#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:32:00 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179484 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/81/4338151.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4338151
loop_
_publ_author_name
'Bassanetti, Irene'
'Twist, Christina P.'
'Kim, Myung-Gil'
'Seyam, Afif M.'
'Bazzi, Hassan S.'
'Wang, Q. Jane'
'Chung, Yip-Wah'
'Marchió, Luciano'
'Delferro, Massimiliano'
'Marks, Tobin J.'
_publ_section_title
;
 Synthesis and characterization of silver(i) pyrazolylmethylpyridine
 complexes and their implementation as metallic silver thin film
 precursors.
;
_journal_issue                   9
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4629
_journal_page_last               4638
_journal_paper_doi               10.1021/ic500321w
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         '2(C36 H54 Ag2 N8 O8)'
_chemical_formula_sum            'C72 H108 Ag4 N16 O16'
_chemical_formula_weight         1885.22
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.455(7)
_cell_angle_beta                 103.456(8)
_cell_angle_gamma                101.335(8)
_cell_formula_units_Z            2
_cell_length_a                   12.286(5)
_cell_length_b                   17.512(7)
_cell_length_c                   21.794(8)
_cell_measurement_reflns_used    10487
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      24.00
_cell_measurement_theta_min      1.03
_cell_volume                     4167(3)
_computing_cell_refinement       Saint
_computing_data_collection       Smart
_computing_data_reduction        Saint
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    Sir2004
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Smart APEXII CCD'
_diffrn_measurement_method       'theta & omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0888
_diffrn_reflns_av_sigmaI/netI    0.1327
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            31563
_diffrn_reflns_theta_full        24.00
_diffrn_reflns_theta_max         24.00
_diffrn_reflns_theta_min         1.03
_diffrn_standards_decay_%        none
_exptl_absorpt_coefficient_mu    0.997
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.773
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.502
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1936
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.03
_refine_diff_density_max         0.435
_refine_diff_density_min         -0.493
_refine_diff_density_rms         0.088
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.960
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1001
_refine_ls_number_reflns         13053
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.960
_refine_ls_R_factor_all          0.1438
_refine_ls_R_factor_gt           0.0579
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0001P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0850
_refine_ls_wR_factor_ref         0.1045
_reflns_number_gt                5826
_reflns_number_total             13053
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500321w_si_002.cif
_cod_data_source_block           ib227th
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338146--4338151.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4338151
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.48739(5) 0.38099(3) 0.07414(3) 0.0603(2) Uani 1 1 d .
Ag3 Ag 0.49610(5) 0.38746(4) 0.55320(3) 0.0726(2) Uani 1 1 d .
Ag4 Ag 0.44207(6) 0.10470(4) 0.48624(3) 0.0758(2) Uani 1 1 d .
Ag2 Ag 0.51842(6) 0.12829(4) -0.00636(4) 0.0820(2) Uani 1 1 d .
N210 N 0.3154(5) 0.0822(4) 0.3886(3) 0.0500(16) Uani 1 1 d .
N21 N 0.6433(5) 0.4048(3) 0.1567(3) 0.0512(17) Uani 1 1 d .
N11 N 0.6945(5) 0.3484(3) 0.1744(3) 0.0488(16) Uani 1 1 d .
N27 N 0.3392(5) 0.3423(4) 0.5842(3) 0.0567(17) Uani 1 1 d .
O112 O 0.6621(5) 0.2036(3) 0.3069(3) 0.0801(18) Uani 1 1 d .
N113 N 0.3170(6) 0.4739(5) 0.0665(4) 0.072(2) Uani 1 1 d .
N24 N 0.6689(5) 0.1794(4) -0.0352(3) 0.0516(16) Uani 1 1 d .
O16 O 0.3321(5) 0.1640(3) -0.2414(3) 0.0811(17) Uani 1 1 d .
N16 N 0.4400(6) 0.2924(3) -0.0353(3) 0.0517(16) Uani 1 1 d .
N112 N 0.5415(6) 0.3042(3) 0.4661(3) 0.0516(16) Uani 1 1 d .
N13 N 0.4393(5) 0.1930(3) 0.0712(3) 0.0515(17) Uani 1 1 d .
N19 N 0.5476(6) 0.2142(3) 0.5813(3) 0.0536(17) Uani 1 1 d .
N14 N 0.7165(5) 0.2574(3) -0.0332(3) 0.0506(16) Uani 1 1 d .
N17 N 0.3009(6) 0.2612(4) 0.5817(3) 0.0573(17) Uani 1 1 d .
N110 N 0.2724(5) 0.1415(3) 0.3715(3) 0.0512(16) Uani 1 1 d .
O13 O 0.2588(5) 0.2985(3) 0.1958(3) 0.0858(18) Uani 1 1 d .
C39 C 0.6980(9) 0.3564(5) 0.6884(5) 0.069(3) Uani 1 1 d .
O19 O 0.7726(5) 0.4269(3) 0.7394(3) 0.097(2) Uani 1 1 d .
C14 C 0.7508(6) 0.1395(4) -0.0466(3) 0.0467(19) Uani 1 1 d .
C15 C 0.6452(6) 0.3164(4) -0.0246(4) 0.055(2) Uani 1 1 d .
H15A H 0.6801 0.3638 -0.0349 0.066 Uiso 1 1 calc R
H15B H 0.6483 0.3370 0.0225 0.066 Uiso 1 1 calc R
C16 C 0.5190(6) 0.2805(4) -0.0678(4) 0.051(2) Uani 1 1 d .
N115 N 0.6596(7) 0.5523(5) 0.6131(4) 0.081(2) Uani 1 1 d .
C31 C 0.8074(6) 0.3827(4) 0.2132(4) 0.051(2) Uani 1 1 d .
C112 C 0.4654(6) 0.2481(4) 0.4070(4) 0.052(2) Uani 1 1 d .
C33 C 0.3195(7) 0.2666(4) 0.1536(5) 0.057(2) Uani 1 1 d .
C53 C 0.3226(6) 0.1778(4) 0.0494(4) 0.050(2) Uani 1 1 d .
H53 H 0.2826 0.1409 0.0053 0.060 Uiso 1 1 calc R
C34 C 0.8218(6) 0.2677(5) -0.0428(3) 0.050(2) Uani 1 1 d .
