#------------------------------------------------------------------------------
#$Date: 2019-11-23 04:09:40 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232084 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/69/4346964.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4346964
loop_
_publ_author_name
'Oms, Olivier'
'Yang, Shu'
'Salomon, William'
'Marrot, Jérôme'
'Dolbecq, Anne'
'Rivière, Eric'
'Bonnefont, Antoine'
'Ruhlmann, Laurent'
'Mialane, Pierre'
_publ_section_title
;
 Heteroanionic Materials Based on Copper Clusters, Bisphosphonates, and
 Polyoxometalates: Magnetic Properties and Comparative Electrocatalytic
 NO(x) Reduction Studies.
;
_journal_issue                   4
_journal_name_full               'Inorganic chemistry'
_journal_page_first              1551
_journal_page_last               1561
_journal_paper_doi               10.1021/acs.inorgchem.5b02456
_journal_volume                  55
_journal_year                    2016
_chemical_formula_sum            'C16 H36 Cu10 N4 Na10 O181 P12 W30'
_chemical_formula_weight         9932.93
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 93.400(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   32.256(3)
_cell_length_b                   28.454(3)
_cell_length_c                   27.131(2)
_cell_measurement_reflns_used    9615
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      24.99
_cell_measurement_theta_min      2.49
_cell_volume                     24857(4)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      200(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1015
_diffrn_reflns_av_unetI/netI     0.0510
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       33
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            656657
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        25.095
_diffrn_reflns_theta_max         25.095
_diffrn_reflns_theta_min         0.632
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    14.838
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS (Sheldrick, V2014/5)'
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    2.654
_exptl_crystal_description       parallelepiped
_exptl_crystal_F_000             17632
_exptl_crystal_size_max          0.160
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.060
_exptl_transmission_factor_max   0.7452
_exptl_transmission_factor_min   0.4883
_refine_diff_density_max         10.007
_refine_diff_density_min         -3.666
_refine_diff_density_rms         0.660
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.037
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2165
_refine_ls_number_reflns         43911
_refine_ls_number_restraints     1148
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.1101
_refine_ls_R_factor_gt           0.0806
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1108P)²+3498.7024P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2163
_refine_ls_wR_factor_ref         0.2422
_reflns_Friedel_coverage         0.000
_reflns_number_gt                31692
_reflns_number_total             43911
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic5b02456_si_002.cif
_cod_data_source_block           P2W15Cuale_
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4346964
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.200
_shelx_estimated_absorpt_t_max   0.470
_exptl_absorpt_special_details   'Blessing, Acta Cryst. (1995) A51, 33-38'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
W1 W 0.86219(2) 0.64597(2) -0.09196(2) 0.01324(12) Uani 1 1 d . U .
W2 W 0.90892(2) 0.74177(2) -0.03789(2) 0.01276(9) Uani 1 1 d . U .
W3 W 0.90897(2) 0.63674(2) 0.02333(2) 0.01417(13) Uani 1 1 d . U .
W4 W 0.86182(2) 0.69444(2) 0.12945(2) 0.01419(9) Uani 1 1 d . U .
W5 W 0.80942(2) 0.59212(2) 0.06925(2) 0.01276(9) Uani 1 1 d . U .
W6 W 0.76352(2) 0.60118(2) -0.04410(2) 0.01379(12) Uani 1 1 d . U .
W7 W 0.76472(2) 0.71604(2) -0.10741(2) 0.01133(12) Uani 1 1 d . U .
W8 W 0.80989(2) 0.81013(2) -0.05377(2) 0.01107(12) Uani 1 1 d . U .
W9 W 0.86242(2) 0.79813(2) 0.07069(2) 0.01089(12) Uani 1 1 d . U .
W10 W 0.76082(2) 0.83135(2) 0.12776(2) 0.00971(12) Uani 1 1 d . U .
W11 W 0.76011(2) 0.72759(2) 0.18663(2) 0.01044(12) Uani 1 1 d . U .
W12 W 0.70796(2) 0.62747(2) 0.12562(2) 0.01252(12) Uani 1 1 d . U .
W13 W 0.66221(2) 0.63596(2) 0.01143(2) 0.01228(12) Uani 1 1 d . U .
W14 W 0.66320(2) 0.74901(2) -0.05106(2) 0.01089(12) Uani 1 1 d . U .
W15 W 0.70834(2) 0.84197(2) 0.00607(2) 0.01014(12) Uani 1 1 d . U .
W16 W 0.48420(2) 0.77457(2) -0.00809(2) 0.01447(13) Uani 1 1 d . U .
W17 W 0.53669(2) 0.87386(2) 0.05383(2) 0.01459(13) Uani 1 1 d . U .
W18 W 0.58237(2) 0.86568(2) 0.16822(2) 0.01272(12) Uani 1 1 d . U .
W19 W 0.58041(2) 0.75318(2) 0.23116(2) 0.01248(12) Uani 1 1 d . U .
W20 W 0.53456(2) 0.66087(2) 0.17391(2) 0.01389(13) Uani 1 1 d . U .
W21 W 0.48253(2) 0.67187(2) 0.05162(2) 0.01472(13) Uani 1 1 d . U .
W22 W 0.38079(2) 0.70669(2) 0.10801(2) 0.01597(13) Uani 1 1 d . U .
W23 W 0.38291(2) 0.81017(2) 0.04880(2) 0.01568(13) Uani 1 1 d . U .
W24 W 0.43581(2) 0.91186(2) 0.10941(2) 0.01749(13) Uani 1 1 d . U .
W25 W 0.48122(2) 0.90168(2) 0.22292(2) 0.01631(13) Uani 1 1 d . U .
W26 W 0.47866(2) 0.78694(2) 0.28679(2) 0.01570(13) Uani 1 1 d . U .
W27 W 0.43279(2) 0.69360(2) 0.23256(2) 0.01592(13) Uani 1 1 d . U .
W28 W 0.33446(2) 0.76319(2) 0.21626(2) 0.01419(9) Uani 1 1 d . U .
W29 W 0.33595(2) 0.86836(2) 0.15483(2) 0.01776(14) Uani 1 1 d . U .
W30 W 0.38206(2) 0.85860(2) 0.27061(2) 0.01761(13) Uani 1 1 d . U .
Cu1 Cu 0.62212(5) 0.79832(6) 0.06364(6) 0.0132(4) Uani 1 1 d . U .
Cu2 Cu 0.66664(5) 0.79065(6) 0.17129(6) 0.0119(4) Uani 1 1 d . U .
Cu3 Cu 0.62180(5) 0.70282(6) 0.11662(6) 0.0126(4) Uani 1 1 d . U .
Cu4 Cu 0.57725(5) 0.71057(6) 0.00835(6) 0.0144(4) Uani 1 1 d . U .
Cu5 Cu 0.01031(5) 0.70987(6) 0.40955(6) 0.0155(3) Uani 1 1 d . U .
Cu6 Cu 0.02721(5) 0.61478(6) 0.40189(6) 0.0174(4) Uani 1 1 d . U .
Cu7 Cu 0.15651(5) 0.65694(6) 0.41936(6) 0.0200(4) Uani 1 1 d . U .
Cu8 Cu 0.08390(5) 0.66361(6) 0.25226(6) 0.0210(4) Uani 1 1 d . U .
Cu9 Cu 0.23290(5) 0.71237(6) 0.27036(6) 0.0157(3) Uani 1 1 d . U .
Cu10 Cu 0.21626(5) 0.61684(6) 0.27753(6) 0.0161(3) Uani 1 1 d . U .
P1 P 0.81648(11) 0.70084(13) 0.00770(13) 0.0157(3) Uani 1 1 d . U .
P2 P 0.70587(11) 0.73680(13) 0.06993(13) 0.0155(3) Uani 1 1 d . U .
P3 P 0.53796(11) 0.76511(13) 0.10975(13) 0.0174(4) Uani 1 1 d . U .
P4 P 0.42727(11) 0.80349(13) 0.17046(13) 0.0161(3) Uani 1 1 d . U .
P5 P 0.01583(11) 0.71471(14) 0.30469(14) 0.0199(8) Uani 1 1 d . U .
P6 P 0.01035(11) 0.60813(13) 0.29279(13) 0.0178(8) Uani 1 1 d . U .
P7 P 0.08776(11) 0.71600(14) 0.46342(14) 0.0193(8) Uani 1 1 d . U .
P8 P 0.09255(11) 0.61056(13) 0.48427(14) 0.0185(8) Uani 1 1 d . U .
P9 P 0.22595(11) 0.71472(13) 0.37452(13) 0.0178(8) Uani 1 1 d . U .
P10 P 0.23626(11) 0.60744(14) 0.38544(13) 0.0180(8) Uani 1 1 d . U .
P11 P 0.15638(11) 0.71953(13) 0.21354(13) 0.0165(8) Uani 1 1 d . U .
P12 P 0.15060(11) 0.61419(13) 0.19583(13) 0.0175(8) Uani 1 1 d . U .
O1 O 0.8749(3) 0.6194(4) -0.1455(3) 0.0222(13) Uani 1 1 d . U .
O2 O 0.8204(3) 0.6080(3) -0.0692(3) 0.0168(16) Uani 1 1 d . U .
O3 O 0.8209(3) 0.6900(3) -0.1136(3) 0.0142(15) Uani 1 1 d . U .
O4 O 0.9011(3) 0.6169(3) -0.0451(3) 0.0178(16) Uani 1 1 d . U .
O5 O 0.9015(3) 0.6980(3) -0.0923(3) 0.0168(12) Uani 1 1 d . U .
O6 O 0.8584(3) 0.6879(3) -0.0158(3) 0.0151(14) Uani 1 1 d . U .
O7 O -0.0482(3) 0.7283(4) 0.4428(4) 0.0228(19) Uani 1 1 d . U .
O8 O 0.9016(3) 0.7681(3) 0.0239(3) 0.0136(16) Uani 1 1 d . U .
O9 O 0.8644(3) 0.7776(3) -0.0643(3) 0.0129(16) Uani 1 1 d . U .
O10 O 0.9384(3) 0.6911(3) -0.0033(3) 0.0168(11) Uani 1 1 d . U .
O11 O 0.9517(3) 0.6027(4) 0.0417(3) 0.0222(13) Uani 1 1 d . U .
O12 O 0.9001(3) 0.6725(3) 0.0800(3) 0.0152(16) Uani 1 1 d . U .
O13 O 0.8635(3) 0.6000(3) 0.0372(4) 0.0183(16) Uani 1 1 d . U .
O14 O 0.8925(3) 0.6821(4) 0.1815(3) 0.0187(13) Uani 1 1 d . U .
O15 O 0.8170(3) 0.7169(3) 0.1591(3) 0.0174(16) Uani 1 1 d . U .
O16 O 0.8323(3) 0.6383(3) 0.1127(3) 0.0161(16) Uani 1 1 d . U .
O17 O 0.8849(3) 0.7563(3) 0.1189(3) 0.0170(12) Uani 1 1 d . U .
O18 O 0.8271(3) 0.7249(3) 0.0577(3) 0.0151(14) Uani 1 1 d . U .
O19 O 0.8231(3) 0.5413(3) 0.1012(3) 0.0166(12) Uani 1 1 d . U .
O20 O 0.7583(3) 0.6036(4) 0.0892(4) 0.0212(17) Uani 1 1 d . U .
O21 O 0.7894(3) 0.5645(3) 0.0083(3) 0.0163(16) Uani 1 1 d . U .
O22 O 0.7930(3) 0.6550(3) 0.0162(3) 0.0150(15) Uani 1 1 d . U .
O23 O 0.7475(3) 0.5580(4) -0.0850(3) 0.0187(13) Uani 1 1 d . U .
O24 O 0.7172(3) 0.6095(3) -0.0110(3) 0.0166(17) Uani 1 1 d . U .
O25 O 0.7522(3) 0.6566(3) -0.0820(3) 0.0191(12) Uani 1 1 d . U .
O26 O 0.7487(3) 0.7096(3) -0.1685(3) 0.0169(18) Uani 1 1 d . U .
O27 O 0.7180(3) 0.7402(3) -0.0841(3) 0.0156(16) Uani 1 1 d . U .
O28 O 0.7904(3) 0.7781(3) -0.1122(3) 0.0149(15) Uani 1 1 d . U .
O29 O 0.7929(3) 0.7332(3) -0.0280(3) 0.0156(10) Uani 1 1 d . U .
O30 O 0.8240(3) 0.8626(3) -0.0808(3) 0.0167(19) Uani 1 1 d . U .
O31 O 0.7582(3) 0.8244(3) -0.0349(3) 0.0168(11) Uani 1 1 d . U .
O32 O 0.8330(3) 0.8175(3) 0.0111(3) 0.0146(16) Uani 1 1 d . U .
O33 O 0.8934(3) 0.8456(3) 0.0845(3) 0.0172(12) Uani 1 1 d . U .
O34 O 0.8174(3) 0.8122(3) 0.1052(3) 0.0176(16) Uani 1 1 d . U .
O35 O 0.7085(3) 0.8330(3) 0.1453(3) 0.0137(16) Uani 1 1 d . U .
O36 O 0.7775(3) 0.8867(3) 0.1490(3) 0.0170(12) Uani 1 1 d . U .
O37 O 0.7488(3) 0.8431(3) 0.0590(3) 0.0166(12) Uani 1 1 d . U .
O38 O 0.7790(3) 0.7927(3) 0.1832(3) 0.0125(15) Uani 1 1 d . U .
O39 O 0.7420(3) 0.7530(3) 0.1046(3) 0.0142(14) Uani 1 1 d . U .
O40 O 0.7079(3) 0.7444(3) 0.1959(3) 0.0156(16) Uani 1 1 d . U .
O41 O 0.7762(3) 0.7132(3) 0.2465(3) 0.0163(12) Uani 1 1 d . U .
O42 O 0.7476(3) 0.6679(3) 0.1581(3) 0.0180(16) Uani 1 1 d . U .
O43 O 0.7078(3) 0.5795(3) 0.1656(3) 0.0191(12) Uani 1 1 d . U .
O44 O 0.6636(3) 0.6598(3) 0.1437(3) 0.0162(16) Uani 1 1 d . U .
O45 O 0.6764(3) 0.6004(3) 0.0693(3) 0.0164(16) Uani 1 1 d . U .
O46 O 0.7073(3) 0.6831(3) 0.0636(3) 0.0148(11) Uani 1 1 d . U .
O47 O 0.6329(3) 0.5970(3) -0.0242(4) 0.022(2) Uani 1 1 d . U .
O48 O 0.6218(3) 0.6697(3) 0.0379(3) 0.0161(14) Uani 1 1 d . U .
O49 O 0.6710(3) 0.6835(3) -0.0362(3) 0.0163(12) Uani 1 1 d . U .
O50 O 0.6356(3) 0.7454(4) -0.1071(3) 0.0212(18) Uani 1 1 d . U .
O51 O 0.6222(3) 0.7533(3) -0.0099(3) 0.0171(11) Uani 1 1 d . U .
