#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:39:21 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179487 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/84/4338436.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4338436
loop_
_publ_author_name
'Fang, Wei-Hui'
'Yang, Guo-Yu'
_publ_section_title
;
 Pillared-layer cluster organic frameworks constructed from nanoscale ln10
 and cu16 clusters.
;
_journal_issue                   11
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5631
_journal_page_last               5636
_journal_paper_doi               10.1021/ic500404z
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C132 H96 Cu8 Dy5 I8 N11 O28'
_chemical_formula_weight         4620.22
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 118.430(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   54.826(8)
_cell_length_b                   14.0542(18)
_cell_length_c                   40.978(6)
_cell_measurement_reflns_used    32540
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      27.4797
_cell_measurement_theta_min      3.0190
_cell_volume                     27767(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'saturn 70'
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0392
_diffrn_reflns_av_sigmaI/netI    0.0390
_diffrn_reflns_limit_h_max       71
_diffrn_reflns_limit_h_min       -71
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       53
_diffrn_reflns_limit_l_min       -52
_diffrn_reflns_number            121910
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         2.00
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    5.704
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.5950
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            'dark red'
_exptl_crystal_density_diffrn    2.210
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallelepiped
_exptl_crystal_F_000             17400
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.14
_refine_diff_density_max         5.627
_refine_diff_density_min         -4.950
_refine_diff_density_rms         0.284
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1825
_refine_ls_number_reflns         31726
_refine_ls_number_restraints     147
_refine_ls_restrained_S_all      1.074
_refine_ls_R_factor_all          0.0865
_refine_ls_R_factor_gt           0.0758
_refine_ls_shift/su_max          0.009
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1205P)²+958.3865P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2101
_refine_ls_wR_factor_ref         0.2213
_reflns_number_gt                27188
_reflns_number_total             31726
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500404z_si_002.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338436--4338437.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               4338436
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.222393(7) 0.92096(3) 0.356617(9) 0.02589(8) Uani 1 1 d . . .
Dy2 Dy 0.241634(6) 0.89633(2) 0.463812(9) 0.02216(7) Uani 1 1 d . . .
Dy3 Dy 0.247791(6) 0.65596(2) 0.414629(9) 0.02267(7) Uani 1 1 d . . .
Dy4 Dy 0.231764(6) 0.42697(2) 0.457751(9) 0.02192(7) Uani 1 1 d . . .
Dy5 Dy 0.240801(7) 0.15152(2) 0.425261(9) 0.02426(7) Uani 1 1 d . . .
Cu1 Cu 0.53144(7) 0.5162(5) 0.66311(19) 0.246(2) Uani 0.80 1 d PU . .
Cu1' Cu 0.52359(15) 0.4392(6) 0.6292(2) 0.0567(7) Uani 0.20 1 d PU . .
Cu2 Cu 0.56128(8) 0.6606(6) 0.66869(15) 0.273(2) Uani 0.80 1 d PU . .
Cu2' Cu 0.5721(3) 0.6133(13) 0.6850(5) 0.1397(13) Uani 0.20 1 d P . .
Cu3 Cu 0.54817(7) 0.4394(3) 0.58179(12) 0.1397(13) Uani 0.80 1 d P . .
Cu3' Cu 0.54826(17) 0.3698(6) 0.5757(3) 0.089(4) Uani 0.20 1 d P . .
Cu4 Cu 0.49844(6) 0.3147(3) 0.52422(15) 0.1965(17) Uani 1 1 d . . .
Cu5 Cu 0.50811(3) 0.78536(18) 0.58587(5) 0.0864(6) Uani 1 1 d . . .
Cu6 Cu 0.57549(5) 0.33386(16) 0.64126(7) 0.1087(8) Uani 1 1 d . . .
Cu7 Cu 0.51609(3) 1.01121(19) 0.56975(6) 0.1001(7) Uani 1 1 d . . .
Cu8 Cu 0.53628(2) 0.85847(11) 0.71142(5) 0.0611(4) Uani 1 1 d . . .
I1 I 0.534324(15) 0.89749(8) 0.64192(2) 0.0726(3) Uani 1 1 d . . .
I2 I 0.51253(3) 0.83020(11) 0.52634(4) 0.0691(4) Uani 0.80 1 d P . .
I2' I 0.51268(8) 0.8600(4) 0.53138(14) 0.0508(11) Uani 0.20 1 d P . .
I3 I 0.55543(2) 0.68752(9) 0.72659(4) 0.0660(3) Uani 0.80 1 d P . .
I3' I 0.5574(2) 0.6885(6) 0.7422(3) 0.158(5) Uani 0.20 1 d P . .
I4 I 0.52723(3) 0.60071(11) 0.60245(4) 0.0795(4) Uani 0.80 1 d P . .
I4' I 0.51983(17) 0.5833(6) 0.5831(3) 0.123(3) Uani 0.20 1 d PU . .
I5 I 0.53310(6) 0.4134(2) 0.51532(8) 0.1814(11) Uani 0.80 1 d PU . .
I5' I 0.5073(8) 0.518(3) 0.5279(10) 0.47(2) Uiso 0.20 1 d P . .
I6 I 0.57479(4) 0.43417(11) 0.69781(5) 0.1074(5) Uani 0.80 1 d P . .
I6' I 0.55594(15) 0.3983(8) 0.7127(4) 0.1965(17) Uani 0.20 1 d P . .
I7 I 0.60127(3) 0.44553(11) 0.61526(5) 0.1193(4) Uani 0.80 1 d P . .
I7' I 0.64513(9) 0.4754(3) 0.64507(16) 0.0768(14) Uani 0.20 1 d P . .
I8 I 0.52281(3) 0.28040(13) 0.60079(5) 0.1281(5) Uani 1 1 d . . .
C1 C 0.4072(4) 1.2775(18) 0.3661(7) 0.136(8) Uani 1 1 d . . .
H1A H 0.4253 1.2759 0.3852 0.164 Uiso 1 1 calc R . .
C2 C 0.3858(3) 1.2442(13) 0.3735(6) 0.104(5) Uani 1 1 d . . .
H2A H 0.3897 1.2183 0.3964 0.125 Uiso 1 1 calc R . .
C3 C 0.3593(2) 1.2525(11) 0.3453(4) 0.088(4) Uani 1 1 d . . .
C4 C 0.3548(4) 1.2966(16) 0.3118(5) 0.158(5) Uani 1 1 d U . .
H4A H 0.3438 1.3535 0.3084 0.190 Uiso 1 1 calc R . .
H4B H 0.3438 1.2538 0.2915 0.190 Uiso 1 1 calc R . .
C5 C 0.3801(5) 1.3240(19) 0.3089(7) 0.135(5) Uani 1 1 d U . .
H5A H 0.3780 1.3523 0.2872 0.161 Uiso 1 1 calc R . .
C6 C 0.3166(2) 1.1558(8) 0.3249(3) 0.058(3) Uani 1 1 d . . .
H6A H 0.3186 1.1349 0.3048 0.070 Uiso 1 1 calc R . .
C7 C 0.2943(2) 1.1204(8) 0.3303(3) 0.050(2) Uani 1 1 d . . .
H7A H 0.2817 1.0770 0.3137 0.059 Uiso 1 1 calc R . .
C8 C 0.29179(15) 1.1521(6) 0.3606(2) 0.0320(16) Uani 1 1 d . . .
C9 C 0.31017(19) 1.2205(7) 0.3845(3) 0.042(2) Uani 1 1 d . . .
H9A H 0.3077 1.2453 0.4038 0.050 Uiso 1 1 calc R . .
C10 C 0.3325(2) 1.2516(9) 0.3792(3) 0.058(3) Uani 1 1 d . . .
H10A H 0.3456 1.2936 0.3960 0.069 Uiso 1 1 calc R . .
C11 C 0.3349(2) 1.2196(8) 0.3491(3) 0.059(3) Uani 1 1 d . . .
C12 C 0.26934(16) 1.1148(6) 0.3689(2) 0.0325(17) Uani 1 1 d . . .
C13 C 0.44239(19) 0.8736(11) 0.4363(3) 0.061(3) Uani 1 1 d . . .
H13A H 0.4573 0.8336 0.4501 0.073 Uiso 1 1 calc R . .
C14 C 0.4160(2) 0.8470(10) 0.4298(3) 0.057(3) Uani 1 1 d . . .
H14A H 0.4139 0.7893 0.4393 0.068 Uiso 1 1 calc R . .
C15 C 0.39330(16) 0.9014(8) 0.4104(3) 0.042(2) Uani 1 1 d . . .
C16 C 0.39749(18) 0.9894(9) 0.3969(3) 0.053(3) Uani 1 1 d . . .
H16A H 0.3828 1.0308 0.3836 0.064 Uiso 1 1 calc R . .
C17 C 0.42420(18) 1.0119(11) 0.4042(4) 0.065(4) Uani 1 1 d . . .
H17A H 0.4270 1.0699 0.3955 0.078 Uiso 1 1 calc R . .
C18 C 0.35909(16) 0.7753(7) 0.4018(3) 0.043(2) Uani 1 1 d . . .
H18A H 0.3722 0.7298 0.4042 0.052 Uiso 1 1 calc R . .
C19 C 0.33273(15) 0.7470(7) 0.3970(3) 0.0368(19) Uani 1 1 d . . .
H19A H 0.3290 0.6826 0.3976 0.044 Uiso 1 1 calc R . .
C20 C 0.31263(14) 0.8125(6) 0.3916(2) 0.0279(16) Uani 1 1 d . . .
C21 C 0.31848(17) 0.9077(7) 0.3915(3) 0.043(2) Uani 1 1 d . . .
H21A H 0.3051 0.9530 0.3879 0.052 Uiso 1 1 calc R . .
C22 C 0.34424(18) 0.9362(7) 0.3967(3) 0.047(2) Uani 1 1 d . . .
H22A H 0.3476 1.0008 0.3962 0.056 Uiso 1 1 calc R . .
C23 C 0.36513(15) 0.8720(7) 0.4029(2) 0.0339(18) Uani 1 1 d . . .
C24 C 0.28543(13) 0.7820(6) 0.38917(19) 0.0247(15) Uani 1 1 d . . .
C25 C 0.4571(2) 0.7797(15) 0.5935(4) 0.089(6) Uani 1 1 d . . .
H25A H 0.4695 0.7907 0.6184 0.107 Uiso 1 1 calc R . .
C26 C 0.4295(2) 0.7730(14) 0.5829(3) 0.080(5) Uani 1 1 d . . .
H26A H 0.4238 0.7789 0.6009 0.096 Uiso 1 1 calc R . .
C27 C 0.41028(14) 0.7582(8) 0.5477(3) 0.042(2) Uani 1 1 d . . .
C28 C 0.4200(2) 0.7544(17) 0.5235(3) 0.104(7) Uani 1 1 d . . .
H28A H 0.4078 0.7461 0.4984 0.125 Uiso 1 1 calc R . .
C29 C 0.4488(2) 0.7631(18) 0.5360(4) 0.116(8) Uani 1 1 d . . .
H29A H 0.4547 0.7626 0.5182 0.140 Uiso 1 1 calc R . .
C30 C 0.37018(16) 0.7367(7) 0.5613(2) 0.040(2) Uani 1 1 d . . .
H30A H 0.3827 0.7261 0.5861 0.047 Uiso 1 1 calc R . .
C31 C 0.34251(15) 0.7364(7) 0.5504(2) 0.0342(19) Uani 1 1 d . . .
H31A H 0.3365 0.7275 0.5679 0.041 Uiso 1 1 calc R . .
C32 C 0.32316(13) 0.7494(5) 0.51320(19) 0.0226(14) Uani 1 1 d . . .
C33 C 0.33232(15) 0.7668(9) 0.4880(2) 0.045(3) Uani 1 1 d . . .
H33A H 0.3196 0.7792 0.4634 0.053 Uiso 1 1 calc R . .
C34 C 0.36065(16) 0.7660(9) 0.4990(2) 0.051(3) Uani 1 1 d . . .
H34A H 0.3665 0.7745 0.4813 0.061 Uiso 1 1 calc R . .
C35 C 0.38028(14) 0.7525(7) 0.5362(2) 0.0347(19) Uani 1 1 d . . .
C36 C 0.29319(13) 0.7480(5) 0.50177(18) 0.0191(13) Uani 1 1 d . . .
C37 C 0.44885(18) 0.3028(9) 0.5360(3) 0.180(8) Uani 1 1 d GU . .
H37A H 0.4608 0.2764 0.5590 0.216 Uiso 1 1 calc R . .
C38 C 0.4217(2) 0.3253(11) 0.5273(3) 0.174(11) Uani 1 1 d G . .
H38A H 0.4155 0.3139 0.5444 0.209 Uiso 1 1 calc R . .
C39 C 0.40395(18) 0.3648(12) 0.4930(3) 0.094(5) Uani 1 1 d G . .
C40 C 0.4133(2) 0.3818(11) 0.4673(3) 0.125(6) Uani 1 1 d GU . .
H40A H 0.4014 0.4082 0.4444 0.150 Uiso 1 1 calc R . .
C41 C 0.4404(3) 0.3593(12) 0.4761(4) 0.181(10) Uani 1 1 d GU . .
H41A H 0.4466 0.3707 0.4589 0.217 Uiso 1 1 calc R . .
N4 N 0.45818(19) 0.3198(11) 0.5104(4) 0.145(6) Uani 1 1 d GU . .
C42 C 0.3615(2) 0.3437(9) 0.4976(4) 0.078(4) Uani 1 1 d . . .
