#------------------------------------------------------------------------------
#$Date: 2016-03-23 23:33:09 +0200 (Wed, 23 Mar 2016) $
#$Revision: 179506 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/03/4340363.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4340363
loop_
_publ_author_name
'Joarder, Biplab'
'Mukherjee, Soumya'
'Xue, Shufang'
'Tang, Jinkui'
'Ghosh, Sujit K.'
_publ_section_title
;
 Structures and magnetic properties of two analogous dy6 wheels with
 electron-donation and -withdrawal effects.
;
_journal_issue                   14
_journal_name_full               'Inorganic chemistry'
_journal_page_first              7554
_journal_page_last               7560
_journal_paper_doi               10.1021/ic500875m
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         'C86 H134 Dy6 O38'
_chemical_formula_sum            'C86 H134 Dy6 O38'
_chemical_formula_weight         2750.93
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                99.709(3)
_cell_angle_beta                 105.197(2)
_cell_angle_gamma                112.518(2)
_cell_formula_units_Z            2
_cell_length_a                   16.873(2)
_cell_length_b                   17.570(2)
_cell_length_c                   22.008(3)
_cell_measurement_temperature    200(2)
_cell_volume                     5545.1(12)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      200(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0379
_diffrn_reflns_av_sigmaI/netI    0.0429
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            88813
_diffrn_reflns_theta_full        28.46
_diffrn_reflns_theta_max         28.46
_diffrn_reflns_theta_min         1.81
_exptl_absorpt_coefficient_mu    4.065
_exptl_crystal_density_diffrn    1.648
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2700
_refine_diff_density_max         8.011
_refine_diff_density_min         -1.182
_refine_diff_density_rms         0.239
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.308
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1171
_refine_ls_number_reflns         27841
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.309
_refine_ls_R_factor_all          0.0543
_refine_ls_R_factor_gt           0.0439
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0876P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1674
_refine_ls_wR_factor_ref         0.1760
_reflns_number_gt                23377
_reflns_number_total             27841
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500875m_si_002.cif
_cod_data_source_block           Compound1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4340363--4340364.cif.
;
_cod_original_cell_volume        5545.0(13)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4340363
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.2653(5) 0.0797(5) 0.2629(4) 0.0252(15) Uani 1 1 d .
H1A H 0.3242 0.1162 0.2621 0.038 Uiso 1 1 calc R
H1B H 0.2229 0.1026 0.2480 0.038 Uiso 1 1 calc R
H1C H 0.2429 0.0225 0.2342 0.038 Uiso 1 1 calc R
C2 C 0.1964(4) 0.0276(4) 0.3399(3) 0.0180(13) Uani 1 1 d .
C3 C 0.1059(5) -0.0033(4) 0.2955(4) 0.0221(14) Uani 1 1 d .
H3 H 0.0951 0.0049 0.2539 0.026 Uiso 1 1 calc R
C4 C 0.0334(5) -0.0461(4) 0.3149(4) 0.0254(15) Uani 1 1 d .
H4 H -0.0266 -0.0664 0.2859 0.030 Uiso 1 1 calc R
C5 C 0.0477(5) -0.0594(4) 0.3758(4) 0.0274(17) Uani 1 1 d .
H5 H -0.0023 -0.0889 0.3873 0.033 Uiso 1 1 calc R
C32A C 0.4719(4) 0.1110(4) 0.7091(3) 0.0176(13) Uani 1 1 d .
C6 C 0.1377(4) -0.0285(4) 0.4209(4) 0.0193(13) Uani 1 1 d .
C7 C 0.2139(4) 0.0142(4) 0.4012(3) 0.0145(12) Uani 1 1 d .
C8 C 0.0878(6) -0.0836(6) 0.5011(5) 0.042(2) Uani 1 1 d .
H8A H 0.1112 -0.0837 0.5458 0.063 Uiso 1 1 calc R
H8B H 0.0568 -0.1419 0.4722 0.063 Uiso 1 1 calc R
H8C H 0.0455 -0.0591 0.4974 0.063 Uiso 1 1 calc R
C66A C -0.0118(8) 0.8585(6) 0.8618(6) 0.049(3) Uani 1 1 d .
C9 C 0.4626(5) 0.2897(5) 0.3324(4) 0.0256(16) Uani 1 1 d .
C10 C 0.4269(5) 0.3584(5) 0.3339(4) 0.0239(15) Uani 1 1 d .
C11 C 0.4714(6) 0.4259(6) 0.3038(5) 0.044(2) Uani 1 1 d .
H11A H 0.5366 0.4547 0.3273 0.066 Uiso 1 1 calc R
H11B H 0.4472 0.4672 0.3064 0.066 Uiso 1 1 calc R
H11C H 0.4587 0.3988 0.2583 0.066 Uiso 1 1 calc R
C12 C 0.3232(5) 0.3107(5) 0.2973(4) 0.0321(18) Uani 1 1 d .
H12A H 0.2963 0.2675 0.3170 0.048 Uiso 1 1 calc R
H12B H 0.3102 0.2837 0.2518 0.048 Uiso 1 1 calc R
H12C H 0.2977 0.3511 0.3001 0.048 Uiso 1 1 calc R
C13 C 0.4463(6) 0.4021(5) 0.4080(4) 0.038(2) Uani 1 1 d .
H13A H 0.4174 0.3587 0.4270 0.057 Uiso 1 1 calc R
H13B H 0.4220 0.4433 0.4104 0.057 Uiso 1 1 calc R
H13C H 0.5114 0.4310 0.4321 0.057 Uiso 1 1 calc R
C14 C 0.2770(4) 0.2014(4) 0.4905(4) 0.0183(13) Uani 1 1 d .
C15 C 0.2073(5) 0.2387(4) 0.4792(4) 0.0216(14) Uani 1 1 d .
C16 C 0.1563(7) 0.2151(7) 0.4058(4) 0.049(3) Uani 1 1 d .
H16A H 0.1995 0.2386 0.3848 0.073 Uiso 1 1 calc R
H16B H 0.1129 0.2384 0.3987 0.073 Uiso 1 1 calc R
H16C H 0.1245 0.1534 0.3872 0.073 Uiso 1 1 calc R
C17 C 0.1385(7) 0.2030(7) 0.5121(6) 0.056(3) Uani 1 1 d .
H17A H 0.1704 0.2179 0.5587 0.083 Uiso 1 1 calc R
H17B H 0.1056 0.1413 0.4937 0.083 Uiso 1 1 calc R
H17C H 0.0959 0.2273 0.5048 0.083 Uiso 1 1 calc R
C18 C 0.2608(7) 0.3358(6) 0.5121(7) 0.062(3) Uani 1 1 d .
H18A H 0.3042 0.3603 0.4916 0.093 Uiso 1 1 calc R
H18B H 0.2930 0.3474 0.5582 0.093 Uiso 1 1 calc R
H18C H 0.2190 0.3611 0.5074 0.093 Uiso 1 1 calc R
C19 C 0.5264(5) 0.3563(4) 0.5579(4) 0.0231(14) Uani 1 1 d .
H19A H 0.4653 0.3278 0.5580 0.035 Uiso 1 1 calc R
H19B H 0.5385 0.4130 0.5542 0.035 Uiso 1 1 calc R
H19C H 0.5699 0.3610 0.5982 0.035 Uiso 1 1 calc R
C20 C 0.6181(4) 0.3396(4) 0.4953(3) 0.0170(13) Uani 1 1 d .
C21 C 0.6809(5) 0.4265(4) 0.5163(3) 0.0206(14) Uani 1 1 d .
H21 H 0.6681 0.4686 0.5372 0.025 Uiso 1 1 calc R
C22 C 0.3634(4) -0.2756(4) 0.5370(3) 0.0156(12) Uani 1 1 d .
C23 C 0.2789(5) -0.3018(4) 0.5457(3) 0.0197(13) Uani 1 1 d .
C24 C 0.2172(5) -0.3884(4) 0.5261(3) 0.0213(14) Uani 1 1 d .
H24 H 0.1625 -0.4053 0.5341 0.026 Uiso 1 1 calc R
C25 C 0.2370(5) -0.4492(4) 0.4948(4) 0.0240(15) Uani 1 1 d .
H25 H 0.1944 -0.5072 0.4806 0.029 Uiso 1 1 calc R
C26 C 0.1748(6) -0.2533(6) 0.5697(7) 0.062(4) Uani 1 1 d .
H26A H 0.1730 -0.2024 0.5920 0.094 Uiso 1 1 calc R
H26B H 0.1522 -0.2982 0.5892 0.094 Uiso 1 1 calc R
H26C H 0.1371 -0.2723 0.5239 0.094 Uiso 1 1 calc R
C27 C 0.3957(6) 0.2736(5) 0.6757(4) 0.0317(18) Uani 1 1 d .
H27A H 0.3639 0.2773 0.6340 0.048 Uiso 1 1 calc R
H27B H 0.4529 0.3250 0.6977 0.048 Uiso 1 1 calc R
H27C H 0.3585 0.2680 0.7026 0.048 Uiso 1 1 calc R
C28 C 0.4599(5) 0.1861(4) 0.7223(3) 0.0204(14) Uani 1 1 d .