O52 O 0.6771(3) 0.8142(3) -0.0495(3) 0.0146(15) Uani 1 1 d . U .
O53 O 0.7076(3) 0.7610(3) 0.0202(3) 0.0138(14) Uani 1 1 d . U .
O54 O 0.7075(3) 0.8993(3) -0.0120(3) 0.0166(19) Uani 1 1 d . U .
O55 O 0.6653(3) 0.8408(3) 0.0442(3) 0.0147(15) Uani 1 1 d . U .
O56 O 0.4677(3) 0.7881(4) -0.0684(3) 0.020(2) Uani 1 1 d . U .
O57 O 0.5358(3) 0.7566(4) -0.0164(3) 0.0197(17) Uani 1 1 d . U .
O58 O 0.4965(3) 0.8343(3) 0.0196(3) 0.0148(11) Uani 1 1 d . U .
O59 O 0.4271(3) 0.7867(4) 0.0192(3) 0.0188(17) Uani 1 1 d . U .
O60 O 0.4648(3) 0.7098(3) -0.0045(3) 0.0185(16) Uani 1 1 d . U .
O61 O 0.5022(3) 0.7485(3) 0.0744(3) 0.0165(14) Uani 1 1 d . U .
O62 O 0.5384(3) 0.9213(3) 0.0137(3) 0.0163(11) Uani 1 1 d . U .
O63 O 0.5796(3) 0.8405(3) 0.0357(3) 0.0170(16) Uani 1 1 d . U .
O64 O 0.5688(3) 0.9002(3) 0.1097(3) 0.0170(16) Uani 1 1 d . U .
O65 O 0.4874(3) 0.8997(3) 0.0893(3) 0.0171(11) Uani 1 1 d . U .
O66 O 0.5369(3) 0.8179(3) 0.1158(3) 0.0154(15) Uani 1 1 d . U .
O67 O 0.6120(3) 0.9039(3) 0.2032(3) 0.0163(12) Uani 1 1 d . U .
O68 O 0.6219(3) 0.8308(3) 0.1419(3) 0.0163(11) Uani 1 1 d . U .
O69 O 0.5728(3) 0.8183(3) 0.2152(3) 0.0163(12) Uani 1 1 d . U .
O70 O 0.5273(3) 0.8925(3) 0.1914(3) 0.0188(17) Uani 1 1 d . U .
O71 O 0.6077(3) 0.7573(4) 0.2872(3) 0.023(2) Uani 1 1 d . U .
O72 O 0.6214(3) 0.7482(3) 0.1906(3) 0.0156(14) Uani 1 1 d . U .
O73 O 0.5659(3) 0.6879(3) 0.2300(3) 0.0157(16) Uani 1 1 d . U .
O74 O 0.5250(3) 0.7612(3) 0.2629(3) 0.0189(12) Uani 1 1 d . U .
O75 O 0.5351(3) 0.7409(3) 0.1599(3) 0.0164(11) Uani 1 1 d . U .
O76 O 0.5343(3) 0.6038(3) 0.1933(4) 0.021(2) Uani 1 1 d . U .
O77 O 0.5782(3) 0.6618(3) 0.1361(3) 0.0158(15) Uani 1 1 d . U .
O78 O 0.4938(3) 0.6602(3) 0.1197(3) 0.0171(16) Uani 1 1 d . U .
O79 O 0.4843(3) 0.6788(3) 0.2146(3) 0.0181(16) Uani 1 1 d . U .
O80 O 0.5349(3) 0.6694(3) 0.0335(3) 0.0174(16) Uani 1 1 d . U .
O81 O 0.4641(3) 0.6179(3) 0.0317(3) 0.0197(12) Uani 1 1 d . U .
O82 O 0.4252(3) 0.6924(4) 0.0732(3) 0.0200(17) Uani 1 1 d . U .
O83 O 0.3494(3) 0.6596(3) 0.0940(3) 0.0194(19) Uani 1 1 d . U .
O84 O 0.4098(3) 0.6873(3) 0.1683(3) 0.0170(11) Uani 1 1 d . U .
O85 O 0.3583(3) 0.7498(3) 0.0589(3) 0.0182(16) Uani 1 1 d . U .
O86 O 0.3421(3) 0.7356(3) 0.1542(3) 0.0190(16) Uani 1 1 d . U .
O87 O 0.4171(3) 0.7778(4) 0.1209(3) 0.0188(12) Uani 1 1 d . U .
O88 O 0.3520(3) 0.8287(4) -0.0021(4) 0.021(2) Uani 1 1 d . U .
O89 O 0.4127(3) 0.8659(4) 0.0665(3) 0.0199(16) Uani 1 1 d . U .
O90 O 0.3446(3) 0.8333(4) 0.0984(3) 0.0199(16) Uani 1 1 d . U .
O91 O 0.4244(3) 0.9632(3) 0.0777(3) 0.0168(12) Uani 1 1 d . U .
O92 O 0.4560(3) 0.9395(3) 0.1707(3) 0.0172(12) Uani 1 1 d . U .
O93 O 0.3819(3) 0.9046(4) 0.1411(4) 0.0214(17) Uani 1 1 d . U .
O94 O 0.4517(3) 0.8481(3) 0.1642(3) 0.0155(15) Uani 1 1 d . U .
O95 O 0.4969(3) 0.9454(3) 0.2633(3) 0.0164(11) Uani 1 1 d . U .
O96 O 0.4239(3) 0.8961(3) 0.2468(3) 0.0189(12) Uani 1 1 d . U .
O97 O 0.4916(3) 0.8463(4) 0.2610(4) 0.0213(11) Uani 1 1 d . U .
O98 O 0.4930(3) 0.7935(4) 0.3487(3) 0.026(2) Uani 1 1 d . U .
O99 O 0.4520(3) 0.7262(4) 0.2910(3) 0.0178(16) Uani 1 1 d . U .
O100 O 0.4224(3) 0.8148(4) 0.2927(3) 0.0212(17) Uani 1 1 d . U .
O101 O 0.4499(3) 0.7701(3) 0.2073(3) 0.0170(11) Uani 1 1 d . U .
O102 O 0.4181(3) 0.6416(4) 0.2604(4) 0.0354(18) Uani 1 1 d . U .
O103 O 0.3793(3) 0.7277(4) 0.2416(3) 0.0195(16) Uani 1 1 d . U .
O104 O 0.2915(3) 0.7330(4) 0.2366(4) 0.0224(17) Uani 1 1 d . U .
O105 O 0.3067(3) 0.8151(3) 0.1809(3) 0.0197(12) Uani 1 1 d . U .
O106 O 0.3426(3) 0.8072(4) 0.2702(4) 0.0237(17) Uani 1 1 d . U .
O107 O 0.3858(3) 0.8174(3) 0.1950(3) 0.0178(14) Uani 1 1 d . U .
O108 O 0.2944(3) 0.9037(4) 0.1354(4) 0.024(2) Uani 1 1 d . U .
O109 O 0.3433(3) 0.8885(4) 0.2230(4) 0.0213(11) Uani 1 1 d . U .
O110 O 0.3699(3) 0.8860(4) 0.3240(4) 0.027(2) Uani 1 1 d . U .
O111 O 0.5800(3) 0.7521(3) 0.0882(3) 0.0149(14) Uani 1 1 d . U .
O112 O 0.6633(3) 0.7495(3) 0.0924(3) 0.0151(13) Uani 1 1 d . U .
O113 O 0.6727(3) 0.8337(4) 0.2464(3) 0.0188(12) Uani 1 1 d . U .
O114 O 0.5721(3) 0.6707(4) -0.0688(4) 0.031(2) Uani 1 1 d . U .
O115 O 0.0088(3) 0.7469(4) 0.3495(4) 0.0246(18) Uani 1 1 d . U .
O116 O 0.0517(3) 0.7491(3) 0.4465(4) 0.0206(17) Uani 1 1 d . U .
O117 O 0.0226(3) 0.6588(3) 0.4568(3) 0.0156(10) Uani 1 1 d . U .
O118 O -0.0146(3) 0.6569(3) 0.3706(3) 0.0175(15) Uani 1 1 d . U .
O119 O 0.0378(3) 0.5901(4) 0.3370(4) 0.0270(19) Uani 1 1 d . U .
O120 O 0.0733(3) 0.5853(4) 0.4381(4) 0.0278(18) Uani 1 1 d . U .
O121 O -0.0211(4) 0.5586(4) 0.4308(6) 0.053(3) Uani 1 1 d . U .
O122 O 0.2066(3) 0.6195(4) 0.4257(4) 0.0210(13) Uani 1 1 d . U .
O123 O 0.1370(3) 0.6251(3) 0.4769(3) 0.0192(18) Uani 1 1 d . U .
O124 O 0.1093(3) 0.6986(3) 0.4172(3) 0.0182(18) Uani 1 1 d . U .
O125 O 0.1808(3) 0.6972(3) 0.3697(3) 0.0167(18) Uani 1 1 d . U .
O126 O 0.1247(3) 0.6099(4) 0.3499(4) 0.0354(18) Uani 1 1 d . . .
O127 O 0.1046(3) 0.6297(4) 0.1962(3) 0.0194(19) Uani 1 1 d . U .
O128 O 0.0361(3) 0.6215(3) 0.2499(3) 0.0186(18) Uani 1 1 d . U .
O129 O 0.0620(3) 0.6997(3) 0.3061(3) 0.0170(17) Uani 1 1 d . U .
O130 O 0.1326(3) 0.7035(4) 0.2589(4) 0.0225(19) Uani 1 1 d . U .
O131 O 0.2334(3) 0.7479(3) 0.3307(4) 0.0170(16) Uani 1 1 d . U .
O132 O 0.2206(3) 0.6612(3) 0.2233(3) 0.0161(15) Uani 1 1 d . U .
O133 O 0.1923(3) 0.7518(3) 0.2323(3) 0.0174(16) Uani 1 1 d . U .
O134 O 0.2590(3) 0.6587(3) 0.3089(3) 0.0180(16) Uani 1 1 d . U .
O135 O 0.2120(3) 0.5864(4) 0.3406(4) 0.0277(19) Uani 1 1 d . U .
O136 O 0.1645(3) 0.5917(4) 0.2462(4) 0.0210(13) Uani 1 1 d . U .
O137 O 0.0023(3) 0.7395(4) 0.2564(4) 0.030(2) Uani 1 1 d . U .
O138 O -0.0231(3) 0.5724(4) 0.2762(4) 0.027(2) Uani 1 1 d . U .
O139 O 0.1173(3) 0.7387(4) 0.5023(4) 0.027(2) Uani 1 1 d . U .
O140 O 0.0899(3) 0.5804(4) 0.5315(4) 0.025(2) Uani 1 1 d . U .
O141 O 0.2379(3) 0.7375(4) 0.4246(4) 0.027(2) Uani 1 1 d . U .
O142 O 0.2705(3) 0.5755(3) 0.4047(4) 0.021(2) Uani 1 1 d . U .
O143 O 0.1290(3) 0.7422(3) 0.1739(4) 0.024(2) Uani 1 1 d . U .
O144 O 0.1576(3) 0.5819(4) 0.1531(4) 0.028(2) Uani 1 1 d . U .
C1 C 0.1838(4) 0.6673(5) 0.1905(5) 0.0174(17) Uani 1 1 d . U .
C2 C 0.1998(4) 0.6730(5) 0.1387(5) 0.0196(14) Uani 1 1 d . U .
H2A H 0.2175 0.6456 0.1319 0.023 Uiso 1 1 calc R U .
H2B H 0.1758 0.6726 0.1143 0.023 Uiso 1 1 calc R U .
C3 C 0.2247(5) 0.7175(5) 0.1308(5) 0.025(3) Uani 1 1 d . U .
H3A H 0.2059 0.7451 0.1300 0.030 Uiso 1 1 calc R U .
H3B H 0.2457 0.7217 0.1586 0.030 Uiso 1 1 calc R U .
C4 C 0.2461(4) 0.7146(5) 0.0829(5) 0.023(2) Uani 1 1 d . U .
H4A H 0.2252 0.7093 0.0553 0.027 Uiso 1 1 calc R U .
H4B H 0.2655 0.6877 0.0841 0.027 Uiso 1 1 calc R U .
N5 N 0.2705(3) 0.7605(4) 0.0734(5) 0.0227(19) Uani 1 1 d . U .
H5A H 0.2673 0.7682 0.0408 0.034 Uiso 1 1 calc R U .
H5B H 0.2979 0.7561 0.0819 0.034 Uiso 1 1 calc R U .
H5C H 0.2605 0.7842 0.0918 0.034 Uiso 1 1 calc R U .
C6 C 0.0594(4) 0.6654(5) 0.4896(5) 0.0159(17) Uani 1 1 d . U .
C7 C 0.0481(4) 0.6731(5) 0.5415(5) 0.019(2) Uani 1 1 d . U .
H7A H 0.0739 0.6766 0.5628 0.022 Uiso 1 1 calc R U .
H7B H 0.0334 0.6449 0.5528 0.022 Uiso 1 1 calc R U .
C8 C 0.0197(4) 0.7176(5) 0.5487(5) 0.0227(19) Uani 1 1 d . U .
H8A H 0.0368 0.7465 0.5489 0.027 Uiso 1 1 calc R U .
H8B H -0.0016 0.7198 0.5210 0.027 Uiso 1 1 calc R U .
C9 C -0.0014(4) 0.7129(6) 0.5979(6) 0.030(2) Uani 1 1 d . U .
H9A H -0.0194 0.6847 0.5971 0.036 Uiso 1 1 calc R U .
H9B H 0.0199 0.7093 0.6254 0.036 Uiso 1 1 calc R U .
N10 N -0.0265(4) 0.7554(4) 0.6056(5) 0.026(3) Uani 1 1 d . U .
H10A H -0.0120 0.7753 0.6265 0.039 Uiso 1 1 calc R U .
H10B H -0.0507 0.7471 0.6189 0.039 Uiso 1 1 calc R U .
H10C H -0.0322 0.7700 0.5761 0.039 Uiso 1 1 calc R U .
C11 C 0.2584(4) 0.6633(5) 0.3623(5) 0.0196(14) Uani 1 1 d . U .
C12 C 0.3044(4) 0.6676(5) 0.3807(6) 0.022(2) Uani 1 1 d . U .
H12A H 0.3060 0.6662 0.4172 0.026 Uiso 1 1 calc R U .
H12B H 0.3196 0.6401 0.3686 0.026 Uiso 1 1 calc R U .
C13 C 0.3265(4) 0.7120(5) 0.3651(5) 0.023(2) Uani 1 1 d . U .
H13A H 0.3161 0.7395 0.3830 0.027 Uiso 1 1 calc R U .
H13B H 0.3210 0.7173 0.3293 0.027 Uiso 1 1 calc R U .
C14 C 0.3743(4) 0.7060(5) 0.3773(5) 0.020(3) Uani 1 1 d . U .