H42A H 0.3687 0.2864 0.5097 0.093 Uiso 1 1 calc R . .
C43 C 0.33561(18) 0.3722(8) 0.4916(3) 0.057(3) Uani 1 1 d . . .
H43A H 0.3253 0.3327 0.4986 0.068 Uiso 1 1 calc R . .
C44 C 0.32485(14) 0.4583(6) 0.4752(2) 0.0325(18) Uani 1 1 d . . .
C45 C 0.33982(19) 0.5157(9) 0.4641(4) 0.068(3) Uani 1 1 d . . .
H45A H 0.3328 0.5744 0.4531 0.081 Uiso 1 1 calc R . .
C46 C 0.3661(2) 0.4847(12) 0.4695(5) 0.095(4) Uani 1 1 d . . .
H46A H 0.3762 0.5227 0.4617 0.114 Uiso 1 1 calc R . .
C47 C 0.3767(2) 0.3984(10) 0.4863(4) 0.076(4) Uani 1 1 d . . .
C48 C 0.29714(14) 0.4923(6) 0.4687(2) 0.0269(16) Uani 1 1 d . . .
C49 C 0.4671(2) 0.0301(12) 0.5792(4) 0.080(4) Uani 1 1 d . . .
H49A H 0.4800 0.0359 0.6041 0.096 Uiso 1 1 calc R . .
C50 C 0.4390(2) 0.0318(12) 0.5697(3) 0.070(4) Uani 1 1 d . . .
H50A H 0.4339 0.0364 0.5882 0.084 Uiso 1 1 calc R . .
C51 C 0.41940(16) 0.0269(8) 0.5340(3) 0.045(2) Uani 1 1 d . . .
C52 C 0.4288(2) 0.0181(11) 0.5079(3) 0.066(4) Uani 1 1 d . . .
H52A H 0.4164 0.0123 0.4828 0.080 Uiso 1 1 calc R . .
C53 C 0.4574(2) 0.0183(12) 0.5208(4) 0.075(4) Uani 1 1 d . . .
H53A H 0.4634 0.0164 0.5030 0.090 Uiso 1 1 calc R . .
C54 C 0.37890(15) -0.0133(6) 0.5441(2) 0.0339(19) Uani 1 1 d . . .
H54A H 0.3912 -0.0420 0.5663 0.041 Uiso 1 1 calc R . .
C55 C 0.35077(14) -0.0118(6) 0.5335(2) 0.0287(16) Uani 1 1 d . . .
H55A H 0.3443 -0.0427 0.5480 0.034 Uiso 1 1 calc R . .
C56 C 0.33206(13) 0.0362(5) 0.50108(19) 0.0230(14) Uani 1 1 d . . .
C57 C 0.34268(15) 0.0784(7) 0.4799(2) 0.0362(19) Uani 1 1 d . . .
H57A H 0.3307 0.1110 0.4584 0.043 Uiso 1 1 calc R . .
C58 C 0.37020(17) 0.0735(8) 0.4896(3) 0.047(2) Uani 1 1 d . . .
H58A H 0.3765 0.1014 0.4744 0.057 Uiso 1 1 calc R . .
C59 C 0.38890(16) 0.0279(7) 0.5217(3) 0.039(2) Uani 1 1 d . . .
C60 C 0.30192(13) 0.0464(5) 0.49107(19) 0.0219(14) Uani 1 1 d . . .
C61 C 0.26361(19) 0.3169(6) 0.2142(2) 0.046(4) Uani 0.545(8) 1 d PG A 1
H61A H 0.2599 0.2645 0.1987 0.055 Uiso 0.545(8) 1 calc PR A 1
C62 C 0.2603(2) 0.3103(7) 0.2458(3) 0.044(4) Uani 0.545(8) 1 d PG A 1
H62A H 0.2544 0.2534 0.2514 0.053 Uiso 0.545(8) 1 calc PR A 1
C63 C 0.2659(3) 0.3886(8) 0.2690(3) 0.038(5) Uani 0.545(8) 1 d PG A 1
C64 C 0.2747(3) 0.4735(7) 0.2606(3) 0.051(4) Uani 0.545(8) 1 d PGU A 1
H64A H 0.2784 0.5259 0.2762 0.061 Uiso 0.545(8) 1 calc PR A 1
C65 C 0.2780(3) 0.4801(7) 0.2291(3) 0.060(5) Uani 0.545(8) 1 d PG A 1
H65A H 0.2838 0.5370 0.2235 0.072 Uiso 0.545(8) 1 calc PR A 1
N6 N 0.2724(2) 0.4018(7) 0.2059(2) 0.0392(18) Uani 0.545(8) 1 d PG . 1
C61' C 0.2453(2) 0.3738(11) 0.2011(3) 0.068(6) Uani 0.455(8) 1 d PGU A 2
H61B H 0.2302 0.3651 0.1777 0.081 Uiso 0.455(8) 1 calc PR A 2
C62' C 0.2418(2) 0.3701(13) 0.2324(4) 0.063(5) Uani 0.455(8) 1 d PGU A 2
H62B H 0.2243 0.3588 0.2300 0.075 Uiso 0.455(8) 1 calc PR A 2
C63' C 0.2644(3) 0.3831(14) 0.2674(3) 0.037(6) Uani 0.455(8) 1 d PGU A 2
C64' C 0.2905(3) 0.3999(15) 0.2711(3) 0.073(10) Uani 0.455(8) 1 d PG A 2
H64B H 0.3056 0.4086 0.2945 0.087 Uiso 0.455(8) 1 calc PR A 2
C65' C 0.2941(2) 0.4036(15) 0.2397(4) 0.057(7) Uani 0.455(8) 1 d PG A 2
H65B H 0.3116 0.4149 0.2421 0.068 Uiso 0.455(8) 1 calc PR A 2
N6' N 0.2715(3) 0.3906(12) 0.2047(3) 0.0392(18) Uani 0.455(8) 1 d PG . 2
C66 C 0.24232(18) 0.3181(7) 0.3039(2) 0.0372(19) Uani 1 1 d . A .
H66A H 0.2338 0.2725 0.2854 0.045 Uiso 1 1 calc R . .
C67 C 0.23713(16) 0.3204(6) 0.33376(19) 0.0289(16) Uani 1 1 d . . .
H67A H 0.2257 0.2746 0.3358 0.035 Uiso 1 1 calc R . .
C68 C 0.24892(14) 0.3912(5) 0.36107(19) 0.0236(14) Uani 1 1 d . . .
C69 C 0.26680(17) 0.4562(7) 0.3591(2) 0.0357(19) Uani 1 1 d . . .
H69A H 0.2748 0.5030 0.3772 0.043 Uiso 1 1 calc R . .
C70 C 0.27299(18) 0.4520(7) 0.3296(2) 0.0390(19) Uani 1 1 d . A .
H70A H 0.2856 0.4945 0.3287 0.047 Uiso 1 1 calc R . .
C71 C 0.26016(17) 0.3839(7) 0.3016(2) 0.0341(18) Uani 1 1 d . . .
C72 C 0.24036(13) 0.4014(5) 0.39049(17) 0.0190(13) Uani 1 1 d . . .
C73 C 0.0889(3) 0.3637(10) 0.1694(4) 0.071(4) Uani 1 1 d . . .
H73A H 0.0698 0.3689 0.1590 0.085 Uiso 1 1 calc R . .
C74 C 0.1056(2) 0.4394(9) 0.1903(3) 0.056(3) Uani 1 1 d . . .
H74A H 0.0974 0.4959 0.1919 0.067 Uiso 1 1 calc R . .
C75 C 0.1340(2) 0.4311(8) 0.2085(3) 0.048(2) Uani 1 1 d . . .
C76 C 0.1450(3) 0.3495(9) 0.2015(4) 0.079(4) Uani 1 1 d . . .
H76A H 0.1640 0.3406 0.2125 0.095 Uiso 1 1 calc R . .
C77 C 0.1262(3) 0.2790(12) 0.1769(4) 0.079(4) Uani 1 1 d . . .
H77A H 0.1334 0.2275 0.1699 0.094 Uiso 1 1 calc R . .
C78 C 0.1594(2) 0.6598(6) 0.2630(3) 0.042(2) Uani 1 1 d . . .
H78A H 0.1530 0.7214 0.2622 0.050 Uiso 1 1 calc R . .
C79 C 0.1435(2) 0.5967(8) 0.2355(3) 0.049(3) Uani 1 1 d . . .
H79A H 0.1266 0.6163 0.2163 0.059 Uiso 1 1 calc R . .
C80 C 0.1525(2) 0.5033(7) 0.2358(3) 0.044(2) Uani 1 1 d . . .
C81 C 0.1785(2) 0.4767(7) 0.2644(3) 0.054(3) Uani 1 1 d . . .
H81A H 0.1855 0.4164 0.2643 0.065 Uiso 1 1 calc R . .
C82 C 0.1943(2) 0.5406(8) 0.2935(3) 0.051(3) Uani 1 1 d . . .
H82A H 0.2109 0.5209 0.3134 0.062 Uiso 1 1 calc R . .
C83 C 0.18496(17) 0.6330(6) 0.2922(2) 0.0319(18) Uani 1 1 d . . .
C84 C 0.20270(17) 0.7000(6) 0.3233(2) 0.0331(18) Uani 1 1 d . . .
C85 C 0.0182(3) 0.279(2) 0.3399(6) 0.157(11) Uani 1 1 d . . .
H85A H 0.0062 0.2710 0.3499 0.188 Uiso 1 1 calc R . .
C86 C 0.0464(2) 0.2664(14) 0.3628(5) 0.094(6) Uani 1 1 d . . .
H86A H 0.0531 0.2613 0.3882 0.113 Uiso 1 1 calc R . .
C87 C 0.0643(3) 0.2613(13) 0.3493(5) 0.092(4) Uani 1 1 d U . .
C88 C 0.0527(5) 0.2742(18) 0.3128(6) 0.124(5) Uani 1 1 d U . .
H88A H 0.0644 0.2727 0.3023 0.149 Uiso 1 1 calc R . .
C89 C 0.0237(5) 0.290(2) 0.2881(8) 0.151(7) Uani 1 1 d U . .
C90 C 0.13766(17) 0.2880(6) 0.4252(3) 0.040(2) Uani 1 1 d . . .
H90A H 0.1467 0.3186 0.4480 0.048 Uiso 1 1 calc R . .
C91 C 0.10884(18) 0.2873(7) 0.4062(3) 0.048(2) Uani 1 1 d . . .
H91A H 0.0988 0.3132 0.4171 0.057 Uiso 1 1 calc R . .
C92 C 0.0954(2) 0.2495(8) 0.3721(3) 0.054(3) Uani 1 1 d . . .
C93 C 0.1104(2) 0.2031(8) 0.3573(3) 0.054(3) Uani 1 1 d . . .
H93A H 0.1010 0.1742 0.3341 0.065 Uiso 1 1 calc R . .
C94 C 0.13847(18) 0.1997(7) 0.3765(3) 0.040(2) Uani 1 1 d . . .
H94A H 0.1482 0.1672 0.3665 0.048 Uiso 1 1 calc R . .
C95 C 0.15309(15) 0.2442(5) 0.4109(2) 0.0290(16) Uani 1 1 d . . .
C96 C 0.18399(14) 0.2495(5) 0.4296(2) 0.0267(15) Uani 1 1 d . . .
C97 C 0.0197(2) 0.7086(10) 0.3034(4) 0.071(4) Uani 1 1 d . . .
H97A H 0.0114 0.7681 0.2974 0.085 Uiso 1 1 calc R . .
C98 C 0.04797(19) 0.7048(8) 0.3157(4) 0.064(3) Uani 1 1 d . . .
H98A H 0.0579 0.7599 0.3175 0.076 Uiso 1 1 calc R . .
C99 C 0.06117(16) 0.6176(7) 0.3255(2) 0.039(2) Uani 1 1 d . . .
C100 C 0.0443(2) 0.5411(9) 0.3199(6) 0.100(7) Uani 1 1 d . . .
H10B H 0.0519 0.4802 0.3248 0.120 Uiso 1 1 calc R . .
C101 C 0.0167(2) 0.5528(10) 0.3072(7) 0.118(8) Uani 1 1 d . . .
H10C H 0.0062 0.4983 0.3039 0.141 Uiso 1 1 calc R . .
C102 C 0.13743(15) 0.6688(6) 0.3559(2) 0.0290(17) Uani 1 1 d . . .
H10D H 0.1482 0.7183 0.3548 0.035 Uiso 1 1 calc R . .
C103 C 0.10880(15) 0.6797(6) 0.3402(3) 0.036(2) Uani 1 1 d . . .
H10E H 0.1007 0.7370 0.3288 0.043 Uiso 1 1 calc R . .
C104 C 0.09202(15) 0.6068(7) 0.3411(2) 0.0330(18) Uani 1 1 d . . .
C105 C 0.10460(15) 0.5215(7) 0.3583(2) 0.0353(19) Uani 1 1 d . . .
H10F H 0.0938 0.4721 0.3595 0.042 Uiso 1 1 calc R . .
C106 C 0.13326(15) 0.5094(6) 0.3737(2) 0.0300(17) Uani 1 1 d . . .
H10G H 0.1413 0.4513 0.3841 0.036 Uiso 1 1 calc R . .
C107 C 0.14985(14) 0.5841(5) 0.37342(19) 0.0226(15) Uani 1 1 d . . .