N116 N 0.3280(8) -0.0406(6) 0.5455(4) 0.084(3) Uani 1 1 d .
C43 C 0.2582(7) 0.2132(4) 0.0878(4) 0.052(2) Uani 1 1 d .
C23 C 0.4414(7) 0.2835(4) 0.1785(4) 0.052(2) Uani 1 1 d .
C56 C 0.3265(6) 0.2590(4) -0.0716(4) 0.051(2) Uani 1 1 d .
H56 H 0.2717 0.2680 -0.0492 0.061 Uiso 1 1 calc R
C310 C 0.1740(7) 0.1068(5) 0.3169(4) 0.058(2) Uani 1 1 d .
C17 C 0.2430(7) 0.3580(4) 0.5560(4) 0.057(2) Uani 1 1 d .
C312 C 0.6186(8) 0.2327(5) 0.3597(5) 0.060(2) Uani 1 1 d .
N114 N 0.3326(8) -0.0275(5) -0.1080(4) 0.083(2) Uani 1 1 d .
C13 C 0.4960(7) 0.2459(5) 0.1337(5) 0.057(2) Uani 1 1 d .
C110 C 0.2417(7) 0.0091(4) 0.3429(4) 0.052(2) Uani 1 1 d .
C19 C 0.5079(7) 0.2600(5) 0.6287(4) 0.056(2) Uani 1 1 d .
C41 C 0.7062(6) 0.5552(4) 0.1769(4) 0.060(2) Uani 1 1 d .
H41 H 0.6227 0.5493 0.1693 0.072 Uiso 1 1 calc R
O113 O 0.4185(5) 0.5106(4) 0.0755(3) 0.110(2) Uani 1 1 d .
C410 C 0.2675(7) -0.0710(4) 0.3435(4) 0.064(2) Uani 1 1 d .
H410 H 0.2829 -0.0719 0.3894 0.076 Uiso 1 1 calc R
C512 C 0.6537(7) 0.3226(4) 0.4706(4) 0.059(2) Uani 1 1 d .
H512 H 0.7061 0.3627 0.5108 0.071 Uiso 1 1 calc R
C24 C 0.8459(6) 0.1928(4) -0.0524(3) 0.054(2) Uani 1 1 d .
H24 H 0.9120 0.1799 -0.0611 0.064 Uiso 1 1 calc R
C74 C 0.8944(6) 0.3508(4) -0.0387(4) 0.054(2) Uani 1 1 d .
H74 H 0.8443 0.3772 -0.0620 0.064 Uiso 1 1 calc R
O313 O 0.2425(5) 0.5117(4) 0.0629(3) 0.109(2) Uani 1 1 d .
C212 C 0.5009(7) 0.2128(4) 0.3505(4) 0.053(2) Uani 1 1 d .
C37 C 0.1841(8) 0.2286(5) 0.5545(4) 0.070(2) Uani 1 1 d .
C36 C 0.3694(9) 0.2042(4) -0.1711(4) 0.062(2) Uani 1 1 d .
O213 O 0.2938(5) 0.4002(4) 0.0613(3) 0.095(2) Uani 1 1 d .
O315 O 0.7297(6) 0.6217(4) 0.6374(3) 0.115(3) Uani 1 1 d .
C21 C 0.8299(6) 0.4655(5) 0.2211(4) 0.064(2) Uani 1 1 d .
H21 H 0.9006 0.5066 0.2454 0.077 Uiso 1 1 calc R
C11 C 0.7291(6) 0.4770(5) 0.1868(4) 0.0469(19) Uani 1 1 d .
C27 C 0.1468(7) 0.2908(5) 0.5379(4) 0.074(3) Uani 1 1 d .
H27 H 0.0698 0.2881 0.5178 0.089 Uiso 1 1 calc R
C412 C 0.6990(7) 0.2868(5) 0.4201(5) 0.063(2) Uani 1 1 d .
C612 C 0.4132(6) 0.1592(4) 0.2824(3) 0.079(3) Uani 1 1 d .
H61A H 0.4519 0.1519 0.2484 0.119 Uiso 1 1 calc R
H61B H 0.3538 0.1859 0.2721 0.119 Uiso 1 1 calc R
H61C H 0.3781 0.1056 0.2833 0.119 Uiso 1 1 calc R
O116 O 0.3988(6) -0.0276(4) 0.5136(4) 0.114(2) Uani 1 1 d .
O314 O 0.2630(6) -0.0929(4) -0.1436(4) 0.135(3) Uani 1 1 d .
C26 C 0.4881(7) 0.2385(5) -0.1364(5) 0.058(2) Uani 1 1 d .
C66 C 0.5770(7) 0.2315(5) -0.1750(4) 0.085(3) Uani 1 1 d .
H66A H 0.6069 0.1855 -0.1724 0.128 Uiso 1 1 calc R
H66B H 0.6400 0.2823 -0.1554 0.128 Uiso 1 1 calc R
H66C H 0.5397 0.2223 -0.2216 0.128 Uiso 1 1 calc R
C111 C 0.3375(6) 0.2288(4) 0.4060(4) 0.063(2) Uani 1 1 d .
H11A H 0.3355 0.2463 0.4523 0.075 Uiso 1 1 calc R
H11B H 0.2993 0.2615 0.3841 0.075 Uiso 1 1 calc R
C710 C 0.1046(7) 0.1552(5) 0.2860(4) 0.072(3) Uani 1 1 d .
H710 H 0.1591 0.2066 0.2897 0.087 Uiso 1 1 calc R
C46 C 0.2870(7) 0.2138(4) -0.1378(4) 0.054(2) Uani 1 1 d .
C59 C 0.6618(8) 0.2417(5) 0.5880(4) 0.058(2) Uani 1 1 d .
H59 H 0.6904 0.2114 0.5558 0.069 Uiso 1 1 calc R
C18 C 0.3814(7) 0.2258(4) 0.6198(4) 0.065(2) Uani 1 1 d .
H18A H 0.3586 0.1658 0.5964 0.078 Uiso 1 1 calc R
H18B H 0.3717 0.2362 0.6642 0.078 Uiso 1 1 calc R
O115 O 0.6899(6) 0.4892(4) 0.6144(4) 0.136(3) Uani 1 1 d .
