#------------------------------------------------------------------------------
#$Date: 2025-08-21 02:27:06 +0300 (Thu, 21 Aug 2025) $
#$Revision: 301840 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/32/4343236.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4343236
loop_
_publ_author_name
'Li, Xiao-Lei'
'Min, Fan-Yong'
'Wang, Chao'
'Lin, Shuang-Yan'
'Liu, Zhiliang'
'Tang, Jinkui'
_publ_section_title
;
 Utilizing 3d-4f magnetic interaction to slow the magnetic relaxation of
 heterometallic complexes.
;
_journal_issue                   9
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4337
_journal_page_last               4344
_journal_paper_doi               10.1021/acs.inorgchem.5b00019
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'C28 H20 Cd0.5 Dy O8'
_chemical_formula_weight         703.14
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                95.506(7)
_cell_angle_beta                 113.574(6)
_cell_angle_gamma                93.738(7)
_cell_formula_units_Z            2
_cell_length_a                   10.024(4)
_cell_length_b                   11.080(4)
_cell_length_c                   12.217(5)
_cell_measurement_reflns_used    2582
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      25.26
_cell_measurement_theta_min      2.24
_cell_volume                     1229.9(8)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0280
_diffrn_reflns_av_sigmaI/netI    0.0626
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            6288
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    3.510
_exptl_absorpt_correction_T_max  0.6393
_exptl_absorpt_correction_T_min  0.5403
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   crystalclear
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.899
_exptl_crystal_density_meas      1.895
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             684
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.14
_refine_diff_density_max         1.147
_refine_diff_density_min         -0.807
_refine_diff_density_rms         0.130
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.995
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     340
_refine_ls_number_reflns         4285
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.995
_refine_ls_R_factor_all          0.0610
_refine_ls_R_factor_gt           0.0408
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0402P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0831
_refine_ls_wR_factor_ref         0.0912
_reflns_number_gt                3247
_reflns_number_total             4285
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic5b00019_si_002.cif
_cod_data_source_block           Dy2Cd
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'multi_scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C28 H20 Cd0.50 Dy O8'
_cod_database_code               4343236
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.8419(8) -0.1236(6) 0.1573(6) 0.0408(17) Uani 1 1 d .
C2 C 0.7346(8) -0.2042(7) 0.0650(7) 0.053(2) Uani 1 1 d .
H2 H 0.7099 -0.1916 -0.0163 0.063 Uiso 1 1 calc R
C3 C 0.6642(10) -0.3012(8) 0.0891(8) 0.071(2) Uani 1 1 d .
H3 H 0.5894 -0.3529 0.0240 0.085 Uiso 1 1 calc R
C4 C 0.6983(11) -0.3263(8) 0.2045(10) 0.077(3) Uani 1 1 d .
H4 H 0.6467 -0.3933 0.2194 0.092 Uiso 1 1 calc R
C5 C 0.8071(9) -0.2534(8) 0.2968(8) 0.056(2) Uani 1 1 d .
H5 H 0.8338 -0.2713 0.3769 0.067 Uiso 1 1 calc R
C6 C 0.8795(8) -0.1540(7) 0.2764(7) 0.0456(18) Uani 1 1 d .
C7 C 0.9969(9) -0.0842(7) 0.3775(6) 0.052(2) Uani 1 1 d .
H7 H 1.0294 -0.1194 0.4504 0.062 Uiso 1 1 calc R
C8 C 1.3206(7) 0.0691(6) 0.2396(6) 0.0369(16) Uani 1 1 d .
C9 C 1.3839(7) -0.0056(7) 0.1785(6) 0.0456(18) Uani 1 1 d .
H9 H 1.3293 -0.0375 0.0962 0.055 Uiso 1 1 calc R
C10 C 1.5235(9) -0.0320(7) 0.2374(7) 0.058(2) Uani 1 1 d .
H10 H 1.5638 -0.0848 0.1958 0.070 Uiso 1 1 calc R
C11 C 1.6093(9) 0.0163(8) 0.3573(8) 0.063(2) Uani 1 1 d .
H11 H 1.7066 -0.0032 0.3973 0.076 Uiso 1 1 calc R
C12 C 1.5505(8) 0.0910(8) 0.4141(7) 0.060(2) Uani 1 1 d .
