#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/03/4340347.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4340347
loop_
_publ_author_name
'Zavras, Athanasios'
'Khairallah, George N.'
'Connell, Timothy U.'
'White, Jonathan M.'
'Edwards, Alison J.'
'Mulder, Roger J.'
'Donnelly, Paul S.'
'O'Hair, Richard A J'
_publ_section_title
;
 Synthesis, Structural Characterization, and Gas-Phase Unimolecular
 Reactivity of the Silver Hydride Nanocluster
 [Ag3((PPh2)2CH2)3(μ3-H)](BF4)2.
;
_journal_issue                   14
_journal_name_full               'Inorganic chemistry'
_journal_page_first              7429
_journal_page_last               7437
_journal_paper_doi               10.1021/ic5007499
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         '(C75 H66 D Ag3 B2 F8 P6, 0.5(C H4 O)'
_chemical_formula_sum            'C75.5 H68 Ag3 B2 D F8 O0.5 P6'
_chemical_formula_weight         1668.36
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-I 2ya'
_space_group_name_H-M_alt        'I 1 2/a 1'
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2012
_cell_angle_alpha                90
_cell_angle_beta                 96.589(2)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   26.9665(10)
_cell_length_b                   13.2190(4)
_cell_length_c                   39.5373(8)
_cell_measurement_reflns_used    35760
_cell_measurement_temperature    130.0(1)
_cell_measurement_theta_max      34.1190
_cell_measurement_theta_min      3.2750
_cell_volume                     14000.8(7)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
;
_computing_structure_refinement  'SHELXL-2012 (Sheldrick, 2012)'
_diffrn_ambient_temperature      130.0(1)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.930
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'SuperNova (Mo) X-ray Source'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.0260
_diffrn_reflns_av_unetI/netI     0.0353
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.930
_diffrn_reflns_limit_h_max       40
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       44
_diffrn_reflns_limit_l_min       -59
_diffrn_reflns_number            73424
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.930
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         34.328
_diffrn_reflns_theta_min         2.848
_exptl_absorpt_coefficient_mu    1.034
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.83227
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.583
_exptl_crystal_description       block
_exptl_crystal_F_000             6712
_exptl_crystal_size_max          0.5500
_exptl_crystal_size_mid          0.3647
_exptl_crystal_size_min          0.2479
_refine_diff_density_max         0.961
_refine_diff_density_min         -0.819
_refine_diff_density_rms         0.093
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.063
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     892
_refine_ls_number_reflns         27244
_refine_ls_number_restraints     21
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.0475
_refine_ls_R_factor_gt           0.0318
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[σ²(Fo²)+(0.0188P)²+22.0535P]
 where P=(Fo²+2Fc²)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0624
_refine_ls_wR_factor_ref         0.0692
_reflns_Friedel_coverage         0.000
_reflns_number_gt                21917
_reflns_number_total             27244
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic5007499_si_002.cif
_cod_data_source_block           shelx
_cod_depositor_comments
'Adding full bibliography for 4340347--4340348.cif.'
_cod_original_formula_sum        'C75.50 H68 Ag3 B2 D F8 O0.50 P6'
_cod_database_code               4340347
#BEGIN Tags that were not found in dictionaries:
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2012-9
#END Tags that were not found in dictionaries
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.73065(6) 0.09251(12) 0.22308(4) 0.0154(3) Uani 1 1 d . . . . .
H1A H 0.7507 0.0458 0.2378 0.019 Uiso 1 1 calc R U . . .
H1B H 0.7330 0.1587 0.2337 0.019 Uiso 1 1 calc R U . . .
C2 C 0.49360(6) 0.29776(12) 0.16620(4) 0.0166(3) Uani 1 1 d . . . . .
H2A H 0.4577 0.2996 0.1667 0.020 Uiso 1 1 calc R U . . .
H2B H 0.5084 0.3491 0.1818 0.020 Uiso 1 1 calc R U . . .
C3 C 0.67215(6) 0.24585(14) 0.04633(4) 0.0187(3) Uani 1 1 d . . . . .
H3A H 0.6841 0.2762 0.0264 0.022 Uiso 1 1 calc R U . . .
H3B H 0.6636 0.1760 0.0409 0.022 Uiso 1 1 calc R U . . .
C4 C 0.77645(6) -0.02941(14) 0.17453(5) 0.0210(3) Uani 1 1 d . . . . .
C5 C 0.76098(9) -0.0776(2) 0.14408(7) 0.0461(7) Uani 1 1 d . . . . .
H5 H 0.7389 -0.0457 0.1276 0.055 Uiso 1 1 calc R U . . .
C6 C 0.77854(12) -0.1737(3) 0.13826(10) 0.0775(12) Uani 1 1 d . . . . .
H6 H 0.7679 -0.2060 0.1178 0.093 Uiso 1 1 calc R U . . .
C7 C 0.81098(11) -0.2220(2) 0.16178(9) 0.0611(9) Uani 1 1 d . . . . .
H7 H 0.8223 -0.2866 0.1574 0.073 Uiso 1 1 calc R U . . .
C8 C 0.82694(9) -0.17472(16) 0.19213(7) 0.0387(5) Uani 1 1 d . . . . .
H8 H 0.8491 -0.2074 0.2083 0.046 Uiso 1 1 calc R U . . .
C9 C 0.81001(8) -0.07823(14) 0.19855(5) 0.0271(4) Uani 1 1 d . . . . .
H9 H 0.8211 -0.0461 0.2189 0.032 Uiso 1 1 calc R U . . .
C10 C 0.81478(6) 0.16357(12) 0.18879(4) 0.0173(3) Uani 1 1 d . . . . .