C108 C 0.18072(14) 0.5688(5) 0.39231(19) 0.0233(15) Uani 1 1 d . . .
C109 C 0.0292(3) 0.9852(13) 0.3807(4) 0.108(8) Uani 0.545(8) 1 d PGU A 1
H10H H 0.0252 0.9854 0.4004 0.130 Uiso 0.545(8) 1 calc PR A 1
C110 C 0.0566(3) 0.9858(14) 0.3875(4) 0.087(5) Uani 0.545(8) 1 d PGU A 1
H11A H 0.0710 0.9864 0.4118 0.105 Uiso 0.545(8) 1 calc PR A 1
C111 C 0.0625(3) 0.9855(16) 0.3581(5) 0.0655(11) Uani 0.545(8) 1 d PGU A 1
C112 C 0.0410(4) 0.9846(15) 0.3218(5) 0.114(8) Uani 0.545(8) 1 d PGU A 1
H11B H 0.0450 0.9844 0.3021 0.137 Uiso 0.545(8) 1 calc PR A 1
C113 C 0.0137(3) 0.9840(14) 0.3149(4) 0.0567(7) Uani 0.545(8) 1 d PGU A 1
N10 N 0.0077(3) 0.9843(14) 0.3444(4) 0.103(8) Uani 0.545(8) 1 d PGU . 1
C09' C 0.0364(3) 1.0275(15) 0.4061(5) 0.120(8) Uani 0.455(8) 1 d PGU A 2
H09A H 0.0344 1.0324 0.4273 0.144 Uiso 0.455(8) 1 calc PR A 2
C10' C 0.0626(3) 1.0122(16) 0.4094(5) 0.091(8) Uani 0.455(8) 1 d PGU A 2
H10I H 0.0780 1.0069 0.4327 0.109 Uiso 0.455(8) 1 calc PR A 2
C12' C 0.0657(4) 1.0049(16) 0.3777(7) 0.060(6) Uani 0.455(8) 1 d PG A 2
C11' C 0.0426(5) 1.0129(17) 0.3428(6) 0.085(7) Uani 0.455(8) 1 d PGU A 2
H11D H 0.0447 1.0080 0.3216 0.102 Uiso 0.455(8) 1 calc PR A 2
C13' C 0.0165(4) 1.0282(17) 0.3395(5) 0.0924(11) Uani 0.455(8) 1 d PGU A 2
H13B H 0.0011 1.0335 0.3162 0.111 Uiso 0.455(8) 1 calc PR A 2
N10' N 0.0134(3) 1.0355(16) 0.3712(6) 0.096(9) Uani 0.455(8) 1 d PGU . 2
C114 C 0.14167(19) 0.9858(7) 0.4129(3) 0.054(3) Uani 1 1 d . . .
H11E H 0.1565 0.9974 0.4363 0.065 Uiso 1 1 calc R . .
C115 C 0.1151(2) 0.9972(9) 0.4081(5) 0.086(4) Uani 1 1 d . A .
H11F H 0.1122 1.0150 0.4278 0.103 Uiso 1 1 calc R . .
C116 C 0.0928(2) 0.9815(10) 0.3730(6) 0.102(7) Uani 1 1 d . . .
C117 C 0.0979(2) 0.9523(10) 0.3442(6) 0.113(9) Uani 1 1 d . A .
H11G H 0.0832 0.9399 0.3208 0.136 Uiso 1 1 calc R . .
C118 C 0.1252(2) 0.9420(8) 0.3509(4) 0.066(4) Uani 1 1 d . . .
H11H H 0.1286 0.9237 0.3317 0.079 Uiso 1 1 calc R A .
C119 C 0.14725(15) 0.9587(6) 0.3857(3) 0.036(2) Uani 1 1 d . A .
C120 C 0.17668(14) 0.9461(5) 0.3925(2) 0.0269(16) Uani 1 1 d . . .
C121 C 0.09147(18) 0.5623(7) 0.2617(2) 0.039(2) Uani 1 1 d . . .
H12A H 0.0964 0.6262 0.2659 0.047 Uiso 1 1 calc R . .
C122 C 0.11192(19) 0.4940(7) 0.2777(2) 0.041(2) Uani 1 1 d . . .
H12B H 0.1302 0.5125 0.2929 0.049 Uiso 1 1 calc R . .
C123 C 0.10542(18) 0.3972(7) 0.2712(3) 0.039(2) Uani 1 1 d . . .
C124 C 0.0774(2) 0.3744(8) 0.2494(4) 0.062(4) Uani 1 1 d . . .
H12C H 0.0718 0.3111 0.2451 0.075 Uiso 1 1 calc R . .
C125 C 0.0580(2) 0.4482(9) 0.2342(4) 0.064(4) Uani 1 1 d . . .
H12D H 0.0396 0.4316 0.2190 0.077 Uiso 1 1 calc R . .
C126 C 0.17191(16) 0.2664(6) 0.3312(2) 0.0311(18) Uani 1 1 d . . .
H12E H 0.1886 0.2774 0.3526 0.037 Uiso 1 1 calc R . .
C127 C 0.15205(18) 0.3361(6) 0.3183(2) 0.0347(19) Uani 1 1 d . . .
H12F H 0.1551 0.3925 0.3316 0.042 Uiso 1 1 calc R . .
C128 C 0.12724(19) 0.3236(7) 0.2855(3) 0.040(2) Uani 1 1 d . . .
C129 C 0.1235(2) 0.2390(8) 0.2663(3) 0.056(3) Uani 1 1 d . . .
H12G H 0.1073 0.2299 0.2440 0.067 Uiso 1 1 calc R . .
C130 C 0.1439(2) 0.1662(7) 0.2800(3) 0.052(3) Uani 1 1 d . . .
H13C H 0.1412 0.1099 0.2667 0.062 Uiso 1 1 calc R . .
C131 C 0.16778(16) 0.1799(6) 0.3131(2) 0.0309(18) Uani 1 1 d . . .
C132 C 0.18884(16) 0.1003(5) 0.3285(2) 0.0270(16) Uani 1 1 d . . .
N1 N 0.4028(3) 1.3104(17) 0.3337(6) 0.140(6) Uani 1 1 d U . .
N2 N 0.44674(17) 0.9545(9) 0.4233(3) 0.067(3) Uani 1 1 d . . .
N3 N 0.46716(16) 0.7714(8) 0.5698(3) 0.061(3) Uani 1 1 d . . .
N5 N 0.47640(16) 0.0209(9) 0.5556(3) 0.066(3) Uani 1 1 d . . .
N7 N 0.0998(2) 0.2854(8) 0.1642(3) 0.067(3) Uani 1 1 d . . .
N8 N 0.0081(4) 0.3014(18) 0.3062(6) 0.150(6) Uani 1 1 d U . .
N9 N 0.00377(15) 0.6350(7) 0.2993(3) 0.051(2) Uani 1 1 d . . .
N11 N 0.06408(15) 0.5387(7) 0.2399(3) 0.048(2) Uani 1 1 d . . .
O1 O 0.25547(12) 1.0439(4) 0.35114(17) 0.0390(13) Uani 1 1 d . . .
O1W O -0.0177(5) 0.9552(19) 0.2520(7) 0.223(11) Uiso 1 1 d . . .
H0B H -0.0286 0.9148 0.2536 0.334 Uiso 1 1 d R . .
H0C H -0.0304 0.9408 0.2613 0.334 Uiso 1 1 d R . .
O2 O 0.26617(12) 1.1602(4) 0.39292(16) 0.0362(13) Uani 1 1 d . . .
O3 O 0.28353(11) 0.6971(5) 0.39732(17) 0.0370(14) Uani 1 1 d . . .
O4 O 0.26670(11) 0.8417(5) 0.38064(19) 0.0405(15) Uani 1 1 d . . .
O5 O 0.27580(9) 0.7743(4) 0.46857(14) 0.0232(11) Uani 1 1 d . . .
O6 O 0.28559(10) 0.7250(4) 0.52497(15) 0.0287(12) Uani 1 1 d . . .
O7 O 0.28982(11) 0.5736(4) 0.45652(17) 0.0326(13) Uani 1 1 d . . .
O8 O 0.28260(10) 0.4339(4) 0.47604(15) 0.0272(11) Uani 1 1 d . . .
O9 O 0.28921(10) 0.1149(4) 0.46966(14) 0.0271(12) Uani 1 1 d . . .
O10 O 0.29139(10) -0.0117(4) 0.50463(15) 0.0272(11) Uani 1 1 d . . .
O11 O 0.24093(10) 0.4821(3) 0.40381(13) 0.0234(10) Uani 1 1 d . . .
O12 O 0.23232(10) 0.3294(3) 0.40173(13) 0.0235(10) Uani 1 1 d . . .
O13 O 0.22476(12) 0.6658(5) 0.34875(16) 0.0388(15) Uani 1 1 d . . .
O14 O 0.19494(14) 0.7833(4) 0.32173(16) 0.0415(16) Uani 1 1 d . . .
O15 O 0.19577(11) 0.3163(4) 0.45251(16) 0.0332(13) Uani 1 1 d . . .
O16 O 0.19633(12) 0.1895(5) 0.42061(17) 0.0377(14) Uani 1 1 d . . .
O17 O 0.18941(10) 0.4907(4) 0.40850(16) 0.0308(13) Uani 1 1 d . . .
O18 O 0.19575(10) 0.6359(4) 0.39192(16) 0.0288(12) Uani 1 1 d . . .
O19 O 0.18023(12) 0.9278(5) 0.36491(17) 0.0403(15) Uani 1 1 d . A .
O20 O 0.19544(11) 0.9526(4) 0.42503(17) 0.0360(14) Uani 1 1 d . A .
O21 O 0.20705(12) 0.1043(4) 0.36191(15) 0.0337(14) Uani 1 1 d . . .
O22 O 0.18752(12) 0.0306(4) 0.30876(15) 0.0347(14) Uani 1 1 d . . .
O23 O 0.22477(9) 0.8041(3) 0.40730(12) 0.0164(9) Uani 1 1 d . . .
O24 O 0.24967(9) 0.9835(3) 0.41899(12) 0.0158(9) Uani 1 1 d . . .
O25 O 0.25572(10) 0.2689(3) 0.47525(12) 0.0190(10) Uani 1 1 d . . .
O26 O 0.25971(9) 0.9032(3) 0.53300(12) 0.0178(9) Uani 1 1 d . . .
O27 O 0.26182(9) 0.4371(3) 0.52445(12) 0.0159(9) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 Dy1 O24 75.06(19) . .
O4 Dy1 O14 95.3(2) . .
O24 Dy1 O14 143.04(18) . .
O4 Dy1 O19 141.3(2) . .
O24 Dy1 O19 89.37(18) . .
O14 Dy1 O19 76.0(2) . .
O4 Dy1 O22 147.7(2) . 1_565
O24 Dy1 O22 117.26(16) . 1_565
O14 Dy1 O22 90.1(2) . 1_565
O19 Dy1 O22 70.9(2) . 1_565
O4 Dy1 O1 74.5(2) . .
O24 Dy1 O1 75.17(17) . .
O14 Dy1 O1 137.5(2) . .
O19 Dy1 O1 135.9(2) . .
O22 Dy1 O1 80.1(2) 1_565 .
O4 Dy1 O23 74.1(2) . .
O24 Dy1 O23 67.47(14) . .
O14 Dy1 O23 75.57(17) . .
O19 Dy1 O23 67.23(18) . .
O22 Dy1 O23 137.81(18) 1_565 .
O1 Dy1 O23 135.97(16) . .
O4 Dy1 N6 78.6(11) . 4
O24 Dy1 N6 137.6(9) . 4
O14 Dy1 N6 71.5(6) . 4
O19 Dy1 N6 130.6(11) . 4
O22 Dy1 N6 73.0(10) 1_565 4
O1 Dy1 N6 66.0(6) . 4
O23 Dy1 N6 134.5(6) . 4
O4 Dy1 N6' 76.3(17) . 4
O24 Dy1 N6' 138.0(14) . 4
O14 Dy1 N6' 69.4(9) . 4
O19 Dy1 N6' 131.4(16) . 4
O22 Dy1 N6' 76.0(15) 1_565 4
O1 Dy1 N6' 68.0(9) . 4
O23 Dy1 N6' 131.0(9) . 4
N6 Dy1 N6' 3.5(13) 4 4
O4 Dy1 O21 133.29(19) . 1_565
O24 Dy1 O21 68.67(15) . 1_565
O14 Dy1 O21 131.3(2) . 1_565
O19 Dy1 O21 67.4(2) . 1_565
O22 Dy1 O21 48.63(17) 1_565 1_565
O1 Dy1 O21 68.6(2) . 1_565
O23 Dy1 O21 115.42(16) . 1_565
N6 Dy1 O21 109.8(6) 4 1_565
N6' Dy1 O21 113.3(10) 4 1_565
O4 Dy1 C132 148.8(2) . 1_565
O24 Dy1 C132 93.30(17) . 1_565
O14 Dy1 C132 110.2(2) . 1_565
O19 Dy1 C132 65.3(2) . 1_565
O22 Dy1 C132 24.10(19) 1_565 1_565
O1 Dy1 C132 74.5(2) . 1_565
O23 Dy1 C132 128.60(19) . 1_565
N6 Dy1 C132 92.3(9) 4 1_565
N6' Dy1 C132 95.7(13) 4 1_565
O21 Dy1 C132 24.64(17) 1_565 1_565
O20 Dy2 O27 69.72(17) . 7_566
O20 Dy2 O24 81.1(2) . .