C44 C 0.7305(7) 0.0487(4) -0.0543(4) 0.066(2) Uani 1 1 d .
H44 H 0.6706 0.0350 -0.0334 0.079 Uiso 1 1 calc R
O316 O 0.3140(8) -0.1037(5) 0.5537(4) 0.159(4) Uani 1 1 d .
O216 O 0.2864(7) 0.0144(5) 0.5625(4) 0.152(4) Uani 1 1 d .
C812 C 0.8300(7) 0.3072(5) 0.4325(4) 0.089(3) Uani 1 1 d .
H81A H 0.8536 0.2572 0.4275 0.133 Uiso 1 1 calc R
H81B H 0.8697 0.3472 0.4776 0.133 Uiso 1 1 calc R
H81C H 0.8495 0.3303 0.4004 0.133 Uiso 1 1 calc R
C12 C 0.6269(6) 0.2619(4) 0.1550(4) 0.071(3) Uani 1 1 d .
H12A H 0.6497 0.2439 0.1928 0.085 Uiso 1 1 calc R
H12B H 0.6473 0.2275 0.1178 0.085 Uiso 1 1 calc R
C49 C 0.7389(7) 0.3125(5) 0.6402(5) 0.065(2) Uani 1 1 d .
O214 O 0.3185(6) 0.0397(4) -0.1057(4) 0.138(3) Uani 1 1 d .
C71 C 0.8845(6) 0.3330(5) 0.2341(5) 0.075(3) Uani 1 1 d .
H71 H 0.8398 0.2901 0.2462 0.090 Uiso 1 1 calc R
C712 C 0.6697(8) 0.1198(5) 0.2926(4) 0.109(4) Uani 1 1 d .
H71A H 0.7198 0.1162 0.3321 0.164 Uiso 1 1 calc R
H71B H 0.7012 0.1046 0.2558 0.164 Uiso 1 1 calc R
H71C H 0.5932 0.0823 0.2805 0.164 Uiso 1 1 calc R
C47 C 0.2497(7) 0.4430(5) 0.5497(5) 0.078(3) Uani 1 1 d .
H47 H 0.3210 0.4605 0.5384 0.093 Uiso 1 1 calc R
C86 C 0.1573(6) 0.1741(5) -0.1741(4) 0.089(3) Uani 1 1 d .
H86A H 0.1153 0.2124 -0.1579 0.134 Uiso 1 1 calc R
H86B H 0.1319 0.1239 -0.1655 0.134 Uiso 1 1 calc R
H86C H 0.1425 0.1606 -0.2219 0.134 Uiso 1 1 calc R
C210 C 0.1545(6) 0.0222(5) 0.2982(4) 0.064(2) Uani 1 1 d .
H210 H 0.0938 -0.0187 0.2622 0.076 Uiso 1 1 calc R
C69 C 0.5340(7) 0.3836(5) 0.7353(4) 0.096(3) Uani 1 1 d .
H69A H 0.5981 0.4210 0.7742 0.143 Uiso 1 1 calc R
H69B H 0.4836 0.3468 0.7487 0.143 Uiso 1 1 calc R
H69C H 0.4908 0.4153 0.7158 0.143 Uiso 1 1 calc R
C94 C 0.9903(6) 0.3387(4) -0.0703(4) 0.079(3) Uani 1 1 d .
H94A H 1.0375 0.3110 -0.0483 0.118 Uiso 1 1 calc R
H94B H 1.0381 0.3921 -0.0650 0.118 Uiso 1 1 calc R
H94C H 0.9560 0.3052 -0.1176 0.118 Uiso 1 1 calc R
C77 C 0.1166(7) 0.1433(5) 0.5495(6) 0.091(3) Uani 1 1 d .
H77 H 0.1700 0.1084 0.5494 0.109 Uiso 1 1 calc R
C63 C 0.5077(7) 0.3402(4) 0.2495(4) 0.077(3) Uani 1 1 d .
H63A H 0.5707 0.3199 0.2670 0.116 Uiso 1 1 calc R
H63B H 0.4565 0.3417 0.2767 0.116 Uiso 1 1 calc R
H63C H 0.5387 0.3954 0.2504 0.116 Uiso 1 1 calc R
C83 C 0.1293(6) 0.1969(4) 0.0597(4) 0.086(3) Uani 1 1 d .
H83A H 0.1050 0.1692 0.0114 0.129 Uiso 1 1 calc R
H83B H 0.1102 0.2490 0.0704 0.129 Uiso 1 1 calc R
H83C H 0.0898 0.1621 0.0791 0.129 Uiso 1 1 calc R
C29 C 0.5810(8) 0.3319(5) 0.6829(4) 0.062(2) Uani 1 1 d .
C89 C 0.8657(7) 0.3400(5) 0.6403(4) 0.091(3) Uani 1 1 d .
H89A H 0.8716 0.3103 0.5970 0.136 Uiso 1 1 calc R
H89B H 0.9162 0.3281 0.6748 0.136 Uiso 1 1 calc R
H89C H 0.8885 0.3990 0.6493 0.136 Uiso 1 1 calc R
C51 C 0.7344(9) 0.5630(5) 0.1147(5) 0.118(4) Uani 1 1 d .
H51A H 0.7116 0.6091 0.1060 0.177 Uiso 1 1 calc R
H51B H 0.6927 0.5124 0.0765 0.177 Uiso 1 1 calc R
H51C H 0.8169 0.5724 0.1221 0.177 Uiso 1 1 calc R
O114 O 0.4209(6) -0.0230(4) -0.0662(4) 0.130(3) Uani 1 1 d .
C810 C 0.0218(8) 0.1794(6) 0.3248(5) 0.129(4) Uani 1 1 d .
H81D H -0.0412 0.1309 0.3149 0.193 Uiso 1 1 calc R
H81E H -0.0089 0.2205 0.3118 0.193 Uiso 1 1 calc R
H81F H 0.0630 0.2021 0.3725 0.193 Uiso 1 1 calc R
C61 C 0.7738(7) 0.6332(5) 0.2400(4) 0.100(3) Uani 1 1 d .
H61D H 0.8551 0.6470 0.2433 0.151 Uiso 1 1 calc R
H61E H 0.7648 0.6225 0.2795 0.151 Uiso 1 1 calc R
H61F H 0.7439 0.6790 0.2366 0.151 Uiso 1 1 calc R
C81 C 0.9264(7) 0.2900(5) 0.1752(5) 0.109(4) Uani 1 1 d .
