#------------------------------------------------------------------------------
#$Date: 2016-02-13 21:28:24 +0200 (Sat, 13 Feb 2016) $
#$Revision: 176429 $
#$URL: svn://www.crystallography.net/cod/cif/4/34/32/4343233.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4343233
loop_
_publ_author_name
'Li, Xiao-Lei'
'Min, Fan-Yong'
'Wang, Chao'
'Lin, Shuang-Yan'
'Liu, Zhiliang'
'Tang, Jinkui'
_publ_section_title
;
 Utilizing 3d-4f magnetic interaction to slow the magnetic relaxation of
 heterometallic complexes.
;
_journal_issue                   9
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4337
_journal_page_last               4344
_journal_paper_doi               10.1021/acs.inorgchem.5b00019
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'C28 H20 Co0.5 Dy O11'
_chemical_formula_weight         724.41
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 108.503(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.913(4)
_cell_length_b                   11.125(3)
_cell_length_c                   20.084(6)
_cell_measurement_reflns_used    4401
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.53
_cell_measurement_theta_min      2.33
_cell_volume                     3159.8(15)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0743
_diffrn_reflns_av_sigmaI/netI    0.0841
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            15576
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.44
_exptl_absorpt_coefficient_mu    2.671
_exptl_absorpt_correction_T_max  0.9007
_exptl_absorpt_correction_T_min  0.6746
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   crystalclear
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.523
_exptl_crystal_density_meas      1.520
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1422
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.773
_refine_diff_density_min         -0.987
_refine_diff_density_rms         0.331
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     367
_refine_ls_number_reflns         5559
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.047
_refine_ls_R_factor_all          0.1001
_refine_ls_R_factor_gt           0.0568
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1033P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1603
_refine_ls_wR_factor_ref         0.1820
_reflns_number_gt                3630
_reflns_number_total             5559
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5b00019_si_002.cif
_cod_data_source_block           Dy2Co
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'multi_scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 
;
_cod_original_sg_symbol_H-M      P21/c
_cod_original_formula_sum        'C28 H20 Co0.50 Dy O11'
_cod_database_code               4343233
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.1742(7) 0.4473(9) -0.0506(5) 0.041(2) Uani 1 1 d .
C2 C 0.1186(8) 0.4312(9) -0.1197(5) 0.044(3) Uani 1 1 d .
H2 H 0.0533 0.4254 -0.1307 0.053 Uiso 1 1 calc R
C3 C 0.1602(8) 0.4235(10) -0.1733(6) 0.056(3) Uani 1 1 d .
H3 H 0.1214 0.4141 -0.2195 0.068 Uiso 1 1 calc R
C4 C 0.2570(9) 0.4295(11) -0.1596(7) 0.066(4) Uani 1 1 d .
H4 H 0.2833 0.4225 -0.1957 0.079 Uiso 1 1 calc R
C5 C 0.3118(9) 0.4454(12) -0.0934(7) 0.070(4) Uani 1 1 d .
H5 H 0.3769 0.4506 -0.0843 0.083 Uiso 1 1 calc R
C6 C 0.2764(8) 0.4547(10) -0.0365(6) 0.052(3) Uani 1 1 d .
C7 C 0.3401(9) 0.4740(13) 0.0311(8) 0.073(4) Uani 1 1 d .
H7 H 0.4032 0.4783 0.0333 0.087 Uiso 1 1 calc R
C8 C 0.3584(7) 0.2651(11) 0.2244(6) 0.054(3) Uani 1 1 d .
C9 C 0.3441(8) 0.1651(10) 0.1777(7) 0.056(3) Uani 1 1 d .
C10 C 0.4022(11) 0.0614(13) 0.1943(10) 0.096(5) Uani 1 1 d .
H10 H 0.3890 -0.0053 0.1649 0.115 Uiso 1 1 calc R
C11 C 0.4790(13) 0.0613(17) 0.2553(11) 0.114(7) Uani 1 1 d .