O27 Dy2 O24 73.73(15) 7_566 .
O20 Dy2 O23 74.96(18) . .
O27 Dy2 O23 132.77(15) 7_566 .
O24 Dy2 O23 70.68(15) . .
O20 Dy2 O6 78.9(2) . 7_566
O27 Dy2 O6 121.66(17) 7_566 7_566
O24 Dy2 O6 147.50(16) . 7_566
O23 Dy2 O6 79.47(17) . 7_566
O20 Dy2 O5 143.32(18) . .
O27 Dy2 O5 141.55(15) 7_566 .
O24 Dy2 O5 90.36(17) . .
O23 Dy2 O5 68.58(15) . .
O6 Dy2 O5 90.49(18) 7_566 .
O20 Dy2 O26 117.32(19) . .
O27 Dy2 O26 76.42(15) 7_566 .
O24 Dy2 O26 135.99(15) . .
O23 Dy2 O26 149.66(15) . .
O6 Dy2 O26 76.35(16) 7_566 .
O5 Dy2 O26 93.46(16) . .
O20 Dy2 O10 132.66(19) . 1_565
O27 Dy2 O10 64.69(15) 7_566 1_565
O24 Dy2 O10 74.75(15) . 1_565
O23 Dy2 O10 130.54(16) . 1_565
O6 Dy2 O10 136.85(17) 7_566 1_565
O5 Dy2 O10 77.52(16) . 1_565
O26 Dy2 O10 63.45(16) . 1_565
O20 Dy2 Dy4 101.89(14) . 7_566
O27 Dy2 Dy4 39.25(10) 7_566 7_566
O24 Dy2 Dy4 100.24(10) . 7_566
O23 Dy2 Dy4 170.65(11) . 7_566
O6 Dy2 Dy4 108.80(13) 7_566 7_566
O5 Dy2 Dy4 114.74(11) . 7_566
O26 Dy2 Dy4 39.57(10) . 7_566
O10 Dy2 Dy4 45.70(12) 1_565 7_566
O20 Dy2 Dy5 67.88(16) . 1_565
O27 Dy2 Dy5 37.30(11) 7_566 1_565
O24 Dy2 Dy5 36.79(10) . 1_565
O23 Dy2 Dy5 100.31(11) . 1_565
O6 Dy2 Dy5 145.42(13) 7_566 1_565
O5 Dy2 Dy5 121.98(13) . 1_565
O26 Dy2 Dy5 110.00(11) . 1_565
O10 Dy2 Dy5 68.41(11) 1_565 1_565
Dy4 Dy2 Dy5 70.430(13) 7_566 1_565
O13 Dy3 O23 80.9(2) . .
O13 Dy3 O7 130.3(2) . .
O23 Dy3 O7 141.15(17) . .
O13 Dy3 O3 73.9(2) . .
O23 Dy3 O3 101.91(19) . .
O7 Dy3 O3 72.2(2) . .
O13 Dy3 O11 84.3(2) . .
O23 Dy3 O11 144.47(16) . .
O7 Dy3 O11 70.55(17) . .
O3 Dy3 O11 104.8(2) . .
O13 Dy3 O26 140.81(18) . 7_566
O23 Dy3 O26 96.01(16) . 7_566
O7 Dy3 O26 73.91(19) . 7_566
O3 Dy3 O26 143.57(17) . 7_566
O11 Dy3 O26 75.76(16) . 7_566
O13 Dy3 O18 72.3(2) . .
O23 Dy3 O18 67.53(16) . .
O7 Dy3 O18 136.62(18) . .
O3 Dy3 O18 145.81(19) . .
O11 Dy3 O18 77.23(17) . .
O26 Dy3 O18 70.53(17) 7_566 .
O13 Dy3 O5 134.9(2) . .
O23 Dy3 O5 67.11(14) . .
O7 Dy3 O5 74.04(17) . .
O3 Dy3 O5 82.26(19) . .
O11 Dy3 O5 139.39(15) . .
O26 Dy3 O5 75.89(16) 7_566 .
O18 Dy3 O5 118.91(17) . .
O13 Dy3 Dy4 116.27(16) . .
O23 Dy3 Dy4 123.35(12) . .
O7 Dy3 Dy4 68.48(14) . .
O3 Dy3 Dy4 134.26(15) . .
O11 Dy3 Dy4 39.94(12) . .
O26 Dy3 Dy4 35.85(10) 7_566 .
O18 Dy3 Dy4 68.15(12) . .
O5 Dy3 Dy4 107.83(12) . .
O17 Dy4 O26 78.61(16) . 7_566
O17 Dy4 O27 141.88(19) . .
O26 Dy4 O27 77.89(15) 7_566 .
O17 Dy4 O15 75.32(19) . .
O26 Dy4 O15 136.72(18) 7_566 .
O27 Dy4 O15 102.87(18) . .
O17 Dy4 O25 137.24(17) . .
O26 Dy4 O25 142.32(15) 7_566 .
O27 Dy4 O25 75.39(14) . .
O15 Dy4 O25 75.64(18) . .
O17 Dy4 O8 136.31(19) . .
O26 Dy4 O8 79.15(17) 7_566 .
O27 Dy4 O8 66.54(17) . .
O15 Dy4 O8 141.67(19) . .
O25 Dy4 O8 66.07(17) . .
O17 Dy4 O11 71.18(18) . .
O26 Dy4 O11 74.91(16) 7_566 .
O27 Dy4 O11 129.38(15) . .
O15 Dy4 O11 126.09(18) . .
O25 Dy4 O11 102.68(16) . .
O8 Dy4 O11 66.93(16) . .
O17 Dy4 O12 82.67(19) . .
O26 Dy4 O12 123.76(16) 7_566 .
O27 Dy4 O12 135.45(15) . .
O15 Dy4 O12 86.40(18) . .
O25 Dy4 O12 64.81(15) . .
O8 Dy4 O12 79.23(17) . .
O11 Dy4 O12 48.84(15) . .
O17 Dy4 O10 77.67(19) . 7_556
O26 Dy4 O10 65.45(16) 7_566 7_556
O27 Dy4 O10 65.37(15) . 7_556
O15 Dy4 O10 75.56(18) . 7_556
O25 Dy4 O10 123.60(16) . 7_556
O8 Dy4 O10 124.61(17) . 7_556
O11 Dy4 O10 133.39(16) . 7_556
O12 Dy4 O10 156.06(15) . 7_556
O17 Dy4 Dy2 107.29(15) . 7_566
O26 Dy4 Dy2 41.42(11) 7_566 7_566
O27 Dy4 Dy2 38.93(10) . 7_566
O15 Dy4 Dy2 117.64(15) . 7_566
O25 Dy4 Dy2 113.79(10) . 7_566
O8 Dy4 Dy2 78.25(13) . 7_566
O11 Dy4 Dy2 112.05(11) . 7_566
O12 Dy4 Dy2 155.40(11) . 7_566
O10 Dy4 Dy2 46.90(11) 7_556 7_566
O17 Dy4 Dy3 69.81(13) . .
O26 Dy4 Dy3 37.30(11) 7_566 .
O27 Dy4 Dy3 106.14(11) . .
O15 Dy4 Dy3 145.01(13) . .
O25 Dy4 Dy3 130.52(12) . .
O8 Dy4 Dy3 69.68(12) . .
O11 Dy4 Dy3 37.65(11) . .
O12 Dy4 Dy3 86.47(10) . .
O10 Dy4 Dy3 99.25(12) 7_556 .
Dy2 Dy4 Dy3 76.529(14) 7_566 .
O2 Dy5 O16 142.7(2) 1_545 .
O2 Dy5 O25 112.78(19) 1_545 .
O16 Dy5 O25 80.77(19) . .
O2 Dy5 O24 77.84(18) 1_545 1_545
O16 Dy5 O24 116.65(18) . 1_545
O25 Dy5 O24 137.22(14) . 1_545
O2 Dy5 O9 72.9(2) 1_545 .
O16 Dy5 O9 143.2(2) . .
O25 Dy5 O9 73.04(17) . .
O24 Dy5 O9 71.16(16) 1_545 .
O2 Dy5 O21 76.5(2) 1_545 .
O16 Dy5 O21 75.6(2) . .
O25 Dy5 O21 148.23(17) . .
O24 Dy5 O21 73.49(17) 1_545 .
O9 Dy5 O21 137.05(19) . .
O2 Dy5 O27 141.84(18) 1_545 7_556
O16 Dy5 O27 73.70(19) . 7_556
O25 Dy5 O27 76.74(15) . 7_556
O24 Dy5 O27 72.24(15) 1_545 7_556
O9 Dy5 O27 75.38(16) . 7_556
O21 Dy5 O27 115.60(18) . 7_556
O2 Dy5 O12 78.02(19) 1_545 .
O16 Dy5 O12 76.5(2) . .
O25 Dy5 O12 66.28(15) . .
O24 Dy5 O12 152.14(15) 1_545 .
O9 Dy5 O12 114.18(17) . .
O21 Dy5 O12 87.52(17) . .
O27 Dy5 O12 135.39(15) 7_556 .
O2 Dy5 Dy2 112.42(15) 1_545 1_545
O16 Dy5 Dy2 92.97(16) . 1_545
O25 Dy5 Dy2 110.20(11) . 1_545
O24 Dy5 Dy2 36.23(11) 1_545 1_545
O9 Dy5 Dy2 73.00(13) . 1_545
O21 Dy5 Dy2 92.14(14) . 1_545
O27 Dy5 Dy2 36.36(10) 7_556 1_545
O12 Dy5 Dy2 169.18(12) . 1_545
Cu1' Cu1 N10 92(6) . 7_566
Cu1' Cu1 N10' 60(5) . 7_566
N10 Cu1 N10' 32(7) 7_566 7_566
Cu1' Cu1 Cu2' 120.8(7) . .
N10 Cu1 Cu2' 142(7) 7_566 .
N10' Cu1 Cu2' 161(6) 7_566 .
Cu1' Cu1 I6 88.4(4) . .
N10 Cu1 I6 140(6) 7_566 .
N10' Cu1 I6 133(5) 7_566 .
Cu2' Cu1 I6 64.5(4) . .
Cu1' Cu1 I6' 94.2(5) . .
N10 Cu1 I6' 104(5) 7_566 .
N10' Cu1 I6' 107(6) 7_566 .
Cu2' Cu1 I6' 91.7(5) . .
I6 Cu1 I6' 36.2(2) . .
Cu1' Cu1 Cu2 119.9(4) . .
N10 Cu1 Cu2 127(7) 7_566 .
N10' Cu1 Cu2 140(6) 7_566 .
Cu2' Cu1 Cu2 21.4(4) . .
I6 Cu1 Cu2 85.25(19) . .
I6' Cu1 Cu2 112.7(3) . .
Cu1' Cu1 I4 68.6(4) . .
N10 Cu1 I4 104(5) 7_566 .
N10' Cu1 I4 89(6) 7_566 .
Cu2' Cu1 I4 75.3(5) . .
I6 Cu1 I4 112.8(2) . .
I6' Cu1 I4 147.1(4) . .
Cu2 Cu1 I4 59.69(18) . .
Cu1 Cu1' N10' 76(7) . 7_566
Cu1 Cu1' I8 156.3(5) . .
N10' Cu1' I8 111(8) 7_566 .
Cu1 Cu1' I4 74.8(4) . .
N10' Cu1' I4 97(7) 7_566 .
I8 Cu1' I4 125.1(3) . .
Cu1 Cu1' I4' 90.0(5) . .
N10' Cu1' I4' 97(7) 7_566 .
I8 Cu1' I4' 111.2(4) . .
I4 Cu1' I4' 15.8(2) . .
Cu1 Cu1' Cu3 123.8(4) . .
N10' Cu1' Cu3 141(6) 7_566 .
I8 Cu1' Cu3 65.9(2) . .
I4 Cu1' Cu3 63.2(2) . .
I4' Cu1' Cu3 54.9(3) . .
Cu1 Cu1' I6 56.7(3) . .
N10' Cu1' I6 121(6) 7_566 .
I8 Cu1' I6 103.0(3) . .
I4 Cu1' I6 101.6(2) . .
I4' Cu1' I6 114.5(3) . .
Cu3 Cu1' I6 96.2(2) . .
Cu1 Cu1' Cu6 109.6(3) . .
N10' Cu1' Cu6 159(7) 7_566 .
I8 Cu1' Cu6 56.52(17) . .
I4 Cu1' Cu6 104.1(3) . .
I4' Cu1' Cu6 103.4(3) . .
Cu3 Cu1' Cu6 53.01(16) . .
I6 Cu1' Cu6 54.92(14) . .
Cu1 Cu1' I6' 53.3(4) . .
N10' Cu1' I6' 95(6) 7_566 .
I8 Cu1' I6' 103.0(3) . .
I4 Cu1' I6' 121.4(3) . .
I4' Cu1' I6' 136.9(4) . .
Cu3 Cu1' I6' 123.5(3) . .
I6 Cu1' I6' 29.32(19) . .
Cu6 Cu1' I6' 74.2(2) . .
Cu2' Cu2 N1 82.8(14) . 5_676
Cu2' Cu2 Cu1 70.1(12) . .
N1 Cu2 Cu1 137.9(8) 5_676 .
Cu2' Cu2 I3 76.2(15) . .
N1 Cu2 I3 123.9(6) 5_676 .
Cu1 Cu2 I3 81.0(2) . .
Cu2' Cu2 I4 114.6(15) . .
