#------------------------------------------------------------------------------
#$Date: 2016-03-23 22:45:38 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179490 $
#$URL: svn://www.crystallography.net/cod/cif/4/33/87/4338733.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4338733
loop_
_publ_author_name
'Sikdar, Nivedita'
'Hazra, Arpan'
'Maji, Tapas Kumar'
_publ_section_title
;
 Stoichiometry-Controlled Two Flexible Interpenetrated Frameworks: Higher
 CO2 Uptake in a Nanoscale Counterpart Supported by Accelerated Adsorption
 Kinetics.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5993
_journal_page_last               6002
_journal_paper_doi               10.1021/ic500234r
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C38 H24 N4 O8 Zn2'
_chemical_formula_weight         795.35
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                92.4270(10)
_cell_angle_beta                 99.1830(10)
_cell_angle_gamma                90.0520(10)
_cell_formula_units_Z            2
_cell_length_a                   15.2090(4)
_cell_length_b                   15.2245(4)
_cell_length_c                   15.8758(4)
_cell_measurement_reflns_used    2896
_cell_measurement_temperature    240(2)
_cell_measurement_theta_max      23.83
_cell_measurement_theta_min      2.10
_cell_volume                     3625.55(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT  A'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      240(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0489
_diffrn_reflns_av_sigmaI/netI    0.0444
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            48826
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.30
_exptl_absorpt_coefficient_mu    0.690
_exptl_absorpt_correction_T_max  0.9469
_exptl_absorpt_correction_T_min  0.9036
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    0.729
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             808
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.08
_refine_diff_density_max         0.681
_refine_diff_density_min         -0.479
_refine_diff_density_rms         0.154
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.126
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     505
_refine_ls_number_reflns         12681
_refine_ls_number_restraints     48
_refine_ls_restrained_S_all      1.138
_refine_ls_R_factor_all          0.0846
_refine_ls_R_factor_gt           0.0645
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1312P)²+4.1108P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2160
_refine_ls_wR_factor_ref         0.2371
_reflns_number_gt                9792
_reflns_number_total             12681
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            ic500234r_si_002.cif
_cod_data_source_block           compound1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338733--4338734.cif.
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4338733
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.8145(6) 0.4180(4) 0.1322(4) 0.087(2) Uani 1 1 d . . .
H1 H 0.7900 0.3849 0.0826 0.104 Uiso 1 1 calc R . .
C2 C 0.8523(3) 0.2764(3) 0.2051(3) 0.0503(12) Uani 1 1 d . . .
C3 C 0.8510(4) 0.3746(3) 0.2044(3) 0.0592(14) Uani 1 1 d . . .
C4 C 0.8844(6) 0.4255(4) 0.2759(4) 0.099(3) Uani 1 1 d . . .
H4 H 0.9081 0.3981 0.3264 0.119 Uiso 1 1 calc R . .
C5 C 0.8840(7) 0.5145(4) 0.2751(4) 0.106(3) Uani 1 1 d . . .
H5 H 0.9073 0.5472 0.3252 0.127 Uiso 1 1 calc R . .
C6 C 0.8499(5) 0.5589(3) 0.2020(4) 0.0707(17) Uani 1 1 d . . .
C7 C 0.8135(6) 0.5068(4) 0.1313(4) 0.097(3) Uani 1 1 d . . .
H7 H 0.7873 0.5339 0.0814 0.117 Uiso 1 1 calc R . .
C8 C 0.8503(5) 0.6566(3) 0.2016(4) 0.0728(17) Uani 1 1 d . . .
C9 C 0.8550(7) 0.7089(4) 0.2753(4) 0.104(3) Uani 1 1 d . . .
H9 H 0.8562 0.6822 0.3277 0.125 Uiso 1 1 calc R . .
C10 C 0.8580(6) 0.7987(4) 0.2742(4) 0.088(2) Uani 1 1 d . . .
H10 H 0.8612 0.8321 0.3258 0.105 Uiso 1 1 calc R . .
C11 C 0.8565(4) 0.8408(3) 0.1999(4) 0.0576(13) Uani 1 1 d . . .
C12 C 0.8507(5) 0.7895(4) 0.1251(4) 0.081(2) Uani 1 1 d . . .