H11 H 0.5203 -0.0038 0.2652 0.137 Uiso 1 1 calc R
C12 C 0.4946(10) 0.1548(16) 0.3006(8) 0.091(5) Uani 1 1 d .
H12 H 0.5446 0.1513 0.3424 0.109 Uiso 1 1 calc R
C13 C 0.4385(9) 0.2534(13) 0.2860(7) 0.074(4) Uani 1 1 d .
H13 H 0.4529 0.3168 0.3178 0.089 Uiso 1 1 calc R
C14 C 0.2690(8) 0.1680(11) 0.1139(7) 0.062(3) Uani 1 1 d .
H14 H 0.2634 0.0992 0.0866 0.074 Uiso 1 1 calc R
C15 C -0.0178(7) 0.3178(8) 0.1125(5) 0.040(2) Uani 1 1 d .
C16 C -0.0993(8) 0.2572(10) 0.0706(6) 0.051(3) Uani 1 1 d .
H16 H -0.1160 0.2622 0.0220 0.061 Uiso 1 1 calc R
C17 C -0.1548(9) 0.1903(11) 0.1005(8) 0.072(4) Uani 1 1 d .
H17 H -0.2068 0.1497 0.0711 0.086 Uiso 1 1 calc R
C18 C -0.1357(10) 0.1816(13) 0.1728(7) 0.076(4) Uani 1 1 d .
H18 H -0.1751 0.1391 0.1922 0.092 Uiso 1 1 calc R
C19 C -0.0564(9) 0.2386(13) 0.2139(7) 0.071(4) Uani 1 1 d .
H19 H -0.0411 0.2317 0.2624 0.085 Uiso 1 1 calc R
C20 C 0.0036(8) 0.3073(9) 0.1869(5) 0.047(3) Uani 1 1 d .
C21 C 0.0732(9) 0.3758(13) 0.2338(6) 0.061(3) Uani 1 1 d .
H21 H 0.0743 0.3726 0.2803 0.073 Uiso 1 1 calc R
C22 C 0.0814(7) 0.7292(9) 0.0980(5) 0.042(2) Uani 1 1 d .
C23 C -0.0014(8) 0.7962(9) 0.0629(5) 0.045(3) Uani 1 1 d .
H23 H -0.0527 0.7583 0.0309 0.054 Uiso 1 1 calc R
C24 C -0.0055(10) 0.9157(10) 0.0761(6) 0.062(3) Uani 1 1 d .
H24 H -0.0595 0.9587 0.0519 0.074 Uiso 1 1 calc R
C25 C 0.0700(11) 0.9760(11) 0.1255(7) 0.074(4) Uani 1 1 d .
H25 H 0.0657 1.0577 0.1339 0.089 Uiso 1 1 calc R
C26 C 0.1491(10) 0.9131(10) 0.1606(7) 0.064(3) Uani 1 1 d .
H26 H 0.1987 0.9525 0.1934 0.077 Uiso 1 1 calc R
C27 C 0.1575(7) 0.7874(9) 0.1481(5) 0.047(3) Uani 1 1 d .
C28 C 0.2413(8) 0.7321(10) 0.1872(6) 0.056(3) Uani 1 1 d .
H28 H 0.2859 0.7819 0.2176 0.068 Uiso 1 1 calc R
Co Co 0.0000 0.5000 0.0000 0.0326(4) Uani 1 2 d S
Dy Dy 0.19268(3) 0.44811(4) 0.12464(2) 0.0395(2) Uani 1 1 d .
O1 O 0.1378(5) 0.4559(6) 0.0007(3) 0.0395(16) Uani 1 1 d .
O2 O 0.3258(5) 0.4864(9) 0.0887(4) 0.070(2) Uani 1 1 d .
O3 O 0.0367(4) 0.3798(6) 0.0848(3) 0.0363(15) Uani 1 1 d .