H14A H 0.3790 0.6955 0.4120 0.024 Uiso 1 1 calc R U .
H14B H 0.3851 0.6814 0.3558 0.024 Uiso 1 1 calc R U .
N15 N 0.3965(4) 0.7483(5) 0.3706(5) 0.030(3) Uani 1 1 d . U .
H15A H 0.3946 0.7564 0.3381 0.045 Uiso 1 1 calc R U .
H15B H 0.4236 0.7440 0.3808 0.045 Uiso 1 1 calc R U .
H15C H 0.3855 0.7716 0.3887 0.045 Uiso 1 1 calc R U .
C16 C -0.0150(4) 0.6613(5) 0.3154(5) 0.0168(17) Uani 1 1 d . U .
C17 C -0.0589(4) 0.6647(5) 0.2967(5) 0.015(2) Uani 1 1 d . U .
H17A H -0.0737 0.6364 0.3078 0.018 Uiso 1 1 calc R U .
H17B H -0.0598 0.6637 0.2602 0.018 Uiso 1 1 calc R U .
C18 C -0.0833(4) 0.7087(5) 0.3124(6) 0.022(2) Uani 1 1 d . U .
H18A H -0.0779 0.7144 0.3482 0.026 Uiso 1 1 calc R U .
H18B H -0.0738 0.7367 0.2945 0.026 Uiso 1 1 calc R U .
C19 C -0.1295(4) 0.7015(5) 0.3011(5) 0.021(3) Uani 1 1 d . U .
H19A H -0.1343 0.6910 0.2664 0.025 Uiso 1 1 calc R U .
H19B H -0.1396 0.6765 0.3227 0.025 Uiso 1 1 calc R U .
N20 N -0.1533(4) 0.7456(5) 0.3086(5) 0.030(2) Uani 1 1 d . U .
H20A H -0.1567 0.7496 0.3414 0.045 Uiso 1 1 calc R U .
H20B H -0.1786 0.7435 0.2920 0.045 Uiso 1 1 calc R U .
H20C H -0.1391 0.7705 0.2969 0.045 Uiso 1 1 calc R U .
Na1 Na 0.87884(17) 0.2670(3) -0.3382(2) 0.0289(16) Uani 1 1 d . . .
Na2 Na 0.7931(2) 0.3817(2) -0.5136(2) 0.0323(17) Uani 1 1 d . . .
Na3 Na 0.80844(19) 0.5450(2) -0.3896(2) 0.0297(15) Uani 1 1 d . U .
Na4 Na 0.67232(19) 0.7198(3) -0.1804(2) 0.0329(15) Uani 1 1 d . U .
Na5 Na 0.7524(2) 0.5327(2) -0.5065(2) 0.0333(16) Uani 1 1 d . U .
Na6 Na 0.8777(2) 0.5545(2) -0.2001(2) 0.0385(17) Uani 1 1 d . U .
Na7 Na 0.9650(2) 0.3768(2) -0.1640(3) 0.0407(19) Uani 1 1 d . . .
Na8 Na 0.7807(2) 0.5745(3) -0.2670(3) 0.0423(18) Uani 1 1 d . U .
Na9 Na 0.5694(3) 0.7199(4) -0.1400(4) 0.020(2) Uani 0.5 1 d . U P
Na10 Na 0.9994(3) 0.5406(3) 0.0468(4) 0.075(3) Uani 1 1 d . U .
Na11 Na 0.7189(4) 0.5097(4) 0.2068(5) 0.029(3) Uani 0.5 1 d . U P
O1W O 0.8083(3) 0.5801(4) 0.5317(4) 0.034(3) Uani 1 1 d . . .
O2W O 0.9544(4) 0.2892(4) 0.8187(4) 0.038(3) Uani 1 1 d . . .
O3W O 0.7407(4) 0.5182(4) 0.5781(4) 0.035(3) Uani 1 1 d . . .
O4W O 0.7993(4) 0.2955(4) 0.4941(5) 0.040(3) Uani 1 1 d . . .
O5W O 0.8764(4) 0.5730(4) 0.6400(5) 0.038(3) Uani 1 1 d . . .
O6W O 0.8511(4) 0.6016(4) 0.7313(4) 0.037(3) Uani 1 1 d . . .
O7W O 0.8024(4) 0.5079(4) 0.6889(4) 0.041(3) Uani 1 1 d . . .
O8W O 0.2737(5) 0.8314(6) 0.3248(6) 0.092(4) Uani 1 1 d . . .
O9W O 0.6618(4) 0.6470(5) 0.8615(4) 0.045(4) Uani 1 1 d . . .
O10W O 0.9469(4) 0.5848(6) 0.7877(6) 0.068(5) Uani 1 1 d . . .
O11W O 0.7985(4) 0.4660(4) 0.4902(5) 0.039(3) Uani 1 1 d . . .
O12W O 0.7996(4) 0.5528(5) 0.8177(5) 0.045(4) Uani 1 1 d . . .
O13W O 0.8433(4) 0.4772(4) 0.5839(5) 0.049(4) Uani 1 1 d . . .
O14W O 0.8881(4) 0.4988(4) 0.8645(5) 0.048(4) Uani 1 1 d . . .
O15W O 0.2633(3) 0.5632(4) 0.2485(5) 0.040(2) Uani 1 1 d . U .
O16W O 0.8777(6) 0.4931(5) 0.7402(5) 0.065(5) Uani 1 1 d . . .
O17W O 0.7688(5) 0.5571(5) 0.4103(6) 0.067(5) Uani 1 1 d . . .
O18W O 0.9738(5) 0.3346(5) 0.9135(5) 0.063(5) Uani 1 1 d . . .
O19W O 0.9671(5) 0.4543(5) 0.8673(6) 0.067(5) Uani 1 1 d . . .
O20W O 0.6944(5) 0.7928(6) 0.7940(5) 0.065(4) Uani 1 1 d . . .
O21W O 0.0824(6) 0.8055(7) 0.3662(8) 0.104(7) Uani 1 1 d . . .
O22W O 0.7173(5) 0.3908(8) 0.4885(7) 0.140(7) Uani 1 1 d . . .
O23W O 0.6970(5) 0.4839(6) 0.4571(7) 0.081(6) Uani 1 1 d . . .
O24W O 0.8396(7) 0.1915(8) 0.6915(11) 0.180(9) Uani 1 1 d . . .
O25W O 0.0417(5) 0.3884(5) 0.8374(6) 0.066(3) Uani 1 1 d . . .
O26W O 0.7581(4) 0.6465(4) 0.7584(4) 0.036(3) Uani 1 1 d . . .
O27W O 0.7129(6) 0.5403(7) 0.7320(8) 0.100(7) Uani 1 1 d . . .
O28W O 0.8004(5) 0.3826(8) 0.3984(5) 0.097(5) Uani 1 1 d . . .
O29W O 0.2185(3) 0.8806(4) 0.2675(5) 0.038(3) Uani 1 1 d . . .
O30W O -0.1331(5) 0.7990(5) 0.2274(6) 0.066(3) Uani 1 1 d . . .
O31W O 0.3768(3) 0.7968(4) 0.4559(4) 0.030(3) Uani 1 1 d . . .
O32W O -0.0476(4) 0.6351(5) 0.5075(5) 0.054(4) Uani 1 1 d . . .
O33W O 0.5522(5) 0.7302(8) 0.3812(5) 0.097(5) Uani 1 1 d . . .
O34W O 0.2958(3) 0.7783(5) 0.4818(4) 0.041(4) Uani 1 1 d . . .
O35W O -0.0546(4) 0.7840(5) 0.1974(4) 0.042(4) Uani 1 1 d . . .
O36W O 0.0201(4) 0.8328(5) 0.4739(6) 0.056(4) Uani 1 1 d . . .
O37W O 0.9062(5) 0.8739(6) -0.0989(6) 0.092(4) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 W1 O2 103.9(4) . .
O1 W1 O3 103.2(4) . .
O2 W1 O3 88.7(4) . .
O1 W1 O4 101.1(4) . .
O2 W1 O4 89.3(4) . .
O3 W1 O4 155.3(4) . .
O1 W1 O5 98.2(4) . .
O2 W1 O5 157.9(4) . .
O3 W1 O5 86.7(4) . .
O4 W1 O5 86.0(4) . .
O1 W1 O6 168.7(4) . .
O2 W1 O6 85.9(4) . .
O3 W1 O6 82.4(3) . .
O4 W1 O6 73.0(3) . .
O5 W1 O6 72.1(3) . .
O7 W2 O8 102.7(4) 4_675 .
O7 W2 O9 103.0(4) 4_675 .
O8 W2 O9 89.4(4) . .
O7 W2 O5 98.7(4) 4_675 .
O8 W2 O5 158.2(4) . .
O9 W2 O5 90.1(4) . .
O7 W2 O10 97.8(4) 4_675 .
O8 W2 O10 87.0(4) . .
O9 W2 O10 159.2(4) . .
O5 W2 O10 85.7(4) . .
O7 W2 O6 168.6(4) 4_675 .
O8 W2 O6 84.6(3) . .
O9 W2 O6 85.7(3) . .
O5 W2 O6 73.6(3) . .
O10 W2 O6 73.6(3) . .
O11 W3 O13 104.5(4) . .
O11 W3 O12 102.9(4) . .
O13 W3 O12 88.8(4) . .
O11 W3 O4 99.8(4) . .
O13 W3 O4 88.2(4) . .
O12 W3 O4 157.1(4) . .
O11 W3 O10 98.8(4) . .
O13 W3 O10 156.6(4) . .
O12 W3 O10 88.6(4) . .
O4 W3 O10 85.2(4) . .
O11 W3 O6 168.3(4) . .
O13 W3 O6 84.6(4) . .
O12 W3 O6 84.3(3) . .
O4 W3 O6 72.8(3) . .
O10 W3 O6 71.9(3) . .
O14 W4 O15 98.2(4) . .
O14 W4 O16 106.3(4) . .
O15 W4 O16 90.0(4) . .
O14 W4 O17 95.8(4) . .
O15 W4 O17 94.0(4) . .
O16 W4 O17 156.8(4) . .
O14 W4 O12 98.1(4) . .
O15 W4 O12 163.6(4) . .
O16 W4 O12 84.1(4) . .
O17 W4 O12 85.7(4) . .
O14 W4 O18 169.0(4) . .
O15 W4 O18 83.4(4) . .
O16 W4 O18 84.5(4) . .
O17 W4 O18 73.3(3) . .
O12 W4 O18 80.8(3) . .
O19 W5 O20 102.3(4) . .
O19 W5 O16 100.9(4) . .
O20 W5 O16 91.0(4) . .
O19 W5 O21 98.8(4) . .
O20 W5 O21 93.8(4) . .
O16 W5 O21 158.2(4) . .
O19 W5 O13 96.2(4) . .
O20 W5 O13 161.3(4) . .
O16 W5 O13 82.8(4) . .
O21 W5 O13 85.9(4) . .
O19 W5 O22 172.1(4) . .
O20 W5 O22 82.4(4) . .
O16 W5 O22 85.3(4) . .
O21 W5 O22 74.3(3) . .
O13 W5 O22 79.6(3) . .
O23 W6 O24 100.9(4) . .
O23 W6 O25 101.7(4) . .
O24 W6 O25 91.3(4) . .
O23 W6 O21 101.1(4) . .
O24 W6 O21 92.3(4) . .
O25 W6 O21 155.9(4) . .
O23 W6 O2 95.5(4) . .
O24 W6 O2 163.4(4) . .
O25 W6 O2 83.4(4) . .
O21 W6 O2 86.5(4) . .
O23 W6 O22 172.8(4) . .
O24 W6 O22 83.3(4) . .
O25 W6 O22 84.0(4) . .
O21 W6 O22 72.7(3) . .
O2 W6 O22 80.6(3) . .
O26 W7 O27 99.8(4) . .
O26 W7 O25 101.5(4) . .
O27 W7 O25 90.7(4) . .
O26 W7 O28 97.8(4) . .
O27 W7 O28 92.6(4) . .
O25 W7 O28 159.6(4) . .
O26 W7 O3 95.9(4) . .
O27 W7 O3 164.2(4) . .
O25 W7 O3 84.9(4) . .
O28 W7 O3 86.5(4) . .
O26 W7 O29 171.7(4) . .
O27 W7 O29 83.4(3) . .
O25 W7 O29 86.1(4) . .
O28 W7 O29 74.3(3) . .
O3 W7 O29 81.2(3) . .
O26 W7 Na4 41.9(3) . .
O27 W7 Na4 58.9(3) . .
O25 W7 Na4 92.3(3) . .
O28 W7 Na4 106.6(3) . .
O3 W7 Na4 136.3(3) . .
O29 W7 Na4 142.2(2) . .
O30 W8 O31 101.2(4) . .
O30 W8 O32 101.6(4) . .
O31 W8 O32 91.7(4) . .
O30 W8 O28 98.1(4) . .
O31 W8 O28 94.5(4) . .
O32 W8 O28 157.7(4) . .
O30 W8 O9 94.8(4) . .
O31 W8 O9 163.9(4) . .
O32 W8 O9 83.3(4) . .
O28 W8 O9 84.9(4) . .
O30 W8 O29 171.5(4) . .
O31 W8 O29 83.8(4) . .
O32 W8 O29 85.0(4) . .
O28 W8 O29 74.5(4) . .
O9 W8 O29 80.6(3) . .
O33 W9 O34 100.8(4) . .
O33 W9 O17 98.7(4) . .
O34 W9 O17 93.9(4) . .
O33 W9 O32 102.3(4) . .
O34 W9 O32 90.0(4) . .
O17 W9 O32 157.5(4) . .
O33 W9 O8 95.3(4) . .
O34 W9 O8 163.6(4) . .
O17 W9 O8 86.5(4) . .
O32 W9 O8 83.6(4) . .
O33 W9 O18 171.4(4) . .
O34 W9 O18 83.1(4) . .
O17 W9 O18 73.3(4) . .
O32 W9 O18 85.2(3) . .
O8 W9 O18 81.4(3) . .
O36 W10 O35 99.5(4) . .
O36 W10 O37 101.8(4) . .
O35 W10 O37 96.6(4) . .
O36 W10 O38 100.6(4) . .
O35 W10 O38 93.2(4) . .
O37 W10 O38 153.7(4) . .
O36 W10 O34 94.4(4) . .
O35 W10 O34 165.7(4) . .
O37 W10 O34 83.6(4) . .
O38 W10 O34 81.0(4) . .
O36 W10 O39 174.9(4) . .
O35 W10 O39 82.2(4) . .
O37 W10 O39 82.7(3) . .
O38 W10 O39 74.5(3) . .
O34 W10 O39 83.6(3) . .
O41 W11 O40 99.4(4) . .
O41 W11 O42 102.5(4) . .
O40 W11 O42 96.8(4) . .
O41 W11 O38 101.1(4) . .
O40 W11 O38 93.0(4) . .
O42 W11 O38 152.6(4) . .
O41 W11 O15 94.7(4) . .