C29 C 0.4931(5) 0.2410(5) 0.7860(4) 0.0270(16) Uani 1 1 d .
H29 H 0.4852 0.2909 0.7933 0.032 Uiso 1 1 calc R
C30 C 0.5372(5) 0.2214(5) 0.8378(4) 0.0297(17) Uani 1 1 d .
H30 H 0.5609 0.2589 0.8804 0.036 Uiso 1 1 calc R
C31 C 0.5467(5) 0.1463(5) 0.8272(4) 0.0282(16) Uani 1 1 d .
H31 H 0.5754 0.1327 0.8630 0.034 Uiso 1 1 calc R
C32 C 0.5141(4) 0.0913(4) 0.7644(3) 0.0199(13) Uani 1 1 d .
C33 C 0.5679(6) -0.0063(6) 0.7987(4) 0.0345(19) Uani 1 1 d .
H33A H 0.5635 -0.0625 0.7822 0.052 Uiso 1 1 calc R
H33B H 0.5461 -0.0050 0.8348 0.052 Uiso 1 1 calc R
H33C H 0.6308 0.0364 0.8135 0.052 Uiso 1 1 calc R
C34 C 0.2667(4) -0.0227(5) 0.6692(4) 0.0209(14) Uani 1 1 d .
C35 C 0.2221(5) -0.0138(5) 0.7200(4) 0.0293(17) Uani 1 1 d .
C36 C 0.2137(7) 0.0703(7) 0.7278(5) 0.043(2) Uani 1 1 d .
H36A H 0.1856 0.0763 0.7599 0.065 Uiso 1 1 calc R
H36B H 0.1765 0.0695 0.6862 0.065 Uiso 1 1 calc R
H36C H 0.2737 0.1181 0.7424 0.065 Uiso 1 1 calc R
C37 C 0.1293(7) -0.0901(8) 0.6955(5) 0.059(3) Uani 1 1 d U
H37A H 0.0996 -0.0862 0.7269 0.088 Uiso 1 1 calc R
H37B H 0.1361 -0.1423 0.6903 0.088 Uiso 1 1 calc R
H37C H 0.0926 -0.0906 0.6538 0.088 Uiso 1 1 calc R
C38 C 0.2836(6) -0.0105(7) 0.7882(4) 0.042(2) Uani 1 1 d .
H38A H 0.2551 -0.0051 0.8201 0.063 Uiso 1 1 calc R
H38B H 0.3429 0.0383 0.8025 0.063 Uiso 1 1 calc R
H38C H 0.2905 -0.0627 0.7838 0.063 Uiso 1 1 calc R
C39 C 0.3545(7) -0.2124(7) 0.7280(5) 0.049(3) Uani 1 1 d .
H39A H 0.3711 -0.2483 0.7519 0.073 Uiso 1 1 calc R
H39B H 0.2938 -0.2460 0.6953 0.073 Uiso 1 1 calc R
H39C H 0.3554 -0.1654 0.7581 0.073 Uiso 1 1 calc R
C40 C 0.6329(5) 0.0404(4) 0.6666(4) 0.0222(14) Uani 1 1 d .
H40A H 0.6891 0.0442 0.6618 0.033 Uiso 1 1 calc R
H40B H 0.6405 0.0524 0.7125 0.033 Uiso 1 1 calc R
H40C H 0.6177 0.0817 0.6493 0.033 Uiso 1 1 calc R
C41 C 0.2820(5) -0.1310(5) 0.4752(4) 0.0252(15) Uani 1 1 d .
H41A H 0.2559 -0.1073 0.4438 0.038 Uiso 1 1 calc R
H41B H 0.2336 -0.1771 0.4809 0.038 Uiso 1 1 calc R
H41C H 0.3194 -0.1528 0.4593 0.038 Uiso 1 1 calc R
C42 C 0.5509(5) 0.1801(5) 0.5820(4) 0.0264(16) Uani 1 1 d .
H42A H 0.5935 0.2106 0.5628 0.040 Uiso 1 1 calc R
H42B H 0.5648 0.1357 0.5947 0.040 Uiso 1 1 calc R
H42C H 0.5559 0.2198 0.6203 0.040 Uiso 1 1 calc R
C43 C 0.3739(5) 0.6033(5) 0.9321(4) 0.0262(16) Uani 1 1 d .
H43A H 0.3425 0.6074 0.8905 0.039 Uiso 1 1 calc R
H43B H 0.4227 0.5894 0.9287 0.039 Uiso 1 1 calc R
H43C H 0.3991 0.6575 0.9656 0.039 Uiso 1 1 calc R
C44 C 0.3451(4) 0.5225(4) 1.0083(3) 0.0150(12) Uani 1 1 d .
C45 C 0.4382(5) 0.5516(5) 1.0433(4) 0.0240(15) Uani 1 1 d .
H45 H 0.4826 0.5848 1.0284 0.029 Uiso 1 1 calc R
C46 C -0.2783(4) 0.5274(4) 0.9689(3) 0.0162(13) Uani 1 1 d .
C47 C -0.3069(5) 0.5503(5) 0.9133(4) 0.0207(14) Uani 1 1 d .
C48 C -0.3989(5) 0.5212(5) 0.8777(4) 0.0244(15) Uani 1 1 d .
H48 H -0.4169 0.5362 0.8397 0.029 Uiso 1 1 calc R
C49 C -0.4634(5) 0.4700(5) 0.8992(4) 0.0272(16) Uani 1 1 d .
H49 H -0.5254 0.4492 0.8746 0.033 Uiso 1 1 calc R
C50 C -0.2601(6) 0.6247(6) 0.8385(4) 0.039(2) Uani 1 1 d .
H50A H -0.2056 0.6637 0.8335 0.058 Uiso 1 1 calc R
H50B H -0.3005 0.6510 0.8388 0.058 Uiso 1 1 calc R
H50C H -0.2906 0.5722 0.8023 0.058 Uiso 1 1 calc R
C51 C 0.2117(5) 0.5101(5) 0.7649(4) 0.0284(16) Uani 1 1 d .
C52 C 0.1782(7) 0.3702(7) 0.6945(6) 0.053(3) Uani 1 1 d .
H52A H 0.1229 0.3673 0.6655 0.080 Uiso 1 1 calc R
H52B H 0.1657 0.3468 0.7292 0.080 Uiso 1 1 calc R
H52C H 0.2001 0.3374 0.6700 0.080 Uiso 1 1 calc R
C53 C 0.3380(7) 0.4683(7) 0.7695(5) 0.045(2) Uani 1 1 d .
H53A H 0.3252 0.4417 0.8027 0.068 Uiso 1 1 calc R
H53B H 0.3825 0.5278 0.7902 0.068 Uiso 1 1 calc R
H53C H 0.3620 0.4387 0.7444 0.068 Uiso 1 1 calc R
C54 C 0.2699(7) 0.5055(8) 0.6707(5) 0.049(3) Uani 1 1 d .
H54A H 0.2139 0.5017 0.6419 0.074 Uiso 1 1 calc R
H54B H 0.2939 0.4760 0.6454 0.074 Uiso 1 1 calc R
H54C H 0.3140 0.5651 0.6911 0.074 Uiso 1 1 calc R
C55 C 0.2505(6) 0.4633(6) 0.7240(4) 0.0341(18) Uani 1 1 d .
C56 C -0.0436(5) 0.3586(4) 0.7376(3) 0.0218(14) Uani 1 1 d .
C57 C -0.1067(5) 0.3103(5) 0.6741(4) 0.0323(18) Uani 1 1 d .
H57 H -0.1109 0.2572 0.6540 0.039 Uiso 1 1 calc R
C58 C -0.1631(5) 0.3413(5) 0.6408(4) 0.0334(18) Uani 1 1 d .
H58 H -0.2055 0.3085 0.5985 0.040 Uiso 1 1 calc R
C58A C -0.0356(4) 0.4413(4) 0.7680(3) 0.0186(13) Uani 1 1 d .
C59 C -0.1573(5) 0.4204(5) 0.6695(3) 0.0287(16) Uani 1 1 d .
H59 H -0.1966 0.4401 0.6471 0.034 Uiso 1 1 calc R
C60 C -0.0925(4) 0.4703(4) 0.7321(3) 0.0172(13) Uani 1 1 d .
C61 C -0.1354(6) 0.5835(6) 0.7284(4) 0.0364(19) Uani 1 1 d .
H61A H -0.1213 0.6397 0.7547 0.055 Uiso 1 1 calc R
H61B H -0.1990 0.5451 0.7178 0.055 Uiso 1 1 calc R
H61C H -0.1237 0.5876 0.6884 0.055 Uiso 1 1 calc R
C62 C 0.0042(6) 0.2493(5) 0.7511(4) 0.0357(19) Uani 1 1 d .
H62A H 0.0492 0.2397 0.7815 0.054 Uiso 1 1 calc R
H62B H 0.0116 0.2420 0.7091 0.054 Uiso 1 1 calc R
H62C H -0.0563 0.2085 0.7461 0.054 Uiso 1 1 calc R
C63 C 0.2211(5) 0.6377(4) 1.0042(3) 0.0204(14) Uani 1 1 d .
