15(8) . .
O29 Eu5 O27 Eu3 125.32(8) 2 .
O29 Eu5 O28 Eu1 52.14(8) . .
O29 Eu5 O28 Eu1 -128.80(8) 2 .
O29 Eu5 O28 Eu2 -52.97(8) . .
O29 Eu5 O28 Eu2 126.09(8) 2 .
O29 Eu5 O29 Eu1 155.44(5) 2 .
O29 Eu5 O29 Eu2 -115.57(5) 2 .
O29 Eu5 O29 Eu3 -25.68(5) 2 .
O29 Eu5 O29 Eu4 65.08(5) 2 2
C1 C2 C3 O3 -174.6(6) . .
C1 C2 C3 C4 0.7(10) . .
C1 C6 C7 O2 -12.9(7) . .
C1 C6 C7 C8 169.5(4) . .
C2 C1 C6 C5 3.6(7) . .
C2 C1 C6 C7 -179.0(4) . .
C2 C3 C4 C5 3.9(10) . .
C3 C4 C5 C6 -4.7(10) . .
C4 C5 C6 C1 0.9(8) . .
C4 C5 C6 C7 -176.6(5) . .
C5 C6 C7 O2 164.5(5) . .
C5 C6 C7 C8 -13.1(7) . .
C6 C1 C2 C3 -4.5(8) . .
C6 C7 C8 C9 134.7(5) . .
C6 C7 C8 C13 -48.6(7) . .
C7 C8 C9 C10 178.8(5) . .
C7 C8 C13 C12 -177.9(5) . .
C8 C9 C10 C11 -1.2(9) . .
C9 C8 C13 C12 -1.2(9) . .
C9 C10 C11 C12 -0.2(11) . .
C10 C11 C12 C13 0.9(12) . .
C11 C12 C13 C8 -0.1(11) . .
C13 C8 C9 C10 1.9(8) . .
C14 O3 C3 C2 -3.5(11) . .
C14 O3 C3 C4 -179.1(7) . .
C15 C16 C17 O6 -179.6(5) . .
C15 C16 C17 C18 -1.9(9) . .
C15 C20 C21 O4 -20.8(8) . .
C15 C20 C21 C22 157.2(5) . .
C16 C15 C20 C19 6.1(7) . .
C16 C15 C20 C21 -175.8(5) . .
C16 C17 C18 C19 5.2(10) . .
C17 C18 C19 C20 -2.8(10) . .
C18 C19 C20 C15 -2.8(9) . .
C18 C19 C20 C21 179.1(6) . .
C19 C20 C21 O4 157.2(5) . .
C19 C20 C21 C22 -24.9(8) . .
C20 C15 C16 C17 -4.0(8) . .
C20 C21 C22 C23 -29.0(8) . .
C20 C21 C22 C27 153.4(5) . .
C21 C22 C23 C24 -179.8(6) . .
C21 C22 C27 C26 -178.9(6) . .
C22 C23 C24 C25 -1.5(12) . .
C23 C22 C27 C26 3.4(10) . .
C23 C24 C25 C26 4.1(13) . .
C24 C25 C26 C27 -2.9(13) . .
C25 C26 C27 C22 -0.9(11) . .
C27 C22 C23 C24 -2.2(10) . .
C28 O6 C17 C16 -172.8(9) . .
C28 O6 C17 C18 9.6(13) . .
C29 C30 C31 O9 -175.6(5) . .
C29 C30 C31 C32 3.9(8) . .
C29 C34 C35 O7 -11.2(8) . .
C29 C34 C35 C36 171.8(5) . .
C30 C29 C34 C33 4.1(7) . .
C30 C29 C34 C35 -178.6(4) . .
C30 C31 C32 C33 -1.5(9) . .
C31 C32 C33 C34 0.5(10) . .
C32 C33 C34 C29 -1.8(9) . .
C32 C33 C34 C35 -179.2(6) . .