O40 W11 O15 165.4(4) . .
O42 W11 O15 83.8(4) . .
O38 W11 O15 80.5(4) . .
O41 W11 O39 175.0(4) . .
O40 W11 O39 82.5(4) . .
O42 W11 O39 81.8(4) . .
O38 W11 O39 74.2(3) . .
O15 W11 O39 83.1(3) . .
O43 W12 O44 101.5(4) . .
O43 W12 O42 102.2(4) . .
O44 W12 O42 95.1(4) . .
O43 W12 O45 99.2(4) . .
O44 W12 O45 91.7(4) . .
O42 W12 O45 155.8(4) . .
O43 W12 O20 94.1(4) . .
O44 W12 O20 164.2(4) . .
O42 W12 O20 83.9(4) . .
O45 W12 O20 83.3(4) . .
O43 W12 O46 171.7(4) . .
O44 W12 O46 82.8(4) . .
O42 W12 O46 84.2(4) . .
O45 W12 O46 73.5(4) . .
O20 W12 O46 81.4(4) . .
O47 W13 O48 100.4(4) . .
O47 W13 O45 102.7(4) . .
O48 W13 O45 95.6(4) . .
O47 W13 O49 100.1(4) . .
O48 W13 O49 91.9(4) . .
O45 W13 O49 154.3(4) . .
O47 W13 O24 93.1(4) . .
O48 W13 O24 166.3(4) . .
O45 W13 O24 83.1(4) . .
O49 W13 O24 83.8(4) . .
O47 W13 O46 174.0(4) . .
O48 W13 O46 83.9(4) . .
O45 W13 O46 72.6(4) . .
O49 W13 O46 83.9(3) . .
O24 W13 O46 82.8(3) . .
O50 W14 O51 101.1(4) . .
O50 W14 O52 100.8(4) . .
O51 W14 O52 95.9(4) . .
O50 W14 O49 100.4(4) . .
O51 W14 O49 91.6(4) . .
O52 W14 O49 155.7(4) . .
O50 W14 O27 91.3(4) . .
O51 W14 O27 167.0(4) . .
O52 W14 O27 85.4(4) . .
O49 W14 O27 82.3(4) . .
O50 W14 O53 172.0(4) . .
O51 W14 O53 85.1(4) . .
O52 W14 O53 73.2(3) . .
O49 W14 O53 84.4(3) . .
O27 W14 O53 83.0(3) . .
O50 W14 Na4 36.9(3) . .
O51 W14 Na4 136.5(3) . .
O52 W14 Na4 102.2(3) . .
O49 W14 Na4 87.9(3) . .
O27 W14 Na4 55.1(3) . .
O53 W14 Na4 138.0(2) . .
O54 W15 O55 100.7(4) . .
O54 W15 O37 101.6(4) . .
O55 W15 O37 94.9(4) . .
O54 W15 O52 99.7(4) . .
O55 W15 O52 93.3(4) . .
O37 W15 O52 155.3(4) . .
O54 W15 O31 94.4(4) . .
O55 W15 O31 164.8(4) . .
O37 W15 O31 83.6(4) . .
O52 W15 O31 82.4(4) . .
O54 W15 O53 172.7(4) . .
O55 W15 O53 82.6(4) . .
O37 W15 O53 84.5(4) . .
O52 W15 O53 73.5(3) . .
O31 W15 O53 82.3(3) . .
O56 W16 O57 100.6(4) . .
O56 W16 O58 102.8(4) . .
O57 W16 O58 97.6(4) . .
O56 W16 O60 100.1(4) . .
O57 W16 O60 92.4(4) . .
O58 W16 O60 152.9(4) . .
O56 W16 O59 94.1(4) . .
O57 W16 O59 164.8(4) . .
O58 W16 O59 83.0(4) . .
O60 W16 O59 81.0(4) . .
O56 W16 O61 173.7(4) . .
O57 W16 O61 81.5(4) . .
O58 W16 O61 82.7(3) . .
O60 W16 O61 73.9(3) . .
O59 W16 O61 83.5(3) . .
O62 W17 O63 100.8(4) . .
O62 W17 O58 101.5(4) . .
O63 W17 O58 93.9(4) . .
O62 W17 O64 98.9(4) . .
O63 W17 O64 91.9(4) . .
O58 W17 O64 157.3(4) . .
O62 W17 O65 94.1(4) . .
O63 W17 O65 165.0(4) . .
O58 W17 O65 85.3(4) . .
O64 W17 O65 83.5(4) . .
O62 W17 O66 172.2(4) . .
O63 W17 O66 82.2(4) . .
O58 W17 O66 85.4(3) . .
O64 W17 O66 73.7(4) . .
O65 W17 O66 82.8(3) . .
O67 W18 O68 100.7(4) . .
O67 W18 O69 100.9(4) . .
O68 W18 O69 91.3(4) . .
O67 W18 O64 103.3(4) . .
O68 W18 O64 95.0(4) . .
O69 W18 O64 153.4(4) . .
O67 W18 O70 93.5(4) . .
O68 W18 O70 165.6(4) . .
O69 W18 O70 83.1(4) . .
O64 W18 O70 84.5(4) . .
O67 W18 O66 174.7(4) . .
O68 W18 O66 82.8(4) . .
O69 W18 O66 83.0(3) . .
O64 W18 O66 72.2(4) . .
O70 W18 O66 83.3(3) . .
O71 W19 O72 101.1(4) . .
O71 W19 O69 100.7(5) . .
O72 W19 O69 91.6(4) . .
O71 W19 O73 101.1(5) . .
O72 W19 O73 95.8(4) . .
O69 W19 O73 155.1(4) . .
O71 W19 O74 92.0(4) . .
O72 W19 O74 166.6(4) . .
O69 W19 O74 83.3(4) . .
O73 W19 O74 84.1(4) . .
O71 W19 O75 171.4(4) . .
O72 W19 O75 85.9(4) . .
O69 W19 O75 83.9(4) . .
O73 W19 O75 73.0(3) . .
O74 W19 O75 81.3(3) . .
O71 W19 Na9 37.2(4) . 4_576
O72 W19 Na9 137.3(3) . 4_576
O69 W19 Na9 89.7(3) . 4_576
O73 W19 Na9 100.6(3) . 4_576
O74 W19 Na9 55.3(3) . 4_576
O75 W19 Na9 136.5(3) . 4_576
O76 W20 O77 102.0(4) . .
O76 W20 O78 102.2(4) . .
O77 W20 O78 95.0(4) . .
O76 W20 O73 98.5(4) . .
O77 W20 O73 93.0(4) . .
O78 W20 O73 155.7(4) . .
O76 W20 O79 92.9(4) . .
O77 W20 O79 164.9(4) . .
O78 W20 O79 83.7(4) . .
O73 W20 O79 82.7(4) . .
O76 W20 O75 171.5(4) . .
O77 W20 O75 83.0(4) . .
O78 W20 O75 84.0(4) . .
O73 W20 O75 74.3(4) . .
O79 W20 O75 81.9(4) . .
O81 W21 O80 101.1(4) . .
O81 W21 O78 101.1(4) . .
O80 W21 O78 97.6(4) . .
O81 W21 O60 99.8(4) . .
O80 W21 O60 92.6(4) . .
O78 W21 O60 154.5(4) . .
O81 W21 O82 92.4(4) . .
O80 W21 O82 165.7(4) . .
O78 W21 O82 84.0(4) . .
O60 W21 O82 80.6(4) . .
O81 W21 O61 174.5(4) . .
O80 W21 O61 82.2(4) . .
O78 W21 O61 82.7(4) . .
O60 W21 O61 75.6(4) . .
O82 W21 O61 83.9(4) . .
O83 W22 O82 100.6(5) . .
O83 W22 O84 102.5(4) . .
O82 W22 O84 91.1(4) . .
O83 W22 O85 98.7(4) . .
O82 W22 O85 93.5(4) . .
O84 W22 O85 157.0(4) . .
O83 W22 O86 94.6(4) . .
O82 W22 O86 164.5(4) . .
O84 W22 O86 82.8(4) . .
O85 W22 O86 86.9(4) . .
O83 W22 O87 172.0(4) . .
O82 W22 O87 82.5(4) . .
O84 W22 O87 84.7(4) . .
O85 W22 O87 73.6(4) . .
O86 W22 O87 82.9(4) . .
O88 W23 O59 101.0(4) . .
O88 W23 O89 101.8(4) . .
O59 W23 O89 91.2(4) . .
O88 W23 O85 99.4(4) . .
O59 W23 O85 94.4(4) . .
O89 W23 O85 156.6(4) . .
O88 W23 O90 95.0(4) . .
O59 W23 O90 163.8(4) . .
O89 W23 O90 83.0(4) . .
O85 W23 O90 85.4(4) . .
O88 W23 O87 171.9(4) . .
O59 W23 O87 83.2(4) . .
O89 W23 O87 84.9(4) . .
O85 W23 O87 73.2(4) . .
O90 W23 O87 81.2(4) . .
O91 W24 O65 100.6(4) . .
O91 W24 O89 102.4(4) . .
O65 W24 O89 91.1(4) . .
O91 W24 O92 97.8(4) . .
O65 W24 O92 93.9(4) . .
O89 W24 O92 157.9(4) . .
O91 W24 O93 97.9(4) . .
O65 W24 O93 161.3(4) . .
O89 W24 O93 82.6(4) . .
O92 W24 O93 85.9(4) . .
O91 W24 O94 171.3(4) . .
O65 W24 O94 82.8(4) . .
O89 W24 O94 85.4(4) . .
O92 W24 O94 73.9(4) . .
O93 W24 O94 79.2(4) . .
O95 W25 O70 101.0(4) . .
O95 W25 O97 102.6(4) . .
O70 W25 O97 90.8(4) . .
O95 W25 O92 99.2(4) . .
O70 W25 O92 93.2(4) . .
O97 W25 O92 156.6(4) . .
O95 W25 O96 95.4(4) . .
O70 W25 O96 163.5(4) . .
O97 W25 O96 83.9(4) . .
O92 W25 O96 85.7(4) . .
O95 W25 O94 172.1(4) . .
O70 W25 O94 84.0(4) . .
O97 W25 O94 83.3(4) . .
O92 W25 O94 74.2(4) . .
O96 W25 O94 79.8(3) . .
O98 W26 O74 102.3(5) . .
O98 W26 O97 102.2(5) . .
O74 W26 O97 91.4(4) . .
O98 W26 O99 97.7(5) . .
O74 W26 O99 92.2(4) . .
O97 W26 O99 158.5(4) . .
O98 W26 O100 94.1(4) . .
O74 W26 O100 163.6(4) . .
O97 W26 O100 84.0(4) . .
O99 W26 O100 86.6(4) . .
O98 W26 O101 170.2(4) . .
O74 W26 O101 83.0(4) . .
O97 W26 O101 85.8(4) . .
O99 W26 O101 73.7(4) . .
O100 W26 O101 81.0(3) . .
O98 W26 Na9 43.6(4) . 4_576
O74 W26 Na9 59.6(3) . 4_576
O97 W26 Na9 93.8(3) . 4_576
O99 W26 Na9 106.3(3) . 4_576
O100 W26 Na9 136.2(3) . 4_576
O101 W26 Na9 142.6(3) . 4_576
O102 W27 O79 101.3(5) . .
O102 W27 O84 102.8(5) . .
O79 W27 O84 92.7(4) . .
O102 W27 O99 97.8(5) . .
O79 W27 O99 94.5(4) . .
O84 W27 O99 156.4(4) . .
O102 W27 O103 95.7(5) . .
O79 W27 O103 162.9(4) . .
O84 W27 O103 82.2(4) . .
O99 W27 O103 84.4(4) . .
O102 W27 O101 170.4(4) . .
O79 W27 O101 84.4(4) . .
O84 W27 O101 84.5(4) . .
O99 W27 O101 73.9(4) . .
O103 W27 O101 78.9(4) . .
O104 W28 O103 103.3(4) . .
O104 W28 O86 103.1(4) . .
O103 W28 O86 88.0(4) . .
O104 W28 O106 98.9(4) . .
O103 W28 O106 90.2(4) . .
O86 W28 O106 157.8(4) . .
O104 W28 O105 100.3(4) . .
O103 W28 O105 156.4(4) . .
O86 W28 O105 87.5(4) . .
O106 W28 O105 85.4(4) . .
O104 W28 O107 168.5(4) . .
O103 W28 O107 84.5(4) . .
O86 W28 O107 85.5(4) . .
O106 W28 O107 72.3(4) . .
O105 W28 O107 72.1(4) . .
O108 W29 O90 102.2(4) . .
O108 W29 O93 103.2(5) . .
O90 W29 O93 88.4(4) . .
O108 W29 O109 99.7(4) . .
O90 W29 O109 158.0(4) . .
O93 W29 O109 88.4(4) . .
O108 W29 O105 100.4(4) . .
O90 W29 O105 88.9(4) . .
O93 W29 O105 156.2(4) . .
O109 W29 O105 85.3(4) . .
O108 W29 O107 169.2(4) . .
O90 W29 O107 85.4(4) . .
O93 W29 O107 84.5(4) . .
O109 W29 O107 72.7(4) . .
O105 W29 O107 71.7(4) . .
O110 W30 O96 103.9(5) . .
O110 W30 O100 102.8(5) . .
O96 W30 O100 89.2(4) . .
O110 W30 O106 99.5(5) . .
O96 W30 O106 156.6(4) . .
O100 W30 O106 86.8(4) . .
O110 W30 O109 101.1(5) . .
O96 W30 O109 88.3(4) . .
O100 W30 O109 155.8(4) . .
O106 W30 O109 86.0(4) . .
O110 W30 O107 169.6(4) . .
O96 W30 O107 84.7(4) . .
O100 W30 O107 82.9(4) . .
O106 W30 O107 71.9(4) . .
O109 W30 O107 72.9(4) . .
O55 Cu1 O63 90.6(4) . .
O55 Cu1 O111 175.6(4) . .
O63 Cu1 O111 93.3(4) . .
O55 Cu1 O112 93.8(4) . .
O63 Cu1 O112 175.3(4) . .
O111 Cu1 O112 82.4(4) . .
O55 Cu1 O68 92.4(4) . .
O63 Cu1 O68 94.1(4) . .
O111 Cu1 O68 85.4(3) . .
O112 Cu1 O68 87.6(3) . .
O55 Cu1 O51 94.1(4) . .
O63 Cu1 O51 92.4(4) . .
O111 Cu1 O51 87.7(3) . .
O112 Cu1 O51 85.4(3) . .
O68 Cu1 O51 170.8(3) . .
O40 Cu2 O68 173.0(4) . .
O40 Cu2 O35 93.8(4) . .
O68 Cu2 O35 90.1(4) . .
O40 Cu2 O72 89.8(4) . .
O68 Cu2 O72 85.8(4) . .
O35 Cu2 O72 174.0(4) . .
O40 Cu2 O113 91.9(4) . .