H63A H 0.2573 0.6095 1.0202 0.031 Uiso 1 1 calc R
H63B H 0.1898 0.6456 1.0336 0.031 Uiso 1 1 calc R
H63C H 0.2604 0.6930 1.0022 0.031 Uiso 1 1 calc R
C64 C 0.1227(7) 0.7083(6) 0.7629(5) 0.044(2) Uani 1 1 d .
H64A H 0.1542 0.7029 0.7331 0.067 Uiso 1 1 calc R
H64B H 0.1541 0.7661 0.7925 0.067 Uiso 1 1 calc R
H64C H 0.0608 0.6961 0.7381 0.067 Uiso 1 1 calc R
C65 C -0.0212(5) 0.7769(4) 0.8822(4) 0.0213(14) Uani 1 1 d .
C66 C 0.0883(7) 0.9153(6) 0.8772(6) 0.062(3) Uani 1 1 d .
H66A H 0.1148 0.8819 0.8589 0.093 Uiso 1 1 calc R
H66B H 0.1196 0.9387 0.9242 0.093 Uiso 1 1 calc R
H66C H 0.0945 0.9617 0.8582 0.093 Uiso 1 1 calc R
C67 C -0.0571(7) 0.8286(7) 0.7851(6) 0.057(3) Uani 1 1 d .
H67A H -0.1217 0.7921 0.7720 0.086 Uiso 1 1 calc R
H67B H -0.0293 0.7972 0.7661 0.086 Uiso 1 1 calc R
H67C H -0.0481 0.8783 0.7698 0.086 Uiso 1 1 calc R
C68 C -0.0637(10) 0.8968(9) 0.8892(8) 0.081(4) Uani 1 1 d U
H68A H -0.1262 0.8540 0.8761 0.122 Uiso 1 1 calc R
H68B H -0.0625 0.9444 0.8727 0.122 Uiso 1 1 calc R
H68C H -0.0361 0.9171 0.9365 0.122 Uiso 1 1 calc R
C69 C 0.0441(7) 0.8702(6) 1.1224(5) 0.052(3) Uani 1 1 d .
H69A H -0.0132 0.8387 1.1275 0.078 Uiso 1 1 calc R
H69B H 0.0483 0.9243 1.1164 0.078 Uiso 1 1 calc R
H69C H 0.0940 0.8808 1.1612 0.078 Uiso 1 1 calc R
C70 C 0.1276(5) 0.8561(4) 1.0510(4) 0.0217(14) Uani 1 1 d .
C71 C 0.1911(5) 0.9419(5) 1.0760(4) 0.0292(17) Uani 1 1 d .
H71 H 0.1844 0.9804 1.1065 0.035 Uiso 1 1 calc R
C72 C 0.2661(6) 0.9704(5) 1.0549(4) 0.0357(19) Uani 1 1 d .
H72 H 0.3099 1.0280 1.0717 0.043 Uiso 1 1 calc R
C73 C 0.2748(5) 0.9135(5) 1.0097(4) 0.0312(18) Uani 1 1 d .
H73 H 0.3251 0.9326 0.9963 0.037 Uiso 1 1 calc R
C74 C 0.2096(5) 0.8277(4) 0.9835(4) 0.0217(14) Uani 1 1 d .
C75 C 0.2895(5) 0.7868(6) 0.9191(5) 0.039(2) Uani 1 1 d .
H75A H 0.2797 0.7400 0.8838 0.058 Uiso 1 1 calc R
H75B H 0.3388 0.7956 0.9576 0.058 Uiso 1 1 calc R
H75C H 0.3050 0.8385 0.9061 0.058 Uiso 1 1 calc R
C76 C -0.1900(5) 0.7077(4) 1.0802(4) 0.0210(14) Uani 1 1 d .
C77 C -0.2047(6) 0.8440(5) 1.0993(4) 0.0306(17) Uani 1 1 d .
H77A H -0.2455 0.8690 1.1028 0.046 Uiso 1 1 calc R
H77B H -0.1837 0.8560 1.0639 0.046 Uiso 1 1 calc R
H77C H -0.1529 0.8683 1.1400 0.046 Uiso 1 1 calc R
C78 C -0.2559(5) 0.7458(5) 1.0854(4) 0.0289(17) Uani 1 1 d .
C79 C -0.2951(6) 0.7241(5) 1.1393(5) 0.041(2) Uani 1 1 d .
H79A H -0.3361 0.7493 1.1413 0.061 Uiso 1 1 calc R
H79B H -0.2457 0.7469 1.1811 0.061 Uiso 1 1 calc R
H79C H -0.3279 0.6625 1.1290 0.061 Uiso 1 1 calc R
C80 C -0.3365(6) 0.7058(6) 1.0178(5) 0.044(2) Uani 1 1 d .
H80A H -0.3793 0.7289 1.0196 0.065 Uiso 1 1 calc R
H80B H -0.3670 0.6442 1.0084 0.065 Uiso 1 1 calc R
H80C H -0.3130 0.7197 0.9838 0.065 Uiso 1 1 calc R
C81 C -0.1405(7) 0.4867(6) 0.8818(5) 0.050(3) Uani 1 1 d .
H81A H -0.1856 0.4792 0.9023 0.075 Uiso 1 1 calc R
H81B H -0.1158 0.4464 0.8883 0.075 Uiso 1 1 calc R
H81C H -0.1688 0.4765 0.8353 0.075 Uiso 1 1 calc R
C82 C 0.1360(4) 0.7966(4) 1.0053(3) 0.0179(13) Uani 1 1 d .
C83 C 0.0778(5) 0.6793(6) 1.1218(5) 0.037(2) Uani 1 1 d .
H83A H 0.0872 0.6580 1.1591 0.056 Uiso 1 1 calc R
H83B H 0.0989 0.7406 1.1369 0.056 Uiso 1 1 calc R
H83C H 0.1116 0.6670 1.0958 0.056 Uiso 1 1 calc R
O38 O 0.1209(3) 0.6487(3) 0.7998(3) 0.0226(10) Uani 1 1 d .
O1 O 0.2744(3) 0.0766(3) 0.3291(2) 0.0173(9) Uani 1 1 d .
O2 O 0.2999(3) 0.0421(3) 0.4427(2) 0.0139(9) Uani 1 1 d .
O3 O 0.1625(3) -0.0333(3) 0.4831(3) 0.0225(10) Uani 1 1 d .
O4 O 0.4364(3) 0.2356(3) 0.3618(2) 0.0214(10) Uani 1 1 d .
O5 O 0.5097(5) 0.2872(4) 0.2976(4) 0.0455(17) Uani 1 1 d .
O6 O 0.3296(3) 0.2152(3) 0.4583(2) 0.0197(10) Uani 1 1 d .
O7 O 0.2797(3) 0.1615(3) 0.5334(2) 0.0205(10) Uani 1 1 d .
O8 O 0.2658(3) -0.2343(3) 0.5755(3) 0.0228(11) Uani 1 1 d .
O9 O 0.5136(3) 0.0118(3) 0.7477(2) 0.0229(10) Uani 1 1 d .
O10 O 0.4441(3) 0.0605(3) 0.6476(2) 0.0157(9) Uani 1 1 d .
O11 O 0.4135(3) 0.1989(3) 0.6648(2) 0.0207(10) Uani 1 1 d .
O12 O 0.5346(3) 0.3075(3) 0.5032(2) 0.0167(9) Uani 1 1 d .
O13 O 0.3365(3) -0.0660(3) 0.5360(2) 0.0168(9) Uani 1 1 d .
O14 O 0.2592(3) 0.0167(3) 0.6270(2) 0.0213(10) Uani 1 1 d .
O15 O 0.3054(3) -0.0715(3) 0.6707(3) 0.0228(10) Uani 1 1 d .
O16 O 0.4201(4) -0.1781(3) 0.6957(3) 0.0277(12) Uani 1 1 d .
O17 O 0.5598(3) -0.0457(3) 0.6307(2) 0.0163(9) Uani 1 1 d .
O18 O 0.4245(3) -0.1926(3) 0.5579(2) 0.0150(9) Uani 1 1 d .
O19 O 0.4610(3) 0.1426(3) 0.5356(2) 0.0145(9) Uani 1 1 d .
O20 O 0.3099(3) 0.5362(3) 0.9493(2) 0.0190(10) Uani 1 1 d .
O21 O 0.1785(3) 0.3389(3) 0.8836(2) 0.0215(10) Uani 1 1 d .
O22 O 0.0163(3) 0.3357(3) 0.7762(2) 0.0228(10) Uani 1 1 d .
O23 O 0.0241(3) 0.4865(3) 0.8286(2) 0.0157(9) Uani 1 1 d .
O24 O -0.0789(3) 0.5507(3) 0.7648(2) 0.0187(10) Uani 1 1 d .
O25 O 0.1961(4) 0.4845(3) 0.8129(3) 0.0265(11) Uani 1 1 d .
O26 O 0.2013(5) 0.5714(5) 0.7507(3) 0.0475(18) Uani 1 1 d .