H12 H 0.8495 0.8169 0.0729 0.097 Uiso 1 1 calc R . .
C13 C 0.8467(6) 0.6994(4) 0.1255(4) 0.089(2) Uani 1 1 d . . .
H13 H 0.8415 0.6662 0.0736 0.106 Uiso 1 1 calc R . .
C15 C 0.6873(3) 0.1022(3) 0.1884(3) 0.0506(12) Uani 1 1 d . . .
C16 C 0.5887(3) 0.1023(4) 0.1896(3) 0.0572(13) Uani 1 1 d . . .
C17 C 0.5560(4) 0.1348(5) 0.2612(4) 0.084(2) Uani 1 1 d . . .
H17 H 0.5961 0.1558 0.3091 0.101 Uiso 1 1 calc R . .
C18 C 0.4669(4) 0.1371(6) 0.2636(4) 0.089(2) Uani 1 1 d . . .
H18 H 0.4469 0.1600 0.3130 0.107 Uiso 1 1 calc R . .
C19 C 0.4050(4) 0.1063(5) 0.1948(4) 0.0725(17) Uani 1 1 d . . .
C20 C 0.4381(4) 0.0736(5) 0.1236(4) 0.083(2) Uani 1 1 d . . .
H20 H 0.3984 0.0527 0.0754 0.100 Uiso 1 1 calc R . .
C21 C 0.5284(4) 0.0713(5) 0.1220(4) 0.0757(18) Uani 1 1 d . . .
H21 H 0.5490 0.0477 0.0731 0.091 Uiso 1 1 calc R . .
C23 C 0.3081(3) 0.1095(5) 0.1992(4) 0.0685(16) Uani 1 1 d . . .
C24 C 0.2465(4) 0.1171(5) 0.1248(4) 0.079(2) Uani 1 1 d . . .
H24 H 0.2663 0.1194 0.0718 0.094 Uiso 1 1 calc R . .
C25 C 0.2761(4) 0.1031(5) 0.2752(4) 0.079(2) Uani 1 1 d . . .
H25 H 0.3165 0.0973 0.3259 0.094 Uiso 1 1 calc R . .
C26 C 0.1865(3) 0.1050(5) 0.2781(4) 0.0696(17) Uani 1 1 d . . .
H26 H 0.1666 0.0999 0.3308 0.084 Uiso 1 1 calc R . .
C27 C 0.1252(3) 0.1142(4) 0.2053(3) 0.0530(12) Uani 1 1 d . . .
C28 C 0.1567(3) 0.1211(5) 0.1287(4) 0.0711(17) Uani 1 1 d . . .
H28 H 0.1161 0.1287 0.0784 0.085 Uiso 1 1 calc R . .
C29 C 0.0275(3) 0.1128(3) 0.2076(3) 0.0468(11) Uani 1 1 d . . .
C30 C 0.9099(4) 0.1001(4) -0.0562(3) 0.0641(15) Uani 1 1 d . . .
H30 H 0.9642 0.0913 -0.0201 0.077 Uiso 1 1 calc R . .
C31 C 0.7605(4) 0.1178(5) -0.0734(4) 0.080(2) Uani 1 1 d . . .
H31 H 0.7079 0.1219 -0.0495 0.096 Uiso 1 1 calc R . .
C32 C 0.9105(4) 0.1039(5) -0.1417(4) 0.0707(17) Uani 1 1 d . . .
H32 H 0.9643 0.0985 -0.1635 0.085 Uiso 1 1 calc R . .
C33 C 0.7544(4) 0.1220(6) -0.1604(4) 0.098(3) Uani 1 1 d . . .
H33 H 0.6989 0.1289 -0.1952 0.117 Uiso 1 1 calc R . .
C34 C 0.8317(4) 0.1158(5) -0.1956(3) 0.0712(17) Uani 1 1 d . A .
C35 C 0.8839(5) 0.1163(5) -0.4036(3) 0.0735(18) Uani 1 1 d . . .