H81G H 0.8631 0.2443 0.1416 0.164 Uiso 1 1 calc R
H81H H 0.9896 0.2694 0.1917 0.164 Uiso 1 1 calc R
H81I H 0.9527 0.3295 0.1555 0.164 Uiso 1 1 calc R
C510 C 0.3728(9) -0.0799(5) 0.3194(5) 0.121(4) Uani 1 1 d .
H51D H 0.3597 -0.0751 0.2757 0.182 Uiso 1 1 calc R
H51E H 0.3837 -0.1336 0.3162 0.182 Uiso 1 1 calc R
H51F H 0.4412 -0.0368 0.3510 0.182 Uiso 1 1 calc R
C73 C 0.2628(7) 0.3833(5) 0.2071(4) 0.095(3) Uani 1 1 d .
H73A H 0.3423 0.4177 0.2281 0.143 Uiso 1 1 calc R
H73B H 0.2173 0.4004 0.2363 0.143 Uiso 1 1 calc R
H73C H 0.2314 0.3892 0.1647 0.143 Uiso 1 1 calc R
C84 C 0.9505(7) 0.4069(4) 0.0368(4) 0.084(3) Uani 1 1 d .
H84A H 0.8906 0.4109 0.0581 0.125 Uiso 1 1 calc R
H84B H 0.9913 0.4616 0.0406 0.125 Uiso 1 1 calc R
H84C H 1.0044 0.3831 0.0587 0.125 Uiso 1 1 calc R
C57 C 0.1503(9) 0.4413(5) 0.4960(5) 0.130(4) Uani 1 1 d .
H57A H 0.0804 0.4311 0.5085 0.196 Uiso 1 1 calc R
H57B H 0.1411 0.3976 0.4544 0.196 Uiso 1 1 calc R
H57C H 0.1643 0.4940 0.4900 0.196 Uiso 1 1 calc R
C910 C 0.0393(9) 0.1052(6) 0.2110(5) 0.141(5) Uani 1 1 d .
H91A H 0.0935 0.0879 0.1883 0.211 Uiso 1 1 calc R
H91B H 0.0027 0.1395 0.1911 0.211 Uiso 1 1 calc R
H91C H -0.0192 0.0568 0.2064 0.211 Uiso 1 1 calc R
C67 C 0.2597(12) 0.5038(5) 0.6144(5) 0.216(8) Uani 1 1 d .
H67A H 0.1907 0.4881 0.6266 0.324 Uiso 1 1 calc R
H67B H 0.2682 0.5580 0.6111 0.324 Uiso 1 1 calc R
H67C H 0.3267 0.5055 0.6484 0.324 Uiso 1 1 calc R
C610 C 0.1647(8) -0.1456(5) 0.2951(5) 0.164(6) Uani 1 1 d .
H61G H 0.1462 -0.1424 0.2508 0.246 Uiso 1 1 calc R
H61H H 0.0982 -0.1452 0.3110 0.246 Uiso 1 1 calc R
H61I H 0.1851 -0.1964 0.2929 0.246 Uiso 1 1 calc R
C79 C 0.8386(8) 0.4185(5) 0.7976(4) 0.117(4) Uani 1 1 d .
H79A H 0.7874 0.4001 0.8209 0.175 Uiso 1 1 calc R
H79B H 0.8936 0.4715 0.8270 0.175 Uiso 1 1 calc R
H79C H 0.8799 0.3782 0.7849 0.175 Uiso 1 1 calc R
C64 C 0.8393(8) 0.0359(5) -0.0171(6) 0.159(5) Uani 1 1 d .
H64A H 0.8219 -0.0186 -0.0144 0.238 Uiso 1 1 calc R
H64B H 0.8703 0.0775 0.0277 0.238 Uiso 1 1 calc R
H64C H 0.8957 0.0405 -0.0407 0.238 Uiso 1 1 calc R
C54 C 0.6870(11) -0.0060(5) -0.1252(5) 0.161(6) Uani 1 1 d .
H54A H 0.6122 -0.0007 -0.1460 0.241 Uiso 1 1 calc R
H54B H 0.6790 -0.0628 -0.1285 0.241 Uiso 1 1 calc R
H54C H 0.7409 0.0096 -0.1480 0.241 Uiso 1 1 calc R
C91 C 0.9878(7) 0.3908(5) 0.2962(5) 0.117(4) Uani 1 1 d .
H91D H 1.0247 0.4380 0.2872 0.175 Uiso 1 1 calc R
H91E H 1.0431 0.3609 0.3061 0.175 Uiso 1 1 calc R
H91F H 0.9603 0.4096 0.3343 0.175 Uiso 1 1 calc R
C76 C 0.3176(9) 0.0755(5) -0.2628(4) 0.131(4) Uani 1 1 d .
H76A H 0.3916 0.0653 -0.2627 0.196 Uiso 1 1 calc R
H76B H 0.2633 0.0484 -0.3077 0.196 Uiso 1 1 calc R
H76C H 0.2882 0.0539 -0.2324 0.196 Uiso 1 1 calc R
C87 C 0.0217(10) 0.1052(6) 0.4822(6) 0.202(7) Uani 1 1 d .
H87A H -0.0286 0.1406 0.4798 0.303 Uiso 1 1 calc R
H87B H -0.0231 0.0511 0.4774 0.303 Uiso 1 1 calc R
H87C H 0.0562 0.0998 0.4464 0.303 Uiso 1 1 calc R
C97 C 0.0734(12) 0.1486(6) 0.6079(7) 0.211(8) Uani 1 1 d .
H97A H 0.1279 0.1930 0.6475 0.317 Uiso 1 1 calc R
H97B H 0.0651 0.0967 0.6152 0.317 Uiso 1 1 calc R
H97C H -0.0011 0.1597 0.5990 0.317 Uiso 1 1 calc R
O215 O 0.5617(6) 0.5429(4) 0.5835(5) 0.165(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
N21 Ag1 N16 126.9(2) .
N21 Ag1 O213 137.3(2) .
N16 Ag1 O213 94.2(2) .
N21 Ag1 O113 114.3(2) .
N16 Ag1 O113 109.2(2) .