N1 Cu2 I4 104.1(6) 5_676 .
Cu1 Cu2 I4 62.4(2) . .
I3 Cu2 I4 132.04(16) . .
Cu2 Cu2' N1 71.8(13) . 5_676
Cu2 Cu2' Cu1 88.5(12) . .
N1 Cu2' Cu1 142.2(11) 5_676 .
Cu2 Cu2' I3 82.8(14) . .
N1 Cu2' I3 122.4(10) 5_676 .
Cu1 Cu2' I3 85.1(6) . .
Cu2 Cu2' I6 143.6(17) . .
N1 Cu2' I6 125.4(10) 5_676 .
Cu1 Cu2' I6 57.9(4) . .
I3 Cu2' I6 105.8(7) . .
Cu2 Cu2' I3' 89.5(15) . .
N1 Cu2' I3' 123.7(10) 5_676 .
Cu1 Cu2' I3' 86.8(6) . .
I3 Cu2' I3' 6.83(18) . .
I6 Cu2' I3' 101.2(6) . .
Cu2 Cu2' I4 49.6(12) . .
N1 Cu2' I4 87.2(8) 5_676 .
Cu1 Cu2' I4 56.3(4) . .
I3 Cu2' I4 114.0(5) . .
I6 Cu2' I4 96.1(6) . .
I3' Cu2' I4 120.1(5) . .
Cu3' Cu3 I5 67.9(8) . .
Cu3' Cu3 I5' 108.4(12) . .
I5 Cu3 I5' 53.9(10) . .
Cu3' Cu3 I7 91.5(5) . .
I5 Cu3 I7 107.09(18) . .
I5' Cu3 I7 139.5(10) . .
Cu3' Cu3 I4' 147.4(6) . .
I5 Cu3 I4' 104.6(3) . .
I5' Cu3 I4' 51.6(10) . .
I7 Cu3 I4' 120.5(3) . .
Cu3' Cu3 Cu6 67.3(7) . .
I5 Cu3 Cu6 133.1(2) . .
I5' Cu3 Cu6 158.8(10) . .
I7 Cu3 Cu6 61.42(11) . .
I4' Cu3 Cu6 120.6(3) . .
Cu3' Cu3 Cu1' 103.0(9) . .
I5 Cu3 Cu1' 137.3(2) . .
I5' Cu3 Cu1' 94.9(10) . .
I7 Cu3 Cu1' 114.9(2) . .
I4' Cu3 Cu1' 59.9(3) . .
Cu6 Cu3 Cu1' 67.17(19) . .
Cu3' Cu3 I4 153.4(8) . .
I5 Cu3 I4 118.42(16) . .
I5' Cu3 I4 66.1(10) . .
I7 Cu3 I4 109.32(17) . .
I4' Cu3 I4 14.6(2) . .
Cu6 Cu3 I4 107.84(18) . .
Cu1' Cu3 I4 53.70(18) . .
Cu3' Cu3 I8 52.0(8) . .
I5 Cu3 I8 103.20(17) . .
I5' Cu3 I8 103.3(10) . .
I7 Cu3 I8 116.48(14) . .
I4' Cu3 I8 103.1(3) . .
Cu6 Cu3 I8 57.01(10) . .
Cu1' Cu3 I8 51.50(18) . .
I4 Cu3 I8 102.65(14) . .
Cu3 Cu3' I5 88.0(8) . .
Cu3 Cu3' Cu6 90.1(8) . .
I5 Cu3' Cu6 165.7(5) . .
Cu3 Cu3' I8 109.0(10) . .
I5 Cu3' I8 127.4(4) . .
Cu6 Cu3' I8 66.5(4) . .
Cu3 Cu3' Cu4 110.8(6) . .
I5 Cu3' Cu4 60.7(3) . .
Cu6 Cu3' Cu4 132.8(5) . .
I8 Cu3' Cu4 66.8(3) . .
Cu3 Cu3' I7 67.1(5) . .
I5 Cu3' I7 105.6(5) . .
Cu6 Cu3' I7 60.8(2) . .
I8 Cu3' I7 127.0(5) . .
Cu4 Cu3' I7 166.3(6) . .
Cu3 Cu3' I5' 53.0(9) . .
I5 Cu3' I5' 48.4(8) . .
Cu6 Cu3' I5' 137.8(9) . .
I8 Cu3' I5' 103.4(9) . .
Cu4 Cu3' I5' 61.2(8) . .
I7 Cu3' I5' 111.3(9) . .
N4 Cu4 I5 138.3(5) . .
N4 Cu4 Cu3' 142.6(6) . .
I5 Cu4 Cu3' 52.5(3) . .
N4 Cu4 I2 89.9(5) . 5_666
I5 Cu4 I2 102.00(19) . 5_666
Cu3' Cu4 I2 126.0(3) . 5_666
N4 Cu4 I8 101.3(4) . .
I5 Cu4 I8 105.45(15) . .
Cu3' Cu4 I8 53.0(3) . .
I2 Cu4 I8 122.05(16) 5_666 .
N4 Cu4 I5' 96.5(10) . .
I5 Cu4 I5' 48.9(9) . .
Cu3' Cu4 I5' 65.5(8) . .
I2 Cu4 I5' 137.8(8) 5_666 .
I8 Cu4 I5' 97.6(7) . .
N4 Cu4 I5' 92.4(9) . 5_666
I5 Cu4 I5' 46.8(8) . 5_666
Cu3' Cu4 I5' 93.2(8) . 5_666
I2 Cu4 I5' 97.3(7) 5_666 5_666
I8 Cu4 I5' 137.9(7) . 5_666
I5' Cu4 I5' 40.9(13) . 5_666
N3 Cu5 I2' 107.8(3) . .
N3 Cu5 I1 114.2(3) . .
I2' Cu5 I1 106.18(13) . .
N3 Cu5 I2 107.3(3) . .
I2' Cu5 I2 10.14(12) . .
I1 Cu5 I2 114.76(9) . .
N3 Cu5 I4 102.8(3) . .
I2' Cu5 I4 114.35(14) . .
I1 Cu5 I4 111.66(7) . .
I2 Cu5 I4 105.11(9) . .
N3 Cu5 I4' 97.1(4) . .
I2' Cu5 I4' 104.3(3) . .
I1 Cu5 I4' 125.9(2) . .
I2 Cu5 I4' 94.4(2) . .
I4 Cu5 I4' 14.6(2) . .
N7 Cu6 Cu3' 126.7(4) 8_556 .
N7 Cu6 Cu3 147.1(4) 8_556 .
Cu3' Cu6 Cu3 22.6(2) . .
N7 Cu6 I7 108.2(4) 8_556 .
Cu3' Cu6 I7 66.2(3) . .
Cu3 Cu6 I7 58.04(11) . .
N7 Cu6 I8 109.1(3) 8_556 .
Cu3' Cu6 I8 57.0(3) . .
Cu3 Cu6 I8 67.15(11) . .
I7 Cu6 I8 122.97(11) . .
N7 Cu6 I6 107.3(3) 8_556 .
Cu3' Cu6 I6 125.7(2) . .
Cu3 Cu6 I6 105.28(14) . .
I7 Cu6 I6 105.14(10) . .
I8 Cu6 I6 103.00(11) . .
N7 Cu6 Cu1' 145.1(4) 8_556 .
Cu3' Cu6 Cu1' 71.5(3) . .
Cu3 Cu6 Cu1' 59.82(18) . .
I7 Cu6 Cu1' 106.51(17) . .
I8 Cu6 Cu1' 51.76(15) . .
I6 Cu6 Cu1' 59.61(16) . .
N5 Cu7 N2 160.4(5) 1_565 5_676
N5 Cu7 I2' 97.3(4) 1_565 .
N2 Cu7 I2' 93.4(4) 5_676 .
N5 Cu7 I2 97.5(4) 1_565 .
N2 Cu7 I2 93.6(4) 5_676 .
I2' Cu7 I2 1.43(14) . .
N5 Cu7 I1 97.3(4) 1_565 .
N2 Cu7 I1 98.5(3) 5_676 .
I2' Cu7 I1 93.07(15) . .
I2 Cu7 I1 91.63(8) . .
N11 Cu8 N9 122.4(4) 8_566 7_566
N11 Cu8 I3 114.8(3) 8_566 .
N9 Cu8 I3 111.7(3) 7_566 .
N11 Cu8 I3' 109.1(3) 8_566 .
N9 Cu8 I3' 108.8(4) 7_566 .
I3 Cu8 I3' 12.7(3) . .
N11 Cu8 I1 95.6(3) 8_566 .
N9 Cu8 I1 104.6(3) 7_566 .
I3 Cu8 I1 103.74(7) . .
I3' Cu8 I1 116.2(3) . .
Cu5 I1 Cu8 120.72(7) . .
Cu5 I1 Cu7 70.98(7) . .
Cu8 I1 Cu7 154.09(7) . .
Cu5 I2 Cu4 115.76(13) . 5_666
Cu5 I2 Cu7 70.70(8) . .
Cu4 I2 Cu7 169.06(10) 5_666 .
Cu5 I2' Cu7 79.49(18) . .
I3' I3 Cu2' 143.0(10) . .
I3' I3 Cu2 162.9(10) . .
I3' I3 Cu8 94.8(8) . .
Cu2' I3 Cu8 117.5(4) . .
Cu2 I3 Cu8 97.5(2) . .
I3 I3' Cu8 72.5(8) . .
Cu8 I3' Cu2' 99.3(5) . .
I4' I4 Cu1' 92.9(7) . .
I4' I4 Cu2 169.3(8) . .
Cu1' I4 Cu2 90.2(2) . .
I4' I4 Cu1 127.8(8) . .
Cu2 I4 Cu1 57.9(2) . .
I4' I4 Cu5 95.6(7) . .
Cu1' I4 Cu5 146.92(19) . .
Cu2 I4 Cu5 87.3(2) . .
Cu1 I4 Cu5 120.20(18) . .
I4' I4 Cu3 60.6(7) . .
Cu1' I4 Cu3 63.1(2) . .
Cu2 I4 Cu3 112.22(19) . .
Cu1 I4 Cu3 93.13(19) . .
Cu5 I4 Cu3 146.66(12) . .
Cu1' I4 I5' 91.7(9) . .
Cu2 I4 I5' 159.8(8) . .
Cu1 I4 I5' 128.1(9) . .
Cu5 I4 I5' 101.8(9) . .
Cu3 I4 I5' 51.8(8) . .
I4' I4 Cu2' 159.1(8) . .
Cu1' I4 Cu2' 76.6(4) . .
Cu1 I4 Cu2' 48.4(4) . .
Cu5 I4 Cu2' 103.1(3) . .
Cu3 I4 Cu2' 98.4(4) . .
I5' I4 Cu2' 149.7(9) . .
I4 I4' I5' 166.7(15) . .
I4 I4' Cu3 104.8(7) . .
I5' I4' Cu3 63.4(11) . .
I4 I4' Cu1' 71.2(7) . .
I5' I4' Cu1' 106.7(12) . .
Cu3 I4' Cu1' 65.2(3) . .
I4 I4' Cu5 69.8(6) . .
I5' I4' Cu5 118.1(12) . .
Cu3 I4' Cu5 155.8(4) . .
Cu1' I4' Cu5 130.0(5) . .
I5' I5 I5' 54.9(16) . 5_666
I5' I5 Cu3' 82.7(10) . .
I5' I5 Cu3' 132.1(11) 5_666 .
I5' I5 Cu3 64.5(9) . .
I5' I5 Cu3 119.0(11) 5_666 .
I5' I5 Cu4 74.3(12) . .
I5' I5 Cu4 79.9(12) 5_666 .
Cu3' I5 Cu4 66.8(3) . .
Cu3 I5 Cu4 78.52(18) . .
I5' I5' I4' 170(4) 5_666 .
I5' I5' I5 63(2) 5_666 .
I4' I5' I5 125.1(17) . .
I5' I5' I5 62.1(19) 5_666 5_666
I4' I5' I5 109.5(19) . 5_666
I5 I5' I5 125.1(16) . 5_666
I5' I5' Cu3 124(3) 5_666 .
I4' I5' Cu3 64.9(9) . .
I5 I5' Cu3 61.6(11) . .
I5 I5' Cu3 171(2) 5_666 .
I5' I5' Cu4 74(2) 5_666 .
I4' I5' Cu4 115.0(17) . .
I5 I5' Cu4 56.8(10) . .
I5 I5' Cu4 107.3(14) 5_666 .
Cu3 I5' Cu4 70.7(11) . .
I5' I5' I4 171(3) 5_666 .
I5 I5' I4 121.9(14) . .
I5 I5' I4 112.5(17) 5_666 .
Cu3 I5' I4 62.0(8) . .
Cu4 I5' I4 114.4(14) . .
I5' I5' Cu3' 109(3) 5_666 .
I4' I5' Cu3' 81.3(11) . .
I5 I5' Cu3' 49.0(9) . .
I5 I5' Cu3' 160.6(19) 5_666 .
Cu4 I5' Cu3' 53.3(8) . .
I4 I5' Cu3' 78.7(9) . .
I5' I5' Cu4 65(2) 5_666 5_666
I4' I5' Cu4 105.8(16) . 5_666
I5 I5' Cu4 101.9(15) . 5_666
I5 I5' Cu4 53.3(9) 5_666 5_666
Cu3 I5' Cu4 133.8(16) . 5_666
Cu4 I5' Cu4 139.1(13) . 5_666
I4 I5' Cu4 106.5(13) . 5_666
Cu3' I5' Cu4 140.9(16) . 5_666
I6' I6 Cu1 74.1(4) . .