H12 H 1.6085 0.1251 0.4952 0.072 Uiso 1 1 calc R
C13 C 1.4067(8) 0.1210(7) 0.3589(6) 0.0470(18) Uani 1 1 d .
C14 C 1.3605(9) 0.2053(7) 0.4274(7) 0.057(2) Uani 1 1 d .
H14 H 1.4304 0.2369 0.5061 0.068 Uiso 1 1 calc R
C15 C 0.8890(7) 0.2691(6) -0.0282(6) 0.0413(17) Uani 1 1 d .
C16 C 0.8406(8) 0.2412(7) -0.1546(6) 0.0470(18) Uani 1 1 d .
H16 H 0.8549 0.1644 -0.1874 0.056 Uiso 1 1 calc R
C17 C 0.7738(9) 0.3228(8) -0.2299(7) 0.064(2) Uani 1 1 d .
H17 H 0.7427 0.3018 -0.3144 0.077 Uiso 1 1 calc R
C18 C 0.7503(10) 0.4355(9) -0.1859(8) 0.074(3) Uani 1 1 d .
H18 H 0.7004 0.4902 -0.2397 0.089 Uiso 1 1 calc R
C19 C 0.7993(10) 0.4669(8) -0.0654(9) 0.076(3) Uani 1 1 d .
H19 H 0.7856 0.5452 -0.0353 0.092 Uiso 1 1 calc R
C20 C 0.8712(8) 0.3856(7) 0.0176(7) 0.051(2) Uani 1 1 d .
C21 C 0.9310(9) 0.4303(8) 0.1419(8) 0.061(2) Uani 1 1 d .
H21 H 0.9187 0.5125 0.1623 0.073 Uiso 1 1 calc R
C22 C 0.6952(8) 0.3031(7) 0.2896(7) 0.0483(19) Uani 1 1 d .
C23 C 0.5873(9) 0.3748(8) 0.2997(8) 0.063(2) Uani 1 1 d .
H23 H 0.4937 0.3687 0.2345 0.076 Uiso 1 1 calc R
C24 C 0.6170(9) 0.4528(7) 0.4026(7) 0.058(2) Uani 1 1 d .
H24 H 0.5445 0.5006 0.4092 0.070 Uiso 1 1 calc R
C25 C 0.7517(10) 0.4612(8) 0.4955(7) 0.068(2) Uani 1 1 d .
H25 H 0.7735 0.5187 0.5649 0.081 Uiso 1 1 calc R
C26 C 0.8560(9) 0.3897(7) 0.4922(7) 0.057(2) Uani 1 1 d .
H26 H 0.9459 0.3944 0.5611 0.068 Uiso 1 1 calc R
C27 C 0.8327(8) 0.3095(7) 0.3887(6) 0.0452(18) Uani 1 1 d .
C28 C 0.6624(9) 0.2264(7) 0.1819(7) 0.057(2) Uani 1 1 d .
H28 H 0.5633 0.2188 0.1250 0.068 Uiso 1 1 calc R
Cd Cd 1.0000 0.0000 0.0000 0.03712(19) Uani 1 2 d S
Dy Dy 1.00280(4) 0.16530(3) 0.24453(3) 0.03958(13) Uani 1 1 d .
O1 O 0.9038(5) -0.0274(4) 0.1361(4) 0.0372(11) Uani 1 1 d .
O2 O 1.0612(6) 0.0165(5) 0.3817(4) 0.0564(14) Uani 1 1 d .
O3 O 1.1814(5) 0.0892(4) 0.1856(4) 0.0423(12) Uani 1 1 d .
O4 O 1.2370(6) 0.2421(5) 0.3947(4) 0.0586(14) Uani 1 1 d .
O5 O 0.9485(5) 0.1900(4) 0.0429(4) 0.0412(11) Uani 1 1 d .
O6 O 0.9968(6) 0.3752(5) 0.2261(5) 0.0605(15) Uani 1 1 d .
O7 O 0.9330(5) 0.2412(5) 0.3874(4) 0.0510(13) Uani 1 1 d .