C11 C 0.83829(7) 0.18238(15) 0.15966(5) 0.0256(4) Uani 1 1 d . . . . .
H11 H 0.8216 0.1691 0.1382 0.031 Uiso 1 1 calc R U . . .
C12 C 0.88636(8) 0.22065(16) 0.16270(6) 0.0312(4) Uani 1 1 d . . . . .
H12 H 0.9019 0.2328 0.1433 0.037 Uiso 1 1 calc R U . . .
C13 C 0.91144(7) 0.24102(15) 0.19454(6) 0.0281(4) Uani 1 1 d . . . . .
H13 H 0.9439 0.2662 0.1965 0.034 Uiso 1 1 calc R U . . .
C14 C 0.88805(7) 0.22378(14) 0.22339(5) 0.0246(4) Uani 1 1 d . . . . .
H14 H 0.9047 0.2384 0.2448 0.030 Uiso 1 1 calc R U . . .
C15 C 0.83975(6) 0.18466(13) 0.22069(5) 0.0201(3) Uani 1 1 d . . . . .
H15 H 0.8243 0.1727 0.2402 0.024 Uiso 1 1 calc R U . . .
C16 C 0.66648(6) -0.07983(12) 0.20298(4) 0.0168(3) Uani 1 1 d . . . . .
C17 C 0.64598(7) -0.10315(14) 0.17003(5) 0.0245(4) Uani 1 1 d . . . . .
H17 H 0.6322 -0.0520 0.1558 0.029 Uiso 1 1 calc R U . . .
C18 C 0.64587(9) -0.20225(16) 0.15813(5) 0.0319(4) Uani 1 1 d . . . . .
H18 H 0.6320 -0.2172 0.1361 0.038 Uiso 1 1 calc R U . . .
C19 C 0.66645(8) -0.27841(15) 0.17920(6) 0.0294(4) Uani 1 1 d . . . . .
H19 H 0.6665 -0.3447 0.1713 0.035 Uiso 1 1 calc R U . . .
C20 C 0.68695(8) -0.25620(14) 0.21196(6) 0.0291(4) Uani 1 1 d . . . . .
H20 H 0.7007 -0.3077 0.2261 0.035 Uiso 1 1 calc R U . . .
C21 C 0.68717(7) -0.15762(14) 0.22402(5) 0.0240(4) Uani 1 1 d . . . . .
H21 H 0.7011 -0.1433 0.2461 0.029 Uiso 1 1 calc R U . . .
C22 C 0.64733(6) 0.03393(12) 0.26077(4) 0.0166(3) Uani 1 1 d . . . . .
C23 C 0.67849(7) 0.04686(15) 0.29096(5) 0.0237(4) Uani 1 1 d . . . . .
H23 H 0.7120 0.0630 0.2905 0.028 Uiso 1 1 calc R U . . .
C24 C 0.65918(8) 0.03542(17) 0.32203(5) 0.0314(4) Uani 1 1 d . . . . .
H24 H 0.6800 0.0440 0.3423 0.038 Uiso 1 1 calc R U . . .
C25 C 0.60958(8) 0.01162(15) 0.32314(5) 0.0298(4) Uani 1 1 d . . . . .
H25 H 0.5972 0.0043 0.3440 0.036 Uiso 1 1 calc R U . . .
C26 C 0.57835(8) -0.00136(15) 0.29317(5) 0.0276(4) Uani 1 1 d . . . . .
H26 H 0.5449 -0.0176 0.2938 0.033 Uiso 1 1 calc R U . . .
C27 C 0.59715(7) 0.00995(14) 0.26220(5) 0.0223(3) Uani 1 1 d . . . . .
H27 H 0.5761 0.0015 0.2421 0.027 Uiso 1 1 calc R U . . .
C28 C 0.48283(6) 0.14947(13) 0.21686(4) 0.0175(3) Uani 1 1 d . . . . .
C29 C 0.46665(7) 0.05210(14) 0.22364(5) 0.0230(3) Uani 1 1 d . . . . .
H29 H 0.4742 -0.0015 0.2099 0.028 Uiso 1 1 calc R U . . .
C30 C 0.43925(7) 0.03447(16) 0.25085(5) 0.0276(4) Uani 1 1 d . . . . .
H30 H 0.4287 -0.0307 0.2552 0.033 Uiso 1 1 calc R U . . .
C31 C 0.42769(7) 0.11385(16) 0.27138(5) 0.0284(4) Uani 1 1 d . . . . .
H31 H 0.4087 0.1023 0.2892 0.034 Uiso 1 1 calc R U . . .
C32 C 0.44439(8) 0.21033(16) 0.26537(5) 0.0293(4) Uani 1 1 d . . . . .
H32 H 0.4371 0.2634 0.2794 0.035 Uiso 1 1 calc R U . . .
C33 C 0.47200(7) 0.22832(14) 0.23837(5) 0.0228(3) Uani 1 1 d . . . . .
H33 H 0.4833 0.2933 0.2346 0.027 Uiso 1 1 calc R U . . .
C34 C 0.48898(6) 0.08472(12) 0.14850(4) 0.0169(3) Uani 1 1 d . . . . .
C35 C 0.43720(7) 0.07196(14) 0.14185(5) 0.0222(3) Uani 1 1 d . . . . .
H35 H 0.4159 0.1078 0.1544 0.027 Uiso 1 1 calc R U . . .
C36 C 0.41780(8) 0.00584(15) 0.11655(5) 0.0287(4) Uani 1 1 d . . . . .
H36 H 0.3834 -0.0028 0.1121 0.034 Uiso 1 1 calc R U . . .
C37 C 0.44948(8) -0.04761(15) 0.09779(6) 0.0320(4) Uani 1 1 d . . . . .