I6' I6 Cu2' 115.3(6) . .
Cu1 I6 Cu2' 57.6(4) . .
I6' I6 Cu6 117.3(5) . .
Cu1 I6 Cu6 98.9(2) . .
Cu2' I6 Cu6 110.8(5) . .
I6' I6 Cu1' 82.3(5) . .
Cu2' I6 Cu1' 80.9(4) . .
Cu6 I6 Cu1' 65.47(17) . .
I6 I6' Cu1 69.7(5) . .
I6 I6' Cu1' 68.4(5) . .
I7' I7 Cu3 170.40(18) . .
I7' I7 Cu6 123.45(18) . .
Cu3 I7 Cu6 60.54(11) . .
I7' I7 Cu3' 168.3(2) . .
Cu6 I7 Cu3' 53.0(3) . .
Cu3' I8 Cu1' 81.4(3) . .
Cu3' I8 Cu6 56.5(2) . .
Cu1' I8 Cu6 71.72(18) . .
Cu3' I8 Cu4 60.3(2) . .
Cu1' I8 Cu4 105.1(2) . .
Cu6 I8 Cu4 116.47(11) . .
Cu1' I8 Cu3 62.6(2) . .
Cu6 I8 Cu3 55.84(9) . .
Cu4 I8 Cu3 66.74(12) . .
N1 C1 C2 123.9(19) . .
N1 C1 H1A 118.0 . .
C2 C1 H1A 118.0 . .
C3 C2 C1 116.3(19) . .
C3 C2 H2A 121.9 . .
C1 C2 H2A 121.9 . .
C2 C3 C4 119.0(14) . .
C2 C3 C11 122.2(15) . .
C4 C3 C11 118.8(13) . .
C3 C4 C5 116.5(18) . .
C3 C4 H4A 108.2 . .
C5 C4 H4A 108.2 . .
C3 C4 H4B 108.2 . .
C5 C4 H4B 108.2 . .
H4A C4 H4B 107.3 . .
N1 C5 C4 122(2) . .
N1 C5 H5A 119.2 . .
C4 C5 H5A 119.2 . .
C11 C6 C7 120.5(10) . .
C11 C6 H6A 119.8 . .
C7 C6 H6A 119.8 . .
C8 C7 C6 118.8(9) . .
C8 C7 H7A 120.6 . .
C6 C7 H7A 120.6 . .
C7 C8 C9 120.2(8) . .
C7 C8 C12 121.8(8) . .
C9 C8 C12 118.0(8) . .
C8 C9 C10 119.5(9) . .
C8 C9 H9A 120.2 . .
C10 C9 H9A 120.2 . .
C11 C10 C9 119.7(10) . .
C11 C10 H10A 120.2 . .
C9 C10 H10A 120.2 . .
C6 C11 C10 121.1(10) . .
C6 C11 C3 121.2(11) . .
C10 C11 C3 117.6(11) . .
O2 C12 O1 126.1(8) . .
O2 C12 C8 115.5(7) . .
O1 C12 C8 118.4(7) . .
N2 C13 C14 121.6(11) . .
N2 C13 H13A 119.2 . .
C14 C13 H13A 119.2 . .
C15 C14 C13 122.8(12) . .
C15 C14 H14A 118.6 . .
C13 C14 H14A 118.6 . .
C14 C15 C16 116.7(9) . .
C14 C15 C23 122.7(10) . .
C16 C15 C23 120.5(8) . .
C17 C16 C15 117.8(10) . .
C17 C16 H16A 121.1 . .
C15 C16 H16A 121.1 . .
N2 C17 C16 124.2(12) . .
N2 C17 H17A 117.9 . .
C16 C17 H17A 117.9 . .
C23 C18 C19 119.2(8) . .
C23 C18 H18A 120.4 . .
C19 C18 H18A 120.4 . .
C20 C19 C18 121.4(8) . .
C20 C19 H19A 119.3 . .
C18 C19 H19A 119.3 . .
C19 C20 C21 118.9(7) . .
C19 C20 C24 120.8(7) . .
C21 C20 C24 120.0(7) . .
C20 C21 C22 120.2(8) . .
C20 C21 H21A 119.9 . .
C22 C21 H21A 119.9 . .
C21 C22 C23 122.4(9) . .
C21 C22 H22A 118.8 . .
C23 C22 H22A 118.8 . .
C22 C23 C18 117.8(7) . .
C22 C23 C15 123.2(9) . .
C18 C23 C15 119.1(8) . .
O4 C24 O3 123.7(7) . .
O4 C24 C20 119.1(7) . .
O3 C24 C20 117.2(7) . .
N3 C25 C26 123.0(12) . .
N3 C25 H25A 118.5 . .
C26 C25 H25A 118.5 . .
C27 C26 C25 122.4(13) . .
C27 C26 H26A 118.8 . .
C25 C26 H26A 118.8 . .
C28 C27 C26 115.0(9) . .
C28 C27 C35 122.5(9) . .
C26 C27 C35 122.4(10) . .
C27 C28 C29 120.0(11) . .
C27 C28 H28A 120.0 . .
C29 C28 H28A 120.0 . .
N3 C29 C28 124.8(13) . .
N3 C29 H29A 117.6 . .
C28 C29 H29A 117.6 . .
C31 C30 C35 121.9(7) . .
C31 C30 H30A 119.1 . .
C35 C30 H30A 119.1 . .
C30 C31 C32 120.5(8) . .
C30 C31 H31A 119.8 . .
C32 C31 H31A 119.8 . .
C33 C32 C31 119.1(7) . .
C33 C32 C36 121.0(6) . .
C31 C32 C36 119.8(7) . .
C32 C33 C34 120.5(7) . .
C32 C33 H33A 119.8 . .
C34 C33 H33A 119.8 . .
C33 C34 C35 120.8(8) . .
C33 C34 H34A 119.6 . .
C35 C34 H34A 119.6 . .
C34 C35 C30 117.1(7) . .
C34 C35 C27 120.1(8) . .
C30 C35 C27 122.8(8) . .
O6 C36 O5 122.0(6) . .
O6 C36 C32 119.1(6) . .
O5 C36 C32 118.8(6) . .
C38 C37 N4 120.0 . .
C38 C37 H37A 120.0 . .
N4 C37 H37A 120.0 . .
C37 C38 C39 120.0 . .
C37 C38 H38A 120.0 . .
C39 C38 H38A 120.0 . .
C40 C39 C38 120.0 . .
C40 C39 C47 120.9(9) . .
C38 C39 C47 118.7(9) . .
C41 C40 C39 120.0 . .
C41 C40 H40A 120.0 . .
C39 C40 H40A 120.0 . .
C40 C41 N4 120.0 . .
C40 C41 H41A 120.0 . .
N4 C41 H41A 120.0 . .
C41 N4 C37 120.0 . .
C41 N4 Cu4 116.7(7) . .
C37 N4 Cu4 122.2(7) . .
C47 C42 C43 121.2(11) . .
C47 C42 H42A 119.4 . .
C43 C42 H42A 119.4 . .
C44 C43 C42 120.6(10) . .
C44 C43 H43A 119.7 . .
C42 C43 H43A 119.7 . .
C45 C44 C43 119.6(8) . .
C45 C44 C48 118.2(8) . .
C43 C44 C48 122.2(8) . .
C44 C45 C46 119.3(11) . .
C44 C45 H45A 120.3 . .
C46 C45 H45A 120.3 . .
C47 C46 C45 120.3(12) . .
C47 C46 H46A 119.9 . .
C45 C46 H46A 119.9 . .
C42 C47 C46 118.9(10) . .
C42 C47 C39 119.3(12) . .
C46 C47 C39 121.8(12) . .
O7 C48 O8 124.9(7) . .
O7 C48 C44 118.3(7) . .
O8 C48 C44 116.8(7) . .
N5 C49 C50 124.6(13) . .
N5 C49 H49A 117.7 . .
C50 C49 H49A 117.7 . .
C51 C50 C49 120.4(12) . .
C51 C50 H50A 119.8 . .
C49 C50 H50A 119.8 . .
C50 C51 C52 116.3(9) . .
C50 C51 C59 123.4(10) . .
C52 C51 C59 120.2(9) . .
C51 C52 C53 118.0(11) . .
C51 C52 H52A 121.0 . .
C53 C52 H52A 121.0 . .
N5 C53 C52 125.6(12) . .
N5 C53 H53A 117.2 . .
C52 C53 H53A 117.2 . .
C55 C54 C59 120.9(7) . .
C55 C54 H54A 119.6 . .
C59 C54 H54A 119.6 . .
C54 C55 C56 120.2(8) . .
C54 C55 H55A 119.9 . .
C56 C55 H55A 119.9 . .
C57 C56 C55 117.5(7) . .
C57 C56 C60 121.4(6) . .
C55 C56 C60 121.0(7) . .
C58 C57 C56 121.9(8) . .
C58 C57 H57A 119.0 . .
C56 C57 H57A 119.0 . .
C57 C58 C59 121.2(9) . .
C57 C58 H58A 119.4 . .
C59 C58 H58A 119.4 . .
C58 C59 C54 118.1(7) . .
C58 C59 C51 121.9(9) . .
C54 C59 C51 119.9(8) . .
O9 C60 O10 125.3(6) . .
O9 C60 C56 115.6(6) . .
O10 C60 C56 119.2(6) . .
C62 C61 N6 120.0 . .
C62 C61 H61A 120.0 . .
N6 C61 H61A 120.0 . .
C61 C62 C63 120.0 . .
C61 C62 H62A 120.0 . .
C63 C62 H62A 120.0 . .
C64 C63 C62 120.0 . .
C64 C63 C71 119.8(7) . .
C62 C63 C71 120.0(7) . .
C63 C64 C65 120.0 . .
C63 C64 H64A 120.0 . .
C65 C64 H64A 120.0 . .
N6 C65 C64 120.0 . .
N6 C65 H65A 120.0 . .
C64 C65 H65A 120.0 . .
C65 N6 C61 120.0 . .
C65 N6 Dy1 118.6(4) . 4_545
C61 N6 Dy1 121.4(4) . 4_545
C62' C61' N6' 120.0 . .
C62' C61' H61B 120.0 . .
N6' C61' H61B 120.0 . .
C63' C62' C61' 120.0 . .
C63' C62' H62B 120.0 . .
C61' C62' H62B 120.0 . .
C62' C63' C64' 120.0 . .
C62' C63' C71 120.0(8) . .
C64' C63' C71 120.0(9) . .
C65' C64' C63' 120.0 . .
C65' C64' H64B 120.0 . .
C63' C64' H64B 120.0 . .
C64' C65' N6' 120.0 . .
C64' C65' H65B 120.0 . .
N6' C65' H65B 120.0 . .
C65' N6' C61' 120.0 . .
C65' N6' Dy1 119.4(5) . 4_545
C61' N6' Dy1 120.1(5) . 4_545
C71 C66 C67 119.6(8) . .
C71 C66 H66A 120.2 . .
C67 C66 H66A 120.2 . .
C66 C67 C68 120.8(8) . .
C66 C67 H67A 119.6 . .
C68 C67 H67A 119.6 . .
C69 C68 C67 119.8(7) . .
C69 C68 C72 119.4(7) . .
C67 C68 C72 120.6(7) . .
C68 C69 C70 119.7(8) . .
C68 C69 H69A 120.2 . .
C70 C69 H69A 120.2 . .
C71 C70 C69 120.2(8) . .
C71 C70 H70A 119.9 . .
C69 C70 H70A 119.9 . .
C66 C71 C70 119.9(8) . .
C66 C71 C63 122.6(8) . .
C70 C71 C63 117.5(8) . .
C66 C71 C63' 118.5(9) . .
C70 C71 C63' 121.5(10) . .
O11 C72 O12 120.2(6) . .
O11 C72 C68 119.1(6) . .
O12 C72 C68 120.7(6) . .
N7 C73 C74 121.4(12) . .
N7 C73 H73A 119.3 . .
C74 C73 H73A 119.3 . .
C75 C74 C73 120.7(12) . .
C75 C74 H74A 119.7 . .
C73 C74 H74A 119.7 . .
C74 C75 C76 116.6(10) . .
C74 C75 C80 122.5(10) . .
C76 C75 C80 120.8(10) . .
C75 C76 C77 118.7(13) . .
C75 C76 H76A 120.7 . .
C77 C76 H76A 120.7 . .
N7 C77 C76 121.7(15) . .
N7 C77 H77A 119.2 . .
C76 C77 H77A 119.2 . .
C79 C78 C83 121.0(9) . .
C79 C78 H78A 119.5 . .
C83 C78 H78A 119.5 . .
C78 C79 C80 121.2(9) . .
C78 C79 H79A 119.4 . .
C80 C79 H79A 119.4 . .
C79 C80 C81 118.1(8) . .
C79 C80 C75 121.5(9) . .
C81 C80 C75 120.2(9) . .
C80 C81 C82 120.5(9) . .
C80 C81 H81A 119.8 . .
C82 C81 H81A 119.8 . .
C83 C82 C81 119.8(9) . .
C83 C82 H82A 120.1 . .
C81 C82 H82A 120.1 . .
C82 C83 C78 119.2(8) . .
C82 C83 C84 118.3(7) . .
C78 C83 C84 122.5(8) . .
O14 C84 O13 125.2(8) . .
O14 C84 C83 118.6(7) . .