O8 O 0.7438(5) 0.1678(5) 0.1513(4) 0.0561(14) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 C1 C2 121.9(6) . .
O1 C1 C6 122.4(7) . .
C2 C1 C6 115.7(7) . .
C3 C2 C1 121.3(8) . .
C2 C3 C4 122.0(9) . .
C5 C4 C3 118.6(8) . .
C4 C5 C6 121.1(8) . .
C5 C6 C1 121.1(8) . .
C5 C6 C7 118.0(7) . .
C1 C6 C7 120.9(7) . .
O2 C7 C6 127.9(7) . .
O3 C8 C13 120.7(6) . .
O3 C8 C9 120.5(6) . .
C13 C8 C9 118.8(6) . .
C10 C9 C8 119.9(7) . .
C9 C10 C11 122.0(7) . .
C12 C11 C10 118.0(7) . .
C11 C12 C13 122.9(8) . .
C8 C13 C12 118.4(6) . .
C8 C13 C14 124.6(6) . .
C12 C13 C14 117.0(7) . .
O4 C14 C13 126.5(7) . .
O5 C15 C20 121.2(6) . .
O5 C15 C16 120.9(6) . .
C20 C15 C16 117.9(6) . .
C17 C16 C15 121.1(7) . .
C16 C17 C18 121.3(8) . .
C19 C18 C17 119.2(8) . .
C18 C19 C20 121.7(8) . .
C15 C20 C21 123.5(7) . .
C15 C20 C19 118.6(7) . .
C21 C20 C19 117.7(7) . .
O6 C21 C20 127.4(8) . .
C28 C22 C27 121.5(7) . .
C28 C22 C23 119.1(7) . .
C27 C22 C23 119.4(7) . .
C24 C23 C22 120.5(8) . .
C25 C24 C23 119.2(7) . .
C26 C25 C24 122.2(8) . .
C25 C26 C27 121.0(8) . .
O7 C27 C26 120.2(7) . .
O7 C27 C22 122.3(6) . .
C26 C27 C22 117.4(7) . .
O8 C28 C22 128.8(7) . .
O5 Cd O5 180.0(3) 2_755 .
O5 Cd O1 77.89(16) 2_755 2_755
O5 Cd O1 102.11(16) . 2_755
O5 Cd O1 102.11(16) 2_755 .
O5 Cd O1 77.89(16) . .
O1 Cd O1 180.0(3) 2_755 .
O5 Cd O3 108.67(15) 2_755 .
O5 Cd O3 71.33(15) . .
O1 Cd O3 105.22(16) 2_755 .
O1 Cd O3 74.78(16) . .
O5 Cd O3 71.33(15) 2_755 2_755
O5 Cd O3 108.67(15) . 2_755
O1 Cd O3 74.78(16) 2_755 2_755
O1 Cd O3 105.22(16) . 2_755
O3 Cd O3 180.00(17) . 2_755
O5 Cd Dy 44.62(11) 2_755 2_755
O5 Cd Dy 135.38(11) . 2_755
O1 Cd Dy 44.14(11) 2_755 2_755
O1 Cd Dy 135.86(11) . 2_755
O3 Cd Dy 135.18(10) . 2_755
O3 Cd Dy 44.82(10) 2_755 2_755
O7 Dy O1 120.77(17) . .
O7 Dy O5 136.32(15) . .
O1 Dy O5 74.92(15) . .
O7 Dy O3 150.86(16) . .
O1 Dy O3 73.25(15) . .
O5 Dy O3 69.54(15) . .
O7 Dy O6 75.52(18) . .
O1 Dy O6 142.08(17) . .
O5 Dy O6 71.54(16) . .
O3 Dy O6 109.95(17) . .
O7 Dy O4 81.63(18) . .
O1 Dy O4 132.72(16) . .
O5 Dy O4 119.20(18) . .
O3 Dy O4 71.56(16) . .
O6 Dy O4 80.34(19) . .
O7 Dy O8 72.83(16) . .
O1 Dy O8 73.19(16) . .
O5 Dy O8 74.44(16) . .
O3 Dy O8 135.71(15) . .
O6 Dy O8 81.16(19) . .
O4 Dy O8 151.48(17) . .