C33 C34 C35 O7 166.2(5) . .
C33 C34 C35 C36 -10.8(8) . .
C34 C29 C30 C31 -5.2(7) . .
C34 C35 C36 C37 130.0(6) . .
C34 C35 C36 C41 -55.5(8) . .
C35 C36 C37 C38 179.1(7) . .
C35 C36 C41 C40 -176.0(6) . .
C36 C37 C38 C39 -9.7(14) . .
C37 C36 C41 C40 -1.5(10) . .
C37 C38 C39 C40 13.0(18) . .
C38 C39 C40 C41 -10.2(18) . .
C39 C40 C41 C36 3.9(13) . .
C41 C36 C37 C38 4.5(11) . .
C42 O9 C31 C30 -1.2(9) . .
C42 O9 C31 C32 179.2(7) . .
C43 C44 C45 O12 179.7(6) . .
C43 C44 C45 C46 1.7(11) . .
C43 C48 C49 O10 -14.2(8) . .
C43 C48 C49 C50 165.9(5) . .
C44 C43 C48 C47 2.1(8) . .
C44 C43 C48 C49 178.4(5) . .
C44 C45 C46 C47 -1.5(13) . .
C45 C46 C47 C48 1.7(13) . .
C46 C47 C48 C43 -2.0(10) . .
C46 C47 C48 C49 -178.4(7) . .
C47 C48 C49 O10 162.0(5) . .
C47 C48 C49 C50 -17.9(8) . .
C48 C43 C44 C45 -2.1(9) . .
C48 C49 C50 C51 -38.7(8) . .
C48 C49 C50 C55 145.2(5) . .
C49 C50 C51 C52 -179.1(6) . .
C49 C50 C55 C54 179.2(5) . .
C50 C51 C52 C53 1.1(11) . .
C51 C50 C55 C54 2.8(9) . .
C51 C52 C53 C54 0.9(11) . .
C52 C53 C54 C55 -1.0(11) . .
C53 C54 C55 C50 -0.9(10) . .
C55 C50 C51 C52 -3.0(9) . .
C56 O12 C45 C44 -176.7(9) . .
C56 O12 C45 C46 1.2(14) . .
C57 C58 C59 O15 -177.4(5) . .
C57 C58 C59 C60 1.0(8) . .
C57 C62 C63 O13 -17.1(7) . .
C57 C62 C63 C64 164.3(4) . .
C58 C57 C62 C61 2.8(6) . .
C58 C57 C62 C63 179.8(4) . .
C58 C59 C60 C61 1.0(9) . .
C59 C60 C61 C62 -1.1(9) . .
C60 C61 C62 C57 -0.8(7) . .
C60 C61 C62 C63 -177.8(5) . .
C61 C62 C63 O13 159.8(5) . .
C61 C62 C63 C64 -18.8(7) . .
C62 C57 C58 C59 -3.0(7) . .
C62 C63 C64 C65 -54.3(7) . .
C62 C63 C64 C69 131.4(5) . .
C63 C64 C65 C66 -172.8(5) . .
C63 C64 C69 C68 177.3(5) . .
C64 C65 C66 C67 -4.8(10) . .
C65 C64 C69 C68 2.9(8) . .
C65 C66 C67 C68 3.8(12) . .
C66 C67 C68 C69 0.5(11) . .
C67 C68 C69 C64 -3.9(10) . .
C69 C64 C65 C66 1.5(8) . .
C70 O15 C59 C58 -5.2(9) . .
C70 O15 C59 C60 176.3(6) . .
C72 C73 C74 C75 1.2(8) . .
C73 C72 C77 O16 173.6(4) . .
C73 C72 C77 C76 -8.7(7) . .
C73 C74 C75 C76 -0.7(8) . .
C74 C75 C76 C77 -4.3(7) . .
C74 C75 C76 C78 176.9(5) . .
C75 C76 C77 O16 -173.7(4) . .