O68 Cu2 O113 94.0(4) . .
O35 Cu2 O113 88.2(3) . .
O72 Cu2 O113 96.4(3) . .
O40 Cu2 O112 88.3(3) . .
O68 Cu2 O112 86.0(3) . .
O35 Cu2 O112 88.5(3) . .
O72 Cu2 O112 86.8(3) . .
O113 Cu2 O112 176.7(3) . .
O77 Cu3 O44 90.9(4) . .
O77 Cu3 O112 174.5(4) . .
O44 Cu3 O112 94.5(4) . .
O77 Cu3 O111 92.4(4) . .
O44 Cu3 O111 176.4(4) . .
O112 Cu3 O111 82.2(4) . .
O77 Cu3 O48 92.6(4) . .
O44 Cu3 O48 93.2(4) . .
O112 Cu3 O48 86.1(3) . .
O111 Cu3 O48 88.1(3) . .
O77 Cu3 O72 93.3(4) . .
O44 Cu3 O72 93.5(3) . .
O112 Cu3 O72 87.4(3) . .
O111 Cu3 O72 84.9(3) . .
O48 Cu3 O72 171.0(3) . .
O80 Cu4 O57 92.5(4) . .
O80 Cu4 O51 174.0(4) . .
O57 Cu4 O51 89.9(4) . .
O80 Cu4 O48 90.7(4) . .
O57 Cu4 O48 173.6(4) . .
O51 Cu4 O48 86.4(4) . .
O80 Cu4 O114 90.4(4) . .
O57 Cu4 O114 90.4(4) . .
O51 Cu4 O114 95.0(4) . .
O48 Cu4 O114 95.0(4) . .
O115 Cu5 O117 161.0(4) . .
O115 Cu5 O116 95.9(4) . .
O117 Cu5 O116 89.1(4) . .
O115 Cu5 O118 88.6(4) . .
O117 Cu5 O118 81.0(4) . .
O116 Cu5 O118 160.7(4) . .
O115 Cu5 O7 103.6(4) . .
O117 Cu5 O7 93.0(4) . .
O116 Cu5 O7 103.2(4) . .
O118 Cu5 O7 94.0(4) . .
O115 Cu5 Cu6 117.6(3) . .
O117 Cu5 Cu6 45.0(3) . .
O116 Cu5 Cu6 117.5(3) . .
O118 Cu5 Cu6 45.0(3) . .
O7 Cu5 Cu6 116.1(3) . .
O115 Cu5 P7 112.3(3) . .
O117 Cu5 P7 64.5(3) . .
O116 Cu5 P7 31.7(3) . .
O118 Cu5 P7 129.8(3) . .
O7 Cu5 P7 121.8(3) . .
Cu6 Cu5 P7 85.83(10) . .
O115 Cu5 P5 30.6(3) . .
O117 Cu5 P5 131.5(3) . .
O116 Cu5 P5 113.5(3) . .
O118 Cu5 P5 63.5(3) . .
O7 Cu5 P5 120.0(3) . .
Cu6 Cu5 P5 87.04(10) . .
P7 Cu5 P5 113.95(12) . .
O120 Cu6 O119 97.7(4) . .
O120 Cu6 O117 89.0(4) . .
O119 Cu6 O117 160.9(4) . .
O120 Cu6 O118 168.1(4) . .
O119 Cu6 O118 88.9(4) . .
O117 Cu6 O118 81.8(4) . .
O120 Cu6 O121 92.3(5) . .
O119 Cu6 O121 102.0(5) . .
O117 Cu6 O121 95.6(4) . .
O118 Cu6 O121 96.1(4) . .
O120 Cu6 Cu5 122.5(3) . .
O119 Cu6 Cu5 117.8(3) . .
O117 Cu6 Cu5 45.1(3) . .
O118 Cu6 Cu5 45.7(3) . .
O121 Cu6 Cu5 119.5(3) . .
O124 Cu7 O122 174.5(4) . .
O124 Cu7 O123 91.0(4) . .
O122 Cu7 O123 88.9(4) . .
O124 Cu7 O125 88.1(4) . .
O122 Cu7 O125 91.0(4) . .
O123 Cu7 O125 169.7(4) . .
O124 Cu7 Na2 127.5(3) . 3_665
O122 Cu7 Na2 49.2(3) . 3_665
O123 Cu7 Na2 50.3(3) . 3_665
O125 Cu7 Na2 123.5(3) . 3_665
O124 Cu7 Na1 47.5(3) . 3_665
O122 Cu7 Na1 133.3(3) . 3_665
O123 Cu7 Na1 137.6(3) . 3_665
O125 Cu7 Na1 44.4(3) . 3_665
Na2 Cu7 Na1 158.11(18) 3_665 3_665
O130 Cu8 O127 92.8(4) . .
O130 Cu8 O128 176.1(4) . .
O127 Cu8 O128 88.7(4) . .
O130 Cu8 O129 87.1(4) . .
O127 Cu8 O129 177.2(4) . .
O128 Cu8 O129 91.5(4) . .
O130 Cu8 Na7 132.8(3) . 3_665
O127 Cu8 Na7 51.7(3) . 3_665
O128 Cu8 Na7 50.5(3) . 3_665
O129 Cu8 Na7 126.8(3) . 3_665
O130 Cu8 Na1 46.4(3) . 3_665
O127 Cu8 Na1 137.2(3) . 3_665
O128 Cu8 Na1 131.2(3) . 3_665
O129 Cu8 Na1 43.5(3) . 3_665
Na7 Cu8 Na1 163.76(19) 3_665 3_665
O131 Cu9 O132 159.3(4) . .
O131 Cu9 O133 96.7(4) . .
O132 Cu9 O133 88.8(4) . .
O131 Cu9 O134 88.5(4) . .
O132 Cu9 O134 80.7(4) . .
O133 Cu9 O134 162.1(4) . .
O131 Cu9 O104 104.3(4) . .
O132 Cu9 O104 94.1(4) . .
O133 Cu9 O104 100.9(4) . .
O134 Cu9 O104 94.3(4) . .
O131 Cu9 Cu10 116.5(3) . .
O132 Cu9 Cu10 44.6(3) . .
O133 Cu9 Cu10 117.9(3) . .
O134 Cu9 Cu10 45.3(3) . .
O104 Cu9 Cu10 117.3(3) . .
O131 Cu9 P11 112.8(3) . .
O132 Cu9 P11 64.1(3) . .
O133 Cu9 P11 31.2(3) . .
O134 Cu9 P11 131.5(3) . .
O104 Cu9 P11 119.3(3) . .
Cu10 Cu9 P11 86.73(9) . .
O131 Cu9 P9 30.8(3) . .
O132 Cu9 P9 129.7(3) . .
O133 Cu9 P9 114.7(3) . .
O134 Cu9 P9 63.6(3) . .
O104 Cu9 P9 121.4(3) . .
Cu10 Cu9 P9 85.79(9) . .
P11 Cu9 P9 114.83(11) . .
O135 Cu10 O132 166.3(4) . .
O135 Cu10 O136 96.7(4) . .
O132 Cu10 O136 90.4(4) . .
O135 Cu10 O134 88.5(4) . .
O132 Cu10 O134 81.7(4) . .
O136 Cu10 O134 163.7(4) . .
O135 Cu10 O15W 95.1(5) . .
O132 Cu10 O15W 95.3(4) . .
O136 Cu10 O15W 99.7(4) . .
O134 Cu10 O15W 95.2(4) . .
O135 Cu10 Cu9 121.7(3) . .
O132 Cu10 Cu9 44.9(3) . .
O136 Cu10 Cu9 119.3(3) . .
O134 Cu10 Cu9 46.2(3) . .
O15W Cu10 Cu9 119.1(3) . .
O29 P1 O22 112.5(5) . .
O29 P1 O18 111.8(5) . .
O22 P1 O18 109.4(5) . .
O29 P1 O6 107.2(5) . .
O22 P1 O6 107.8(5) . .
O18 P1 O6 108.1(5) . .
O53 P2 O39 110.1(5) . .
O53 P2 O46 110.3(5) . .
O39 P2 O46 110.0(5) . .
O53 P2 O112 108.6(5) . .
O39 P2 O112 110.0(5) . .
O46 P2 O112 107.7(5) . .
O66 P3 O61 110.7(5) . .
O66 P3 O75 110.3(5) . .
O61 P3 O75 109.6(5) . .
O66 P3 O111 107.7(5) . .
O61 P3 O111 109.4(5) . .
O75 P3 O111 109.1(5) . .
O94 P4 O101 111.3(5) . .
O94 P4 O87 112.6(5) . .
O101 P4 O87 110.1(6) . .
O94 P4 O107 107.3(5) . .
O101 P4 O107 105.2(5) . .
O87 P4 O107 110.1(5) . .
O137 P5 O129 112.0(6) . .
O137 P5 O115 110.5(6) . .
O129 P5 O115 109.3(6) . .
O137 P5 C16 112.6(6) . .
O129 P5 C16 107.1(6) . .
O115 P5 C16 105.0(6) . .
O137 P5 Cu5 147.3(5) . .
O129 P5 Cu5 94.5(4) . .
O115 P5 Cu5 39.5(4) . .
C16 P5 Cu5 74.9(4) . .
O128 P6 O138 110.5(6) . .
O128 P6 O119 111.6(6) . .
O138 P6 O119 111.8(6) . .
O128 P6 C16 108.8(6) . .
O138 P6 C16 108.9(6) . .
O119 P6 C16 105.1(6) . .
O139 P7 O116 112.1(6) . .
O139 P7 O124 113.9(6) . .
O116 P7 O124 108.6(5) . .
O139 P7 C6 111.3(6) . .
O116 P7 C6 101.9(6) . .
O124 P7 C6 108.4(6) . .
O139 P7 Cu5 152.0(4) . .
O116 P7 Cu5 42.0(4) . .
O124 P7 Cu5 89.2(4) . .
C6 P7 Cu5 73.2(4) . .
O123 P8 O120 110.9(6) . .
O123 P8 O140 111.1(5) . .
O120 P8 O140 112.0(6) . .
O123 P8 C6 109.0(6) . .
O120 P8 C6 104.1(6) . .
O140 P8 C6 109.5(6) . .
O141 P9 O125 113.5(6) . .
O141 P9 O131 112.4(6) . .
O125 P9 O131 108.8(5) . .
O141 P9 C11 112.3(6) . .
O125 P9 C11 105.9(6) . .
O131 P9 C11 103.3(6) . .
O141 P9 Cu9 149.1(4) . .
O125 P9 Cu9 92.2(4) . .
O131 P9 Cu9 39.4(4) . .
C11 P9 Cu9 73.9(4) . .
O142 P10 O135 111.9(6) . .
O142 P10 O122 111.4(6) . .
O135 P10 O122 110.0(6) . .
O142 P10 C11 110.2(6) . .
O135 P10 C11 104.7(6) . .
O122 P10 C11 108.5(6) . .
O143 P11 O133 112.4(6) . .
O143 P11 O130 113.2(6) . .
O133 P11 O130 108.0(5) . .
O143 P11 C1 112.1(6) . .
O133 P11 C1 103.0(6) . .
O130 P11 C1 107.4(6) . .
O143 P11 Cu9 151.5(5) . .
O133 P11 Cu9 41.5(4) . .
O130 P11 Cu9 90.2(4) . .
C1 P11 Cu9 73.1(4) . .
O144 P12 O127 111.6(6) . .
O144 P12 O136 112.1(6) . .
O127 P12 O136 109.8(5) . .
O144 P12 C1 108.8(6) . .
O127 P12 C1 108.9(6) . .
O136 P12 C1 105.4(6) . .
W1 O1 Na6 153.5(6) . .
W1 O2 W6 149.8(5) . .
W1 O3 W7 148.6(5) . .
W1 O4 W3 123.5(5) . .
W2 O5 W1 122.4(5) . .
P1 O6 W2 125.3(5) . .
P1 O6 W3 123.0(5) . .
W2 O6 W3 92.6(3) . .
P1 O6 W1 123.7(5) . .
W2 O6 W1 91.9(3) . .
W3 O6 W1 90.7(3) . .
W2 O7 Cu5 163.7(6) 4_476 .
W2 O8 W9 147.9(5) . .
W2 O9 W8 148.3(5) . .
W2 O10 W3 121.9(4) . .
W3 O11 Na10 161.2(6) . .
W3 O12 W4 149.0(5) . .
W3 O13 W5 150.1(5) . .
W4 O15 W11 166.3(6) . .
W5 O16 W4 155.0(5) . .
W9 O17 W4 122.8(5) . .
P1 O18 W4 129.4(5) . .
P1 O18 W9 126.6(5) . .
W4 O18 W9 89.9(3) . .
W5 O20 W12 165.0(6) . .
W5 O21 W6 121.9(5) . .
P1 O22 W5 130.4(5) . .
P1 O22 W6 128.4(5) . .
W5 O22 W6 89.9(3) . .
W6 O24 W13 162.2(5) . .
W7 O25 W6 154.7(6) . .
W7 O26 Na4 110.6(4) . .
W7 O27 W14 164.2(6) . .
W7 O27 Na4 89.9(3) . .
W14 O27 Na4 90.7(3) . .
W8 O28 W7 119.8(5) . .
P1 O29 W7 128.1(5) . .
P1 O29 W8 129.5(5) . .
W7 O29 W8 90.3(3) . .
W8 O31 W15 163.7(5) . .
W8 O32 W9 155.6(5) . .
W9 O34 W10 166.4(5) . .
W10 O35 Cu2 139.5(5) . .
W10 O36 Na3 134.3(5) . 4_576
W10 O36 Na8 133.2(5) . 4_576
Na3 O36 Na8 92.4(4) 4_576 4_576
W15 O37 W10 146.4(5) . .
W10 O38 W11 119.8(4) . .
P2 O39 W11 128.4(5) . .
P2 O39 W10 128.2(5) . .
W11 O39 W10 89.6(3) . .
W11 O40 Cu2 139.4(5) . .
W12 O42 W11 148.4(6) . .
W12 O43 Na11 166.8(6) . .
W12 O44 Cu3 140.3(5) . .
W13 O45 W12 121.9(5) . .
P2 O46 W12 126.7(5) . .
P2 O46 W13 127.2(5) . .
W12 O46 W13 91.5(3) . .
W13 O48 Cu4 132.5(5) . .
W13 O48 Cu3 128.2(4) . .
Cu4 O48 Cu3 95.5(4) . .
W13 O49 W14 144.0(5) . .
W14 O50 Na9 139.3(6) . .
W14 O50 Na4 118.6(5) . .
Na9 O50 Na4 94.0(4) . .
W14 O51 Cu4 134.1(5) . .
W14 O51 Cu1 126.9(5) . .
Cu4 O51 Cu1 94.9(4) . .
W14 O52 W15 121.7(5) . .
P2 O53 W15 126.5(5) . .
P2 O53 W14 127.5(5) . .
W15 O53 W14 91.1(3) . .
