#------------------------------------------------------------------------------
#$Date: 2019-11-23 04:22:47 +0200 (Sat, 23 Nov 2019) $
#$Revision: 232108 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/34/70/4347009.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4347009
loop_
_publ_author_name
'Chakkaradhari, Gomathy'
'Chen, Yi-Ting'
'Karttunen, Antti J.'
'Dau, Minh Thuy'
'Jänis, Janne'
'Tunik, Sergey P.'
'Chou, Pi-Tai'
'Ho, Mei-Lin'
'Koshevoy, Igor O.'
_publ_section_title
;
 Luminescent Triphosphine Cyanide d(10) Metal Complexes.
;
_journal_issue                   5
_journal_name_full               'Inorganic chemistry'
_journal_page_first              2174
_journal_page_last               2184
_journal_paper_doi               10.1021/acs.inorgchem.5b02581
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C85 H66 Ag2 N P6, B F4'
_chemical_formula_sum            'C85 H66 Ag2 B F4 N P6'
_chemical_formula_weight         1589.75
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/6
_cell_angle_alpha                90
_cell_angle_beta                 97.585(3)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   29.6803(14)
_cell_length_b                   29.5784(14)
_cell_length_c                   38.912(2)
_cell_measurement_reflns_used    9844
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      26.69
_cell_measurement_theta_min      2.46
_cell_volume                     33862(3)
_computing_cell_refinement       'SAINT (Bruker AXS, 2009)'
_computing_data_collection       'APEX2 (Bruker AXS, 2010)'
_computing_data_reduction        'SAINT (Bruker AXS, 2009)'
_computing_molecular_graphics    'Diamond v.3.2g (Brandenburg, 2011)'
_computing_publication_material  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/6 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 0.974
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device       '62mm x 62mm CCD camera on κ-goniostat'
_diffrn_measurement_device_type  'Bruker KAPPA APEX II DUO CCD'
_diffrn_measurement_method       'φ scans and ω scans with κ offset'
_diffrn_radiation_monochromator  'curved graphite crystal'
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0930
_diffrn_reflns_av_unetI/netI     0.0519
_diffrn_reflns_Laue_measured_fraction_full 0.974
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       35
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_k_min       -35
_diffrn_reflns_limit_l_max       46
_diffrn_reflns_limit_l_min       -46
_diffrn_reflns_number            227452
_diffrn_reflns_point_group_measured_fraction_full 0.974
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.050
_diffrn_reflns_theta_min         1.504
_exptl_absorpt_coefficient_mu    0.625
_exptl_absorpt_correction_T_max  0.909
_exptl_absorpt_correction_T_min  0.877
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'SADABS (Sheldrick, 2008)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.247
_exptl_crystal_description       block
_exptl_crystal_F_000             12928
_exptl_crystal_size_max          0.216
_exptl_crystal_size_mid          0.202
_exptl_crystal_size_min          0.155
_refine_diff_density_max         4.976
_refine_diff_density_min         -4.062
_refine_diff_density_rms         0.190
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1769
_refine_ls_number_reflns         29875
_refine_ls_number_restraints     92
_refine_ls_restrained_S_all      1.098
_refine_ls_R_factor_all          0.1187
_refine_ls_R_factor_gt           0.0987
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1037P)²+1240.6205P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2519
_refine_ls_wR_factor_ref         0.2652
_reflns_Friedel_coverage         0.000
_reflns_number_gt                22907
_reflns_number_total             29875
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            ic5b02581_si_003.cif
_cod_data_source_block           5
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4347009
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.877
_shelx_estimated_absorpt_t_max   0.909
_shelxl_version_number           2014/6
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
N1 N 0.2099(3) 0.7081(3) 0.13007(19) 0.0215(12) Uani 1 1 d . . .
N2 N 0.7309(3) 0.6877(3) 0.13006(19) 0.0221(12) Uani 1 1 d . . .
C3 C 0.3857(3) 0.6186(3) 0.0877(2) 0.0209(19) Uani 1 1 d . . .
C4 C 0.3970(4) 0.6513(4) 0.0642(3) 0.032(2) Uani 1 1 d . . .
H4 H 0.3957 0.6826 0.0697 0.039 Uiso 1 1 calc R U .
C5 C 0.4100(4) 0.6380(5) 0.0332(3) 0.046(3) Uani 1 1 d . . .
H5 H 0.4178 0.6602 0.0173 0.056 Uiso 1 1 calc R U .
C6 C 0.4119(4) 0.5935(5) 0.0249(3) 0.041(3) Uani 1 1 d . . .
H6 H 0.4214 0.5849 0.0035 0.049 Uiso 1 1 calc R U .
C7 C 0.4003(4) 0.5605(4) 0.0473(3) 0.042(3) Uani 1 1 d . . .
H7 H 0.4014 0.5295 0.0411 0.051 Uiso 1 1 calc R U .