O27 O 0.1555(3) 0.5860(3) 0.9401(2) 0.0154(9) Uani 1 1 d .
O28 O 0.2075(3) 0.7664(3) 0.9339(3) 0.0223(10) Uani 1 1 d .
O29 O 0.0749(3) 0.7133(3) 0.9827(2) 0.0150(9) Uani 1 1 d .
O30 O 0.0490(3) 0.8205(3) 1.0658(3) 0.0247(11) Uani 1 1 d .
O31 O -0.1492(3) 0.7264(3) 1.0405(3) 0.0214(10) Uani 1 1 d .
O32 O -0.2356(3) 0.6057(3) 0.8988(3) 0.0268(12) Uani 1 1 d .
O33 O -0.1880(3) 0.5520(3) 1.0018(2) 0.0143(9) Uani 1 1 d .
O34 O 0.0111(3) 0.7313(3) 0.8559(3) 0.0224(10) Uani 1 1 d .
O35 O -0.0623(3) 0.7582(3) 0.9209(3) 0.0219(10) Uani 1 1 d .
O36 O -0.0174(3) 0.6384(3) 1.0825(2) 0.0183(9) Uani 1 1 d .
O37 O -0.0703(3) 0.5702(3) 0.9098(2) 0.0149(9) Uani 1 1 d .
Dy1 Dy 0.422068(19) 0.152459(17) 0.431202(15) 0.01214(8) Uani 1 1 d .
Dy2 Dy 0.336906(19) 0.064339(18) 0.557002(15) 0.01341(8) Uani 1 1 d .
Dy3 Dy 0.41408(2) -0.085040(18) 0.627583(15) 0.01457(8) Uani 1 1 d .
Dy4 Dy 0.13257(2) 0.450162(18) 0.890088(15) 0.01378(8) Uani 1 1 d .
Dy5 Dy 0.054245(19) 0.625818(17) 0.882195(14) 0.01259(8) Uani 1 1 d .
Dy6 Dy -0.072999(19) 0.667596(18) 0.988916(15) 0.01369(8) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 H1A 109.5 . .
O1 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
O1 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
O1 C2 C7 113.7(6) . .
O1 C2 C3 124.6(6) . .
C7 C2 C3 121.5(6) . .
C4 C3 C2 118.6(7) . .
C4 C3 H3 120.7 . .
C2 C3 H3 120.7 . .
C5 C4 C3 121.7(6) . .
C5 C4 H4 119.1 . .
C3 C4 H4 119.1 . .
C4 C5 C6 120.3(7) . .
C4 C5 H5 119.8 . .
C6 C5 H5 119.8 . .
O10 C32A C28 122.1(6) . .
O10 C32A C32 121.6(6) . .
C28 C32A C32 116.3(6) . .
O3 C6 C5 127.0(6) . .
O3 C6 C7 114.1(6) . .
C5 C6 C7 118.9(7) . .
O2 C7 C2 121.3(6) . .
O2 C7 C6 119.9(6) . .
C2 C7 C6 118.8(6) . .
O3 C8 H8A 109.5 . .
O3 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
O3 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
C68 C66A C66 117.7(10) . .
C68 C66A C65 110.0(8) . .
C66 C66A C65 108.6(7) . .
C68 C66A C67 107.8(10) . .
C66 C66A C67 105.4(8) . .
C65 C66A C67 106.7(8) . .
O5 C9 O4 123.7(7) . .
O5 C9 C10 118.2(6) . .
O4 C9 C10 117.8(7) . .
C11 C10 C12 110.9(6) . .
C11 C10 C9 112.9(7) . .
C12 C10 C9 107.0(6) . .
C11 C10 C13 109.9(7) . .
C12 C10 C13 108.5(7) . .
C9 C10 C13 107.5(6) . .
C10 C11 H11A 109.5 . .
C10 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
C10 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
C10 C12 H12A 109.5 . .
C10 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C10 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C10 C13 H13A 109.5 . .
C10 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
C10 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
O6 C14 O7 124.3(6) . .
O6 C14 C15 117.7(6) . .
O7 C14 C15 117.9(6) . .
C16 C15 C17 109.1(8) . .
C16 C15 C18 112.7(8) . .
C17 C15 C18 107.7(8) . .
C16 C15 C14 109.4(6) . .
C17 C15 C14 110.7(6) . .
C18 C15 C14 107.2(6) . .
C15 C16 H16A 109.5 . .
C15 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C15 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C15 C17 H17A 109.5 . .
C15 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C15 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C15 C18 H18A 109.5 . .
C15 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C15 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
O12 C19 H19A 109.5 . .
O12 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
O12 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
O12 C20 C21 125.2(6) . .
O12 C20 C22 113.8(5) . 2_656
C21 C20 C22 121.0(6) . 2_656
C25 C21 C20 118.7(7) 2_656 .
C25 C21 H21 120.7 2_656 .
C20 C21 H21 120.7 . .
O18 C22 C23 121.3(6) . .
O18 C22 C20 120.7(6) . 2_656
C23 C22 C20 118.0(6) . 2_656
C24 C23 O8 125.4(6) . .
C24 C23 C22 120.9(7) . .
O8 C23 C22 113.6(5) . .
C25 C24 C23 119.8(7) . .
C25 C24 H24 120.1 . .
C23 C24 H24 120.1 . .
C24 C25 C21 121.5(6) . 2_656
C24 C25 H25 119.2 . .
C21 C25 H25 119.2 2_656 .
O8 C26 H26A 109.5 . .
O8 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
O8 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
O11 C27 H27A 109.5 . .
O11 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
O11 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C29 C28 C32A 122.0(7) . .
C29 C28 O11 125.3(6) . .
C32A C28 O11 112.7(6) . .
C30 C29 C28 119.7(7) . .
C30 C29 H29 120.1 . .
C28 C29 H29 120.1 . .
C29 C30 C31 120.1(7) . .
C29 C30 H30 120.0 . .
C31 C30 H30 120.0 . .
C32 C31 C30 120.8(7) . .
C32 C31 H31 119.6 . .
C30 C31 H31 119.6 . .
C31 C32 O9 126.3(7) . .
C31 C32 C32A 120.9(7) . .
O9 C32 C32A 112.7(6) . .
O9 C33 H33A 109.5 . .
O9 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
O9 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
O14 C34 O15 124.6(6) . .
O14 C34 C35 117.3(6) . .
O15 C34 C35 118.0(6) . .
C37 C35 C36 110.9(8) . .
C37 C35 C34 107.7(7) . .
C36 C35 C34 109.1(6) . .
C37 C35 C38 110.9(7) . .
C36 C35 C38 108.5(7) . .
C34 C35 C38 109.6(6) . .
C35 C36 H36A 109.5 . .
C35 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C35 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C35 C37 H37A 109.5 . .
C35 C37 H37B 109.5 . .
H37A C37 H37B 109.5 . .
C35 C37 H37C 109.5 . .
H37A C37 H37C 109.5 . .
H37B C37 H37C 109.5 . .
C35 C38 H38A 109.5 . .
C35 C38 H38B 109.5 . .
H38A C38 H38B 109.5 . .
C35 C38 H38C 109.5 . .
H38A C38 H38C 109.5 . .
H38B C38 H38C 109.5 . .
O16 C39 H39A 109.5 . .
O16 C39 H39B 109.5 . .
H39A C39 H39B 109.5 . .
O16 C39 H39C 109.5 . .
H39A C39 H39C 109.5 . .
H39B C39 H39C 109.5 . .
O17 C40 H40A 109.5 . .
O17 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
O17 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
O13 C41 H41A 109.5 . .
O13 C41 H41B 109.5 . .
H41A C41 H41B 109.5 . .
O13 C41 H41C 109.5 . .
H41A C41 H41C 109.5 . .
H41B C41 H41C 109.5 . .
O19 C42 H42A 109.5 . .
O19 C42 H42B 109.5 . .
H42A C42 H42B 109.5 . .
O19 C42 H42C 109.5 . .
H42A C42 H42C 109.5 . .
H42B C42 H42C 109.5 . .
O20 C43 H43A 109.5 . .
O20 C43 H43B 109.5 . .
H43A C43 H43B 109.5 . .
O20 C43 H43C 109.5 . .
H43A C43 H43C 109.5 . .
H43B C43 H43C 109.5 . .
O20 C44 C45 125.0(6) . .
O20 C44 C46 114.5(5) . 2_567
C45 C44 C46 120.4(6) . 2_567
C49 C45 C44 118.6(6) 2_567 .
C49 C45 H45 120.7 2_567 .
C44 C45 H45 120.7 . .
O33 C46 C47 121.6(6) . .
O33 C46 C44 119.9(6) . 2_567
C47 C46 C44 118.5(6) . 2_567
C48 C47 C46 121.6(6) . .
C48 C47 O32 124.7(6) . .
C46 C47 O32 113.7(6) . .
C49 C48 C47 119.2(6) . .
C49 C48 H48 120.4 . .
C47 C48 H48 120.4 . .
C48 C49 C45 121.5(6) . 2_567
C48 C49 H49 119.2 . .