O4 O 0.1334(6) 0.4396(8) 0.2223(4) 0.061(2) Uani 1 1 d .
O5 O 0.2101(6) 0.2452(6) 0.0882(4) 0.062(2) Uani 1 1 d .
O6 O 0.3069(5) 0.3620(7) 0.2140(4) 0.061(2) Uani 1 1 d .
O7 O 0.0865(5) 0.6101(6) 0.0838(3) 0.0409(16) Uani 1 1 d .
O8 O 0.2646(5) 0.6237(8) 0.1867(4) 0.067(2) Uani 1 1 d .
O9 O 0.3230(11) 0.4581(14) 0.3677(9) 0.182(7) Uani 1 1 d U
O10 O 0.5592(12) 0.2839(17) 0.4973(9) 0.192(7) Uani 1 1 d U
O11 O 0.5454(9) 0.2021(13) 0.6278(8) 0.153(5) Uani 1 1 d U
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 C2 122.1(9) . .
O1 C1 C6 120.7(9) . .
C2 C1 C6 117.2(10) . .
C1 C2 C3 120.4(11) . .
C1 C2 H2 119.8 . .
C3 C2 H2 119.8 . .
C4 C3 C2 122.1(11) . .
C4 C3 H3 119.0 . .
C2 C3 H3 119.0 . .
C5 C4 C3 118.4(12) . .
C5 C4 H4 120.8 . .
C3 C4 H4 120.8 . .
C4 C5 C6 123.4(12) . .
C4 C5 H5 118.3 . .
C6 C5 H5 118.3 . .
C7 C6 C5 118.9(11) . .
C7 C6 C1 122.6(11) . .
C5 C6 C1 118.5(11) . .
O2 C7 C6 130.5(11) . .
O2 C7 H7 114.7 . .
C6 C7 H7 114.7 . .
O6 C8 C13 120.2(12) . .
O6 C8 C9 125.7(10) . .
C13 C8 C9 114.1(11) . .
C14 C9 C10 118.9(13) . .
C14 C9 C8 119.3(10) . .
C10 C9 C8 121.8(12) . .
C11 C10 C9 118.8(16) . .
C11 C10 H10 120.6 . .
C9 C10 H10 120.6 . .
C12 C11 C10 120.7(15) . .
C12 C11 H11 119.7 . .
C10 C11 H11 119.7 . .
C11 C12 C13 121.0(15) . .
C11 C12 H12 119.5 . .
C13 C12 H12 119.5 . .
C12 C13 C8 123.4(14) . .
C12 C13 H13 118.3 . .
C8 C13 H13 118.3 . .
O5 C14 C9 131.2(12) . .
O5 C14 H14 114.4 . .
C9 C14 H14 114.4 . .
O3 C15 C16 121.9(9) . .
O3 C15 C20 121.5(9) . .
C16 C15 C20 116.6(10) . .
C17 C16 C15 121.3(11) . .
C17 C16 H16 119.4 . .
C15 C16 H16 119.4 . .
C16 C17 C18 122.5(12) . .
C16 C17 H17 118.7 . .
C18 C17 H17 118.7 . .
C19 C18 C17 116.7(11) . .
C19 C18 H18 121.6 . .
C17 C18 H18 121.6 . .
C18 C19 C20 123.6(12) . .
C18 C19 H19 118.2 . .
C20 C19 H19 118.2 . .
C21 C20 C19 117.8(11) . .
C21 C20 C15 122.3(10) . .
C19 C20 C15 119.2(11) . .
O4 C21 C20 128.8(11) . .
O4 C21 H21 115.6 . .
C20 C21 H21 115.6 . .
O7 C22 C27 120.6(9) . .
O7 C22 C23 120.2(9) . .
C27 C22 C23 119.2(9) . .
C24 C23 C22 120.1(11) . .
C24 C23 H23 120.0 . .