O7 Dy O2 76.84(17) . .
O1 Dy O2 71.14(17) . .
O5 Dy O2 142.40(16) . .
O3 Dy O2 85.43(16) . .
O6 Dy O2 145.47(18) . .
O4 Dy O2 75.5(2) . .
O8 Dy O2 109.78(19) . .
C1 O1 Cd 132.0(4) . .
C1 O1 Dy 133.6(4) . .
Cd O1 Dy 93.25(16) . .
C7 O2 Dy 131.5(5) . .
C8 O3 Cd 129.9(4) . .
C8 O3 Dy 136.8(4) . .
Cd O3 Dy 90.78(15) . .
C14 O4 Dy 133.7(5) . .
C15 O5 Cd 130.1(4) . .
C15 O5 Dy 136.2(4) . .
Cd O5 Dy 92.80(15) . .
C21 O6 Dy 132.5(5) . .
C27 O7 Dy 134.3(4) . .
C28 O8 Dy 130.9(5) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O1 1.298(8) .
C1 C2 1.392(10) .
C1 C6 1.429(9) .
C2 C3 1.367(11) .
C3 C4 1.373(11) .
C4 C5 1.356(12) .
C5 C6 1.377(10) .
C6 C7 1.429(10) .
C7 O2 1.238(8) .
C8 O3 1.329(7) .
C8 C13 1.402(9) .
C8 C9 1.405(9) .
C9 C10 1.360(9) .
C10 C11 1.398(11) .
C11 C12 1.340(10) .
C12 C13 1.404(9) .
C13 C14 1.416(10) .
C14 O4 1.249(8) .
C15 O5 1.295(7) .
C15 C20 1.407(9) .
C15 C16 1.416(9) .
C16 C17 1.363(9) .
C17 C18 1.384(11) .
C18 C19 1.353(11) .
C19 C20 1.427(10) .
C20 C21 1.414(10) .
C21 O6 1.223(8) .
C22 C28 1.402(10) .
C22 C27 1.416(10) .
C22 C23 1.420(10) .
C23 C24 1.369(11) .
C24 C25 1.363(11) .
C25 C26 1.363(10) .
C26 C27 1.401(10) .
C27 O7 1.302(7) .
C28 O8 1.222(8) .
Cd O5 2.263(4) 2_755
Cd O5 2.263(4) .
Cd O1 2.265(4) 2_755
Cd O1 2.265(4) .
Cd O3 2.337(4) .
Cd O3 2.337(4) 2_755
Cd Dy 3.3400(11) 2_755
Dy O7 2.240(4) .
Dy O1 2.330(4) .
Dy O5 2.349(4) .
Dy O3 2.355(4) .
Dy O6 2.360(5) .
Dy O4 2.366(5) .
Dy O8 2.385(5) .
Dy O2 2.396(5) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
O1 C1 C2 C3 -176.1(7) .
C6 C1 C2 C3 4.2(10) .
C1 C2 C3 C4 -2.0(13) .
C2 C3 C4 C5 -1.2(13) .
C3 C4 C5 C6 1.9(13) .
C4 C5 C6 C1 0.4(11) .
C4 C5 C6 C7 -177.5(7) .
O1 C1 C6 C5 176.9(6) .
C2 C1 C6 C5 -3.4(9) .
O1 C1 C6 C7 -5.2(10) .
C2 C1 C6 C7 174.5(6) .
C5 C6 C7 O2 -168.8(7) .
C1 C6 C7 O2 13.2(11) .
O3 C8 C9 C10 -175.6(7) .
C13 C8 C9 C10 3.8(11) .
C8 C9 C10 C11 -2.1(12) .
C9 C10 C11 C12 -0.2(13) .
C10 C11 C12 C13 0.8(13) .
O3 C8 C13 C12 176.2(6) .
C9 C8 C13 C12 -3.2(11) .
O3 C8 C13 C14 -5.8(12) .
C9 C8 C13 C14 174.8(7) .
C11 C12 C13 C8 0.9(12) .
C11 C12 C13 C14 -177.3(8) .
C8 C13 C14 O4 2.8(14) .
C12 C13 C14 O4 -179.2(8) .