H37 H 0.4362 -0.0916 0.0807 0.038 Uiso 1 1 calc R U . . .
C38 C 0.50046(8) -0.03619(15) 0.10415(5) 0.0305(4) Uani 1 1 d . . . . .
H38 H 0.5215 -0.0725 0.0916 0.037 Uiso 1 1 calc R U . . .
C39 C 0.52028(7) 0.03002(13) 0.12953(5) 0.0225(3) Uani 1 1 d . . . . .
H39 H 0.5547 0.0379 0.1339 0.027 Uiso 1 1 calc R U . . .
C40 C 0.45614(6) 0.27365(13) 0.09519(4) 0.0180(3) Uani 1 1 d . . . . .
C41 C 0.40656(7) 0.29579(15) 0.09949(5) 0.0274(4) Uani 1 1 d . . . . .
H41 H 0.3993 0.3376 0.1172 0.033 Uiso 1 1 calc R U . . .
C42 C 0.36827(8) 0.25506(17) 0.07723(6) 0.0343(5) Uani 1 1 d . . . . .
H42 H 0.3353 0.2698 0.0801 0.041 Uiso 1 1 calc R U . . .
C43 C 0.37862(8) 0.19304(16) 0.05095(6) 0.0315(4) Uani 1 1 d . . . . .
H43 H 0.3526 0.1662 0.0362 0.038 Uiso 1 1 calc R U . . .
C44 C 0.42739(8) 0.17049(15) 0.04639(5) 0.0279(4) Uani 1 1 d . . . . .
H44 H 0.4343 0.1286 0.0286 0.033 Uiso 1 1 calc R U . . .
C45 C 0.46606(7) 0.21084(14) 0.06859(5) 0.0217(3) Uani 1 1 d . . . . .
H45 H 0.4990 0.1956 0.0656 0.026 Uiso 1 1 calc R U . . .
C46 C 0.49857(6) 0.46305(13) 0.11968(4) 0.0188(3) Uani 1 1 d . . . . .
C47 C 0.46703(8) 0.50713(16) 0.09343(5) 0.0301(4) Uani 1 1 d . . . . .
H47 H 0.4485 0.4665 0.0774 0.036 Uiso 1 1 calc R U . . .
C48 C 0.46313(9) 0.61189(17) 0.09108(6) 0.0396(5) Uani 1 1 d . . . . .
H48 H 0.4416 0.6409 0.0737 0.047 Uiso 1 1 calc R U . . .
C49 C 0.49076(9) 0.67271(16) 0.11418(6) 0.0375(5) Uani 1 1 d . . . . .
H49 H 0.4879 0.7427 0.1125 0.045 Uiso 1 1 calc R U . . .
C50 C 0.52266(9) 0.63022(16) 0.13988(6) 0.0360(5) Uani 1 1 d . . . . .
H50 H 0.5416 0.6715 0.1554 0.043 Uiso 1 1 calc R U . . .
C51 C 0.52667(8) 0.52555(14) 0.14270(5) 0.0277(4) Uani 1 1 d . . . . .
H51 H 0.5483 0.4972 0.1601 0.033 Uiso 1 1 calc R U . . .
C52 C 0.56827(7) 0.27180(15) 0.02283(4) 0.0226(3) Uani 1 1 d . . . . .
C53 C 0.56233(7) 0.17029(17) 0.01506(5) 0.0300(4) Uani 1 1 d . . . . .
H53 H 0.5839 0.1227 0.0261 0.036 Uiso 1 1 calc R U . . .
C54 C 0.52361(9) 0.1392(2) -0.00957(6) 0.0410(6) Uani 1 1 d . . . . .
H54 H 0.5200 0.0711 -0.0152 0.049 Uiso 1 1 calc R U . . .
C55 C 0.49092(8) 0.2095(2) -0.02547(6) 0.0441(6) Uani 1 1 d . . . . .
H55 H 0.4655 0.1888 -0.0419 0.053 Uiso 1 1 calc R U . . .
C56 C 0.49599(8) 0.3090(2) -0.01709(6) 0.0430(6) Uani 1 1 d . . . . .
H56 H 0.4734 0.3558 -0.0275 0.052 Uiso 1 1 calc R U . . .
C57 C 0.53426(8) 0.34152(19) 0.00674(5) 0.0333(5) Uani 1 1 d . . . . .
H57 H 0.5374 0.4099 0.0121 0.040 Uiso 1 1 calc R U . . .
C58 C 0.62478(6) 0.44564(14) 0.04551(4) 0.0201(3) Uani 1 1 d . . . . .
C59 C 0.61990(7) 0.51947(15) 0.06997(5) 0.0249(4) Uani 1 1 d . . . . .
H59 H 0.6139 0.5007 0.0918 0.030 Uiso 1 1 calc R U . . .
C60 C 0.62399(8) 0.62145(16) 0.06187(6) 0.0326(4) Uani 1 1 d . . . . .
H60 H 0.6212 0.6705 0.0784 0.039 Uiso 1 1 calc R U . . .
C61 C 0.63225(8) 0.65005(17) 0.02938(6) 0.0343(5) Uani 1 1 d . . . . .
H61 H 0.6346 0.7183 0.0240 0.041 Uiso 1 1 calc R U . . .
C62 C 0.63698(8) 0.57709(17) 0.00473(6) 0.0323(5) Uani 1 1 d . . . . .
H62 H 0.6423 0.5965 -0.0172 0.039 Uiso 1 1 calc R U . . .
C63 C 0.63378(7) 0.47519(15) 0.01273(5) 0.0257(4) Uani 1 1 d . . . . .
H63 H 0.6376 0.4264 -0.0037 0.031 Uiso 1 1 calc R U . . .