O213 Ag1 O113 49.77(18) .
N27 Ag3 N112 122.4(2) .
N27 Ag3 O115 134.1(2) .
N112 Ag3 O115 98.6(3) .
N27 Ag3 O215 114.2(2) .
N112 Ag3 O215 118.5(3) .
O115 Ag3 O215 49.2(2) .
N210 Ag4 N19 137.5(2) .
N210 Ag4 O116 108.1(2) .
N19 Ag4 O116 109.7(2) .
N210 Ag4 O116 118.1(2) 2_656
N19 Ag4 O116 95.4(2) 2_656
O116 Ag4 O116 64.7(3) 2_656
N24 Ag2 N13 129.9(2) .
N24 Ag2 O114 115.7(2) .
N13 Ag2 O114 114.5(2) .
C110 N210 N110 104.6(6) .
C110 N210 Ag4 128.2(5) .
N110 N210 Ag4 124.8(4) .
C11 N21 N11 103.4(5) .
C11 N21 Ag1 125.0(5) .
N11 N21 Ag1 128.6(4) .
C31 N11 N21 113.3(6) .
C31 N11 C12 125.8(6) .
N21 N11 C12 120.8(6) .
C17 N27 N17 104.1(6) .
C17 N27 Ag3 115.2(5) .
N17 N27 Ag3 123.0(4) .
C312 O112 C712 114.7(6) .
O113 N113 O213 118.1(8) .
O113 N113 O313 119.3(8) .
O213 N113 O313 122.6(8) .
N14 N24 C14 103.6(5) .
N14 N24 Ag2 131.6(5) .
C14 N24 Ag2 123.6(5) .
C36 O16 C76 113.6(6) .
C16 N16 C56 117.9(6) .
C16 N16 Ag1 123.3(5) .
C56 N16 Ag1 118.1(5) .
C512 N112 C112 117.3(7) .
C512 N112 Ag3 115.4(5) .
C112 N112 Ag3 126.5(6) .
C13 N13 C53 117.6(7) .
C13 N13 Ag2 126.9(5) .
C53 N13 Ag2 115.4(5) .
C59 N19 C19 116.9(7) .
C59 N19 Ag4 115.2(5) .
C19 N19 Ag4 127.5(6) .
C34 N14 N24 113.3(6) .
C34 N14 C15 129.5(6) .
N24 N14 C15 117.2(6) .
C37 N17 N27 112.7(6) .
C37 N17 C18 125.9(7) .
N27 N17 C18 120.0(6) .
N210 N110 C310 111.7(6) .
N210 N110 C111 119.8(6) .
C310 N110 C111 128.1(6) .
C33 O13 C73 114.7(6) .
C49 C39 O19 119.0(9) .
C49 C39 C29 120.0(8) .
O19 C39 C29 120.9(9) .
C39 O19 C79 118.0(6) .
N24 C14 C24 110.6(6) .
N24 C14 C44 120.8(6) .
C24 C14 C44 128.5(7) .
N14 C15 C16 115.1(6) .
N14 C15 H15A 108.5 .
C16 C15 H15A 108.5 .
N14 C15 H15B 108.5 .
C16 C15 H15B 108.5 .
H15A C15 H15B 107.5 .
N16 C16 C26 122.7(7) .
N16 C16 C15 116.1(7) .
C26 C16 C15 121.3(8) .
O215 N115 O315 120.3(9) .
O215 N115 O115 117.9(9) .
O315 N115 O115 121.6(9) .
N11 C31 C21 104.6(6) .
N11 C31 C71 123.3(7) .
C21 C31 C71 131.9(7) .
N112 C112 C212 122.3(7) .
N112 C112 C111 114.3(7) .
C212 C112 C111 123.3(7) .
O13 C33 C43 119.1(8) .
O13 C33 C23 120.2(8) .
C43 C33 C23 120.6(8) .
N13 C53 C43 124.5(7) .
N13 C53 H53 117.7 .
C43 C53 H53 117.7 .
N14 C34 C24 106.5(6) .
N14 C34 C74 122.6(6) .
C24 C34 C74 130.8(7) .
O316 N116 O216 130.1(11) .
O316 N116 O116 115.8(10) .
O216 N116 O116 114.1(9) .
C53 C43 C33 116.6(7) .
C53 C43 C83 122.1(7) .
C33 C43 C83 121.3(8) .
C13 C23 C33 116.9(7) .
C13 C23 C63 122.2(8) .
C33 C23 C63 120.8(8) .
C46 C56 N16 124.3(7) .
C46 C56 H56 117.9 .
N16 C56 H56 117.9 .
N110 C310 C210 105.9(6) .
N110 C310 C710 124.9(7) .
C210 C310 C710 129.2(7) .
N27 C17 C27 110.8(7) .
N27 C17 C47 119.8(7) .
C27 C17 C47 129.4(7) .
C212 C312 C412 122.1(9) .
C212 C312 O112 121.4(8) .
C412 C312 O112 116.3(8) .
O314 N114 O214 124.2(10) .
O314 N114 O114 121.7(10) .
O214 N114 O114 113.9(9) .
N13 C13 C23 123.7(7) .
N13 C13 C12 115.3(8) .
C23 C13 C12 121.0(8) .
N210 C110 C210 110.8(6) .
N210 C110 C410 119.3(7) .
C210 C110 C410 129.7(7) .
N19 C19 C29 122.3(8) .
N19 C19 C18 114.8(7) .
C29 C19 C18 122.8(8) .
C51 C41 C11 110.1(6) .
C51 C41 C61 111.7(7) .
C11 C41 C61 111.5(6) .
C51 C41 H41 107.8 .
C11 C41 H41 107.8 .
C61 C41 H41 107.8 .
N113 O113 Ag1 92.7(5) .
C110 C410 C610 110.4(7) .
C110 C410 C510 110.5(7) .
C610 C410 C510 106.8(7) .
C110 C410 H410 109.7 .
C610 C410 H410 109.7 .
C510 C410 H410 109.7 .
N112 C512 C412 125.1(7) .
N112 C512 H512 117.5 .
C412 C512 H512 117.5 .
C34 C24 C14 106.1(7) .
C34 C24 H24 127.0 .
C14 C24 H24 127.0 .
C34 C74 C94 110.5(6) .