O5 C15 C16 C17 178.0(7) .
C20 C15 C16 C17 -2.4(11) .
C15 C16 C17 C18 -0.2(13) .
C16 C17 C18 C19 2.4(14) .
C17 C18 C19 C20 -1.7(15) .
O5 C15 C20 C21 7.8(12) .
C16 C15 C20 C21 -171.8(7) .
O5 C15 C20 C19 -177.4(7) .
C16 C15 C20 C19 3.0(11) .
C18 C19 C20 C15 -0.9(13) .
C18 C19 C20 C21 174.1(9) .
C15 C20 C21 O6 -4.8(14) .
C19 C20 C21 O6 -179.6(8) .
C28 C22 C23 C24 -178.5(8) .
C27 C22 C23 C24 2.2(12) .
C22 C23 C24 C25 0.1(13) .
C23 C24 C25 C26 -3.5(14) .
C24 C25 C26 C27 4.4(14) .
C25 C26 C27 O7 -179.4(7) .
C25 C26 C27 C22 -1.9(12) .
C28 C22 C27 O7 -3.1(12) .
C23 C22 C27 O7 176.2(7) .
C28 C22 C27 C26 179.4(7) .
C23 C22 C27 C26 -1.3(11) .
C27 C22 C28 O8 -8.9(14) .
C23 C22 C28 O8 171.8(8) .
C2 C1 O1 Cd -46.5(9) .
C6 C1 O1 Cd 133.2(5) .
C2 C1 O1 Dy 149.5(5) .
C6 C1 O1 Dy -30.9(9) .
O5 Cd O1 C1 -23.0(6) 2_755
O5 Cd O1 C1 157.0(6) .
O1 Cd O1 C1 0(100) 2_755
O3 Cd O1 C1 -129.3(6) .
O3 Cd O1 C1 50.7(6) 2_755
Dy Cd O1 C1 11.5(6) 2_755
O5 Cd O1 Dy 145.51(15) 2_755
O5 Cd O1 Dy -34.49(15) .
O1 Cd O1 Dy 0(100) 2_755
O3 Cd O1 Dy 39.19(14) .
O3 Cd O1 Dy -140.81(14) 2_755
Dy Cd O1 Dy 180.0 2_755
O7 Dy O1 C1 -23.0(6) .
O5 Dy O1 C1 -158.3(6) .
O3 Dy O1 C1 129.0(6) .
O6 Dy O1 C1 -129.9(5) .
O4 Dy O1 C1 85.7(6) .
O8 Dy O1 C1 -80.3(6) .
O2 Dy O1 C1 38.1(5) .
O7 Dy O1 Cd 168.87(14) .
O5 Dy O1 Cd 33.53(14) .
O3 Dy O1 Cd -39.20(14) .
O6 Dy O1 Cd 62.0(3) .
O4 Dy O1 Cd -82.5(2) .
O8 Dy O1 Cd 111.48(18) .
O2 Dy O1 Cd -130.05(19) .
C6 C7 O2 Dy 13.3(11) .
O7 Dy O2 C7 100.9(6) .
O1 Dy O2 C7 -28.5(6) .
O5 Dy O2 C7 -55.1(7) .
O3 Dy O2 C7 -102.4(6) .
O6 Dy O2 C7 138.4(6) .
O4 Dy O2 C7 -174.5(7) .
O8 Dy O2 C7 34.9(7) .
C13 C8 O3 Cd -171.5(5) .
C9 C8 O3 Cd 7.9(9) .
C13 C8 O3 Dy -15.1(10) .
C9 C8 O3 Dy 164.3(5) .
O5 Cd O3 C8 27.6(6) 2_755
O5 Cd O3 C8 -152.4(6) .
O1 Cd O3 C8 -54.5(5) 2_755
O1 Cd O3 C8 125.5(5) .
O3 Cd O3 C8 0(100) 2_755
Dy Cd O3 C8 -15.9(6) 2_755
O5 Cd O3 Dy -136.53(15) 2_755
O5 Cd O3 Dy 43.47(15) .
O1 Cd O3 Dy 141.37(15) 2_755
O1 Cd O3 Dy -38.63(15) .