C64 C 0.77252(6) 0.18787(13) 0.06290(4) 0.0191(3) Uani 1 1 d . . . . .
C65 C 0.76441(8) 0.09090(16) 0.05025(7) 0.0387(6) Uani 1 1 d . . . . .
H65 H 0.7340 0.0592 0.0518 0.046 Uiso 1 1 calc R U . . .
C66 C 0.80136(8) 0.04089(17) 0.03530(8) 0.0486(7) Uani 1 1 d . . . . .
H66 H 0.7954 -0.0240 0.0267 0.058 Uiso 1 1 calc R U . . .
C67 C 0.84681(7) 0.08608(15) 0.03296(6) 0.0300(4) Uani 1 1 d . . . . .
H67 H 0.8714 0.0521 0.0227 0.036 Uiso 1 1 calc R U . . .
C68 C 0.85562(7) 0.18184(14) 0.04589(5) 0.0232(4) Uani 1 1 d . . . . .
H68 H 0.8863 0.2126 0.0444 0.028 Uiso 1 1 calc R U . . .
C69 C 0.81899(6) 0.23285(14) 0.06110(5) 0.0215(3) Uani 1 1 d . . . . .
H69 H 0.8254 0.2971 0.0701 0.026 Uiso 1 1 calc R U . . .
C70 C 0.73861(6) 0.38274(14) 0.08388(5) 0.0207(3) Uani 1 1 d . . . . .
C71 C 0.73357(7) 0.43582(17) 0.11363(5) 0.0294(4) Uani 1 1 d . . . . .
H71 H 0.7265 0.4016 0.1331 0.035 Uiso 1 1 calc R U . . .
C72 C 0.73917(8) 0.54066(19) 0.11415(7) 0.0436(6) Uani 1 1 d . . . . .
H72 H 0.7356 0.5766 0.1339 0.052 Uiso 1 1 calc R U . . .
C73 C 0.74997(9) 0.59112(18) 0.08549(8) 0.0475(7) Uani 1 1 d . . . . .
H73 H 0.7530 0.6612 0.0859 0.057 Uiso 1 1 calc R U . . .
C74 C 0.75639(8) 0.53829(18) 0.05606(7) 0.0401(5) Uani 1 1 d . . . . .
H74 H 0.7646 0.5726 0.0369 0.048 Uiso 1 1 calc R U . . .
C75 C 0.75060(7) 0.43500(16) 0.05515(5) 0.0281(4) Uani 1 1 d . . . . .
H75 H 0.7547 0.3997 0.0353 0.034 Uiso 1 1 calc R U . . .
C76 C 0.7490(8) -0.2258(3) -0.0041(4) 0.037(3) Uani 0.5 1 d D . P . .
F1 F 0.61387(5) 0.36317(9) 0.20066(3) 0.0304(3) Uani 1 1 d . . . . .
F2 F 0.67278(5) 0.48510(9) 0.21363(3) 0.0337(3) Uani 1 1 d . . . . .
F3 F 0.69503(5) 0.33513(9) 0.19222(3) 0.0358(3) Uani 1 1 d . . . . .
F4 F 0.64673(5) 0.44554(11) 0.15836(3) 0.0394(3) Uani 1 1 d . . . . .
F5 F 0.60930(6) -0.12515(11) 0.07967(4) 0.0485(4) Uani 1 1 d . . . . .
F6 F 0.65120(8) 0.02196(12) 0.07887(5) 0.0721(6) Uani 1 1 d . . . . .
F7 F 0.68726(11) -0.1274(3) 0.07092(12) 0.0653(11) Uani 0.729(12) 1 d D U P A 1
F8 F 0.6314(3) -0.0617(4) 0.02943(6) 0.0854(13) Uani 0.729(12) 1 d D U P A 1
F7' F 0.6847(3) -0.1157(9) 0.0536(4) 0.103(3) Uani 0.271(12) 1 d D U P A 2
F8' F 0.6087(5) -0.0540(10) 0.0351(3) 0.093(3) Uani 0.271(12) 1 d D U P A 2
Ag1 Ag 0.69758(2) 0.17627(2) 0.13539(2) 0.02081(3) Uani 1 1 d . . . . .
Ag2 Ag 0.60895(2) 0.15683(2) 0.18044(2) 0.01590(3) Uani 1 1 d . . . . .
Ag3 Ag 0.59249(2) 0.27278(2) 0.11294(2) 0.01637(3) Uani 1 1 d . . . . .
P1 P 0.75478(2) 0.09869(3) 0.18131(2) 0.01591(8) Uani 1 1 d . . . . .
P2 P 0.66513(2) 0.05032(3) 0.21803(2) 0.01399(7) Uani 1 1 d . . . . .
P3 P 0.51747(2) 0.17230(3) 0.18052(2) 0.01426(7) Uani 1 1 d . . . . .
P4 P 0.50804(2) 0.32656(3) 0.12285(2) 0.01515(8) Uani 1 1 d . . . . .
P5 P 0.61608(2) 0.31360(3) 0.05630(2) 0.01669(8) Uani 1 1 d . . . . .
P6 P 0.72239(2) 0.24946(4) 0.08216(2) 0.01801(8) Uani 1 1 d . . . . .
B1 B 0.65727(8) 0.40795(16) 0.19119(5) 0.0228(4) Uani 1 1 d . . . . .
B2 B 0.64265(10) -0.0712(2) 0.06426(7) 0.0406(6) Uani 1 1 d D . . . .
O1 O 0.75658(14) -0.2115(3) 0.03530(11) 0.0505(9) Uani 0.5 1 d D . P . .