C36B C 0.9495(10) 0.0691(11) -0.4407(9) 0.090(4) Uani 0.50 1 d PU A 1
H36B H 0.9954 0.0387 -0.4076 0.108 Uiso 0.50 1 calc PR A 1
C37B C 0.8228(12) 0.1573(13) -0.4506(10) 0.106(5) Uani 0.50 1 d PU A 1
H37B H 0.7789 0.1885 -0.4267 0.127 Uiso 0.50 1 calc PR A 1
C38B C 0.8229(12) 0.1544(12) -0.5427(10) 0.104(5) Uani 0.50 1 d PU A 1
H38B H 0.7781 0.1848 -0.5774 0.125 Uiso 0.50 1 calc PR A 1
C40B C 0.9421(9) 0.0706(10) -0.5274(7) 0.075(3) Uani 0.50 1 d PU A 1
H40B H 0.9842 0.0392 -0.5537 0.091 Uiso 0.50 1 calc PR A 1
C36A C 0.9420(13) 0.1653(13) -0.4387(11) 0.114(5) Uani 0.50 1 d PU A 2
H36A H 0.9867 0.1985 -0.4035 0.137 Uiso 0.50 1 calc PR A 2
C37A C 0.8216(10) 0.0699(10) -0.4557(8) 0.083(4) Uani 0.50 1 d PU A 2
H37A H 0.7764 0.0398 -0.4343 0.100 Uiso 0.50 1 calc PR A 2
C38A C 0.9350(11) 0.1660(12) -0.5280(9) 0.101(5) Uani 0.50 1 d PU A 2
H38A H 0.9711 0.2046 -0.5525 0.121 Uiso 0.50 1 calc PR A 2
C40A C 0.8254(10) 0.0675(10) -0.5413(8) 0.080(4) Uani 0.50 1 d PU A 2
H40A H 0.7858 0.0291 -0.5767 0.096 Uiso 0.50 1 calc PR A 2
C44 C 0.8595(3) 0.9390(3) 0.1993(4) 0.0535(13) Uani 1 1 d . . .
N1 N 0.8370(3) 0.1082(3) -0.0216(2) 0.0466(9) Uani 1 1 d . . .
N2 N 0.8223(4) 0.1179(5) -0.2869(3) 0.093(2) Uani 1 1 d . . .
N3 N 0.8926(4) 0.1165(5) -0.3119(3) 0.0891(18) Uani 1 1 d . A .
N4 N 0.8792(3) 0.1137(3) -0.5775(2) 0.0503(10) Uani 1 1 d . . .
O1 O 0.7372(2) 0.1176(3) 0.2578(2) 0.0600(9) Uani 1 1 d . . .
O2 O 0.7115(2) 0.0878(3) 0.1174(2) 0.0585(9) Uani 1 1 d . . .
O3 O 0.8769(3) 0.2424(2) 0.2756(2) 0.0590(9) Uani 1 1 d . . .
O4 O 0.8294(3) 0.2347(2) 0.1352(2) 0.0580(9) Uani 1 1 d . . .
O5 O 0.8623(3) 0.9798(2) 0.2695(3) 0.0649(10) Uani 1 1 d . . .
O6 O 0.8593(3) 0.9727(2) 0.1289(3) 0.0650(10) Uani 1 1 d . . .
O7 O 0.0032(2) 0.1051(3) 0.2795(2) 0.0568(9) Uani 1 1 d . . .
O8 O -0.0239(2) 0.1180(3) 0.1382(2) 0.0576(9) Uani 1 1 d . . .
Zn1 Zn 0.84151(3) 0.10346(3) 0.10680(3) 0.03576(18) Uani 1 1 d . . .
Zn2 Zn 0.87253(3) 0.11197(3) 0.29318(3) 0.03574(18) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C7 C1 C3 121.5(6) . .
O4 C2 O3 125.3(4) . .
O4 C2 C3 117.4(5) . .
O3 C2 C3 117.3(5) . .
C4 C3 C1 117.2(5) . .
C4 C3 C2 121.3(5) . .
C1 C3 C2 121.4(5) . .
C5 C4 C3 121.4(6) . .
C4 C5 C6 121.9(6) . .
C7 C6 C5 116.1(5) . .
C7 C6 C8 122.4(6) . .
C5 C6 C8 121.5(6) . .
C1 C7 C6 121.8(6) . .
C9 C8 C13 116.9(5) . .
C9 C8 C6 122.5(6) . .
C13 C8 C6 120.6(6) . .
C10 C9 C8 121.9(6) . .
C11 C10 C9 121.4(6) . .