C22 C23 H23 120.0 . .
C23 C24 C25 121.8(12) . .
C23 C24 H24 119.1 . .
C25 C24 H24 119.1 . .
C26 C25 C24 119.1(11) . .
C26 C25 H25 120.4 . .
C24 C25 H25 120.4 . .
C25 C26 C27 121.4(12) . .
C25 C26 H26 119.3 . .
C27 C26 H26 119.3 . .
C28 C27 C22 125.1(10) . .
C28 C27 C26 116.5(10) . .
C22 C27 C26 118.5(10) . .
O8 C28 C27 128.4(10) . .
O8 C28 H28 115.8 . .
C27 C28 H28 115.8 . .
O3 Co O3 180.0(3) . 3_565
O3 Co O1 81.0(2) . .
O3 Co O1 99.0(2) 3_565 .
O3 Co O1 99.0(2) . 3_565
O3 Co O1 81.0(2) 3_565 3_565
O1 Co O1 180.0(4) . 3_565
O3 Co O7 77.9(2) . .
O3 Co O7 102.1(2) 3_565 .
O1 Co O7 77.7(2) . .
O1 Co O7 102.3(2) 3_565 .
O3 Co O7 102.1(2) . 3_565
O3 Co O7 77.9(2) 3_565 3_565
O1 Co O7 102.3(2) . 3_565
O1 Co O7 77.7(2) 3_565 3_565
O7 Co O7 180.0(3) . 3_565
O3 Co Dy 133.36(17) . 3_565
O3 Co Dy 46.64(17) 3_565 3_565
O1 Co Dy 132.59(18) . 3_565
O1 Co Dy 47.41(18) 3_565 3_565
O7 Co Dy 132.43(17) . 3_565
O7 Co Dy 47.57(17) 3_565 3_565
O6 Dy O3 123.5(3) . .
O6 Dy O2 79.9(3) . .
O3 Dy O2 143.0(2) . .
O6 Dy O1 140.8(3) . .
O3 Dy O1 71.1(2) . .
O2 Dy O1 73.4(3) . .
O6 Dy O7 148.3(3) . .
O3 Dy O7 69.2(2) . .
O2 Dy O7 107.0(3) . .
O1 Dy O7 68.7(2) . .
O6 Dy O8 80.3(3) . .
O3 Dy O8 132.9(3) . .
O2 Dy O8 74.3(3) . .
O1 Dy O8 118.0(3) . .
O7 Dy O8 72.4(2) . .
O6 Dy O4 73.3(3) . .
O3 Dy O4 71.4(2) . .
O2 Dy O4 145.5(3) . .
O1 Dy O4 140.3(2) . .
O7 Dy O4 86.2(3) . .
O8 Dy O4 79.9(3) . .
O6 Dy O5 73.6(3) . .
O3 Dy O5 77.4(2) . .
O2 Dy O5 83.9(3) . .
O1 Dy O5 75.5(2) . .
O7 Dy O5 137.0(2) . .
O8 Dy O5 148.5(3) . .
O4 Dy O5 108.3(3) . .
C1 O1 Co 131.1(6) . .
C1 O1 Dy 137.2(6) . .
Co O1 Dy 91.5(2) . .
C7 O2 Dy 132.3(8) . .
C15 O3 Co 129.9(5) . .
C15 O3 Dy 135.0(6) . .
Co O3 Dy 92.6(2) . .
C21 O4 Dy 131.4(8) . .
C14 O5 Dy 131.6(8) . .
C8 O6 Dy 137.4(8) . .
C22 O7 Co 131.2(6) . .
C22 O7 Dy 138.0(6) . .
Co O7 Dy 90.4(2) . .
C28 O8 Dy 135.4(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.311(12) .
C1 C2 1.383(14) .
C1 C6 1.461(14) .
C2 C3 1.405(15) .
C2 H2 0.9300 .
C3 C4 1.384(16) .
C3 H3 0.9300 .