D1 D 0.6309(10) 0.1856(19) 0.1392(7) 0.046(7) Uiso 1 1 d . . . . .
H1 H 0.7301(13) -0.179(5) 0.0380(6) 0.08(2) Uiso 0.5 1 d D . P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
D D 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P2 C1 P1 110.42(8) . .
P4 C2 P3 111.61(9) . .
P5 C3 P6 111.85(9) . .
C5 C4 C9 119.17(19) . .
C5 C4 P1 119.10(17) . .
C9 C4 P1 121.66(14) . .
C4 C5 C6 119.5(3) . .
C7 C6 C5 121.5(3) . .
C6 C7 C8 119.7(2) . .
C7 C8 C9 120.0(2) . .
C8 C9 C4 120.2(2) . .
C15 C10 C11 119.58(16) . .
C15 C10 P1 124.77(13) . .
C11 C10 P1 115.29(13) . .
C12 C11 C10 120.12(18) . .
C11 C12 C13 120.33(19) . .
C14 C13 C12 119.71(17) . .
C13 C14 C15 120.52(18) . .
C10 C15 C14 119.73(17) . .
C17 C16 C21 118.89(16) . .
C17 C16 P2 119.65(13) . .
C21 C16 P2 121.45(13) . .
C16 C17 C18 120.71(18) . .
C19 C18 C17 119.80(19) . .
C20 C19 C18 120.04(18) . .
C19 C20 C21 120.52(18) . .
C20 C21 C16 120.04(18) . .
C23 C22 C27 119.08(16) . .
C23 C22 P2 125.77(13) . .
C27 C22 P2 115.10(13) . .
C22 C23 C24 119.52(18) . .
C25 C24 C23 120.88(19) . .
C24 C25 C26 119.89(18) . .
C25 C26 C27 119.66(18) . .
C26 C27 C22 120.96(17) . .
C29 C28 C33 118.66(16) . .
C29 C28 P3 120.20(14) . .
C33 C28 P3 121.13(13) . .
C30 C29 C28 120.54(18) . .
C31 C30 C29 120.09(18) . .
C32 C31 C30 119.93(17) . .
C31 C32 C33 120.24(19) . .
C32 C33 C28 120.50(17) . .
C39 C34 C35 119.25(16) . .
C39 C34 P3 118.10(13) . .
C35 C34 P3 122.65(14) . .
C36 C35 C34 119.82(18) . .
C35 C36 C37 120.18(18) . .
C38 C37 C36 120.63(19) . .
C37 C38 C39 119.58(19) . .
C38 C39 C34 120.54(18) . .
C45 C40 C41 119.12(17) . .
C45 C40 P4 118.96(13) . .
C41 C40 P4 121.91(14) . .
C42 C41 C40 119.65(19) . .
C43 C42 C41 120.63(19) . .
C42 C43 C44 120.39(19) . .
C43 C44 C45 119.44(19) . .
C40 C45 C44 120.76(18) . .
C51 C46 C47 118.73(17) . .
C51 C46 P4 118.81(14) . .
C47 C46 P4 122.28(15) . .
C48 C47 C46 120.1(2) . .
C49 C48 C47 120.5(2) . .
C48 C49 C50 119.9(2) . .
C49 C50 C51 120.2(2) . .
C46 C51 C50 120.51(19) . .
C53 C52 C57 119.01(18) . .
C53 C52 P5 120.65(16) . .
C57 C52 P5 120.11(16) . .
C52 C53 C54 119.7(2) . .
C55 C54 C53 120.2(2) . .
C56 C55 C54 119.9(2) . .
C55 C56 C57 120.9(2) . .
C56 C57 C52 120.2(2) . .
C59 C58 C63 119.19(17) . .
C59 C58 P5 119.05(14) . .
C63 C58 P5 121.68(15) . .
C58 C59 C60 120.22(19) . .
C61 C60 C59 120.3(2) . .
C60 C61 C62 120.0(2) . .
C61 C62 C63 120.1(2) . .
C62 C63 C58 120.18(19) . .
C65 C64 C69 118.78(17) . .
C65 C64 P6 118.15(14) . .
C69 C64 P6 123.05(14) . .
C66 C65 C64 120.34(19) . .
C67 C66 C65 120.8(2) . .
C68 C67 C66 119.46(19) . .
C67 C68 C69 120.44(18) . .
C68 C69 C64 120.16(17) . .
C71 C70 C75 119.49(19) . .
C71 C70 P6 118.37(15) . .
C75 C70 P6 121.76(15) . .
C70 C71 C72 119.6(2) . .
C73 C72 C71 120.2(2) . .
C72 C73 C74 120.4(2) . .
C75 C74 C73 119.9(2) . .
C74 C75 C70 120.4(2) . .
C76 C76 O1 171(4) 2_655 2_655
C76 C76 O1 7(3) 2_655 .
O1 C76 O1 164.2(5) 2_655 .
P1 Ag1 P6 125.504(15) . .
P1 Ag1 Ag3 147.603(11) . .
P6 Ag1 Ag3 85.653(11) . .
P1 Ag1 Ag2 90.041(11) . .
P6 Ag1 Ag2 143.949(12) . .
Ag3 Ag1 Ag2 58.308(4) . .
P2 Ag2 P3 126.535(14) . .
P2 Ag2 Ag3 146.658(11) . .
P3 Ag2 Ag3 85.124(11) . .
P2 Ag2 Ag1 86.173(11) . .
P3 Ag2 Ag1 144.536(11) . .
Ag3 Ag2 Ag1 60.688(4) . .
P5 Ag3 P4 115.017(15) . .
P5 Ag3 Ag2 151.226(12) . .
P4 Ag3 Ag2 92.868(11) . .