C45 C49 H49 119.2 2_567 .
O32 C50 H50A 109.5 . .
O32 C50 H50B 109.5 . .
H50A C50 H50B 109.5 . .
O32 C50 H50C 109.5 . .
H50A C50 H50C 109.5 . .
H50B C50 H50C 109.5 . .
O26 C51 O25 124.3(7) . .
O26 C51 C55 118.7(7) . .
O25 C51 C55 117.0(7) . .
C55 C52 H52A 109.5 . .
C55 C52 H52B 109.5 . .
H52A C52 H52B 109.5 . .
C55 C52 H52C 109.5 . .
H52A C52 H52C 109.5 . .
H52B C52 H52C 109.5 . .
C55 C53 H53A 109.5 . .
C55 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
C55 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C55 C54 H54A 109.5 . .
C55 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C55 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
C52 C55 C53 109.8(8) . .
C52 C55 C54 111.8(8) . .
C53 C55 C54 110.1(7) . .
C52 C55 C51 106.0(7) . .
C53 C55 C51 109.1(7) . .
C54 C55 C51 109.9(7) . .
O22 C56 C57 126.1(7) . .
O22 C56 C58A 113.8(6) . .
C57 C56 C58A 120.1(7) . .
C58 C57 C56 119.9(8) . .
C58 C57 H57 120.0 . .
C56 C57 H57 120.0 . .
C57 C58 C59 120.9(7) . .
C57 C58 H58 119.6 . .
C59 C58 H58 119.6 . .
O23 C58A C60 122.6(6) . .
O23 C58A C56 119.7(6) . .
C60 C58A C56 117.7(6) . .
C58 C59 C60 119.6(7) . .
C58 C59 H59 120.2 . .
C60 C59 H59 120.2 . .
O24 C60 C59 124.8(6) . .
O24 C60 C58A 113.5(6) . .
C59 C60 C58A 121.7(7) . .
O24 C61 H61A 109.5 . .
O24 C61 H61B 109.5 . .
H61A C61 H61B 109.5 . .
O24 C61 H61C 109.5 . .
H61A C61 H61C 109.5 . .
H61B C61 H61C 109.5 . .
O22 C62 H62A 109.5 . .
O22 C62 H62B 109.5 . .
H62A C62 H62B 109.5 . .
O22 C62 H62C 109.5 . .
H62A C62 H62C 109.5 . .
H62B C62 H62C 109.5 . .
O27 C63 H63A 109.5 . .
O27 C63 H63B 109.5 . .
H63A C63 H63B 109.5 . .
O27 C63 H63C 109.5 . .
H63A C63 H63C 109.5 . .
H63B C63 H63C 109.5 . .
O38 C64 H64A 109.5 . .
O38 C64 H64B 109.5 . .
H64A C64 H64B 109.5 . .
O38 C64 H64C 109.5 . .
H64A C64 H64C 109.5 . .
H64B C64 H64C 109.5 . .
O35 C65 O34 124.6(6) . .
O35 C65 C66A 118.5(6) . .
O34 C65 C66A 116.9(6) . .
C66A C66 H66A 109.5 . .
C66A C66 H66B 109.5 . .
H66A C66 H66B 109.5 . .
C66A C66 H66C 109.5 . .
H66A C66 H66C 109.5 . .
H66B C66 H66C 109.5 . .
C66A C67 H67A 109.5 . .
C66A C67 H67B 109.5 . .
H67A C67 H67B 109.5 . .
C66A C67 H67C 109.5 . .
H67A C67 H67C 109.5 . .
H67B C67 H67C 109.5 . .
C66A C68 H68A 109.5 . .
C66A C68 H68B 109.5 . .
H68A C68 H68B 109.5 . .
C66A C68 H68C 109.5 . .
H68A C68 H68C 109.5 . .
H68B C68 H68C 109.5 . .
O30 C69 H69A 109.5 . .
O30 C69 H69B 109.5 . .
H69A C69 H69B 109.5 . .
O30 C69 H69C 109.5 . .
H69A C69 H69C 109.5 . .
H69B C69 H69C 109.5 . .
C71 C70 O30 124.8(7) . .
C71 C70 C82 121.8(7) . .
O30 C70 C82 113.4(6) . .
C70 C71 C72 119.0(7) . .
C70 C71 H71 120.5 . .
C72 C71 H71 120.5 . .
C73 C72 C71 120.0(7) . .
C73 C72 H72 120.0 . .
C71 C72 H72 120.0 . .
C72 C73 C74 120.9(7) . .
C72 C73 H73 119.6 . .
C74 C73 H73 119.6 . .
O28 C74 C73 125.8(7) . .
O28 C74 C82 113.7(6) . .
C73 C74 C82 120.5(7) . .
O28 C75 H75A 109.5 . .
O28 C75 H75B 109.5 . .
H75A C75 H75B 109.5 . .
O28 C75 H75C 109.5 . .
H75A C75 H75C 109.5 . .
H75B C75 H75C 109.5 . .
O31 C76 O21 124.6(6) . 2_567
O31 C76 C78 116.9(6) . .
O21 C76 C78 118.5(6) 2_567 .
C78 C77 H77A 109.5 . .
C78 C77 H77B 109.5 . .
H77A C77 H77B 109.5 . .
C78 C77 H77C 109.5 . .
H77A C77 H77C 109.5 . .
H77B C77 H77C 109.5 . .
C76 C78 C77 108.5(6) . .
C76 C78 C79 111.7(6) . .
C77 C78 C79 110.9(7) . .
C76 C78 C80 107.6(7) . .
C77 C78 C80 109.5(7) . .
C79 C78 C80 108.6(7) . .
C78 C79 H79A 109.5 . .
C78 C79 H79B 109.5 . .
H79A C79 H79B 109.5 . .
C78 C79 H79C 109.5 . .
H79A C79 H79C 109.5 . .
H79B C79 H79C 109.5 . .
C78 C80 H80A 109.5 . .
C78 C80 H80B 109.5 . .
H80A C80 H80B 109.5 . .
C78 C80 H80C 109.5 . .
H80A C80 H80C 109.5 . .
H80B C80 H80C 109.5 . .
O37 C81 H81A 109.5 . .
O37 C81 H81B 109.5 . .
H81A C81 H81B 109.5 . .
O37 C81 H81C 109.5 . .
H81A C81 H81C 109.5 . .
H81B C81 H81C 109.5 . .
O29 C82 C70 121.1(6) . .
O29 C82 C74 121.2(6) . .
C70 C82 C74 117.7(6) . .
O36 C83 H83A 109.5 . .
O36 C83 H83B 109.5 . .
H83A C83 H83B 109.5 . .
O36 C83 H83C 109.5 . .
H83A C83 H83C 109.5 . .
H83B C83 H83C 109.5 . .
C64 O38 Dy5 128.2(5) . .
C2 O1 C1 117.8(5) . .
C2 O1 Dy1 115.3(4) . .
C1 O1 Dy1 126.9(4) . .
C7 O2 Dy1 120.3(4) . .
C7 O2 Dy2 122.4(4) . .
Dy1 O2 Dy2 105.74(16) . .
C6 O3 C8 114.8(6) . .
C6 O3 Dy2 115.4(4) . .
C8 O3 Dy2 129.5(5) . .
C9 O4 Dy1 167.1(5) . .
C14 O6 Dy1 134.9(4) . .
C14 O7 Dy2 135.5(4) . .
C23 O8 C26 115.9(6) . .
C23 O8 Dy3 114.6(4) . .
C26 O8 Dy3 129.3(5) . .
C32 O9 C33 115.8(6) . .
C32 O9 Dy3 116.0(4) . .
C33 O9 Dy3 128.3(5) . .
C32A O10 Dy3 120.5(4) . .
C32A O10 Dy2 123.1(4) . .
Dy3 O10 Dy2 105.45(17) . .
C28 O11 C27 115.2(5) . .
C28 O11 Dy2 114.6(4) . .
C27 O11 Dy2 128.4(4) . .
C20 O12 C19 117.2(5) . .
C20 O12 Dy1 115.0(4) . .
C19 O12 Dy1 126.7(4) . .
C41 O13 Dy3 124.9(4) . .
C41 O13 Dy2 122.6(4) . .
Dy3 O13 Dy2 111.82(19) . .
C34 O14 Dy2 136.1(4) . .
C34 O15 Dy3 133.7(4) . .
C39 O16 Dy3 125.2(5) . .
C40 O17 Dy3 122.2(4) . .
C40 O17 Dy1 123.9(4) . 2_656
Dy3 O17 Dy1 113.83(18) . 2_656
C22 O18 Dy3 123.7(4) . .
C22 O18 Dy1 120.7(4) . 2_656
Dy3 O18 Dy1 110.15(17) . 2_656
C42 O19 Dy2 123.1(4) . .
C42 O19 Dy1 125.3(4) . .
Dy2 O19 Dy1 111.63(18) . .
C44 O20 C43 116.3(5) . .
C44 O20 Dy4 115.4(4) . .
C43 O20 Dy4 127.9(4) . .
C76 O21 Dy4 135.0(5) 2_567 .
C56 O22 C62 115.9(6) . .