W15 O54 Na5 138.6(5) . 4_576
W15 O55 Cu1 140.0(5) . .
W16 O57 Cu4 141.0(6) . .
W16 O58 W17 147.3(5) . .
W23 O59 W16 166.2(6) . .
W21 O60 W16 119.1(5) . .
P3 O61 W21 129.4(5) . .
P3 O61 W16 128.4(5) . .
W21 O61 W16 89.7(3) . .
W17 O63 Cu1 140.1(5) . .
W18 O64 W17 122.8(5) . .
W24 O65 W17 164.3(5) . .
P3 O66 W17 127.2(5) . .
P3 O66 W18 127.5(5) . .
W17 O66 W18 91.0(3) . .
W18 O68 Cu2 132.8(5) . .
W18 O68 Cu1 128.7(4) . .
Cu2 O68 Cu1 95.6(4) . .
W18 O69 W19 144.8(5) . .
W25 O70 W18 163.7(6) . .
W19 O71 Na4 139.6(5) . 4_576
W19 O71 Na9 118.1(5) . 4_576
Na4 O71 Na9 95.9(4) 4_576 4_576
W19 O72 Cu2 134.4(5) . .
W19 O72 Cu3 127.3(5) . .
Cu2 O72 Cu3 93.8(4) . .
W19 O73 W20 120.9(5) . .
W26 O74 W19 162.6(6) . .
W26 O74 Na9 88.6(4) . 4_576
W19 O74 Na9 90.3(4) . 4_576
P3 O75 W20 126.1(5) . .
P3 O75 W19 126.1(5) . .
W20 O75 W19 91.2(3) . .
W20 O77 Cu3 141.0(5) . .
W21 O78 W20 146.4(5) . .
W27 O79 W20 163.3(5) . .
W21 O80 Cu4 139.8(5) . .
W22 O82 W21 165.1(5) . .
W27 O84 W22 156.7(6) . .
W23 O85 W22 121.9(5) . .
W28 O86 W22 148.3(5) . .
P4 O87 W22 127.7(5) . .
P4 O87 W23 126.7(6) . .
W22 O87 W23 90.5(3) . .
W24 O89 W23 156.2(6) . .
W29 O90 W23 149.5(5) . .
W24 O92 W25 121.1(5) . .
W29 O93 W24 150.3(6) . .
P4 O94 W25 131.2(5) . .
P4 O94 W24 128.1(5) . .
W25 O94 W24 89.6(3) . .
W30 O96 W25 149.2(6) . .
W26 O97 W25 155.3(5) . .
W26 O98 Na9 108.0(5) . 4_576
W27 O99 W26 120.5(5) . .
W30 O100 W26 149.0(6) . .
P4 O101 W26 128.3(6) . .
P4 O101 W27 130.6(5) . .
W26 O101 W27 90.5(3) . .
W28 O103 W27 150.6(5) . .
W28 O104 Cu9 165.3(6) . .
W29 O105 W28 123.6(5) . .
W28 O106 W30 123.6(5) . .
P4 O107 W28 124.4(6) . .
P4 O107 W30 125.2(5) . .
W28 O107 W30 92.2(3) . .
P4 O107 W29 121.7(5) . .
W28 O107 W29 92.6(3) . .
W30 O107 W29 91.5(3) . .
W29 O109 W30 122.9(5) . .
P3 O111 Cu1 125.8(6) . .
P3 O111 Cu3 126.0(5) . .
Cu1 O111 Cu3 97.3(4) . .
P2 O112 Cu3 125.7(5) . .
P2 O112 Cu1 124.7(5) . .
Cu3 O112 Cu1 98.1(4) . .
P2 O112 Cu2 117.2(5) . .
Cu3 O112 Cu2 91.5(3) . .
Cu1 O112 Cu2 90.1(3) . .
Cu2 O113 Na4 111.3(4) . 4_576
Cu4 O114 Na9 115.5(6) . .
P5 O115 Cu5 109.9(6) . .
P7 O116 Cu5 106.3(5) . .
C6 O117 Cu6 116.9(8) . .
C6 O117 Cu5 115.4(8) . .
Cu6 O117 Cu5 89.9(4) . .
C16 O118 Cu6 116.6(7) . .
C16 O118 Cu5 116.6(8) . .
Cu6 O118 Cu5 89.3(4) . .
P6 O119 Cu6 117.6(6) . .
P8 O120 Cu6 118.1(6) . .
P10 O122 Cu7 127.8(6) . .
P10 O122 Na2 138.0(6) . 3_665
Cu7 O122 Na2 92.9(4) . 3_665
P8 O123 Cu7 126.1(6) . .
P8 O123 Na2 142.1(6) . 3_665
Cu7 O123 Na2 91.6(4) . 3_665
P7 O124 Cu7 124.2(6) . .
P7 O124 Na1 133.9(6) . 3_665
Cu7 O124 Na1 96.3(4) . 3_665
P9 O125 Cu7 123.0(5) . .
P9 O125 Na1 131.0(6) . 3_665
Cu7 O125 Na1 98.8(4) . 3_665
P12 O127 Cu8 121.3(6) . .
P12 O127 Na7 149.6(6) . 3_665
Cu8 O127 Na7 88.0(4) . 3_665
P6 O128 Cu8 126.5(6) . .
P6 O128 Na7 142.8(6) . 3_665
Cu8 O128 Na7 89.2(4) . 3_665
P5 O129 Cu8 121.2(6) . .
P5 O129 Na1 133.1(6) . 3_665
Cu8 O129 Na1 100.0(4) . 3_665
P11 O130 Cu8 122.2(6) . .
P11 O130 Na1 136.7(6) . 3_665
Cu8 O130 Na1 97.2(4) . 3_665
P9 O131 Cu9 109.8(5) . .
C1 O132 Cu10 116.6(8) . .
C1 O132 Cu9 115.9(8) . .
Cu10 O132 Cu9 90.6(4) . .
P11 O133 Cu9 107.3(5) . .
C11 O134 Cu10 115.6(8) . .
C11 O134 Cu9 114.9(8) . .
Cu10 O134 Cu9 88.5(4) . .
P10 O135 Cu10 118.0(6) . .
P12 O136 Cu10 115.2(6) . .
O132 C1 C2 105.4(10) . .
O132 C1 P11 106.1(9) . .
C2 C1 P11 114.7(10) . .
O132 C1 P12 107.9(9) . .
C2 C1 P12 112.6(10) . .
P11 C1 P12 109.6(7) . .
C3 C2 C1 115.3(12) . .
C3 C2 H2A 108.5 . .
C1 C2 H2A 108.5 . .
C3 C2 H2B 108.5 . .
C1 C2 H2B 108.5 . .
H2A C2 H2B 107.5 . .
C4 C3 C2 110.4(12) . .
C4 C3 H3A 109.6 . .
C2 C3 H3A 109.6 . .
C4 C3 H3B 109.6 . .
C2 C3 H3B 109.6 . .
H3A C3 H3B 108.1 . .
C3 C4 N5 111.0(12) . .
C3 C4 H4A 109.4 . .
N5 C4 H4A 109.4 . .
C3 C4 H4B 109.4 . .
N5 C4 H4B 109.4 . .
H4A C4 H4B 108.0 . .
C4 N5 H5A 109.5 . .
C4 N5 H5B 109.5 . .
H5A N5 H5B 109.5 . .
C4 N5 H5C 109.5 . .
H5A N5 H5C 109.5 . .
H5B N5 H5C 109.5 . .
O117 C6 C7 111.2(11) . .
O117 C6 P7 105.5(8) . .
C7 C6 P7 113.5(10) . .
O117 C6 P8 106.8(9) . .
C7 C6 P8 111.2(9) . .
P7 C6 P8 108.3(7) . .
C6 C7 C8 114.1(11) . .
C6 C7 H7A 108.7 . .
C8 C7 H7A 108.7 . .
C6 C7 H7B 108.7 . .
C8 C7 H7B 108.7 . .
H7A C7 H7B 107.6 . .
C9 C8 C7 109.0(12) . .
C9 C8 H8A 109.9 . .
C7 C8 H8A 109.9 . .
C9 C8 H8B 109.9 . .
C7 C8 H8B 109.9 . .
H8A C8 H8B 108.3 . .
N10 C9 C8 109.1(13) . .
N10 C9 H9A 109.9 . .
C8 C9 H9A 109.9 . .
N10 C9 H9B 109.9 . .
C8 C9 H9B 109.9 . .
H9A C9 H9B 108.3 . .
C9 N10 H10A 109.5 . .
C9 N10 H10B 109.5 . .
H10A N10 H10B 109.5 . .
C9 N10 H10C 109.5 . .
H10A N10 H10C 109.5 . .
H10B N10 H10C 109.5 . .
O134 C11 C12 105.1(11) . .
O134 C11 P9 107.0(9) . .
C12 C11 P9 115.0(10) . .
O134 C11 P10 106.8(9) . .
C12 C11 P10 109.8(10) . .
P9 C11 P10 112.5(7) . .
C13 C12 C11 115.8(12) . .
C13 C12 H12A 108.3 . .
C11 C12 H12A 108.3 . .
C13 C12 H12B 108.3 . .
C11 C12 H12B 108.3 . .
H12A C12 H12B 107.4 . .
C12 C13 C14 108.9(12) . .
C12 C13 H13A 109.9 . .
C14 C13 H13A 109.9 . .
C12 C13 H13B 109.9 . .
C14 C13 H13B 109.9 . .
H13A C13 H13B 108.3 . .
N15 C14 C13 112.3(12) . .
N15 C14 H14A 109.1 . .
C13 C14 H14A 109.1 . .
N15 C14 H14B 109.1 . .
C13 C14 H14B 109.1 . .
H14A C14 H14B 107.9 . .
C14 N15 H15A 109.5 . .
C14 N15 H15B 109.5 . .
H15A N15 H15B 109.5 . .
C14 N15 H15C 109.5 . .
H15A N15 H15C 109.5 . .
H15B N15 H15C 109.5 . .
C17 C16 O118 107.3(10) . .
C17 C16 P6 112.0(10) . .
O118 C16 P6 106.6(9) . .
C17 C16 P5 113.9(10) . .
O118 C16 P5 104.6(8) . .
P6 C16 P5 111.7(7) . .
C16 C17 C18 116.7(11) . .
C16 C17 H17A 108.1 . .
C18 C17 H17A 108.1 . .
C16 C17 H17B 108.1 . .
C18 C17 H17B 108.1 . .
H17A C17 H17B 107.3 . .
C19 C18 C17 109.9(12) . .
C19 C18 H18A 109.7 . .
C17 C18 H18A 109.7 . .
C19 C18 H18B 109.7 . .
C17 C18 H18B 109.7 . .
H18A C18 H18B 108.2 . .
N20 C19 C18 111.5(12) . .
N20 C19 H19A 109.3 . .
C18 C19 H19A 109.3 . .
N20 C19 H19B 109.3 . .
C18 C19 H19B 109.3 . .
H19A C19 H19B 108.0 . .
C19 N20 H20A 109.5 . .
C19 N20 H20B 109.5 . .
H20A N20 H20B 109.5 . .
C19 N20 H20C 109.5 . .
H20A N20 H20C 109.5 . .
H20B N20 H20C 109.5 . .
O129 Na1 O125 128.9(5) 3_665 3_665
O129 Na1 O130 70.8(4) 3_665 3_665
O125 Na1 O130 90.5(4) 3_665 3_665
O129 Na1 O124 89.8(4) 3_665 3_665
O125 Na1 O124 70.3(4) 3_665 3_665
O130 Na1 O124 135.1(5) 3_665 3_665
O129 Na1 O21W 92.1(5) 3_665 3_665
O125 Na1 O21W 131.5(6) 3_665 3_665
O130 Na1 O21W 131.7(6) 3_665 3_665
O124 Na1 O21W 87.5(5) 3_665 3_665
O129 Na1 O24W 129.2(7) 3_665 1_554
O125 Na1 O24W 93.9(6) 3_665 1_554
O130 Na1 O24W 84.7(6) 3_665 1_554
O124 Na1 O24W 135.0(7) 3_665 1_554
O21W Na1 O24W 71.7(7) 3_665 1_554
O129 Na1 Cu8 36.5(3) 3_665 3_665
O125 Na1 Cu8 105.4(3) 3_665 3_665
O130 Na1 Cu8 36.5(3) 3_665 3_665
O124 Na1 Cu8 108.7(3) 3_665 3_665
O21W Na1 Cu8 122.7(5) 3_665 3_665
O24W Na1 Cu8 116.1(6) 1_554 3_665
O129 Na1 Cu7 103.7(3) 3_665 3_665
O125 Na1 Cu7 36.8(2) 3_665 3_665
O130 Na1 Cu7 108.3(3) 3_665 3_665
O124 Na1 Cu7 36.2(2) 3_665 3_665
O21W Na1 Cu7 119.8(5) 3_665 3_665
O24W Na1 Cu7 126.4(6) 1_554 3_665
Cu8 Na1 Cu7 100.5(2) 3_665 3_665
O122 Na2 O11W 88.5(4) 3_665 1_554
O122 Na2 O28W 174.1(5) 3_665 1_554
O11W Na2 O28W 91.2(7) 1_554 1_554
O122 Na2 O123 68.8(4) 3_665 3_665
O11W Na2 O123 89.9(4) 1_554 3_665
O28W Na2 O123 105.3(5) 1_554 3_665
O122 Na2 O22W 85.7(5) 3_665 1_554
O11W Na2 O22W 87.9(6) 1_554 1_554
O28W Na2 O22W 100.2(6) 1_554 1_554
O123 Na2 O22W 154.4(6) 3_665 1_554
O122 Na2 O4W 84.6(4) 3_665 1_554
O11W Na2 O4W 168.8(5) 1_554 1_554
O28W Na2 O4W 94.7(6) 1_554 1_554
O123 Na2 O4W 79.5(4) 3_665 1_554
O22W Na2 O4W 100.3(6) 1_554 1_554
O122 Na2 Cu7 37.9(2) 3_665 3_665
O11W Na2 Cu7 106.2(4) 1_554 3_665
O28W Na2 Cu7 137.0(5) 1_554 3_665
O123 Na2 Cu7 38.1(2) 3_665 3_665
O22W Na2 Cu7 119.0(5) 1_554 3_665
O4W Na2 Cu7 63.2(3) 1_554 3_665
O1W Na3 O13W 92.7(5) 1_554 1_554
O1W Na3 O7W 175.1(5) 1_554 1_554
O13W Na3 O7W 88.6(5) 1_554 1_554
O1W Na3 O5W 96.6(5) 1_554 1_554
O13W Na3 O5W 86.1(5) 1_554 1_554
O7W Na3 O5W 88.3(5) 1_554 1_554
O1W Na3 O3W 81.5(4) 1_554 1_554
O13W Na3 O3W 93.9(5) 1_554 1_554
O7W Na3 O3W 93.6(5) 1_554 1_554
O5W Na3 O3W 178.1(5) 1_554 1_554
O1W Na3 O36 94.1(4) 1_554 4_575
O13W Na3 O36 172.0(5) 1_554 4_575
O7W Na3 O36 85.0(4) 1_554 4_575
O5W Na3 O36 89.0(4) 1_554 4_575
O3W Na3 O36 91.2(4) 1_554 4_575
O1W Na3 Na5 42.6(3) 1_554 .