P5 Ag3 Ag1 91.558(11) . .
P4 Ag3 Ag1 153.392(11) . .
Ag2 Ag3 Ag1 61.004(4) . .
C4 P1 C10 99.63(8) . .
C4 P1 C1 104.03(8) . .
C10 P1 C1 105.84(8) . .
C4 P1 Ag1 117.54(6) . .
C10 P1 Ag1 113.06(6) . .
C1 P1 Ag1 114.98(5) . .
C22 P2 C16 101.99(8) . .
C22 P2 C1 106.68(8) . .
C16 P2 C1 105.46(7) . .
C22 P2 Ag2 114.95(6) . .
C16 P2 Ag2 112.31(6) . .
C1 P2 Ag2 114.31(5) . .
C34 P3 C28 103.23(8) . .
C34 P3 C2 104.70(8) . .
C28 P3 C2 101.42(8) . .
C34 P3 Ag2 106.74(6) . .
C28 P3 Ag2 125.94(6) . .
C2 P3 Ag2 112.74(6) . .
C40 P4 C46 104.33(8) . .
C40 P4 C2 104.51(8) . .
C46 P4 C2 103.04(8) . .
C40 P4 Ag3 117.18(6) . .
C46 P4 Ag3 113.56(6) . .
C2 P4 Ag3 112.78(5) . .
C58 P5 C52 102.71(9) . .
C58 P5 C3 106.61(8) . .
C52 P5 C3 103.13(8) . .
C58 P5 Ag3 118.58(6) . .
C52 P5 Ag3 111.06(6) . .
C3 P5 Ag3 113.18(6) . .
C70 P6 C64 105.23(8) . .
C70 P6 C3 101.91(8) . .
C64 P6 C3 100.52(8) . .
C70 P6 Ag1 115.78(6) . .
C64 P6 Ag1 117.85(6) . .
C3 P6 Ag1 113.34(6) . .
F2 B1 F4 110.47(17) . .
F2 B1 F3 108.84(17) . .
F4 B1 F3 110.11(16) . .
F2 B1 F1 109.90(16) . .
F4 B1 F1 108.27(17) . .
F3 B1 F1 109.23(16) . .
F5 B2 F6 112.0(2) . .
F5 B2 F8 114.7(3) . .
F6 B2 F8 110.3(3) . .
F5 B2 F7' 121.6(6) . .
F6 B2 F7' 114.0(5) . .
F5 B2 F8' 92.9(6) . .
F6 B2 F8' 105.3(6) . .
F7' B2 F8' 107.3(4) . .
F5 B2 F7 103.6(3) . .
F6 B2 F7 107.2(3) . .
F8 B2 F7 108.6(3) . .
C76 O1 C76 1.9(7) 2_655 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 P2 1.8416(16) .
C1 P1 1.8451(16) .
C2 P4 1.8403(16) .
C2 P3 1.8444(16) .
C3 P5 1.8385(17) .
C3 P6 1.8452(17) .
C4 C5 1.383(3) .
C4 C9 1.393(3) .
C4 P1 1.8212(19) .
C5 C6 1.384(4) .
C6 C7 1.360(5) .
C7 C8 1.377(4) .
C8 C9 1.388(3) .
C10 C15 1.388(2) .
C10 C11 1.399(2) .
C10 P1 1.8250(17) .
C11 C12 1.384(3) .
C12 C13 1.385(3) .
C13 C14 1.384(3) .
C14 C15 1.394(2) .
C16 C17 1.390(2) .
C16 C21 1.398(2) .
C16 P2 1.8222(17) .
C17 C18 1.392(3) .
C18 C19 1.382(3) .
C19 C20 1.380(3) .
C20 C21 1.387(3) .
C22 C23 1.389(2) .
C22 C27 1.397(2) .
C22 P2 1.8216(17) .
C23 C24 1.397(3) .
C24 C25 1.380(3) .
C25 C26 1.383(3) .
C26 C27 1.386(3) .
C28 C29 1.395(2) .
C28 C33 1.397(2) .
C28 P3 1.8265(17) .
C29 C30 1.393(3) .
C30 C31 1.384(3) .
C31 C32 1.382(3) .
C32 C33 1.390(3) .
C34 C39 1.394(2) .
C34 C35 1.401(2) .
C34 P3 1.8194(17) .
C35 C36 1.385(3) .
C36 C37 1.388(3) .
C37 C38 1.377(3) .
C38 C39 1.391(3) .
C40 C45 1.390(2) .
C40 C41 1.398(2) .
C40 P4 1.8145(18) .
C41 C42 1.386(3) .
C42 C43 1.377(3) .
C43 C44 1.380(3) .
C44 C45 1.390(3) .
C46 C51 1.388(3) .
C46 C47 1.392(3) .
C46 P4 1.8247(17) .
C47 C48 1.391(3) .
C48 C49 1.371(4) .
C49 C50 1.374(3) .
C50 C51 1.391(3) .
C52 C53 1.382(3) .
C52 C57 1.400(3) .
C52 P5 1.8241(18) .
C53 C54 1.405(3) .
C54 C55 1.381(4) .
C55 C56 1.359(4) .
C56 C57 1.384(3) .
C58 C59 1.391(3) .
C58 C63 1.402(3) .
C58 P5 1.8184(18) .
C59 C60 1.393(3) .
C60 C61 1.381(3) .
C61 C62 1.387(3) .
C62 C63 1.388(3) .
C64 C65 1.384(3) .
C64 C69 1.396(2) .
C64 P6 1.8184(18) .
C65 C66 1.384(3) .
C66 C67 1.376(3) .
C67 C68 1.376(3) .
C68 C69 1.389(2) .
C70 C71 1.390(3) .