C56 O22 Dy4 116.6(4) . .
C62 O22 Dy4 127.4(4) . .
C58A O23 Dy5 124.3(4) . .
C58A O23 Dy4 125.5(4) . .
Dy5 O23 Dy4 109.37(18) . .
C60 O24 C61 114.9(6) . .
C60 O24 Dy5 115.3(4) . .
C61 O24 Dy5 129.6(5) . .
C51 O25 Dy4 162.4(5) . .
C63 O27 Dy5 122.4(4) . .
C63 O27 Dy4 123.7(4) . .
Dy5 O27 Dy4 113.60(19) . .
C74 O28 C75 116.9(6) . .
C74 O28 Dy5 114.6(4) . .
C75 O28 Dy5 128.5(5) . .
C82 O29 Dy5 120.8(4) . .
C82 O29 Dy6 121.3(4) . .
Dy5 O29 Dy6 105.56(17) . .
C70 O30 C69 117.4(6) . .
C70 O30 Dy6 115.7(4) . .
C69 O30 Dy6 126.8(5) . .
C76 O31 Dy6 134.7(4) . .
C47 O32 C50 116.4(6) . .
C47 O32 Dy6 115.4(4) . .
C50 O32 Dy6 128.1(4) . .
C46 O33 Dy4 122.5(4) . 2_567
C46 O33 Dy6 121.3(4) . .
Dy4 O33 Dy6 107.07(17) 2_567 .
C65 O34 Dy5 134.3(4) . .
C65 O35 Dy6 136.0(4) . .
C83 O36 Dy6 122.4(4) . .
C83 O36 Dy4 125.7(4) . 2_567
Dy6 O36 Dy4 111.56(19) . 2_567
C81 O37 Dy5 125.8(5) . .
C81 O37 Dy6 121.8(5) . .
Dy5 O37 Dy6 112.36(17) . .
O19 Dy1 O4 149.08(17) . .
O19 Dy1 O17 105.28(16) . 2_656
O4 Dy1 O17 95.71(17) . 2_656
O19 Dy1 O2 69.34(15) . .
O4 Dy1 O2 135.36(16) . .
O17 Dy1 O2 86.95(15) 2_656 .
O19 Dy1 O18 87.24(16) . 2_656
O4 Dy1 O18 80.07(16) . 2_656
O17 Dy1 O18 67.41(15) 2_656 2_656
O2 Dy1 O18 139.56(14) . 2_656
O19 Dy1 O6 87.85(16) . .
O4 Dy1 O6 83.97(17) . .
O17 Dy1 O6 151.58(16) 2_656 .
O2 Dy1 O6 74.05(15) . .
O18 Dy1 O6 139.60(15) 2_656 .
O19 Dy1 O12 75.75(15) . .
O4 Dy1 O12 73.33(16) . .
O17 Dy1 O12 132.52(15) 2_656 .
O2 Dy1 O12 133.36(15) . .
O18 Dy1 O12 65.23(15) 2_656 .
O6 Dy1 O12 74.70(15) . .
O19 Dy1 O1 134.24(15) . .
O4 Dy1 O1 72.50(15) . .
O17 Dy1 O1 75.83(15) 2_656 .
O2 Dy1 O1 65.02(15) . .
O18 Dy1 O1 131.09(15) 2_656 .
O6 Dy1 O1 77.01(16) . .
O12 Dy1 O1 137.32(14) . .
O19 Dy1 Dy2 33.90(11) . .
O4 Dy1 Dy2 155.03(13) . .
O17 Dy1 Dy2 106.07(11) 2_656 .
O2 Dy1 Dy2 37.28(11) . .
O18 Dy1 Dy2 119.30(11) 2_656 .
O6 Dy1 Dy2 71.06(12) . .
O12 Dy1 Dy2 99.46(10) . .
O1 Dy1 Dy2 100.79(10) . .
O19 Dy1 Dy3 99.90(11) . 2_656
O4 Dy1 Dy3 85.51(13) . 2_656
O17 Dy1 Dy3 32.82(11) 2_656 2_656
O2 Dy1 Dy3 115.72(10) . 2_656
O18 Dy1 Dy3 34.73(11) 2_656 2_656
O6 Dy1 Dy3 169.15(11) . 2_656
O12 Dy1 Dy3 99.71(10) . 2_656
O1 Dy1 Dy3 102.30(11) . 2_656
Dy2 Dy1 Dy3 119.435(11) . 2_656
O19 Dy2 O13 100.56(16) . .
O19 Dy2 O7 88.56(16) . .
O13 Dy2 O7 153.36(17) . .
O19 Dy2 O14 153.69(17) . .
O13 Dy2 O14 85.29(17) . .
O7 Dy2 O14 97.61(16) . .
O19 Dy2 O10 84.34(15) . .
O13 Dy2 O10 70.15(16) . .
O7 Dy2 O10 136.13(16) . .
O14 Dy2 O10 73.48(16) . .
O19 Dy2 O2 69.60(15) . .
O13 Dy2 O2 85.36(15) . .
O7 Dy2 O2 74.36(16) . .
O14 Dy2 O2 136.69(16) . .
O10 Dy2 O2 140.29(15) . .
O19 Dy2 O3 133.48(16) . .
O13 Dy2 O3 80.37(16) . .
O7 Dy2 O3 75.35(16) . .
O14 Dy2 O3 72.66(16) . .
O10 Dy2 O3 136.35(15) . .
O2 Dy2 O3 64.10(15) . .
O19 Dy2 O11 82.69(16) . .
O13 Dy2 O11 133.45(15) . .
O7 Dy2 O11 72.21(16) . .
O14 Dy2 O11 75.02(16) . .
O10 Dy2 O11 63.95(15) . .
O2 Dy2 O11 136.66(14) . .
O3 Dy2 O11 129.93(15) . .
O19 Dy2 Dy3 100.01(11) . .
O13 Dy2 Dy3 34.05(12) . .
O7 Dy2 Dy3 167.31(12) . .
O14 Dy2 Dy3 70.62(12) . .
O10 Dy2 Dy3 37.26(10) . .
O2 Dy2 Dy3 117.33(10) . .
O3 Dy2 Dy3 104.57(11) . .
O11 Dy2 Dy3 99.42(10) . .
O19 Dy2 Dy1 34.47(11) . .
O13 Dy2 Dy1 102.26(12) . .
O7 Dy2 Dy1 71.54(12) . .
O14 Dy2 Dy1 168.14(12) . .
O10 Dy2 Dy1 117.54(11) . .
O2 Dy2 Dy1 36.97(10) . .
O3 Dy2 Dy1 99.35(10) . .
O11 Dy2 Dy1 105.15(10) . .
Dy3 Dy2 Dy1 120.576(11) . .
O13 Dy3 O17 107.59(16) . .
O13 Dy3 O18 87.01(16) . .
O17 Dy3 O18 68.33(15) . .
O13 Dy3 O10 70.26(16) . .
O17 Dy3 O10 88.59(15) . .
O18 Dy3 O10 141.24(15) . .
O13 Dy3 O15 86.70(17) . .
O17 Dy3 O15 152.61(18) . .
O18 Dy3 O15 137.24(16) . .
O10 Dy3 O15 74.10(16) . .
O13 Dy3 O16 148.14(18) . .
O17 Dy3 O16 94.07(17) . .
O18 Dy3 O16 79.47(17) . .
O10 Dy3 O16 134.90(18) . .
O15 Dy3 O16 84.06(17) . .
O13 Dy3 O9 134.81(15) . .
O17 Dy3 O9 76.34(16) . .
O18 Dy3 O9 132.42(15) . .
O10 Dy3 O9 64.80(15) . .
O15 Dy3 O9 77.10(17) . .
O16 Dy3 O9 72.17(17) . .
O13 Dy3 O8 78.58(16) . .
O17 Dy3 O8 131.82(15) . .
O18 Dy3 O8 64.29(15) . .
O10 Dy3 O8 135.41(15) . .
O15 Dy3 O8 73.00(16) . .
O16 Dy3 O8 69.56(18) . .
O9 Dy3 O8 133.11(16) . .
O13 Dy3 Dy2 34.14(11) . .
O17 Dy3 Dy2 106.82(11) . .
O18 Dy3 Dy2 118.99(11) . .
O10 Dy3 Dy2 37.29(11) . .
O15 Dy3 Dy2 71.88(12) . .
O16 Dy3 Dy2 155.93(12) . .
O9 Dy3 Dy2 100.81(11) . .
O8 Dy3 Dy2 103.12(11) . .
O13 Dy3 Dy1 101.17(12) . 2_656
O17 Dy3 Dy1 33.35(11) . 2_656
O18 Dy3 Dy1 35.12(10) . 2_656
O10 Dy3 Dy1 117.79(11) . 2_656
O15 Dy3 Dy1 167.33(11) . 2_656
O16 Dy3 Dy1 84.07(12) . 2_656
O9 Dy3 Dy1 103.35(11) . 2_656
O8 Dy3 Dy1 98.64(10) . 2_656
Dy2 Dy3 Dy1 119.977(11) . 2_656
O36 Dy4 O25 150.14(18) 2_567 .