C34 C74 C84 108.0(6) .
C94 C74 C84 109.0(6) .
C34 C74 H74 109.8 .
C94 C74 H74 109.8 .
C84 C74 H74 109.8 .
C312 C212 C112 116.9(8) .
C312 C212 C612 121.5(8) .
C112 C212 C612 121.5(8) .
N17 C37 C27 104.2(7) .
N17 C37 C77 124.4(8) .
C27 C37 C77 131.3(8) .
C46 C36 C26 121.0(8) .
C46 C36 O16 119.2(8) .
C26 C36 O16 119.7(9) .
N113 O213 Ag1 99.4(5) .
C31 C21 C11 107.7(6) .
C31 C21 H21 126.1 .
C11 C21 H21 126.1 .
N21 C11 C21 111.0(6) .
N21 C11 C41 119.0(6) .
C21 C11 C41 129.9(7) .
C37 C27 C17 108.2(7) .
C37 C27 H27 125.9 .
C17 C27 H27 125.9 .
C312 C412 C512 115.9(8) .
C312 C412 C812 123.2(9) .
C512 C412 C812 120.8(8) .
C212 C612 H61A 109.5 .
C212 C612 H61B 109.5 .
H61A C612 H61B 109.5 .
C212 C612 H61C 109.5 .
H61A C612 H61C 109.5 .
H61B C612 H61C 109.5 .
N116 O116 Ag4 122.3(6) .
N116 O116 Ag4 118.8(6) 2_656
Ag4 O116 Ag4 115.3(3) 2_656
C16 C26 C36 116.9(8) .
C16 C26 C66 123.2(8) .
C36 C26 C66 119.9(8) .
C26 C66 H66A 109.5 .
C26 C66 H66B 109.5 .
H66A C66 H66B 109.5 .
C26 C66 H66C 109.5 .
H66A C66 H66C 109.5 .
H66B C66 H66C 109.5 .
N110 C111 C112 113.9(6) .
N110 C111 H11A 108.8 .
C112 C111 H11A 108.8 .
N110 C111 H11B 108.8 .
C112 C111 H11B 108.8 .
H11A C111 H11B 107.7 .
C310 C710 C810 110.0(7) .
C310 C710 C910 110.9(7) .
C810 C710 C910 111.5(8) .
C310 C710 H710 108.1 .
C810 C710 H710 108.1 .
C910 C710 H710 108.1 .
C56 C46 C36 117.2(8) .
C56 C46 C86 120.8(8) .
C36 C46 C86 122.0(8) .
N19 C59 C49 123.8(7) .
N19 C59 H59 118.1 .
C49 C59 H59 118.1 .
N17 C18 C19 115.0(6) .
N17 C18 H18A 108.5 .
C19 C18 H18A 108.5 .
N17 C18 H18B 108.5 .
C19 C18 H18B 108.5 .
H18A C18 H18B 107.5 .
N115 O115 Ag3 96.8(6) .
C54 C44 C64 112.1(8) .
C54 C44 C14 111.4(7) .
C64 C44 C14 110.0(6) .
C54 C44 H44 107.7 .
C64 C44 H44 107.7 .
C14 C44 H44 107.7 .
C412 C812 H81A 109.5 .
C412 C812 H81B 109.5 .
H81A C812 H81B 109.5 .
C412 C812 H81C 109.5 .
H81A C812 H81C 109.5 .
H81B C812 H81C 109.5 .
N11 C12 C13 115.3(6) .
N11 C12 H12A 108.5 .
C13 C12 H12A 108.5 .
N11 C12 H12B 108.5 .
C13 C12 H12B 108.5 .
H12A C12 H12B 107.5 .
C39 C49 C59 118.4(8) .
C39 C49 C89 122.7(8) .
C59 C49 C89 118.9(9) .
C31 C71 C91 109.2(7) .
C31 C71 C81 109.9(7) .
C91 C71 C81 111.2(7) .
C31 C71 H71 108.8 .
C91 C71 H71 108.8 .
C81 C71 H71 108.8 .
O112 C712 H71A 109.5 .
O112 C712 H71B 109.5 .
H71A C712 H71B 109.5 .
O112 C712 H71C 109.5 .
H71A C712 H71C 109.5 .
H71B C712 H71C 109.5 .
C67 C47 C57 110.7(8) .
C67 C47 C17 109.5(8) .
C57 C47 C17 113.1(7) .
C67 C47 H47 107.8 .
C57 C47 H47 107.8 .
C17 C47 H47 107.8 .
C46 C86 H86A 109.5 .
C46 C86 H86B 109.5 .
H86A C86 H86B 109.5 .
C46 C86 H86C 109.5 .
H86A C86 H86C 109.5 .
H86B C86 H86C 109.5 .
C310 C210 C110 106.9(7) .
C310 C210 H210 126.6 .
C110 C210 H210 126.6 .
C29 C69 H69A 109.5 .
C29 C69 H69B 109.5 .
H69A C69 H69B 109.5 .
C29 C69 H69C 109.5 .
H69A C69 H69C 109.5 .
H69B C69 H69C 109.5 .
C74 C94 H94A 109.5 .
C74 C94 H94B 109.5 .
H94A C94 H94B 109.5 .
C74 C94 H94C 109.5 .
H94A C94 H94C 109.5 .
H94B C94 H94C 109.5 .
C97 C77 C87 113.9(10) .
C97 C77 C37 111.7(8) .
C87 C77 C37 107.2(8) .
C97 C77 H77 108.0 .
C87 C77 H77 108.0 .
C37 C77 H77 108.0 .
C23 C63 H63A 109.5 .
C23 C63 H63B 109.5 .
H63A C63 H63B 109.5 .
C23 C63 H63C 109.5 .
H63A C63 H63C 109.5 .
H63B C63 H63C 109.5 .
C43 C83 H83A 109.5 .
C43 C83 H83B 109.5 .
H83A C83 H83B 109.5 .
C43 C83 H83C 109.5 .
H83A C83 H83C 109.5 .
H83B C83 H83C 109.5 .
C39 C29 C19 118.5(8) .
C39 C29 C69 120.0(8) .
C19 C29 C69 121.5(9) .
C49 C89 H89A 109.5 .
C49 C89 H89B 109.5 .
H89A C89 H89B 109.5 .