C70 C75 1.399(3) .
C70 P6 1.8147(19) .
C71 C72 1.394(3) .
C72 C73 1.375(4) .
C73 C74 1.385(4) .
C74 C75 1.374(3) .
C76 C76 0.32(3) 2_655
C76 O1 1.242(18) 2_655
C76 O1 1.558(17) .
F1 B1 1.400(2) .
F2 B1 1.384(2) .
F3 B1 1.399(2) .
F4 B1 1.389(2) .
F5 B2 1.347(3) .
F6 B2 1.368(3) .
F7 B2 1.413(3) .
F8 B2 1.381(3) .
F7' B2 1.384(4) .
F8' B2 1.405(4) .
Ag1 P1 2.4667(5) .
Ag1 P6 2.4769(5) .
Ag1 Ag3 3.1415(2) .
Ag1 Ag2 3.1511(2) .
Ag2 P2 2.4432(4) .
Ag2 P3 2.4756(4) .
Ag2 Ag3 3.06550(18) .
Ag3 P5 2.4572(4) .
Ag3 P4 2.4596(4) .
O1 C76 1.242(18) 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C9 C4 C5 C6 0.9(4) . .
P1 C4 C5 C6 177.9(2) . .
C4 C5 C6 C7 -0.3(5) . .
C5 C6 C7 C8 -0.1(6) . .
C6 C7 C8 C9 -0.1(4) . .
C7 C8 C9 C4 0.7(3) . .
C5 C4 C9 C8 -1.1(3) . .
P1 C4 C9 C8 -178.03(15) . .
C15 C10 C11 C12 0.8(3) . .
P1 C10 C11 C12 -172.67(16) . .
C10 C11 C12 C13 -0.3(3) . .
C11 C12 C13 C14 -0.6(3) . .
C12 C13 C14 C15 1.0(3) . .
C11 C10 C15 C14 -0.4(3) . .
P1 C10 C15 C14 172.40(14) . .
C13 C14 C15 C10 -0.5(3) . .
C21 C16 C17 C18 0.2(3) . .
P2 C16 C17 C18 -178.99(16) . .
C16 C17 C18 C19 -0.2(3) . .
C17 C18 C19 C20 0.2(3) . .
C18 C19 C20 C21 -0.1(3) . .
C19 C20 C21 C16 0.1(3) . .
C17 C16 C21 C20 -0.1(3) . .
P2 C16 C21 C20 179.04(15) . .
C27 C22 C23 C24 0.2(3) . .
P2 C22 C23 C24 177.57(15) . .
C22 C23 C24 C25 -0.1(3) . .
C23 C24 C25 C26 0.1(3) . .
C24 C25 C26 C27 -0.2(3) . .
C25 C26 C27 C22 0.3(3) . .
C23 C22 C27 C26 -0.3(3) . .
P2 C22 C27 C26 -177.92(15) . .
C33 C28 C29 C30 1.5(3) . .
P3 C28 C29 C30 -178.56(15) . .
C28 C29 C30 C31 0.2(3) . .
C29 C30 C31 C32 -1.6(3) . .
C30 C31 C32 C33 1.2(3) . .
C31 C32 C33 C28 0.5(3) . .
C29 C28 C33 C32 -1.8(3) . .
P3 C28 C33 C32 178.20(15) . .
C39 C34 C35 C36 -0.3(3) . .
P3 C34 C35 C36 178.43(14) . .
C34 C35 C36 C37 -0.1(3) . .
C35 C36 C37 C38 0.4(3) . .
C36 C37 C38 C39 -0.4(3) . .
C37 C38 C39 C34 0.0(3) . .
C35 C34 C39 C38 0.3(3) . .
P3 C34 C39 C38 -178.46(15) . .
C45 C40 C41 C42 -0.1(3) . .
P4 C40 C41 C42 178.67(16) . .
C40 C41 C42 C43 0.0(3) . .
C41 C42 C43 C44 0.0(3) . .
C42 C43 C44 C45 0.1(3) . .
C41 C40 C45 C44 0.2(3) . .
P4 C40 C45 C44 -178.64(14) . .
C43 C44 C45 C40 -0.1(3) . .
C51 C46 C47 C48 -1.6(3) . .
P4 C46 C47 C48 -176.51(17) . .
C46 C47 C48 C49 1.0(4) . .
C47 C48 C49 C50 0.1(4) . .
C48 C49 C50 C51 -0.6(4) . .
C47 C46 C51 C50 1.1(3) . .
P4 C46 C51 C50 176.21(17) . .
C49 C50 C51 C46 0.0(3) . .
C57 C52 C53 C54 2.2(3) . .
P5 C52 C53 C54 176.68(15) . .
C52 C53 C54 C55 -1.4(3) . .
C53 C54 C55 C56 -0.5(3) . .
C54 C55 C56 C57 1.4(4) . .
C55 C56 C57 C52 -0.5(3) . .
C53 C52 C57 C56 -1.3(3) . .
P5 C52 C57 C56 -175.82(17) . .
C63 C58 C59 C60 -0.1(3) . .
P5 C58 C59 C60 -176.90(15) . .
C58 C59 C60 C61 0.9(3) . .
C59 C60 C61 C62 -0.6(3) . .
C60 C61 C62 C63 -0.5(3) . .
C61 C62 C63 C58 1.3(3) . .
C59 C58 C63 C62 -1.0(3) . .
P5 C58 C63 C62 175.74(15) . .
C69 C64 C65 C66 -1.7(3) . .
P6 C64 C65 C66 179.9(2) . .
C64 C65 C66 C67 0.5(4) . .
C65 C66 C67 C68 0.5(4) . .
C66 C67 C68 C69 -0.2(3) . .