C4 C5 1.334(18) .
C4 H4 0.9300 .
C5 C6 1.406(17) .
C5 H5 0.9300 .
C6 C7 1.405(17) .
C7 O2 1.248(15) .
C7 H7 0.9300 .
C8 O6 1.302(13) .
C8 C13 1.427(16) .
C8 C9 1.427(17) .
C9 C14 1.410(16) .
C9 C10 1.417(16) .
C10 C11 1.39(2) .
C10 H10 0.9300 .
C11 C12 1.35(2) .
C11 H11 0.9300 .
C12 C13 1.354(18) .
C12 H12 0.9300 .
C13 H13 0.9300 .
C14 O5 1.219(13) .
C14 H14 0.9300 .
C15 O3 1.316(11) .
C15 C16 1.411(14) .
C15 C20 1.431(14) .
C16 C17 1.383(14) .
C16 H16 0.9300 .
C17 C18 1.393(18) .
C17 H17 0.9300 .
C18 C19 1.364(19) .
C18 H18 0.9300 .
C19 C20 1.410(15) .
C19 H19 0.9300 .
C20 C21 1.388(16) .
C21 O4 1.222(14) .
C21 H21 0.9300 .
C22 O7 1.362(12) .
C22 C27 1.413(14) .
C22 C23 1.422(14) .
C23 C24 1.360(14) .
C23 H23 0.9300 .
C24 C25 1.412(17) .
C24 H24 0.9300 .
C25 C26 1.360(18) .
C25 H25 0.9300 .
C26 C27 1.434(15) .
C26 H26 0.9300 .
C27 C28 1.391(15) .
C28 O8 1.256(13) .
C28 H28 0.9300 .
Co O3 2.097(6) .
Co O3 2.097(6) 3_565
Co O1 2.108(6) .
Co O1 2.108(6) 3_565
Co O7 2.149(6) .
Co O7 2.149(6) 3_565
Co Dy 3.2079(8) 3_565
Dy O6 2.258(7) .
Dy O3 2.335(6) .
Dy O2 2.356(8) .
Dy O1 2.363(7) .
Dy O7 2.368(6) .
Dy O8 2.381(8) .
Dy O4 2.396(8) .
Dy O5 2.412(7) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O1 C1 C2 C3 179.4(9) .
C6 C1 C2 C3 -0.5(15) .
C1 C2 C3 C4 1.1(17) .
C2 C3 C4 C5 -1.3(19) .
C3 C4 C5 C6 1(2) .
C4 C5 C6 C7 -178.6(13) .
C4 C5 C6 C1 -0.4(19) .
O1 C1 C6 C7 -1.6(17) .
C2 C1 C6 C7 178.3(12) .
O1 C1 C6 C5 -179.8(10) .
C2 C1 C6 C5 0.2(15) .
C5 C6 C7 O2 179.2(15) .
C1 C6 C7 O2 1(2) .
O6 C8 C9 C14 0.4(18) .
C13 C8 C9 C14 -177.9(11) .
O6 C8 C9 C10 -178.1(12) .
C13 C8 C9 C10 3.6(18) .
C14 C9 C10 C11 176.7(15) .
C8 C9 C10 C11 -5(2) .
C9 C10 C11 C12 5(3) .
C10 C11 C12 C13 -3(3) .
C11 C12 C13 C8 2(3) .
O6 C8 C13 C12 179.3(13) .
C9 C8 C13 C12 -2.2(19) .
C10 C9 C14 O5 179.7(14) .
C8 C9 C14 O5 1(2) .
O3 C15 C16 C17 178.6(10) .
C20 C15 C16 C17 -0.5(15) .
C15 C16 C17 C18 1.9(19) .
C16 C17 C18 C19 -3(2) .
C17 C18 C19 C20 2(2) .
C18 C19 C20 C21 170.2(13) .
C18 C19 C20 C15 -0.9(19) .