C75 C76 C77 C72 8.8(6) . .
C75 C76 C78 O17 156.1(5) . .
C75 C76 C78 C79 -25.3(7) . .
C76 C78 C79 C80 154.9(5) . .
C76 C78 C79 C84 -28.0(7) . .
C77 C72 C73 O18 -178.4(5) . .
C77 C72 C73 C74 3.6(8) . .
C77 C76 C78 O17 -22.6(7) . .
C77 C76 C78 C79 156.1(4) . .
C78 C76 C77 O16 5.1(7) . .
C78 C76 C77 C72 -172.4(4) . .
C78 C79 C80 C81 178.9(5) . .
C78 C79 C84 C83 -179.7(5) . .
C79 C80 C81 C82 -0.8(10) . .
C80 C79 C84 C83 -2.7(9) . .
C80 C81 C82 C83 0.7(11) . .
C81 C82 C83 C84 -1.6(12) . .
C82 C83 C84 C79 2.6(10) . .
C84 C79 C80 C81 1.8(9) . .
C86 O18 C73 C72 -3.3(9) . .
C86 O18 C73 C74 174.8(6) . .
C87 C88 C89 O21 -179.8(5) . .
C87 C88 C89 C90 0.2(8) . .
C87 C92 C93 O20 -17.0(7) . .
C87 C92 C93 C94 165.5(4) . .
C88 C87 C92 C91 3.3(7) . .
C88 C87 C92 C93 179.3(4) . .
C88 C89 C90 C91 1.7(9) . .
C89 C90 C91 C92 -1.0(9) . .
C90 C91 C92 C87 -1.6(8) . .
C90 C91 C92 C93 -177.6(5) . .
C91 C92 C93 O20 158.9(5) . .
C91 C92 C93 C94 -18.6(7) . .
C92 C87 C88 C89 -2.7(7) . .
C92 C93 C94 C95 -37.3(8) . .
C92 C93 C94 C99 143.2(5) . .
C93 C94 C95 C96 -177.4(6) . .
C93 C94 C99 C98 -179.7(6) . .
C94 C95 C96 C97 -5.8(11) . .
C95 C94 C99 C98 0.7(10) . .
C95 C96 C97 C98 6.8(14) . .
C96 C97 C98 C99 -3.9(14) . .
C97 C98 C99 C94 0.1(12) . .
C99 C94 C95 C96 2.1(10) . .
C100 O21 C89 C88 175.5(6) . .
C100 O21 C89 C90 -4.5(9) . .
C101 C102 C103 O24 178.7(5) . .
C101 C102 C103 C104 -0.3(8) . .
C101 C106 C107 O23 20.7(8) . .
C101 C106 C107 C108 -157.9(5) . .
C102 C101 C106 C105 -2.7(6) . .
C102 C101 C106 C107 178.7(5) . .
C102 C103 C104 C105 -1.9(9) . .
C103 C104 C105 C106 1.7(9) . .
C104 C105 C106 C101 0.6(8) . .
C104 C105 C106 C107 179.2(6) . .
C105 C106 C107 O23 -157.8(5) . .
C105 C106 C107 C108 23.6(8) . .
C106 C101 C102 C103 2.6(7) . .
C106 C107 C108 C109 -148.9(5) . .
C106 C107 C108 C113 37.8(8) . .
C107 C108 C109 C110 -175.8(5) . .
C107 C108 C113 C112 173.2(6) . .
C108 C109 C110 C111 2.4(10) . .
C109 C108 C113 C112 0.1(10) . .
C109 C110 C111 C112 -0.3(13) . .
C110 C111 C112 C113 -1.8(13) . .
C111 C112 C113 C108 1.9(11) . .
C113 C108 C109 C110 -2.4(9) . .
C114 O24 C103 C102 -1.4(10) . .
C114 O24 C103 C104 177.6(7) . .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
1 0.410 0.056 -0.041 8610.4 168.8