O3 Cd O3 Dy 0(100) 2_755
Dy Cd O3 Dy 180.0 2_755
O7 Dy O3 C8 -0.5(8) .
O1 Dy O3 C8 -124.4(6) .
O5 Dy O3 C8 155.8(6) .
O6 Dy O3 C8 95.5(6) .
O4 Dy O3 C8 23.5(6) .
O8 Dy O3 C8 -166.6(6) .
O2 Dy O3 C8 -52.8(6) .
O7 Dy O3 Cd 161.6(3) .
O1 Dy O3 Cd 37.69(14) .
O5 Dy O3 Cd -42.07(15) .
O6 Dy O3 Cd -102.41(18) .
O4 Dy O3 Cd -174.4(2) .
O8 Dy O3 Cd -4.5(3) .
O2 Dy O3 Cd 109.35(18) .
C13 C14 O4 Dy 20.6(13) .
O7 Dy O4 C14 142.9(7) .
O1 Dy O4 C14 18.3(8) .
O5 Dy O4 C14 -78.1(7) .
O3 Dy O4 C14 -25.6(7) .
O6 Dy O4 C14 -140.5(8) .
O8 Dy O4 C14 169.3(6) .
O2 Dy O4 C14 64.4(7) .
C20 C15 O5 Cd -177.6(5) .
C16 C15 O5 Cd 2.0(9) .
C20 C15 O5 Dy 16.0(10) .
C16 C15 O5 Dy -164.4(5) .
O5 Cd O5 C15 78(100) 2_755
O1 Cd O5 C15 43.5(6) 2_755
O1 Cd O5 C15 -136.5(6) .
O3 Cd O5 C15 145.7(6) .
O3 Cd O5 C15 -34.3(6) 2_755
Dy Cd O5 C15 9.4(6) 2_755
O5 Cd O5 Dy -111(100) 2_755
O1 Cd O5 Dy -145.84(15) 2_755
O1 Cd O5 Dy 34.16(15) .
O3 Cd O5 Dy -43.66(15) .
O3 Cd O5 Dy 136.34(15) 2_755
Dy Cd O5 Dy 180.0 2_755
O7 Dy O5 C15 17.0(7) .
O1 Dy O5 C15 136.1(6) .
O3 Dy O5 C15 -146.5(6) .
O6 Dy O5 C15 -26.0(6) .
O4 Dy O5 C15 -93.1(6) .
O8 Dy O5 C15 59.7(6) .
O2 Dy O5 C15 162.1(6) .
O7 Dy O5 Cd -152.6(2) .
O1 Dy O5 Cd -33.55(15) .
O3 Dy O5 Cd 43.86(15) .
O6 Dy O5 Cd 164.4(2) .
O4 Dy O5 Cd 97.32(19) .
O8 Dy O5 Cd -109.90(19) .
O2 Dy O5 Cd -7.5(3) .
C20 C21 O6 Dy -21.4(13) .
O7 Dy O6 C21 -123.1(7) .
O1 Dy O6 C21 -1.2(8) .
O5 Dy O6 C21 27.8(7) .
O3 Dy O6 C21 86.9(7) .
O4 Dy O6 C21 153.1(7) .
O8 Dy O6 C21 -48.7(7) .
O2 Dy O6 C21 -160.9(6) .
C26 C27 O7 Dy -148.5(6) .
C22 C27 O7 Dy 34.1(11) .
O1 Dy O7 C27 -92.3(7) .
O5 Dy O7 C27 8.4(8) .
O3 Dy O7 C27 155.4(6) .
O6 Dy O7 C27 50.3(7) .
O4 Dy O7 C27 132.5(7) .
O8 Dy O7 C27 -34.7(7) .
O2 Dy O7 C27 -150.5(7) .
C22 C28 O8 Dy -7.0(13) .
O7 Dy O8 C28 20.6(7) .
O1 Dy O8 C28 151.3(7) .
O5 Dy O8 C28 -130.1(7) .
O3 Dy O8 C28 -166.5(6) .
O6 Dy O8 C28 -56.9(7) .
O4 Dy O8 C28 -6.9(9) .
O2 Dy O8 C28 89.2(7) .
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1 PubChem 139143130