O3 C15 C20 C21 10.2(15) .
C16 C15 C20 C21 -170.6(10) .
O3 C15 C20 C19 -179.2(9) .
C16 C15 C20 C19 0.0(15) .
C19 C20 C21 O4 178.5(12) .
C15 C20 C21 O4 -10.7(19) .
O7 C22 C23 C24 -178.6(10) .
C27 C22 C23 C24 2.0(16) .
C22 C23 C24 C25 -1.5(18) .
C23 C24 C25 C26 0(2) .
C24 C25 C26 C27 0(2) .
O7 C22 C27 C28 -0.9(17) .
C23 C22 C27 C28 178.5(10) .
O7 C22 C27 C26 179.3(10) .
C23 C22 C27 C26 -1.3(15) .
C25 C26 C27 C28 -179.7(12) .
C25 C26 C27 C22 0.1(19) .
C22 C27 C28 O8 -1(2) .
C26 C27 C28 O8 178.5(12) .
C2 C1 O1 Co -20.4(14) .
C6 C1 O1 Co 159.5(7) .
C2 C1 O1 Dy 166.2(7) .
C6 C1 O1 Dy -13.9(15) .
O3 Co O1 C1 147.5(8) .
O3 Co O1 C1 -32.5(8) 3_565
O1 Co O1 C1 -4(100) 3_565
O7 Co O1 C1 -133.0(8) .
O7 Co O1 C1 47.0(8) 3_565
Dy Co O1 C1 4.5(9) 3_565
O3 Co O1 Dy -37.0(2) .
O3 Co O1 Dy 143.0(2) 3_565
O1 Co O1 Dy 172(100) 3_565
O7 Co O1 Dy 42.5(2) .
O7 Co O1 Dy -137.5(2) 3_565
Dy Co O1 Dy 180.0 3_565
O6 Dy O1 C1 -30.4(11) .
O3 Dy O1 C1 -150.7(9) .
O2 Dy O1 C1 18.7(9) .
O7 Dy O1 C1 135.0(9) .
O8 Dy O1 C1 80.1(9) .
O4 Dy O1 C1 -170.5(8) .
O5 Dy O1 C1 -69.2(9) .
O6 Dy O1 Co 154.6(3) .
O3 Dy O1 Co 34.3(2) .
O2 Dy O1 Co -156.3(3) .
O7 Dy O1 Co -40.0(2) .
O8 Dy O1 Co -94.9(3) .
O4 Dy O1 Co 14.4(5) .
O5 Dy O1 Co 115.8(3) .
C6 C7 O2 Dy 14(2) .
O6 Dy O2 C7 133.4(13) .
O3 Dy O2 C7 -0.7(16) .
O1 Dy O2 C7 -17.6(13) .
O7 Dy O2 C7 -78.5(13) .
O8 Dy O2 C7 -144.0(14) .
O4 Dy O2 C7 172.8(11) .
O5 Dy O2 C7 59.0(13) .
C16 C15 O3 Co 43.8(12) .
C20 C15 O3 Co -137.1(8) .
C16 C15 O3 Dy -159.6(7) .
C20 C15 O3 Dy 19.5(13) .
O3 Co O3 C15 -140.3(10) 3_565
O1 Co O3 C15 -158.7(8) .
O1 Co O3 C15 21.3(8) 3_565
O7 Co O3 C15 122.1(8) .
O7 Co O3 C15 -57.9(8) 3_565
Dy Co O3 C15 -16.3(8) 3_565
O3 Co O3 Dy 56.0(2) 3_565
O1 Co O3 Dy 37.5(2) .
O1 Co O3 Dy -142.5(2) 3_565
O7 Co O3 Dy -41.7(2) .
O7 Co O3 Dy 138.3(2) 3_565
Dy Co O3 Dy 180.0 3_565
O6 Dy O3 C15 24.0(9) .
O2 Dy O3 C15 146.0(8) .