C67 C68 C69 C64 -1.1(3) . .
C65 C64 C69 C68 2.0(3) . .
P6 C64 C69 C68 -179.68(14) . .
C75 C70 C71 C72 1.8(3) . .
P6 C70 C71 C72 -171.30(16) . .
C70 C71 C72 C73 -0.5(3) . .
C71 C72 C73 C74 -1.3(4) . .
C72 C73 C74 C75 1.8(4) . .
C73 C74 C75 C70 -0.5(3) . .
C71 C70 C75 C74 -1.3(3) . .
P6 C70 C75 C74 171.55(16) . .
C5 C4 P1 C10 -121.42(18) . .
C9 C4 P1 C10 55.51(16) . .
C5 C4 P1 C1 129.44(18) . .
C9 C4 P1 C1 -53.62(16) . .
C5 C4 P1 Ag1 1.0(2) . .
C9 C4 P1 Ag1 177.96(13) . .
C15 C10 P1 C4 -96.71(16) . .
C11 C10 P1 C4 76.33(15) . .
C15 C10 P1 C1 10.98(17) . .
C11 C10 P1 C1 -175.98(14) . .
C15 C10 P1 Ag1 137.70(14) . .
C11 C10 P1 Ag1 -49.26(15) . .
P2 C1 P1 C4 -86.08(10) . .
P2 C1 P1 C10 169.43(8) . .
P2 C1 P1 Ag1 43.88(10) . .
C23 C22 P2 C16 107.79(16) . .
C27 C22 P2 C16 -74.72(14) . .
C23 C22 P2 C1 -2.58(18) . .
C27 C22 P2 C1 174.91(13) . .
C23 C22 P2 Ag2 -130.41(15) . .
C27 C22 P2 Ag2 47.07(14) . .
C17 C16 P2 C22 136.97(15) . .
C21 C16 P2 C22 -42.20(16) . .
C17 C16 P2 C1 -111.73(15) . .
C21 C16 P2 C1 69.10(16) . .
C17 C16 P2 Ag2 13.38(16) . .
C21 C16 P2 Ag2 -165.79(13) . .
P1 C1 P2 C22 174.05(8) . .
P1 C1 P2 C16 66.12(10) . .
P1 C1 P2 Ag2 -57.74(9) . .
C39 C34 P3 C28 -136.77(14) . .
C35 C34 P3 C28 44.51(16) . .
C39 C34 P3 C2 117.44(14) . .
C35 C34 P3 C2 -61.28(16) . .
C39 C34 P3 Ag2 -2.31(15) . .
C35 C34 P3 Ag2 178.97(13) . .
C29 C28 P3 C34 35.49(16) . .
C33 C28 P3 C34 -144.55(15) . .
C29 C28 P3 C2 143.76(15) . .
C33 C28 P3 C2 -36.28(16) . .
C29 C28 P3 Ag2 -86.92(15) . .
C33 C28 P3 Ag2 93.04(15) . .
P4 C2 P3 C34 -56.81(11) . .
P4 C2 P3 C28 -163.94(9) . .
P4 C2 P3 Ag2 58.83(10) . .
C45 C40 P4 C46 122.57(14) . .
C41 C40 P4 C46 -56.19(17) . .
C45 C40 P4 C2 -129.57(14) . .
C41 C40 P4 C2 51.67(17) . .
C45 C40 P4 Ag3 -3.94(16) . .
C41 C40 P4 Ag3 177.30(13) . .
C51 C46 P4 C40 168.04(15) . .
C47 C46 P4 C40 -17.05(18) . .
C51 C46 P4 C2 59.10(16) . .
C47 C46 P4 C2 -125.98(16) . .
C51 C46 P4 Ag3 -63.22(16) . .
C47 C46 P4 Ag3 111.69(15) . .
P3 C2 P4 C40 87.71(10) . .
P3 C2 P4 C46 -163.48(9) . .
P3 C2 P4 Ag3 -40.64(10) . .
C59 C58 P5 C52 125.47(15) . .
C63 C58 P5 C52 -51.29(16) . .
C59 C58 P5 C3 -126.46(15) . .
C63 C58 P5 C3 56.78(16) . .
C59 C58 P5 Ag3 2.62(17) . .
C63 C58 P5 Ag3 -174.14(13) . .
C53 C52 P5 C58 158.83(15) . .
C57 C52 P5 C58 -26.78(17) . .
C53 C52 P5 C3 48.12(17) . .
C57 C52 P5 C3 -137.48(16) . .
C53 C52 P5 Ag3 -73.41(16) . .
C57 C52 P5 Ag3 100.98(15) . .
P6 C3 P5 C58 86.50(11) . .
P6 C3 P5 C52 -165.72(9) . .
P6 C3 P5 Ag3 -45.63(10) . .
C71 C70 P6 C64 -135.47(15) . .
C75 C70 P6 C64 51.61(17) . .
C71 C70 P6 C3 120.00(15) . .
C75 C70 P6 C3 -52.92(17) . .
C71 C70 P6 Ag1 -3.47(16) . .
C75 C70 P6 Ag1 -176.39(13) . .
C65 C64 P6 C70 -163.56(17) . .
C69 C64 P6 C70 18.08(17) . .
C65 C64 P6 C3 -58.01(18) . .
C69 C64 P6 C3 123.64(16) . .
C65 C64 P6 Ag1 65.62(18) . .
C69 C64 P6 Ag1 -112.73(14) . .
P5 C3 P6 C70 -66.85(11) . .
P5 C3 P6 C64 -175.04(9) . .
P5 C3 P6 Ag1 58.26(10) . .
O1 C76 O1 C76 -158(61) 2_655 2_655