C49 C89 H89C 109.5 .
H89A C89 H89C 109.5 .
H89B C89 H89C 109.5 .
C41 C51 H51A 109.5 .
C41 C51 H51B 109.5 .
H51A C51 H51B 109.5 .
C41 C51 H51C 109.5 .
H51A C51 H51C 109.5 .
H51B C51 H51C 109.5 .
N114 O114 Ag2 105.0(6) .
C710 C810 H81D 109.5 .
C710 C810 H81E 109.5 .
H81D C810 H81E 109.5 .
C710 C810 H81F 109.5 .
H81D C810 H81F 109.5 .
H81E C810 H81F 109.5 .
C41 C61 H61D 109.5 .
C41 C61 H61E 109.5 .
H61D C61 H61E 109.5 .
C41 C61 H61F 109.5 .
H61D C61 H61F 109.5 .
H61E C61 H61F 109.5 .
C71 C81 H81G 109.5 .
C71 C81 H81H 109.5 .
H81G C81 H81H 109.5 .
C71 C81 H81I 109.5 .
H81G C81 H81I 109.5 .
H81H C81 H81I 109.5 .
C410 C510 H51D 109.5 .
C410 C510 H51E 109.5 .
H51D C510 H51E 109.5 .
C410 C510 H51F 109.5 .
H51D C510 H51F 109.5 .
H51E C510 H51F 109.5 .
O13 C73 H73A 109.5 .
O13 C73 H73B 109.5 .
H73A C73 H73B 109.5 .
O13 C73 H73C 109.5 .
H73A C73 H73C 109.5 .
H73B C73 H73C 109.5 .
C74 C84 H84A 109.5 .
C74 C84 H84B 109.5 .
H84A C84 H84B 109.5 .
C74 C84 H84C 109.5 .
H84A C84 H84C 109.5 .
H84B C84 H84C 109.5 .
C47 C57 H57A 109.5 .
C47 C57 H57B 109.5 .
H57A C57 H57B 109.5 .
C47 C57 H57C 109.5 .
H57A C57 H57C 109.5 .
H57B C57 H57C 109.5 .
C710 C910 H91A 109.5 .
C710 C910 H91B 109.5 .
H91A C910 H91B 109.5 .
C710 C910 H91C 109.5 .
H91A C910 H91C 109.5 .
H91B C910 H91C 109.5 .
C47 C67 H67A 109.5 .
C47 C67 H67B 109.5 .
H67A C67 H67B 109.5 .
C47 C67 H67C 109.5 .
H67A C67 H67C 109.5 .
H67B C67 H67C 109.5 .
C410 C610 H61G 109.5 .
C410 C610 H61H 109.5 .
H61G C610 H61H 109.5 .
C410 C610 H61I 109.5 .
H61G C610 H61I 109.5 .
H61H C610 H61I 109.5 .
O19 C79 H79A 109.5 .
O19 C79 H79B 109.5 .
H79A C79 H79B 109.5 .
O19 C79 H79C 109.5 .
H79A C79 H79C 109.5 .
H79B C79 H79C 109.5 .
C44 C64 H64A 109.5 .
C44 C64 H64B 109.5 .
H64A C64 H64B 109.5 .
C44 C64 H64C 109.5 .
H64A C64 H64C 109.5 .
H64B C64 H64C 109.5 .
C44 C54 H54A 109.5 .
C44 C54 H54B 109.5 .
H54A C54 H54B 109.5 .
C44 C54 H54C 109.5 .
H54A C54 H54C 109.5 .
H54B C54 H54C 109.5 .
C71 C91 H91D 109.5 .
C71 C91 H91E 109.5 .
H91D C91 H91E 109.5 .
C71 C91 H91F 109.5 .
H91D C91 H91F 109.5 .
H91E C91 H91F 109.5 .
O16 C76 H76A 109.5 .
O16 C76 H76B 109.5 .
H76A C76 H76B 109.5 .
O16 C76 H76C 109.5 .
H76A C76 H76C 109.5 .
H76B C76 H76C 109.5 .
C77 C87 H87A 109.5 .
C77 C87 H87B 109.5 .
H87A C87 H87B 109.5 .
C77 C87 H87C 109.5 .
H87A C87 H87C 109.5 .
H87B C87 H87C 109.5 .
C77 C97 H97A 109.5 .
C77 C97 H97B 109.5 .
H97A C97 H97B 109.5 .
C77 C97 H97C 109.5 .
H97A C97 H97C 109.5 .
H97B C97 H97C 109.5 .
N115 O215 Ag3 96.0(6) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N21 2.170(6) .
Ag1 N16 2.284(6) .
Ag1 O213 2.431(6) .
Ag1 O113 2.569(6) .
Ag3 N27 2.265(6) .
Ag3 N112 2.279(6) .
Ag3 O115 2.461(7) .
Ag3 O215 2.512(7) .
Ag4 N210 2.196(5) .
Ag4 N19 2.245(6) .
Ag4 O116 2.550(7) .
Ag4 O116 2.585(7) 2_656
Ag2 N24 2.201(6) .
Ag2 N13 2.267(6) .
Ag2 O114 2.472(7) .
N210 C110 1.345(7) .
N210 N110 1.360(7) .
N21 C11 1.340(8) .
N21 N11 1.373(7) .
N11 C31 1.349(8) .
N11 C12 1.456(7) .
N27 C17 1.320(8) .
N27 N17 1.385(7) .
O112 C312 1.381(9) .
O112 C712 1.433(8) .
N113 O113 1.226(7) .
N113 O213 1.231(7) .
N113 O313 1.231(7) .
N24 N14 1.360(6) .
N24 C14 1.360(8) .
O16 C36 1.396(8) .
O16 C76 1.437(8) .
N16 C16 1.340(8) .
N16 C56 1.343(8) .
N112 C512 1.325(8) .
N112 C112 1.349(8) .
N13 C13 1.321(8) .
N13 C53 1.345(8) .
N19 C59 1.348(8) .
N19 C19 1.356(8) .
N14 C34 1.345(8) .
N14 C15 1.477(7) .
N17 C37 1.347(8) .
N17 C18 1.490(8) .
N110 C310 1.361(8) .
N110 C111 1.446(7) .
O13 C33 1.375(8) .
O13 C73 1.420(8) .