O1 Dy O3 C15 163.1(8) .
O7 Dy O3 C15 -123.2(8) .
O8 Dy O3 C15 -85.8(8) .
O4 Dy O3 C15 -30.1(8) .
O5 Dy O3 C15 84.4(8) .
O6 Dy O3 Co -173.7(2) .
O2 Dy O3 Co -51.7(5) .
O1 Dy O3 Co -34.6(2) .
O7 Dy O3 Co 39.1(2) .
O8 Dy O3 Co 76.5(4) .
O4 Dy O3 Co 132.2(3) .
O5 Dy O3 Co -113.3(3) .
C20 C21 O4 Dy -17.5(19) .
O6 Dy O4 C21 -106.7(11) .
O3 Dy O4 C21 28.5(10) .
O2 Dy O4 C21 -147.4(10) .
O1 Dy O4 C21 48.3(12) .
O7 Dy O4 C21 97.8(10) .
O8 Dy O4 C21 170.5(11) .
O5 Dy O4 C21 -40.9(11) .
C9 C14 O5 Dy 6(2) .
O6 Dy O5 C14 -9.8(11) .
O3 Dy O5 C14 -140.8(11) .
O2 Dy O5 C14 71.4(11) .
O1 Dy O5 C14 145.7(11) .
O7 Dy O5 C14 179.9(10) .
O8 Dy O5 C14 25.3(14) .
O4 Dy O5 C14 -75.5(11) .
C13 C8 O6 Dy 167.1(8) .
C9 C8 O6 Dy -11.2(18) .
O3 Dy O6 C8 74.7(11) .
O2 Dy O6 C8 -74.0(11) .
O1 Dy O6 C8 -26.7(13) .
O7 Dy O6 C8 179.9(9) .
O8 Dy O6 C8 -149.7(11) .
O4 Dy O6 C8 128.0(11) .
O5 Dy O6 C8 12.6(10) .
C27 C22 O7 Co -166.8(7) .
C23 C22 O7 Co 13.8(13) .
C27 C22 O7 Dy 3.7(15) .
C23 C22 O7 Dy -175.7(6) .
O3 Co O7 C22 -145.4(8) .
O3 Co O7 C22 34.6(8) 3_565
O1 Co O7 C22 131.3(8) .
O1 Co O7 C22 -48.7(8) 3_565
O7 Co O7 C22 51(9) 3_565
Dy Co O7 C22 -6.3(9) 3_565
O3 Co O7 Dy 40.9(2) .
O3 Co O7 Dy -139.1(2) 3_565
O1 Co O7 Dy -42.4(2) .
O1 Co O7 Dy 137.6(2) 3_565
O7 Co O7 Dy -123(9) 3_565
Dy Co O7 Dy 180.0 3_565
O6 Dy O7 C22 28.5(11) .
O3 Dy O7 C22 149.2(9) .
O2 Dy O7 C22 -69.9(9) .
O1 Dy O7 C22 -133.8(9) .
O8 Dy O7 C22 -3.0(9) .
O4 Dy O7 C22 77.6(9) .
O5 Dy O7 C22 -169.4(8) .
O6 Dy O7 Co -158.6(4) .
O3 Dy O7 Co -38.0(2) .
O2 Dy O7 Co 103.0(3) .
O1 Dy O7 Co 39.1(2) .
O8 Dy O7 Co 169.8(3) .
O4 Dy O7 Co -109.5(3) .
O5 Dy O7 Co 3.5(5) .
C27 C28 O8 Dy 1(2) .
O6 Dy O8 C28 -163.1(12) .
O3 Dy O8 C28 -35.8(13) .
O2 Dy O8 C28 114.7(12) .
O1 Dy O8 C28 53.8(12) .
O7 Dy O8 C28 0.7(11) .
O4 Dy O8 C28 -88.5(12) .
O5 Dy O8 C28 162.8(10) .