O13 C84 C83 116.2(8) . .
N8 C85 C86 122(2) . .
N8 C85 H85A 118.8 . .
C86 C85 H85A 118.8 . .
C87 C86 C85 122.1(18) . .
C87 C86 H86A 118.9 . .
C85 C86 H86A 118.9 . .
C88 C87 C86 113.9(16) . .
C88 C87 C92 120.2(17) . .
C86 C87 C92 125.8(15) . .
C87 C88 C89 126(2) . .
C87 C88 H88A 116.9 . .
C89 C88 H88A 116.9 . .
N8 C89 C88 113(2) . .
C95 C90 C91 121.4(9) . .
C95 C90 H90A 119.3 . .
C91 C90 H90A 119.3 . .
C92 C91 C90 120.0(10) . .
C92 C91 H91A 120.0 . .
C90 C91 H91A 120.0 . .
C91 C92 C93 119.7(9) . .
C91 C92 C87 119.7(12) . .
C93 C92 C87 120.5(12) . .
C94 C93 C92 120.3(10) . .
C94 C93 H93A 119.8 . .
C92 C93 H93A 119.8 . .
C93 C94 C95 121.2(10) . .
C93 C94 H94A 119.4 . .
C95 C94 H94A 119.4 . .
C90 C95 C94 117.1(7) . .
C90 C95 C96 122.4(7) . .
C94 C95 C96 120.4(8) . .
O16 C96 O15 124.5(7) . .
O16 C96 C95 117.4(7) . .
O15 C96 C95 118.1(7) . .
N9 C97 C98 125.4(11) . .
N9 C97 H97A 117.3 . .
C98 C97 H97A 117.3 . .
C97 C98 C99 118.8(10) . .
C97 C98 H98A 120.6 . .
C99 C98 H98A 120.6 . .
C100 C99 C98 115.5(9) . .
C100 C99 C104 121.8(9) . .
C98 C99 C104 122.7(9) . .
C101 C100 C99 120.8(12) . .
C101 C100 H10B 119.6 . .
C99 C100 H10B 119.6 . .
N9 C101 C100 125.1(12) . .
N9 C101 H10C 117.5 . .
C100 C101 H10C 117.5 . .
C107 C102 C103 120.1(7) . .
C107 C102 H10D 120.0 . .
C103 C102 H10D 120.0 . .
C104 C103 C102 121.4(8) . .
C104 C103 H10E 119.3 . .
C102 C103 H10E 119.3 . .
C103 C104 C105 118.2(7) . .
C103 C104 C99 122.6(8) . .
C105 C104 C99 119.1(8) . .
C104 C105 C106 120.7(8) . .
C104 C105 H10F 119.6 . .
C106 C105 H10F 119.6 . .
C107 C106 C105 120.3(7) . .
C107 C106 H10G 119.9 . .
C105 C106 H10G 119.9 . .
C102 C107 C106 119.2(6) . .
C102 C107 C108 122.9(7) . .
C106 C107 C108 117.9(6) . .
O17 C108 O18 125.3(6) . .
O17 C108 C107 116.6(6) . .
O18 C108 C107 118.0(6) . .
C110 C109 N10 120.0 . .
C110 C109 H10H 120.0 . .
N10 C109 H10H 120.0 . .
C109 C110 C111 120.0 . .
C109 C110 H11A 120.0 . .
C111 C110 H11A 120.0 . .
C112 C111 C110 120.0 . .
C112 C111 C116 131.1(14) . .
C110 C111 C116 108.8(14) . .
C111 C112 C113 120.0 . .
C111 C112 H11B 120.0 . .
C113 C112 H11B 120.0 . .
C112 C113 N10 120.0 . .
C113 N10 C109 120.0 . .
C113 N10 Cu1 122.6(7) . 7_566
C109 N10 Cu1 117.4(7) . 7_566
C10' C09' N10' 120.0 . .
C10' C09' H09A 120.0 . .
N10' C09' H09A 120.0 . .
C12' C10' C09' 120.0 . .
C12' C10' H10I 120.0 . .
C09' C10' H10I 120.0 . .
C10' C12' C11' 120.0 . .
C10' C12' C116 130.7(15) . .
C11' C12' C116 109.2(15) . .
C13' C11' C12' 120.0 . .
C13' C11' H11D 120.0 . .
C12' C11' H11D 120.0 . .
C11' C13' N10' 120.0 . .
C11' C13' H13B 120.0 . .
N10' C13' H13B 120.0 . .
C13' N10' C09' 120.0 . .
C13' N10' Cu1' 124.4(10) . 7_566
C09' N10' Cu1' 115.6(10) . 7_566
C13' N10' Cu1 88.7(9) . 7_566
C09' N10' Cu1 142.0(10) . 7_566
C119 C114 C115 123.7(12) . .
C119 C114 H11E 118.2 . .
C115 C114 H11E 118.2 . .
C114 C115 C116 118.6(16) . .
C114 C115 H11F 120.7 . .
C116 C115 H11F 120.7 . .
C115 C116 C117 119.1(12) . .
C115 C116 C111 133(2) . .
C117 C116 C111 107.5(16) . .
C115 C116 C12' 104.6(18) . .
C117 C116 C12' 136.4(16) . .
C118 C117 C116 119.5(15) . .
C118 C117 H11G 120.2 . .
C116 C117 H11G 120.2 . .
C119 C118 C117 121.0(16) . .
C119 C118 H11H 119.5 . .
C117 C118 H11H 119.5 . .
C114 C119 C118 118.1(9) . .
C114 C119 C120 121.6(8) . .
C118 C119 C120 120.3(10) . .
O20 C120 O19 125.1(7) . .
O20 C120 C119 117.2(8) . .
O19 C120 C119 117.7(7) . .
N11 C121 C122 122.0(9) . .
N11 C121 H12A 119.0 . .
C122 C121 H12A 119.0 . .
C121 C122 C123 120.6(8) . .
C121 C122 H12B 119.7 . .
C123 C122 H12B 119.7 . .
C124 C123 C122 116.6(9) . .
C124 C123 C128 122.0(9) . .
C122 C123 C128 121.4(8) . .
C123 C124 C125 119.0(10) . .
C123 C124 H12C 120.5 . .
C125 C124 H12C 120.5 . .
N11 C125 C124 124.5(9) . .
N11 C125 H12D 117.8 . .
C124 C125 H12D 117.8 . .
C127 C126 C131 121.5(7) . .
C127 C126 H12E 119.2 . .
C131 C126 H12E 119.2 . .
C126 C127 C128 120.9(8) . .
C126 C127 H12F 119.6 . .
C128 C127 H12F 119.6 . .
C129 C128 C127 117.9(8) . .
C129 C128 C123 120.1(8) . .
C127 C128 C123 122.0(8) . .
C128 C129 C130 121.2(8) . .
C128 C129 H12G 119.4 . .
C130 C129 H12G 119.4 . .
C131 C130 C129 119.2(9) . .
C131 C130 H13C 120.4 . .
C129 C130 H13C 120.4 . .
C130 C131 C126 119.2(8) . .
C130 C131 C132 119.0(8) . .
C126 C131 C132 121.8(6) . .
O22 C132 O21 120.8(7) . .
O22 C132 C131 120.8(6) . .
O21 C132 C131 118.4(7) . .
O22 C132 Dy1 55.1(4) . 1_545
O21 C132 Dy1 66.1(4) . 1_545
C131 C132 Dy1 170.2(6) . 1_545
C5 N1 C1 122(2) . .
C5 N1 Cu2 124(2) . 5_676
C1 N1 Cu2 113.4(13) . 5_676
C5 N1 Cu2' 102(2) . 5_676
C1 N1 Cu2' 133.8(14) . 5_676
C13 N2 C17 116.8(9) . .
C13 N2 Cu7 121.5(8) . 5_676
C17 N2 Cu7 121.7(9) . 5_676
C29 N3 C25 114.5(10) . .
C29 N3 Cu5 123.0(9) . .
C25 N3 Cu5 122.3(8) . .
C49 N5 C53 115.0(10) . .
C49 N5 Cu7 124.0(9) . 1_545
C53 N5 Cu7 121.1(9) . 1_545
C77 N7 C73 120.0(12) . .
C77 N7 Cu6 118.9(10) . 8_455
C73 N7 Cu6 120.7(9) . 8_455
C85 N8 C89 120(2) . .
C97 N9 C101 114.2(9) . .
C97 N9 Cu8 125.5(8) . 7_566
C101 N9 Cu8 119.8(8) . 7_566
C125 N11 C121 117.2(8) . .
C125 N11 Cu8 122.4(7) . 8_465
C121 N11 Cu8 119.6(7) . 8_465
C12 O1 Dy1 137.3(5) . .
C12 O2 Dy5 139.6(5) . 1_565
C24 O3 Dy3 118.7(5) . .
C24 O4 Dy1 164.5(5) . .
C36 O5 Dy2 115.7(4) . .
C36 O5 Dy3 123.6(4) . .
Dy2 O5 Dy3 104.90(16) . .
C36 O6 Dy2 141.0(5) . 7_566
C48 O7 Dy3 138.4(5) . .
C48 O8 Dy4 133.0(4) . .
C60 O9 Dy5 135.9(5) . .
C60 O10 Dy4 113.7(5) . 7_556
C60 O10 Dy2 124.2(4) . 1_545
Dy4 O10 Dy2 87.40(14) 7_556 1_545
C72 O11 Dy3 160.1(5) . .
C72 O11 Dy4 97.2(4) . .
Dy3 O11 Dy4 102.42(18) . .
C72 O12 Dy5 148.5(5) . .
C72 O12 Dy4 92.9(4) . .
Dy5 O12 Dy4 104.06(17) . .
C84 O13 Dy3 138.2(6) . .
C84 O14 Dy1 128.1(5) . .
C96 O15 Dy4 130.0(5) . .
C96 O16 Dy5 143.1(5) . .
C108 O17 Dy4 137.8(4) . .
C108 O18 Dy3 134.5(5) . .
C120 O19 Dy1 132.7(5) . .
C120 O20 Dy2 139.7(5) . .
C132 O21 Dy5 166.8(5) . .
C132 O21 Dy1 89.2(5) . 1_545
Dy5 O21 Dy1 103.39(18) . 1_545
C132 O22 Dy1 100.8(4) . 1_545
Dy3 O23 Dy2 114.20(16) . .
Dy3 O23 Dy1 118.37(19) . .
Dy2 O23 Dy1 106.08(16) . .
Dy2 O24 Dy1 111.87(17) . .
Dy2 O24 Dy5 106.97(17) . 1_565
Dy1 O24 Dy5 113.95(17) . 1_565
Dy5 O25 Dy4 115.94(17) . .
Dy4 O26 Dy3 106.85(17) 7_566 7_566
Dy4 O26 Dy2 99.01(16) 7_566 .
Dy3 O26 Dy2 144.28(19) 7_566 .
Dy2 O27 Dy4 101.82(16) 7_566 .
Dy2 O27 Dy5 106.33(17) 7_566 7_556
Dy4 O27 Dy5 129.11(18) . 7_556
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O4 2.415(6) .
Dy1 O24 2.429(4) .
Dy1 O14 2.451(6) .
Dy1 O19 2.493(7) .
Dy1 O22 2.511(5) 1_565
Dy1 O1 2.591(6) .
Dy1 O23 2.602(5) .
Dy1 N6 2.72(4) 4
Dy1 N6' 2.72(7) 4
Dy1 O21 2.751(6) 1_565
Dy1 C132 3.008(7) 1_565
Dy2 O20 2.395(5) .
Dy2 O27 2.416(4) 7_566
Dy2 O24 2.417(5) .
Dy2 O23 2.420(4) .
Dy2 O6 2.450(5) 7_566
Dy2 O5 2.478(5) .
Dy2 O26 2.521(4) .
Dy2 O10 2.750(5) 1_565
Dy3 O13 2.378(6) .
Dy3 O23 2.379(4) .
Dy3 O7 2.414(5) .
Dy3 O3 2.449(6) .
Dy3 O11 2.480(5) .
Dy3 O26 2.511(5) 7_566
Dy3 O18 2.561(5) .
Dy3 O5 2.603(5) .
Dy4 O17 2.409(5) .
Dy4 O26 2.427(5) 7_566
Dy4 O27 2.433(4) .
Dy4 O15 2.441(5) .
Dy4 O25 2.505(4) .
Dy4 O8 2.520(5) .
Dy4 O11 2.607(5) .
Dy4 O12 2.686(5) .
Dy4 O10 2.696(6) 7_556
Dy5 O2 2.337(6) 1_545
Dy5 O16 2.413(6) .
Dy5 O25 2.448(4) .
Dy5 O24 2.449(4) 1_545
Dy5 O9 2.454(5) .
Dy5 O21 2.456(5) .
Dy5 O27 2.469(5) 7_556
Dy5 O12 2.640(5) .
Cu1 Cu1' 1.648(11) .
Cu1 N10 2.02(9) 7_566
Cu1 N10' 2.29(18) 7_566
Cu1 Cu2' 2.396(18) .
Cu1 I6 2.405(5) .
Cu1 I6' 2.466(13) .
Cu1 Cu2 2.547(9) .
Cu1 I4 2.664(6) .
Cu1' N10' 2.05(9) 7_566
Cu1' I8 2.509(8) .
Cu1' I4 2.570(8) .
Cu1' I4' 2.711(12) .
Cu1' Cu3 2.845(9) .
Cu1' I6 2.876(7) .