C39 C49 1.363(10) .
C39 O19 1.364(9) .
C39 C29 1.383(10) .
O19 C79 1.404(8) .
C14 C24 1.402(8) .
C14 C44 1.512(9) .
C15 C16 1.506(9) .
C15 H15A 0.9700 .
C15 H15B 0.9700 .
C16 C26 1.373(9) .
N115 O215 1.178(8) .
N115 O315 1.220(8) .
N115 O115 1.239(8) .
C31 C21 1.371(8) .
C31 C71 1.492(9) .
C112 C212 1.409(9) .
C112 C111 1.534(9) .
C33 C43 1.383(9) .
C33 C23 1.406(9) .
C53 C43 1.378(9) .
C53 H53 0.9300 .
C34 C24 1.366(8) .
C34 C74 1.515(9) .
N116 O316 1.158(8) .
N116 O216 1.182(9) .
N116 O116 1.260(9) .
C43 C83 1.493(9) .
C23 C13 1.389(10) .
C23 C63 1.489(9) .
C56 C46 1.335(9) .
C56 H56 0.9300 .
C310 C210 1.369(9) .
C310 C710 1.503(9) .
C17 C27 1.376(9) .
C17 C47 1.524(9) .
C312 C212 1.371(10) .
C312 C412 1.373(10) .
N114 O314 1.190(8) .
N114 O214 1.211(9) .
N114 O114 1.215(8) .
C13 C12 1.510(9) .
C110 C210 1.376(9) .
C110 C410 1.501(9) .
C19 C29 1.399(9) .
C19 C18 1.495(9) .
C41 C51 1.513(9) .
C41 C11 1.517(9) .
C41 C61 1.529(9) .
C41 H41 0.9800 .
C410 C610 1.523(10) .
C410 C510 1.524(10) .
C410 H410 0.9800 .
C512 C412 1.387(10) .
C512 H512 0.9300 .
C24 H24 0.9300 .
C74 C94 1.516(8) .
C74 C84 1.543(9) .
C74 H74 0.9800 .
C212 C612 1.506(9) .
C37 C27 1.373(9) .
C37 C77 1.519(10) .
C36 C46 1.384(10) .
C36 C26 1.389(10) .
C21 C11 1.374(8) .
C21 H21 0.9300 .
C27 H27 0.9300 .
C412 C812 1.517(9) .
C612 H61A 0.9600 .
C612 H61B 0.9600 .
C612 H61C 0.9600 .
O116 Ag4 2.585(7) 2_656
C26 C66 1.528(9) .
C66 H66A 0.9600 .
C66 H66B 0.9600 .
C66 H66C 0.9600 .
C111 H11A 0.9700 .
C111 H11B 0.9700 .
C710 C810 1.511(10) .
C710 C910 1.530(10) .
C710 H710 0.9800 .
C46 C86 1.516(9) .
C59 C49 1.386(9) .
C59 H59 0.9300 .
C18 H18A 0.9700 .
C18 H18B 0.9700 .
C44 C54 1.455(10) .
C44 C64 1.488(10) .
C44 H44 0.9800 .
C812 H81A 0.9600 .
C812 H81B 0.9600 .
C812 H81C 0.9600 .
C12 H12A 0.9700 .
C12 H12B 0.9700 .
C49 C89 1.537(10) .
C71 C91 1.530(10) .
C71 C81 1.536(10) .
C71 H71 0.9800 .
C712 H71A 0.9600 .
C712 H71B 0.9600 .
C712 H71C 0.9600 .
C47 C67 1.452(11) .
C47 C57 1.470(10) .
C47 H47 0.9800 .
C86 H86A 0.9600 .
C86 H86B 0.9600 .
C86 H86C 0.9600 .
C210 H210 0.9300 .
C69 C29 1.532(9) .
C69 H69A 0.9600 .
C69 H69B 0.9600 .
C69 H69C 0.9600 .
C94 H94A 0.9600 .
C94 H94B 0.9600 .
C94 H94C 0.9600 .
C77 C97 1.474(12) .
C77 C87 1.507(11) .
C77 H77 0.9800 .
C63 H63A 0.9600 .
C63 H63B 0.9600 .
C63 H63C 0.9600 .
C83 H83A 0.9600 .
C83 H83B 0.9600 .
C83 H83C 0.9600 .
C89 H89A 0.9600 .
C89 H89B 0.9600 .
C89 H89C 0.9600 .
C51 H51A 0.9600 .
C51 H51B 0.9600 .
C51 H51C 0.9600 .
C810 H81D 0.9600 .
C810 H81E 0.9600 .
C810 H81F 0.9600 .
C61 H61D 0.9600 .
C61 H61E 0.9600 .
C61 H61F 0.9600 .
C81 H81G 0.9600 .
C81 H81H 0.9600 .
C81 H81I 0.9600 .
C510 H51D 0.9600 .
C510 H51E 0.9600 .
C510 H51F 0.9600 .
C73 H73A 0.9600 .
C73 H73B 0.9600 .
C73 H73C 0.9600 .
C84 H84A 0.9600 .
C84 H84B 0.9600 .
C84 H84C 0.9600 .
C57 H57A 0.9600 .
C57 H57B 0.9600 .
C57 H57C 0.9600 .
C910 H91A 0.9600 .
C910 H91B 0.9600 .
C910 H91C 0.9600 .
C67 H67A 0.9600 .
C67 H67B 0.9600 .
C67 H67C 0.9600 .
C610 H61G 0.9600 .
C610 H61H 0.9600 .
C610 H61I 0.9600 .
C79 H79A 0.9600 .
C79 H79B 0.9600 .
C79 H79C 0.9600 .
C64 H64A 0.9600 .
C64 H64B 0.9600 .
C64 H64C 0.9600 .
C54 H54A 0.9600 .
C54 H54B 0.9600 .
C54 H54C 0.9600 .
C91 H91D 0.9600 .
C91 H91E 0.9600 .
C91 H91F 0.9600 .
C76 H76A 0.9600 .
C76 H76B 0.9600 .
C76 H76C 0.9600 .
C87 H87A 0.9600 .
C87 H87B 0.9600 .
C87 H87C 0.9600 .
C97 H97A 0.9600 .
C97 H97B 0.9600 .
C97 H97C 0.9600 .