O13W Na3 Na5 82.9(4) 1_554 .
O7W Na3 Na5 133.0(4) 1_554 .
O5W Na3 Na5 136.6(4) 1_554 .
O3W Na3 Na5 41.6(3) 1_554 .
O36 Na3 Na5 105.0(3) 4_575 .
O1W Na3 Na8 138.7(4) 1_554 .
O13W Na3 Na8 128.3(4) 1_554 .
O7W Na3 Na8 40.8(3) 1_554 .
O5W Na3 Na8 83.5(4) 1_554 .
O3W Na3 Na8 98.0(4) 1_554 .
O36 Na3 Na8 44.7(3) 4_575 .
Na5 Na3 Na8 134.7(2) . .
O71 Na4 O20W 85.3(5) 4_575 1_554
O71 Na4 O9W 105.9(5) 4_575 1_554
O20W Na4 O9W 166.5(5) 1_554 1_554
O71 Na4 O50 76.1(4) 4_575 .
O20W Na4 O50 98.5(5) 1_554 .
O9W Na4 O50 77.6(4) 1_554 .
O71 Na4 O26 161.7(4) 4_575 .
O20W Na4 O26 79.8(5) 1_554 .
O9W Na4 O26 90.3(4) 1_554 .
O50 Na4 O26 116.6(4) . .
O71 Na4 O113 85.2(4) 4_575 4_575
O20W Na4 O113 106.9(5) 1_554 4_575
O9W Na4 O113 81.8(4) 1_554 4_575
O50 Na4 O113 147.0(4) . 4_575
O26 Na4 O113 88.8(4) . 4_575
O71 Na4 O27 131.9(4) 4_575 .
O20W Na4 O27 86.8(4) 1_554 .
O9W Na4 O27 80.2(4) 1_554 .
O50 Na4 O27 58.4(3) . .
O26 Na4 O27 58.2(3) . .
O113 Na4 O27 142.0(4) 4_575 .
O71 Na4 W7 161.7(4) 4_575 .
O20W Na4 W7 86.0(4) 1_554 .
O9W Na4 W7 81.1(3) 1_554 .
O50 Na4 W7 89.3(3) . .
O26 Na4 W7 27.5(2) . .
O113 Na4 W7 112.8(3) 4_575 .
O27 Na4 W7 31.24(18) . .
O71 Na4 Na9 43.9(3) 4_575 .
O20W Na4 Na9 113.6(5) 1_554 .
O9W Na4 Na9 72.2(4) 1_554 .
O50 Na4 Na9 41.8(3) . .
O26 Na4 Na9 153.8(4) . .
O113 Na4 Na9 107.1(3) 4_575 .
O27 Na4 Na9 98.7(3) . .
W7 Na4 Na9 127.4(2) . .
O71 Na4 W14 100.4(3) 4_575 .
O20W Na4 W14 97.4(4) 1_554 .
O9W Na4 W14 73.7(3) 1_554 .
O50 Na4 W14 24.5(2) . .
O26 Na4 W14 92.2(3) . .
O113 Na4 W14 155.4(3) 4_575 .
O27 Na4 W14 34.21(18) . .
W7 Na4 W14 64.76(10) . .
Na9 Na4 W14 64.6(2) . .
O3W Na5 O54 94.0(4) 1_554 4_575
O3W Na5 O11W 91.9(5) 1_554 1_554
O54 Na5 O11W 174.1(5) 4_575 1_554
O3W Na5 O23W 98.0(6) 1_554 1_554
O54 Na5 O23W 90.6(5) 4_575 1_554
O11W Na5 O23W 88.6(6) 1_554 1_554
O3W Na5 O1W 80.9(4) 1_554 1_554
O54 Na5 O1W 90.5(4) 4_575 1_554
O11W Na5 O1W 90.5(4) 1_554 1_554
O23W Na5 O1W 178.5(6) 1_554 1_554
O3W Na5 O17W 172.5(5) 1_554 1_554
O54 Na5 O17W 83.0(5) 4_575 1_554
O11W Na5 O17W 91.2(5) 1_554 1_554
O23W Na5 O17W 88.9(6) 1_554 1_554
O1W Na5 O17W 92.3(5) 1_554 1_554
O3W Na5 Na3 42.6(3) 1_554 .
O54 Na5 Na3 104.3(3) 4_575 .
O11W Na5 Na3 80.2(3) 1_554 .
O23W Na5 Na3 137.7(5) 1_554 .
O1W Na5 Na3 40.9(3) 1_554 .
O17W Na5 Na3 131.6(5) 1_554 .
O14W Na6 O1 93.8(5) 1_554 .
O14W Na6 O16W 90.4(5) 1_554 1_554
O1 Na6 O16W 175.4(5) . 1_554
O14W Na6 O6W 166.1(6) 1_554 1_554
O1 Na6 O6W 91.4(4) . 1_554
O16W Na6 O6W 84.1(5) 1_554 1_554
O14W Na6 O10W 104.3(6) 1_554 1_554
O1 Na6 O10W 83.0(5) . 1_554
O16W Na6 O10W 97.5(6) 1_554 1_554
O6W Na6 O10W 89.2(5) 1_554 1_554
O14W Na6 O12W 86.9(5) 1_554 1_554
O1 Na6 O12W 79.8(4) . 1_554
O16W Na6 O12W 98.8(6) 1_554 1_554
O6W Na6 O12W 81.3(5) 1_554 1_554
O10W Na6 O12W 160.2(6) 1_554 1_554
O14W Na6 Na8 124.3(4) 1_554 .
O1 Na6 Na8 97.4(3) . .
O16W Na6 Na8 78.9(5) 1_554 .
O6W Na6 Na8 42.0(3) 1_554 .
O10W Na6 Na8 131.1(5) 1_554 .
O12W Na6 Na8 42.8(3) 1_554 .
O128 Na7 O19W 109.8(6) 3_665 1_554
O128 Na7 O127 71.0(4) 3_665 3_665
O19W Na7 O127 102.2(5) 1_554 3_665
O128 Na7 O18W 150.7(5) 3_665 1_554
O19W Na7 O18W 98.7(6) 1_554 1_554
O127 Na7 O18W 109.9(5) 3_665 1_554
O128 Na7 O25W 88.1(5) 3_665 1_654
O19W Na7 O25W 82.2(6) 1_554 1_654
O127 Na7 O25W 159.0(5) 3_665 1_654
O18W Na7 O25W 89.4(6) 1_554 1_654
O128 Na7 O2W 80.9(4) 3_665 1_554
O19W Na7 O2W 167.7(6) 1_554 1_554
O127 Na7 O2W 75.1(4) 3_665 1_554
O18W Na7 O2W 71.5(5) 1_554 1_554
O25W Na7 O2W 104.7(5) 1_654 1_554
O128 Na7 Cu8 40.3(3) 3_665 3_665
O19W Na7 Cu8 130.0(5) 1_554 3_665
O127 Na7 Cu8 40.3(3) 3_665 3_665
O18W Na7 Cu8 121.9(4) 1_554 3_665
O25W Na7 Cu8 122.2(4) 1_654 3_665
O2W Na7 Cu8 54.9(3) 1_554 3_665
O128 Na7 Na10 139.3(4) 3_665 3_765
O19W Na7 Na10 34.8(4) 1_554 3_765
O127 Na7 Na10 123.5(4) 3_665 3_765
O18W Na7 Na10 66.1(4) 1_554 3_765
O25W Na7 Na10 71.3(4) 1_654 3_765
O2W Na7 Na10 137.4(4) 1_554 3_765
Cu8 Na7 Na10 162.1(3) 3_665 3_765
O26W Na8 O7W 167.2(5) 1_554 1_554
O26W Na8 O27W 93.4(6) 1_554 1_554
O7W Na8 O27W 88.1(6) 1_554 1_554
O26W Na8 O6W 92.1(5) 1_554 1_554
O7W Na8 O6W 86.5(5) 1_554 1_554
O27W Na8 O6W 174.5(7) 1_554 1_554
O26W Na8 O12W 90.5(5) 1_554 1_554
O7W Na8 O12W 102.1(5) 1_554 1_554
O27W Na8 O12W 94.9(6) 1_554 1_554
O6W Na8 O12W 85.1(5) 1_554 1_554
O26W Na8 O36 83.4(4) 1_554 4_575
O7W Na8 O36 83.8(4) 1_554 4_575
O27W Na8 O36 100.3(6) 1_554 4_575
O6W Na8 O36 80.3(4) 1_554 4_575
O12W Na8 O36 163.9(5) 1_554 4_575
O26W Na8 Na6 105.9(4) 1_554 .
O7W Na8 Na6 81.5(4) 1_554 .
O27W Na8 Na6 135.6(6) 1_554 .
O6W Na8 Na6 42.2(3) 1_554 .
O12W Na8 Na6 46.6(3) 1_554 .
O36 Na8 Na6 121.1(3) 4_575 .
O26W Na8 Na3 126.0(4) 1_554 .
O7W Na8 Na3 41.3(3) 1_554 .
O27W Na8 Na3 99.9(5) 1_554 .
O6W Na8 Na3 76.7(3) 1_554 .
O12W Na8 Na3 139.1(4) 1_554 .
O36 Na8 Na3 42.9(3) 4_575 .
Na6 Na8 Na3 100.0(2) . .
O33W Na9 O50 85.5(7) 4_575 .
O33W Na9 O114 102.8(8) 4_575 .
O50 Na9 O114 83.5(5) . .
O33W Na9 O71 104.4(8) 4_575 4_575
O50 Na9 O71 75.0(4) . 4_575
O114 Na9 O71 143.5(6) . 4_575
O33W Na9 O98 79.8(7) 4_575 4_575
O50 Na9 O98 162.0(6) . 4_575
O114 Na9 O98 89.8(5) . 4_575
O71 Na9 O98 118.5(5) 4_575 4_575
O33W Na9 O74 89.9(7) 4_575 4_575
O50 Na9 O74 130.8(5) . 4_575
O114 Na9 O74 144.7(5) . 4_575
O71 Na9 O74 58.9(4) 4_575 4_575
O98 Na9 O74 59.8(4) 4_575 4_575
O33W Na9 W26 87.5(6) 4_575 4_575
O50 Na9 W26 161.3(5) . 4_575
O114 Na9 W26 115.0(5) . 4_575
O71 Na9 W26 90.1(4) 4_575 4_575
O98 Na9 W26 28.5(2) 4_575 4_575
O74 Na9 W26 31.8(2) 4_575 4_575
O33W Na9 Na4 116.8(7) 4_575 .
O50 Na9 Na4 44.2(3) . .
O114 Na9 Na4 105.1(4) . .
O71 Na9 Na4 40.2(3) 4_575 .
O98 Na9 Na4 153.5(5) 4_575 .
O74 Na9 Na4 97.9(4) 4_575 .
W26 Na9 Na4 126.8(3) 4_575 .
O33W Na9 W19 102.1(7) 4_575 4_575
O50 Na9 W19 99.3(4) . 4_575
O114 Na9 W19 155.1(5) . 4_575
O71 Na9 W19 24.7(2) 4_575 4_575
O98 Na9 W19 93.8(4) 4_575 4_575
O74 Na9 W19 34.4(2) 4_575 4_575
W26 Na9 W19 65.34(18) 4_575 4_575
Na4 Na9 W19 63.6(2) . 4_575
O11 Na10 O19W 104.8(6) . 3_766
O11 Na10 Na10 119.9(6) . 3_765
O19W Na10 Na10 134.6(6) 3_766 3_765
O11 Na10 Na7 76.3(4) . 3_765
O19W Na10 Na7 32.4(4) 3_766 3_765
Na10 Na10 Na7 162.3(4) 3_765 3_765
Na3 O1W Na5 96.5(4) 1_556 1_556
Na5 O3W Na3 95.9(5) 1_556 1_556
Na8 O6W Na6 95.8(5) 1_556 1_556
Na8 O7W Na3 97.9(5) 1_556 1_556
Na2 O11W Na5 137.7(6) 1_556 1_556
Na8 O12W Na6 90.6(5) 1_556 1_556
Na7 O19W Na10 112.8(7) 1_556 3_766
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O1 1.709(10) .
W1 O2 1.861(9) .
W1 O3 1.895(9) .
W1 O4 1.920(9) .
W1 O5 1.951(9) .
W1 O6 2.396(9) .
W2 O7 1.732(10) 4_675
W2 O8 1.863(9) .
W2 O9 1.868(9) .
W2 O5 1.935(9) .
W2 O10 1.937(9) .
W2 O6 2.342(9) .
W3 O11 1.733(10) .
W3 O13 1.857(9) .
W3 O12 1.880(9) .
W3 O4 1.942(9) .
W3 O10 1.974(9) .
W3 O6 2.387(9) .
W4 O14 1.713(9) .
W4 O15 1.811(9) .
W4 O16 1.900(9) .
W4 O17 1.938(9) .
W4 O12 1.977(9) .
W4 O18 2.355(9) .
W5 O19 1.729(9) .
W5 O20 1.796(9) .
W5 O16 1.887(9) .
W5 O21 1.908(9) .
W5 O13 2.009(9) .
W5 O22 2.337(9) .
W6 O23 1.715(10) .
W6 O24 1.803(9) .
W6 O25 1.907(10) .
W6 O21 1.915(9) .
W6 O2 2.004(9) .
W6 O22 2.396(9) .
W7 O26 1.715(9) .
W7 O27 1.805(9) .
W7 O25 1.878(10) .
W7 O28 1.957(9) .
W7 O3 1.975(9) .
W7 O29 2.340(9) .
W7 Na4 3.480(6) .
W8 O30 1.735(9) .
W8 O31 1.818(9) .
W8 O32 1.881(9) .
W8 O28 1.904(9) .
W8 O9 2.023(9) .
W8 O29 2.371(9) .
W9 O33 1.708(9) .
W9 O34 1.819(9) .
W9 O17 1.882(9) .
W9 O32 1.907(9) .
W9 O8 2.033(9) .
W9 O18 2.392(9) .
W10 O36 1.750(9) .
W10 O35 1.779(8) .
W10 O37 1.913(9) .
W10 O38 1.927(9) .
W10 O34 2.033(9) .
W10 O39 2.384(9) .
W11 O41 1.726(9) .
W11 O40 1.782(9) .
W11 O42 1.900(9) .
W11 O38 1.954(9) .
W11 O15 2.045(9) .
W11 O39 2.379(8) .
W12 O43 1.743(9) .
W12 O44 1.794(9) .
W12 O42 1.897(9) .
W12 O45 1.945(9) .
W12 O20 2.065(9) .
W12 O46 2.310(9) .