C10 C11 C12 117.6(5) . .
C10 C11 C44 121.1(5) . .
C12 C11 C44 121.3(5) . .
C13 C12 C11 121.4(6) . .
C12 C13 C8 120.8(6) . .
O1 C15 O2 126.1(4) . .
O1 C15 C16 117.2(5) . .
O2 C15 C16 116.7(5) . .
C21 C16 C17 117.5(5) . .
C21 C16 C15 122.5(5) . .
C17 C16 C15 120.0(5) . .
C18 C17 C16 121.3(6) . .
C17 C18 C19 121.6(6) . .
C20 C19 C18 116.8(5) . .
C20 C19 C23 122.8(6) . .
C18 C19 C23 120.4(5) . .
C21 C20 C19 121.1(6) . .
C16 C21 C20 121.7(5) . .
C25 C23 C24 118.0(5) . .
C25 C23 C19 121.9(5) . .
C24 C23 C19 120.1(5) . .
C28 C24 C23 120.3(5) . .
C26 C25 C23 121.3(5) . .
C25 C26 C27 121.2(5) . .
C26 C27 C28 118.0(5) . .
C26 C27 C29 121.4(5) . .
C28 C27 C29 120.5(5) . .
C24 C28 C27 121.2(5) . .
O8 C29 O7 125.2(4) . .
O8 C29 C27 117.5(4) . .
O7 C29 C27 117.3(4) . .
N1 C30 C32 123.3(5) . .
N1 C31 C33 123.2(6) . .
C30 C32 C34 119.2(5) . .
C31 C33 C34 118.4(6) . .
C32 C34 C33 118.1(5) . .
C32 C34 N2 125.1(5) . .
C33 C34 N2 116.7(6) . .
C37B C35 C37A 61.1(11) . .
C37B C35 C36A 85.9(12) . .
C37A C35 C36A 118.3(10) . .
C37B C35 C36B 120.2(9) . .
C37A C35 C36B 88.5(10) . .
C36A C35 C36B 63.8(11) . .
C37B C35 N3 123.6(9) . .
C37A C35 N3 123.2(8) . .
C36A C35 N3 118.5(9) . .
C36B C35 N3 116.3(8) . .
C40B C36B C35 116.1(11) . .
C35 C37B C38B 118.3(13) . .
N4 C38B C37B 123.3(14) . .
N4 C40B C36B 124.5(11) . .
C35 C36A C38A 119.5(14) . .
C35 C37A C40A 118.0(11) . .
N4 C38A C36A 120.9(14) . .
N4 C40A C37A 125.3(12) . .
O6 C44 O5 125.9(5) . .
O6 C44 C11 117.3(5) . .
O5 C44 C11 116.8(5) . .
C30 N1 C31 117.8(4) . .
C30 N1 Zn1 121.0(4) . .
C31 N1 Zn1 121.2(3) . .
N3 N2 C34 112.5(6) . .
N2 N3 C35 113.0(6) . .
C38B N4 C40A 62.9(10) . .
C38B N4 C38A 83.2(12) . .
C40A N4 C38A 117.3(9) . .
C38B N4 C40B 117.6(10) . .
C40A N4 C40B 83.6(9) . .
C38A N4 C40B 66.9(10) . .
C38B N4 Zn2 120.4(8) . 1_554
C40A N4 Zn2 122.0(6) . 1_554
C38A N4 Zn2 120.7(7) . 1_554
C40B N4 Zn2 122.0(6) . 1_554
C15 O1 Zn2 132.6(3) . .
C15 O2 Zn1 119.3(3) . .
C2 O3 Zn2 123.8(3) . .
C2 O4 Zn1 128.7(3) . .
C44 O5 Zn2 127.4(4) . 1_565
C44 O6 Zn1 125.1(4) . 1_565
C29 O7 Zn2 121.4(3) . 1_455
C29 O8 Zn1 131.8(3) . 1_455
O2 Zn1 N1 102.45(16) . .
O2 Zn1 O8 161.32(15) . 1_655
N1 Zn1 O8 96.23(15) . 1_655
O2 Zn1 O4 88.53(15) . .
N1 Zn1 O4 98.91(15) . .
O8 Zn1 O4 88.52(16) 1_655 .