O36 Dy4 O27 103.84(16) 2_567 .
O25 Dy4 O27 97.16(18) . .
O36 Dy4 O33 69.01(16) 2_567 2_567
O25 Dy4 O33 135.15(17) . 2_567
O27 Dy4 O33 83.79(16) . 2_567
O36 Dy4 O23 86.65(16) 2_567 .
O25 Dy4 O23 81.69(17) . .
O27 Dy4 O23 68.12(16) . .
O33 Dy4 O23 137.27(15) 2_567 .
O36 Dy4 O21 85.52(17) 2_567 .
O25 Dy4 O21 86.18(18) . .
O27 Dy4 O21 151.16(17) . .
O33 Dy4 O21 74.09(16) 2_567 .
O23 Dy4 O21 140.43(17) . .
O36 Dy4 O20 133.76(15) 2_567 .
O25 Dy4 O20 71.76(17) . .
O27 Dy4 O20 76.00(15) . .
O33 Dy4 O20 64.99(15) 2_567 .
O23 Dy4 O20 131.78(15) . .
O21 Dy4 O20 77.94(16) . .
O36 Dy4 O22 77.01(16) 2_567 .
O25 Dy4 O22 73.16(18) . .
O27 Dy4 O22 132.10(15) . .
O33 Dy4 O22 136.08(15) 2_567 .
O23 Dy4 O22 64.10(15) . .
O21 Dy4 O22 76.35(16) . .
O20 Dy4 O22 137.40(16) . .
O36 Dy4 Dy6 34.06(12) 2_567 2_567
O25 Dy4 Dy6 156.27(13) . 2_567
O27 Dy4 Dy6 102.36(11) . 2_567
O33 Dy4 Dy6 36.48(11) 2_567 2_567
O23 Dy4 Dy6 118.08(11) . 2_567
O21 Dy4 Dy6 70.22(12) . 2_567
O20 Dy4 Dy6 99.92(10) . 2_567
O22 Dy4 Dy6 102.54(11) . 2_567
O36 Dy4 Dy5 97.07(12) 2_567 .
O25 Dy4 Dy5 89.06(13) . .
O27 Dy4 Dy5 32.96(11) . .
O33 Dy4 Dy5 111.63(11) 2_567 .
O23 Dy4 Dy5 35.17(11) . .
O21 Dy4 Dy5 174.24(12) . .
O20 Dy4 Dy5 103.63(11) . .
O22 Dy4 Dy5 99.17(11) . .
Dy6 Dy4 Dy5 114.642(11) 2_567 .
O37 Dy5 O27 105.37(16) . .
O37 Dy5 O23 89.24(16) . .
O27 Dy5 O23 68.90(16) . .
O37 Dy5 O29 69.28(15) . .
O27 Dy5 O29 87.28(16) . .
O23 Dy5 O29 142.71(15) . .
O37 Dy5 O34 88.91(16) . .
O27 Dy5 O34 151.61(17) . .
O23 Dy5 O34 136.98(17) . .
O29 Dy5 O34 74.79(17) . .
O37 Dy5 O38 149.95(17) . .
O27 Dy5 O38 95.29(16) . .
O23 Dy5 O38 77.96(16) . .
O29 Dy5 O38 134.43(16) . .
O34 Dy5 O38 82.58(17) . .
O37 Dy5 O28 134.20(16) . .
O27 Dy5 O28 75.69(16) . .
O23 Dy5 O28 130.25(16) . .
O29 Dy5 O28 65.01(16) . .
O34 Dy5 O28 76.80(17) . .
O38 Dy5 O28 71.63(17) . .
O37 Dy5 O24 78.51(15) . .
O27 Dy5 O24 132.74(15) . .
O23 Dy5 O24 64.04(15) . .
O29 Dy5 O24 134.65(15) . .
O34 Dy5 O24 73.50(16) . .
O38 Dy5 O24 71.44(16) . .
O28 Dy5 O24 134.83(15) . .
O37 Dy5 Dy6 33.85(11) . .
O27 Dy5 Dy6 106.94(11) . .
O23 Dy5 Dy6 121.88(11) . .
O29 Dy5 Dy6 37.54(11) . .
O34 Dy5 Dy6 71.64(12) . .
O38 Dy5 Dy6 154.21(12) . .
O28 Dy5 Dy6 100.93(11) . .
O24 Dy5 Dy6 101.06(10) . .
O37 Dy5 Dy4 99.55(11) . .
O27 Dy5 Dy4 33.44(11) . .
O23 Dy5 Dy4 35.47(11) . .
O29 Dy5 Dy4 116.42(11) . .
O34 Dy5 Dy4 167.75(13) . .
O38 Dy5 Dy4 85.71(12) . .
O28 Dy5 Dy4 102.86(11) . .
O24 Dy5 Dy4 99.37(10) . .
Dy6 Dy5 Dy4 120.070(10) . .
O37 Dy6 O36 103.59(17) . .
O37 Dy6 O31 152.47(17) . .
O36 Dy6 O31 88.60(17) . .
O37 Dy6 O33 87.25(16) . .
O36 Dy6 O33 69.29(16) . .
O31 Dy6 O33 73.93(16) . .
O37 Dy6 O35 88.72(16) . .
O36 Dy6 O35 151.77(17) . .
O31 Dy6 O35 91.84(17) . .
O33 Dy6 O35 137.57(16) . .
O37 Dy6 O29 68.61(15) . .
O36 Dy6 O29 87.36(16) . .
O31 Dy6 O29 137.53(16) . .
O33 Dy6 O29 141.66(15) . .
O35 Dy6 O29 73.44(16) . .
O37 Dy6 O30 132.67(16) . .
O36 Dy6 O30 78.53(17) . .
O31 Dy6 O30 73.52(16) . .
O33 Dy6 O30 134.16(16) . .
O35 Dy6 O30 74.57(17) . .
O29 Dy6 O30 64.24(16) . .
O37 Dy6 O32 77.26(17) . .
O36 Dy6 O32 133.87(16) . .
O31 Dy6 O32 76.56(18) . .
O33 Dy6 O32 64.66(15) . .
O35 Dy6 O32 73.26(16) . .
O29 Dy6 O32 132.13(16) . .
O30 Dy6 O32 134.74(17) . .
O37 Dy6 Dy5 33.79(10) . .
O36 Dy6 Dy5 105.75(12) . .
O31 Dy6 Dy5 162.62(12) . .
O33 Dy6 Dy5 119.95(11) . .
O35 Dy6 Dy5 70.87(12) . .
O29 Dy6 Dy5 36.90(11) . .
O30 Dy6 Dy5 99.34(11) . .
O32 Dy6 Dy5 99.25(12) . .
O37 Dy6 Dy4 104.38(11) . 2_567
O36 Dy6 Dy4 34.37(12) . 2_567
O31 Dy6 Dy4 72.07(12) . 2_567
O33 Dy6 Dy4 36.45(11) . 2_567
O35 Dy6 Dy4 163.72(12) . 2_567
O29 Dy6 Dy4 120.08(10) . 2_567
O30 Dy6 Dy4 102.23(12) . 2_567
O32 Dy6 Dy4 99.88(10) . 2_567
Dy5 Dy6 Dy4 125.283(12) . 2_567
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.438(8) .
C1 H1A 0.9600 .
C1 H1B 0.9600 .
C1 H1C 0.9600 .
C2 O1 1.377(8) .
C2 C7 1.384(9) .
C2 C3 1.409(9) .
C3 C4 1.388(10) .
C3 H3 0.9300 .
C4 C5 1.374(11) .
C4 H4 0.9300 .
C5 C6 1.408(10) .
C5 H5 0.9300 .
C32A O10 1.335(8) .
C32A C28 1.404(9) .
C32A C32 1.409(10) .
C6 O3 1.351(8) .
C6 C7 1.436(9) .
C7 O2 1.338(7) .
C8 O3 1.432(8) .
C8 H8A 0.9600 .
C8 H8B 0.9600 .
C8 H8C 0.9600 .
C66A C68 1.474(15) .
C66A C66 1.504(14) .
C66A C65 1.537(9) .
C66A C67 1.559(15) .
C9 O5 1.248(10) .
C9 O4 1.246(8) .
C9 C10 1.542(10) .
C10 C11 1.501(10) .
C10 C12 1.525(10) .
C10 C13 1.569(12) .
C11 H11A 0.9600 .
C11 H11B 0.9600 .
C11 H11C 0.9600 .
C12 H12A 0.9600 .
C12 H12B 0.9600 .
C12 H12C 0.9600 .
C13 H13A 0.9600 .
C13 H13B 0.9600 .
C13 H13C 0.9600 .
C14 O6 1.255(8) .
C14 O7 1.269(8) .
C14 C15 1.539(9) .
C15 C16 1.516(11) .
C15 C17 1.517(11) .
C15 C18 1.520(11) .
C16 H16A 0.9600 .
C16 H16B 0.9600 .
C16 H16C 0.9600 .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C18 H18A 0.9600 .
C18 H18B 0.9600 .
C18 H18C 0.9600 .
C19 O12 1.424(8) .