Cu1' Cu6 3.033(8) .
Cu1' I6' 3.065(16) .
Cu2 Cu2' 0.928(17) .
Cu2 N1 2.060(16) 5_676
Cu2 I3 2.569(6) .
Cu2 I4 2.595(5) .
Cu2' N1 2.15(3) 5_676
Cu2' I3 2.51(2) .
Cu2' I6 2.562(18) .
Cu2' I3' 3.01(3) .
Cu2' I4 3.098(18) .
Cu3 Cu3' 1.011(9) .
Cu3 I5 2.468(6) .
Cu3 I5' 2.53(4) .
Cu3 I7 2.561(4) .
Cu3 I4' 2.565(10) .
Cu3 Cu6 2.628(4) .
Cu3 I4 2.846(5) .
Cu3 I8 2.927(5) .
Cu3' I5 2.288(13) .
Cu3' Cu6 2.424(12) .
Cu3' I8 2.438(13) .
Cu3' Cu4 2.651(9) .
Cu3' I7 2.779(9) .
Cu3' I5' 3.01(4) .
Cu4 N4 2.002(8) .
Cu4 I5 2.516(5) .
Cu4 I2 2.759(5) 5_666
Cu4 I8 2.805(6) .
Cu4 I5' 2.90(5) .
Cu4 I5' 3.09(4) 5_666
Cu5 N3 2.026(8) .
Cu5 I2' 2.585(6) .
Cu5 I1 2.585(2) .
Cu5 I2 2.640(3) .
Cu5 I4 2.760(3) .
Cu5 I4' 2.927(9) .
Cu6 N7 2.067(11) 8_556
Cu6 I7 2.651(3) .
Cu6 I8 2.664(3) .
Cu6 I6 2.728(3) .
Cu7 N5 1.972(8) 1_565
Cu7 N2 1.979(9) 5_676
Cu7 I2' 2.597(6) .
Cu7 I2 3.057(3) .
Cu7 I1 3.080(3) .
Cu8 N11 2.020(8) 8_566
Cu8 N9 2.026(8) 7_566
Cu8 I3 2.577(2) .
Cu8 I3' 2.692(8) .
Cu8 I1 2.852(2) .
I2 Cu4 2.759(5) 5_666
I3 I3' 0.594(12) .
I4 I4' 0.741(11) .
I4 I5' 2.95(4) .
I4' I5' 2.22(4) .
I5 I5' 2.27(4) .
I5 I5' 2.29(4) 5_666
I5' I5' 2.10(7) 5_666
I5' I5 2.29(4) 5_666
I5' Cu4 3.09(4) 5_666
I6 I6' 1.515(12) .
I7 I7' 2.157(5) .
C1 N1 1.31(3) .
C1 C2 1.42(3) .
C1 H1A 0.9300 .
C2 C3 1.36(2) .
C2 H2A 0.9300 .
C3 C4 1.42(3) .
C3 C11 1.493(15) .
C4 C5 1.50(3) .
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C5 N1 1.19(3) .
C5 H5A 0.9300 .
C6 C11 1.357(16) .
C6 C7 1.431(14) .
C6 H6A 0.9300 .
C7 C8 1.386(13) .
C7 H7A 0.9300 .
C8 C9 1.401(12) .
C8 C12 1.519(11) .
C9 C10 1.412(14) .
C9 H9A 0.9300 .
C10 C11 1.378(17) .
C10 H10A 0.9300 .
C12 O2 1.252(10) .
C12 O1 1.254(10) .
C13 N2 1.323(19) .
C13 C14 1.393(14) .
C13 H13A 0.9300 .
C14 C15 1.351(14) .
C14 H14A 0.9300 .
C15 C16 1.417(15) .
C15 C23 1.482(11) .
C16 C17 1.385(12) .
C16 H16A 0.9300 .
C17 N2 1.368(16) .
C17 H17A 0.9300 .
C18 C23 1.396(13) .
C18 C19 1.420(11) .
C18 H18A 0.9300 .
C19 C20 1.370(11) .
C19 H19A 0.9300 .
C20 C21 1.376(13) .
C20 C24 1.510(9) .
C21 C22 1.382(12) .
C21 H21A 0.9300 .
C22 C23 1.384(12) .
C22 H22A 0.9300 .
C24 O4 1.240(9) .
C24 O3 1.257(10) .
C25 N3 1.330(19) .
C25 C26 1.367(15) .
C25 H25A 0.9300 .
C26 C27 1.337(14) .
C26 H26A 0.9300 .
C27 C28 1.330(16) .
C27 C35 1.482(10) .
C28 C29 1.415(15) .
C28 H28A 0.9300 .
C29 N3 1.272(16) .
C29 H29A 0.9300 .
C30 C31 1.363(11) .
C30 C35 1.399(13) .
C30 H30A 0.9300 .
C31 C32 1.393(10) .
C31 H31A 0.9300 .
C32 C33 1.368(11) .
C32 C36 1.479(9) .
C33 C34 1.396(11) .
C33 H33A 0.9300 .
C34 C35 1.399(12) .
C34 H34A 0.9300 .
C36 O6 1.249(9) .
C36 O5 1.289(8) .
C37 C38 1.3900 .
C37 N4 1.3900 .
C37 H37A 0.9300 .
C38 C39 1.3900 .
C38 H38A 0.9300 .
C39 C40 1.3900 .
C39 C47 1.465(13) .
C40 C41 1.3900 .
C40 H40A 0.9300 .
C41 N4 1.3900 .
C41 H41A 0.9300 .
C42 C47 1.367(19) .
C42 C43 1.376(15) .
C42 H42A 0.9300 .
C43 C44 1.373(13) .
C43 H43A 0.9300 .
C44 C45 1.373(13) .
C44 C48 1.492(10) .
C45 C46 1.418(15) .
C45 H45A 0.9300 .
C46 C47 1.38(2) .
C46 H46A 0.9300 .
C48 O7 1.236(10) .
C48 O8 1.274(10) .
C49 N5 1.298(19) .
C49 C50 1.395(15) .
C49 H49A 0.9300 .
C50 C51 1.344(14) .
C50 H50A 0.9300 .
C51 C52 1.393(16) .
C51 C59 1.499(11) .
C52 C53 1.395(13) .
C52 H52A 0.9300 .
C53 N5 1.306(16) .
C53 H53A 0.9300 .
C54 C55 1.390(10) .
C54 C59 1.399(13) .
C54 H54A 0.9300 .
C55 C56 1.406(10) .
C55 H55A 0.9300 .
C56 C57 1.388(11) .
C56 C60 1.508(9) .
C57 C58 1.367(11) .
C57 H57A 0.9300 .
C58 C59 1.380(13) .
C58 H58A 0.9300 .
C60 O9 1.265(9) .
C60 O10 1.271(9) .
C61 C62 1.3900 .
C61 N6 1.3900 .
C61 H61A 0.9300 .
C62 C63 1.3900 .
C62 H62A 0.9300 .
C63 C64 1.3900 .
C63 C71 1.513(11) .
C64 C65 1.3900 .
C64 H64A 0.9300 .
C65 N6 1.3900 .
C65 H65A 0.9300 .
N6 Dy1 2.722(8) 4_545
C61' C62' 1.3900 .
C61' N6' 1.3900 .
C61' H61B 0.9300 .
C62' C63' 1.3900 .
C62' H62B 0.9300 .
C63' C64' 1.3900 .
C63' C71 1.524(13) .
C64' C65' 1.3900 .
C64' H64B 0.9300 .
C65' N6' 1.3900 .
C65' H65B 0.9300 .
N6' Dy1 2.722(10) 4_545
C66 C71 1.380(13) .
C66 C67 1.384(11) .
C66 H66A 0.9300 .
C67 C68 1.403(10) .
C67 H67A 0.9300 .
C68 C69 1.370(12) .
C68 C72 1.495(10) .
C69 C70 1.403(12) .
C69 H69A 0.9300 .
C70 C71 1.400(12) .
C70 H70A 0.9300 .
C72 O11 1.251(8) .
C72 O12 1.275(8) .
C73 N7 1.315(19) .
C73 C74 1.398(16) .
C73 H73A 0.9300 .
C74 C75 1.373(15) .
C74 H74A 0.9300 .
C75 C76 1.385(18) .
C75 C80 1.492(13) .
C76 C77 1.438(18) .
C76 H76A 0.9300 .
C77 N7 1.290(18) .
C77 H77A 0.9300 .
C78 C79 1.371(12) .
C78 C83 1.392(12) .
C78 H78A 0.9300 .
C79 C80 1.399(15) .
C79 H79A 0.9300 .
C80 C81 1.399(14) .
C81 C82 1.413(14) .
C81 H81A 0.9300 .
C82 C83 1.387(13) .
C82 H82A 0.9300 .
C83 C84 1.509(11) .
C84 O14 1.236(11) .
C84 O13 1.257(10) .
C85 N8 1.26(3) .
C85 C86 1.388(18) .
C85 H85A 0.9300 .
C86 C87 1.34(2) .
C86 H86A 0.9300 .
C87 C88 1.33(3) .
C87 C92 1.516(16) .
C88 C89 1.44(3) .
C88 H88A 0.9300 .
C89 N8 1.38(4) .
C90 C95 1.381(13) .
C90 C91 1.390(12) .
C90 H90A 0.9300 .
C91 C92 1.341(16) .
C91 H91A 0.9300 .
C92 C93 1.390(18) .
C93 C94 1.357(14) .
C93 H93A 0.9300 .
C94 C95 1.396(12) .
C94 H94A 0.9300 .
C95 C96 1.492(10) .
C96 O16 1.242(10) .
C96 O15 1.266(10) .
C97 N9 1.313(15) .
C97 C98 1.381(13) .
C97 H97A 0.9300 .
C98 C99 1.381(15) .
C98 H98A 0.9300 .
C99 C100 1.363(15) .
C99 C104 1.504(11) .
C100 C101 1.355(16) .
C100 H10B 0.9300 .
C101 N9 1.314(16) .
C101 H10C 0.9300 .
C102 C107 1.389(10) .
C102 C103 1.393(10) .
C102 H10D 0.9300 .
C103 C104 1.389(12) .
C103 H10E 0.9300 .
C104 C105 1.396(12) .
C105 C106 1.397(10) .
C105 H10F 0.9300 .
C106 C107 1.392(10) .
C106 H10G 0.9300 .
C107 C108 1.504(9) .
C108 O17 1.254(9) .
C108 O18 1.258(9) .
C109 C110 1.3900 .
C109 N10 1.3900 .
C109 H10H 0.9300 .
C110 C111 1.3900 .
C110 H11A 0.9300 .
C111 C112 1.3900 .
C111 C116 1.471(17) .
C112 C113 1.3900 .
C112 H11B 0.9300 .
C113 N10 1.3900 .
N10 Cu1 2.020(13) 7_566
C09' C10' 1.3900 .
C09' N10' 1.3900 .
C09' H09A 0.9300 .
C10' C12' 1.3900 .
C10' H10I 0.9300 .
C12' C11' 1.3900 .
C12' C116 1.62(2) .
C11' C13' 1.3900 .
C11' H11D 0.9300 .
C13' N10' 1.3900 .
C13' H13B 0.9300 .
N10' Cu1' 2.052(18) 7_566
N10' Cu1 2.294(17) 7_566
C114 C119 1.344(16) .
C114 C115 1.383(14) .
C114 H11E 0.9300 .
C115 C116 1.39(2) .
C115 H11F 0.9300 .
C116 C117 1.40(3) .
C117 C118 1.395(19) .
C117 H11G 0.9300 .
C118 C119 1.380(14) .
C118 H11H 0.9300 .
C119 C120 1.511(10) .
C120 O20 1.240(9) .
C120 O19 1.262(11) .
C121 N11 1.373(11) .
C121 C122 1.381(12) .
C121 H12A 0.9300 .
C122 C123 1.400(14) .
C122 H12B 0.9300 .
C123 C124 1.396(13) .
C123 C128 1.475(12) .
C124 C125 1.402(15) .
C124 H12C 0.9300 .
C125 N11 1.307(15) .
C125 H12D 0.9300 .
C126 C127 1.370(11) .
C126 C131 1.386(12) .
C126 H12E 0.9300 .
C127 C128 1.395(12) .
C127 H12F 0.9300 .
C128 C129 1.386(14) .
C129 C130 1.421(14) .
C129 H12G 0.9300 .
C130 C131 1.378(12) .
C130 H13C 0.9300 .
C131 C132 1.513(11) .
C132 O22 1.251(10) .
C132 O21 1.254(9) .
C132 Dy1 3.008(7) 1_545
N1 Cu2 2.060(16) 5_676
N1 Cu2' 2.15(3) 5_676
N2 Cu7 1.979(9) 5_676
N5 Cu7 1.972(8) 1_545
N7 Cu6 2.067(11) 8_455
N9 Cu8 2.026(8) 7_566
N11 Cu8 2.020(8) 8_465
O1W H0B 0.8491 .
O1W H0C 0.9603 .
O2 Dy5 2.337(6) 1_565
O6 Dy2 2.450(5) 7_566
O10 Dy4 2.696(6) 7_556
O10 Dy2 2.750(5) 1_545
O21 Dy1 2.751(6) 1_545
O22 Dy1 2.511(5) 1_545
O24 Dy5 2.449(4) 1_565
O26 Dy4 2.427(5) 7_566
O26 Dy3 2.511(5) 7_566
O27 Dy2 2.416(4) 7_566
O27 Dy5 2.469(5) 7_556