O2 Zn1 O6 88.40(16) . 1_545
N1 Zn1 O6 103.34(17) . 1_545
O8 Zn1 O6 87.35(16) 1_655 1_545
O4 Zn1 O6 157.68(16) . 1_545
O2 Zn1 Zn2 85.30(11) . .
N1 Zn1 Zn2 171.41(12) . .
O8 Zn1 Zn2 76.06(10) 1_655 .
O4 Zn1 Zn2 77.38(10) . .
O6 Zn1 Zn2 80.34(12) 1_545 .
O3 Zn2 O5 161.66(16) . 1_545
O3 Zn2 O7 88.77(16) . 1_655
O5 Zn2 O7 88.89(16) 1_545 1_655
O3 Zn2 N4 99.84(16) . 1_556
O5 Zn2 N4 98.44(17) 1_545 1_556
O7 Zn2 N4 102.35(16) 1_655 1_556
O3 Zn2 O1 87.85(16) . .
O5 Zn2 O1 87.61(16) 1_545 .
O7 Zn2 O1 158.26(15) 1_655 .
N4 Zn2 O1 99.39(16) 1_556 .
O3 Zn2 Zn1 82.25(10) . .
O5 Zn2 Zn1 79.41(12) 1_545 .
O7 Zn2 Zn1 83.93(10) 1_655 .
N4 Zn2 Zn1 173.37(12) 1_556 .
O1 Zn2 Zn1 74.33(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C7 1.353(8) .
C1 C3 1.387(8) .
C2 O4 1.255(6) .
C2 O3 1.255(6) .
C2 C3 1.495(7) .
C3 C4 1.374(8) .
C4 C5 1.356(9) .
C5 C6 1.395(9) .
C6 C7 1.386(9) .
C6 C8 1.488(8) .
C8 C9 1.379(9) .
C8 C13 1.390(9) .
C9 C10 1.368(8) .
C10 C11 1.363(8) .
C11 C12 1.385(8) .
C11 C44 1.496(7) .
C12 C13 1.373(8) .
C15 O1 1.247(6) .
C15 O2 1.252(6) .
C15 C16 1.502(7) .
C16 C21 1.362(8) .
C16 C17 1.384(8) .
C17 C18 1.362(8) .
C18 C19 1.388(8) .
C19 C20 1.384(8) .
C19 C23 1.488(8) .
C20 C21 1.378(8) .
C23 C25 1.378(8) .
C23 C24 1.394(8) .
C24 C28 1.378(8) .
C25 C26 1.371(7) .
C26 C27 1.376(7) .
C27 C28 1.385(7) .
C27 C29 1.492(6) .
C29 O8 1.251(6) .
C29 O7 1.264(6) .
C30 N1 1.317(7) .
C30 C32 1.362(8) .
C31 N1 1.326(7) .
C31 C33 1.373(8) .
C32 C34 1.375(8) .
C33 C34 1.381(9) .
C34 N2 1.436(7) .
C35 C37B 1.276(17) .
C35 C37A 1.334(15) .
C35 C36A 1.357(17) .
C35 C36B 1.418(14) .
C35 N3 1.440(7) .
C36B C40B 1.364(17) .
C37B C38B 1.46(2) .
C38B N4 1.242(15) .
C40B N4 1.334(12) .
C36A C38A 1.41(2) .
C37A C40A 1.368(17) .
C38A N4 1.305(15) .
C40A N4 1.295(12) .
C44 O6 1.249(6) .
C44 O5 1.248(7) .
N1 Zn1 2.033(4) .
N2 N3 1.199(8) .
N4 Zn2 2.039(4) 1_554
O1 Zn2 2.048(3) .
O2 Zn1 2.026(3) .
O3 Zn2 2.020(3) .
O4 Zn1 2.045(3) .
O5 Zn2 2.033(3) 1_565
O6 Zn1 2.047(3) 1_565
O7 Zn2 2.036(3) 1_455
O8 Zn1 2.038(3) 1_455
Zn1 O8 2.038(3) 1_655
Zn1 O6 2.047(3) 1_545
Zn1 Zn2 2.9183(7) .
Zn2 O5 2.033(3) 1_545
Zn2 O7 2.036(3) 1_655
Zn2 N4 2.039(4) 1_556