C19 H19A 0.9600 .
C19 H19B 0.9600 .
C19 H19C 0.9600 .
C20 O12 1.374(8) .
C20 C21 1.391(8) .
C20 C22 1.410(9) 2_656
C21 C25 1.386(10) 2_656
C21 H21 0.9300 .
C22 O18 1.332(7) .
C22 C23 1.396(9) .
C22 C20 1.410(9) 2_656
C23 C24 1.384(9) .
C23 O8 1.379(8) .
C24 C25 1.368(11) .
C24 H24 0.9300 .
C25 C21 1.386(10) 2_656
C25 H25 0.9300 .
C26 O8 1.405(9) .
C26 H26A 0.9600 .
C26 H26B 0.9600 .
C26 H26C 0.9600 .
C27 O11 1.451(8) .
C27 H27A 0.9600 .
C27 H27B 0.9600 .
C27 H27C 0.9600 .
C28 C29 1.388(10) .
C28 O11 1.406(8) .
C29 C30 1.362(11) .
C29 H29 0.9300 .
C30 C31 1.378(11) .
C30 H30 0.9300 .
C31 C32 1.376(10) .
C31 H31 0.9300 .
C32 O9 1.380(8) .
C33 O9 1.414(8) .
C33 H33A 0.9600 .
C33 H33B 0.9600 .
C33 H33C 0.9600 .
C34 O14 1.258(8) .
C34 O15 1.260(8) .
C34 C35 1.521(10) .
C35 C37 1.499(12) .
C35 C36 1.523(11) .
C35 C38 1.562(12) .
C36 H36A 0.9600 .
C36 H36B 0.9600 .
C36 H36C 0.9600 .
C37 H37A 0.9600 .
C37 H37B 0.9600 .
C37 H37C 0.9600 .
C38 H38A 0.9600 .
C38 H38B 0.9600 .
C38 H38C 0.9600 .
C39 O16 1.465(9) .
C39 H39A 0.9600 .
C39 H39B 0.9600 .
C39 H39C 0.9600 .
C40 O17 1.445(8) .
C40 H40A 0.9600 .
C40 H40B 0.9600 .
C40 H40C 0.9600 .
C41 O13 1.405(8) .
C41 H41A 0.9600 .
C41 H41B 0.9600 .
C41 H41C 0.9600 .
C42 O19 1.405(8) .
C42 H42A 0.9600 .
C42 H42B 0.9600 .
C42 H42C 0.9600 .
C43 O20 1.446(8) .
C43 H43A 0.9600 .
C43 H43B 0.9600 .
C43 H43C 0.9600 .
C44 O20 1.379(7) .
C44 C45 1.392(9) .
C44 C46 1.407(9) 2_567
C45 C49 1.390(10) 2_567
C45 H45 0.9300 .
C46 O33 1.358(7) .
C46 C47 1.378(9) .
C46 C44 1.407(9) 2_567
C47 C48 1.379(9) .
C47 O32 1.380(8) .
C48 C49 1.371(10) .
C48 H48 0.9300 .
C49 C45 1.390(10) 2_567
C49 H49 0.9300 .
C50 O32 1.420(8) .
C50 H50A 0.9600 .
C50 H50B 0.9600 .
C50 H50C 0.9600 .
C51 O26 1.233(10) .
C51 O25 1.265(9) .
C51 C55 1.545(11) .
C52 C55 1.510(14) .
C52 H52A 0.9600 .
C52 H52B 0.9600 .
C52 H52C 0.9600 .
C53 C55 1.512(12) .
C53 H53A 0.9600 .
C53 H53B 0.9600 .
C53 H53C 0.9600 .
C54 C55 1.532(12) .
C54 H54A 0.9600 .
C54 H54B 0.9600 .
C54 H54C 0.9600 .
C56 O22 1.371(9) .
C56 C57 1.392(10) .
C56 C58A 1.433(10) .
C57 C58 1.380(12) .
C57 H57 0.9300 .
C58 C59 1.381(12) .
C58 H58 0.9300 .
C58A O23 1.322(8) .
C58A C60 1.385(9) .
C59 C60 1.389(9) .
C59 H59 0.9300 .
C60 O24 1.375(8) .
C61 O24 1.434(8) .
C61 H61A 0.9600 .
C61 H61B 0.9600 .
C61 H61C 0.9600 .
C62 O22 1.439(8) .
C62 H62A 0.9600 .
C62 H62B 0.9600 .
C62 H62C 0.9600 .
C63 O27 1.422(8) .
C63 H63A 0.9600 .
C63 H63B 0.9600 .
C63 H63C 0.9600 .
C64 O38 1.427(9) .
C64 H64A 0.9600 .
C64 H64B 0.9600 .
C64 H64C 0.9600 .
C65 O35 1.241(8) .
C65 O34 1.272(8) .
C66 H66A 0.9600 .
C66 H66B 0.9600 .
C66 H66C 0.9600 .
C67 H67A 0.9600 .
C67 H67B 0.9600 .
C67 H67C 0.9600 .
C68 H68A 0.9600 .
C68 H68B 0.9600 .
C68 H68C 0.9600 .
C69 O30 1.436(10) .
C69 H69A 0.9600 .
C69 H69B 0.9600 .
C69 H69C 0.9600 .
C70 C71 1.378(9) .
C70 O30 1.385(8) .
C70 C82 1.398(10) .
C71 C72 1.403(11) .
C71 H71 0.9300 .
C72 C73 1.365(12) .
C72 H72 0.9300 .
C73 C74 1.385(9) .
C73 H73 0.9300 .
C74 O28 1.380(9) .
C74 C82 1.399(10) .
C75 O28 1.430(9) .
C75 H75A 0.9600 .
C75 H75B 0.9600 .
C75 H75C 0.9600 .
C76 O31 1.261(8) .
C76 O21 1.266(8) 2_567
C76 C78 1.518(10) .
C77 C78 1.536(10) .
C77 H77A 0.9600 .
C77 H77B 0.9600 .
C77 H77C 0.9600 .
C78 C79 1.535(11) .
C78 C80 1.553(12) .
C79 H79A 0.9600 .
C79 H79B 0.9600 .
C79 H79C 0.9600 .
C80 H80A 0.9600 .
C80 H80B 0.9600 .
C80 H80C 0.9600 .
C81 O37 1.385(9) .
C81 H81A 0.9600 .
C81 H81B 0.9600 .
C81 H81C 0.9600 .
C82 O29 1.335(7) .
C83 O36 1.422(9) .
C83 H83A 0.9600 .
C83 H83B 0.9600 .
C83 H83C 0.9600 .
O38 Dy5 2.384(5) .
O1 Dy1 2.559(5) .
O2 Dy1 2.334(4) .
O2 Dy2 2.351(5) .
O3 Dy2 2.633(5) .
O4 Dy1 2.280(4) .
O6 Dy1 2.363(5) .
O7 Dy2 2.327(5) .
O8 Dy3 2.628(5) .
O9 Dy3 2.583(5) .
O10 Dy3 2.345(4) .
O10 Dy2 2.346(5) .
O11 Dy2 2.655(5) .
O12 Dy1 2.558(4) .
O13 Dy3 2.251(5) .
O13 Dy2 2.256(4) .
O14 Dy2 2.334(5) .
O15 Dy3 2.344(5) .
O16 Dy3 2.409(5) .
O17 Dy3 2.263(4) .
O17 Dy1 2.295(5) 2_656
O18 Dy3 2.318(4) .
O18 Dy1 2.341(4) 2_656
O19 Dy2 2.241(4) .
O19 Dy1 2.275(4) .
O20 Dy4 2.601(4) .
O21 C76 1.266(8) 2_567
O21 Dy4 2.360(5) .
O22 Dy4 2.622(5) .
O23 Dy5 2.324(4) .
O23 Dy4 2.341(4) .
O24 Dy5 2.645(5) .
O25 Dy4 2.282(5) .
O27 Dy5 2.260(4) .
O27 Dy4 2.289(4) .
O28 Dy5 2.588(5) .
O29 Dy5 2.326(5) .
O29 Dy6 2.361(4) .
O30 Dy6 2.593(5) .
O31 Dy6 2.322(5) .
O32 Dy6 2.603(5) .
O33 Dy4 2.330(4) 2_567
O33 Dy6 2.331(4) .
O34 Dy5 2.340(5) .
O35 Dy6 2.353(4) .
O36 Dy6 2.258(5) .
O36 Dy4 2.276(4) 2_567
O37 Dy5 2.245(4) .
O37 Dy6 2.248(4) .
Dy1 O17 2.295(5) 2_656
Dy1 O18 2.341(4) 2_656
Dy1 Dy2 3.7356(5) .
Dy1 Dy3 3.8193(5) 2_656
Dy2 Dy3 3.7322(5) .
Dy3 Dy1 3.8193(5) 2_656
Dy4 O36 2.275(5) 2_567
Dy4 O33 2.330(4) 2_567
Dy4 Dy6 3.7485(5) 2_567
Dy4 Dy5 3.8061(6) .
Dy5 Dy6 3.7328(5) .
Dy6 Dy4 3.7484(5) 2_567