W13 O47 1.717(9) .
W13 O48 1.803(9) .
W13 O45 1.899(9) .
W13 O49 1.904(9) .
W13 O24 2.052(9) .
W13 O46 2.382(9) .
W14 O50 1.719(9) .
W14 O51 1.785(9) .
W14 O52 1.908(9) .
W14 O49 1.920(9) .
W14 O27 2.043(9) .
W14 O53 2.363(8) .
W14 Na4 3.634(6) .
W15 O54 1.703(9) .
W15 O55 1.781(9) .
W15 O37 1.882(9) .
W15 O52 1.933(9) .
W15 O31 2.071(9) .
W15 O53 2.337(9) .
W16 O56 1.733(9) .
W16 O57 1.768(9) .
W16 O58 1.891(9) .
W16 O60 1.951(10) .
W16 O59 2.054(9) .
W16 O61 2.397(9) .
W17 O62 1.738(9) .
W17 O63 1.774(9) .
W17 O58 1.914(9) .
W17 O64 1.935(9) .
W17 O65 2.043(9) .
W17 O66 2.314(9) .
W18 O67 1.699(9) .
W18 O68 1.797(9) .
W18 O69 1.894(9) .
W18 O64 1.896(9) .
W18 O70 2.065(9) .
W18 O66 2.403(9) .
W19 O71 1.716(9) .
W19 O72 1.775(9) .
W19 O69 1.915(9) .
W19 O73 1.916(9) .
W19 O74 2.044(9) .
W19 O75 2.378(9) .
W19 Na9 3.617(11) 4_576
W20 O76 1.708(10) .
W20 O77 1.791(9) .
W20 O78 1.914(9) .
W20 O73 1.935(9) .
W20 O79 2.078(9) .
W20 O75 2.309(10) .
W21 O81 1.722(10) .
W21 O80 1.789(9) .
W21 O78 1.890(9) .
W21 O60 1.926(9) .
W21 O82 2.056(9) .
W21 O61 2.343(9) .
W22 O83 1.710(9) .
W22 O82 1.809(9) .
W22 O84 1.916(9) .
W22 O85 1.922(9) .
W22 O86 1.997(9) .
W22 O87 2.355(10) .
W23 O88 1.736(9) .
W23 O59 1.806(9) .
W23 O89 1.902(10) .
W23 O85 1.919(10) .
W23 O90 1.993(9) .
W23 O87 2.373(9) .
W24 O91 1.725(9) .
W24 O65 1.815(9) .
W24 O89 1.875(10) .
W24 O92 1.918(9) .
W24 O93 1.995(9) .
W24 O94 2.382(9) .
W25 O95 1.714(9) .
W25 O70 1.777(9) .
W25 O97 1.902(10) .
W25 O92 1.922(9) .
W25 O96 2.000(9) .
W25 O94 2.365(9) .
W26 O98 1.727(9) .
W26 O74 1.817(9) .
W26 O97 1.886(10) .
W26 O99 1.936(10) .
W26 O100 1.994(9) .
W26 O101 2.345(9) .
W26 Na9 3.446(10) 4_576
W27 O102 1.741(12) .
W27 O79 1.810(9) .
W27 O84 1.863(9) .
W27 O99 1.909(9) .
W27 O103 2.008(9) .
W27 O101 2.357(10) .
W28 O104 1.749(10) .
W28 O103 1.862(9) .
W28 O86 1.888(10) .
W28 O106 1.933(10) .
W28 O105 1.949(10) .
W28 O107 2.359(9) .
W29 O108 1.734(10) .
W29 O90 1.862(10) .
W29 O93 1.862(10) .
W29 O109 1.937(10) .
W29 O105 1.940(10) .
W29 O107 2.382(9) .
W30 O110 1.710(10) .
W30 O96 1.866(9) .
W30 O100 1.875(10) .
W30 O106 1.937(10) .
W30 O109 1.941(10) .
W30 O107 2.373(9) .
Cu1 O55 1.940(9) .
Cu1 O63 1.941(9) .
Cu1 O111 2.032(9) .
Cu1 O112 2.046(9) .
Cu1 O68 2.317(9) .
Cu1 O51 2.371(9) .
Cu2 O40 1.962(9) .
Cu2 O68 1.971(9) .
Cu2 O35 1.972(9) .
Cu2 O72 1.989(9) .
Cu2 O113 2.377(10) .
Cu2 O112 2.436(9) .
Cu3 O77 1.926(9) .
Cu3 O44 1.934(9) .
Cu3 O112 2.024(9) .
Cu3 O111 2.063(9) .
Cu3 O48 2.333(9) .
Cu3 O72 2.387(9) .
Cu4 O80 1.953(9) .
Cu4 O57 1.962(10) .
Cu4 O51 1.977(9) .
Cu4 O48 1.980(9) .
Cu4 O114 2.377(10) .
Cu5 O115 1.939(10) .
Cu5 O117 1.962(9) .
Cu5 O116 1.967(10) .
Cu5 O118 1.984(10) .
Cu5 O7 2.203(10) .
Cu5 Cu6 2.770(2) .
Cu5 P7 2.824(4) .
Cu5 P5 2.864(4) .
Cu6 O120 1.926(10) .
Cu6 O119 1.944(10) .
Cu6 O117 1.958(9) .
Cu6 O118 1.959(9) .
Cu6 O121 2.395(12) .
Cu7 O124 1.930(9) .
Cu7 O122 1.934(9) .
Cu7 O123 1.941(9) .
Cu7 O125 1.967(9) .
Cu7 Na2 3.146(6) 3_665
Cu7 Na1 3.246(6) 3_665
Cu8 O130 1.937(10) .
Cu8 O127 1.951(10) .
Cu8 O128 1.951(9) .
Cu8 O129 1.952(9) .
Cu8 Na7 3.018(7) 3_665
Cu8 Na1 3.234(6) 3_665
Cu9 O131 1.923(10) .
Cu9 O132 1.961(9) .
Cu9 O133 1.969(9) .
Cu9 O134 2.007(9) .
Cu9 O104 2.226(10) .
Cu9 Cu10 2.780(2) .
Cu9 P11 2.839(4) .
Cu9 P9 2.849(4) .
Cu10 O135 1.930(10) .
Cu10 O132 1.950(9) .
Cu10 O136 1.963(9) .
Cu10 O134 1.977(9) .
Cu10 O15W 2.321(11) .
P1 O29 1.510(10) .
P1 O22 1.533(10) .
P1 O18 1.539(10) .
P1 O6 1.572(10) .
P2 O53 1.518(9) .
P2 O39 1.526(9) .
P2 O46 1.538(10) .
P2 O112 1.576(10) .
P3 O66 1.512(10) .
P3 O61 1.531(10) .
P3 O75 1.534(10) .
P3 O111 1.553(10) .
P4 O94 1.508(10) .
P4 O101 1.533(10) .
P4 O87 1.548(10) .
P4 O107 1.579(10) .
P5 O137 1.529(11) .
P5 O129 1.547(10) .
P5 O115 1.549(11) .
P5 C16 1.849(15) .
P6 O128 1.518(10) .
P6 O138 1.532(11) .
P6 O119 1.535(11) .
P6 C16 1.840(14) .
P7 O139 1.522(11) .
P7 O116 1.547(10) .
P7 O124 1.549(10) .
P7 C6 1.868(14) .
P8 O123 1.516(10) .
P8 O120 1.542(11) .
P8 O140 1.548(11) .
P8 C6 1.902(14) .
P9 O141 1.534(11) .
P9 O125 1.536(10) .
P9 O131 1.549(10) .
P9 C11 1.842(15) .
P10 O142 1.500(10) .
P10 O135 1.530(10) .
P10 O122 1.534(10) .
P10 C11 1.866(15) .
P11 O143 1.497(10) .
P11 O133 1.541(10) .
P11 O130 1.557(10) .
P11 C1 1.857(15) .
P12 O144 1.507(11) .
P12 O127 1.548(10) .
P12 O136 1.551(10) .
P12 C1 1.863(14) .
O1 Na6 2.374(12) .
O7 W2 1.732(10) 4_476
O11 Na10 2.343(13) .
O26 Na4 2.484(11) .
O27 Na4 2.979(10) .
O36 Na3 2.449(11) 4_576
O36 Na8 2.529(12) 4_576
O43 Na11 2.298(15) .
O50 Na9 2.375(14) .
O50 Na4 2.484(11) .
O54 Na5 2.415(11) 4_576
O71 Na4 2.307(11) 4_576
O71 Na9 2.477(14) 4_576
O74 Na9 2.973(14) 4_576
O98 Na9 2.497(14) 4_576
O113 Na4 2.503(11) 4_576
O114 Na9 2.383(15) .
O117 C6 1.455(16) .
O118 C16 1.502(16) .
O122 Na2 2.385(12) 3_665
O123 Na2 2.421(11) 3_665
O124 Na1 2.407(11) 3_665
O125 Na1 2.297(11) 3_665
O127 Na7 2.370(11) 3_665
O128 Na7 2.330(12) 3_665
O129 Na1 2.261(11) 3_665
O130 Na1 2.360(11) 3_665
O132 C1 1.452(15) .
O134 C11 1.454(16) .
C1 C2 1.533(19) .
C2 C3 1.52(2) .
C2 H2A 0.9900 .
C2 H2B 0.9900 .
C3 C4 1.51(2) .
C3 H3A 0.9900 .
C3 H3B 0.9900 .
C4 N5 1.553(19) .
C4 H4A 0.9900 .
C4 H4B 0.9900 .
N5 H5A 0.9100 .
N5 H5B 0.9100 .
N5 H5C 0.9100 .
C6 C7 1.493(19) .
C7 C8 1.58(2) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C8 C9 1.54(2) .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 N10 1.48(2) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
N10 H10A 0.9100 .
N10 H10B 0.9100 .
N10 H10C 0.9100 .
C11 C12 1.541(19) .
C12 C13 1.52(2) .
C12 H12A 0.9900 .
C12 H12B 0.9900 .
C13 C14 1.567(19) .
C13 H13A 0.9900 .
C13 H13B 0.9900 .
C14 N15 1.42(2) .
C14 H14A 0.9900 .
C14 H14B 0.9900 .
N15 H15A 0.9100 .
N15 H15B 0.9100 .
N15 H15C 0.9100 .
C16 C17 1.480(19) .
C17 C18 1.55(2) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C19 1.517(19) .
C18 H18A 0.9900 .
C18 H18B 0.9900 .
C19 N20 1.49(2) .
C19 H19A 0.9900 .
C19 H19B 0.9900 .
N20 H20A 0.9100 .
N20 H20B 0.9100 .
N20 H20C 0.9100 .
Na1 O129 2.261(11) 3_665
Na1 O125 2.297(11) 3_665
Na1 O130 2.360(11) 3_665
Na1 O124 2.407(11) 3_665
Na1 O21W 2.55(2) 3_665
Na1 O24W 2.64(3) 1_554
Na1 Cu8 3.234(6) 3_665
Na1 Cu7 3.246(6) 3_665
Na2 O122 2.385(12) 3_665
Na2 O11W 2.408(14) 1_554
Na2 O28W 2.413(16) 1_554
Na2 O123 2.420(11) 3_665
Na2 O22W 2.463(19) 1_554
Na2 O4W 2.468(14) 1_554
Na2 Cu7 3.146(6) 3_665
Na3 O1W 2.355(12) 1_554
Na3 O13W 2.367(15) 1_554
Na3 O7W 2.397(14) 1_554
Na3 O5W 2.424(13) 1_554
Na3 O3W 2.429(13) 1_554
Na3 O36 2.449(11) 4_575
Na3 Na5 3.573(9) .
Na3 Na8 3.594(10) .
Na4 O71 2.307(11) 4_575
Na4 O20W 2.316(17) 1_554
Na4 O9W 2.395(15) 1_554
Na4 O113 2.503(11) 4_575
Na4 Na9 3.556(12) .
Na5 O3W 2.384(14) 1_554
Na5 O54 2.415(11) 4_575
Na5 O11W 2.418(13) 1_554
Na5 O23W 2.426(18) 1_554
Na5 O1W 2.434(13) 1_554
Na5 O17W 2.452(17) 1_554
Na6 O14W 2.371(15) 1_554
Na6 O16W 2.382(15) 1_554
Na6 O6W 2.409(13) 1_554
Na6 O10W 2.431(16) 1_554
Na6 O12W 2.595(15) 1_554
Na6 Na8 3.569(10) .
Na7 O128 2.330(12) 3_665
Na7 O19W 2.361(17) 1_554
Na7 O127 2.370(11) 3_665
Na7 O18W 2.422(16) 1_554
Na7 O25W 2.494(18) 1_654
Na7 O2W 2.557(14) 1_554
Na7 Cu8 3.018(7) 3_665
Na7 Na10 4.062(13) 3_765
Na8 O26W 2.296(14) 1_554
Na8 O7W 2.369(14) 1_554
Na8 O27W 2.39(2) 1_554
Na8 O6W 2.401(14) 1_554
Na8 O12W 2.424(15) 1_554
Na8 O36 2.529(12) 4_575
Na9 O33W 1.64(2) 4_575
Na9 O71 2.477(14) 4_575
Na9 O98 2.497(14) 4_575
Na9 O74 2.974(14) 4_575
Na9 W26 3.446(10) 4_575
Na9 W19 3.617(11) 4_575
Na10 O19W 2.51(2) 3_766
Na10 Na10 3.44(2) 3_765
Na10 Na7 4.062(13) 3_765
O1W Na3 2.355(12) 1_556
O1W Na5 2.434(13) 1_556
O2W Na7 2.557(14) 1_556
O3W Na5 2.384(14) 1_556
O3W Na3 2.429(13) 1_556
O4W Na2 2.469(14) 1_556
O5W Na3 2.424(13) 1_556
O6W Na8 2.401(14) 1_556
O6W Na6 2.409(13) 1_556
O7W Na8 2.369(14) 1_556
O7W Na3 2.397(14) 1_556
O9W Na4 2.395(15) 1_556
O10W Na6 2.432(16) 1_556
O11W Na2 2.408(14) 1_556
O11W Na5 2.418(13) 1_556
O12W Na8 2.424(15) 1_556
O12W Na6 2.595(15) 1_556
O13W Na3 2.367(15) 1_556
O14W Na6 2.371(15) 1_556
O16W Na6 2.382(15) 1_556
O17W Na5 2.452(17) 1_556
O18W Na7 2.422(16) 1_556
O19W Na7 2.361(17) 1_556
O19W Na10 2.51(2) 3_766
O20W Na4 2.316(17) 1_556
O21W Na1 2.55(2) 3_665
O22W Na2 2.463(19) 1_556
O23W Na5 2.426(18) 1_556
O24W Na1 2.64(3) 1_556
O25W Na7 2.494(18) 1_456
O26W Na8 2.296(14) 1_556
O27W Na8 2.39(2) 1_556
O28W Na2 2.413(16) 1_556
O33W Na9 1.64(2) 4_576