C8 C 0.3870(3) 0.5730(4) 0.0790(3) 0.030(2) Uani 1 1 d . . .
H8 H 0.3789 0.5505 0.0946 0.036 Uiso 1 1 calc R U .
C9 C 0.3529(3) 0.5881(3) 0.1505(2) 0.0187(18) Uani 1 1 d . . .
C10 C 0.3074(3) 0.5804(3) 0.1515(3) 0.026(2) Uani 1 1 d . . .
H10 H 0.2856 0.6016 0.1412 0.031 Uiso 1 1 calc R U .
C11 C 0.2931(4) 0.5419(3) 0.1675(3) 0.036(3) Uani 1 1 d . . .
H11 H 0.2617 0.5370 0.1687 0.043 Uiso 1 1 calc R U .
C12 C 0.3254(4) 0.5105(3) 0.1820(2) 0.027(2) Uani 1 1 d . . .
H12 H 0.3157 0.4837 0.1924 0.033 Uiso 1 1 calc R U .
C13 C 0.3710(4) 0.5180(3) 0.1811(3) 0.030(2) Uani 1 1 d . . .
H13 H 0.3927 0.4964 0.1910 0.036 Uiso 1 1 calc R U .
C14 C 0.3853(3) 0.5565(3) 0.1661(2) 0.024(2) Uani 1 1 d . . .
H14 H 0.4169 0.5621 0.1662 0.028 Uiso 1 1 calc R U .
C15 C 0.4239(3) 0.6537(3) 0.1542(2) 0.0164(17) Uani 1 1 d . . .
C16 C 0.4650(3) 0.6346(3) 0.1462(2) 0.0213(19) Uani 1 1 d . . .
H16 H 0.4646 0.6152 0.1267 0.026 Uiso 1 1 calc R U .
C17 C 0.5056(3) 0.6443(3) 0.1664(3) 0.026(2) Uani 1 1 d . . .
H17 H 0.5330 0.6313 0.1608 0.031 Uiso 1 1 calc R U .
C18 C 0.5066(3) 0.6727(3) 0.1947(2) 0.022(2) Uani 1 1 d . . .
H18 H 0.5345 0.6784 0.2089 0.027 Uiso 1 1 calc R U .
C19 C 0.4668(3) 0.6928(3) 0.2022(2) 0.0163(17) Uani 1 1 d . . .
H19 H 0.4677 0.7128 0.2214 0.020 Uiso 1 1 calc R U .
C20 C 0.4248(3) 0.6837(3) 0.1816(2) 0.0163(18) Uani 1 1 d . . .
C21 C 0.3681(3) 0.6983(3) 0.2355(2) 0.0157(17) Uani 1 1 d . . .
C22 C 0.3880(3) 0.6584(3) 0.2504(2) 0.0176(18) Uani 1 1 d . . .
H22 H 0.4067 0.6403 0.2379 0.021 Uiso 1 1 calc R U .
C23 C 0.3800(3) 0.6459(3) 0.2835(2) 0.023(2) Uani 1 1 d . . .
H23 H 0.3936 0.6190 0.2935 0.028 Uiso 1 1 calc R U .
C24 C 0.3528(3) 0.6715(3) 0.3021(2) 0.025(2) Uani 1 1 d . . .
H24 H 0.3479 0.6624 0.3247 0.030 Uiso 1 1 calc R U .
C25 C 0.3324(4) 0.7111(3) 0.2875(2) 0.028(2) Uani 1 1 d . . .
H25 H 0.3136 0.7290 0.3001 0.033 Uiso 1 1 calc R U .
C26 C 0.3402(3) 0.7236(3) 0.2541(2) 0.0221(19) Uani 1 1 d . . .
H26 H 0.3260 0.7501 0.2438 0.027 Uiso 1 1 calc R U .
C27 C 0.3941(3) 0.7722(3) 0.1934(2) 0.0135(17) Uani 1 1 d . . .
C28 C 0.4156(3) 0.7909(3) 0.2244(2) 0.0214(19) Uani 1 1 d . . .
H28 H 0.4192 0.7729 0.2448 0.026 Uiso 1 1 calc R U .
C29 C 0.4315(3) 0.8346(3) 0.2259(2) 0.024(2) Uani 1 1 d . . .
H29 H 0.4462 0.8467 0.2470 0.029 Uiso 1 1 calc R U .
C30 C 0.4256(3) 0.8613(3) 0.1954(2) 0.025(2) Uani 1 1 d . . .
H30 H 0.4360 0.8917 0.1961 0.030 Uiso 1 1 calc R U .
C31 C 0.4052(3) 0.8435(3) 0.1654(2) 0.0183(18) Uani 1 1 d . . .
H31 H 0.4021 0.8615 0.1450 0.022 Uiso 1 1 calc R U .
C32 C 0.3887(3) 0.7993(3) 0.1634(2) 0.0157(17) Uani 1 1 d . . .
C33 C 0.4088(3) 0.7765(3) 0.0950(2) 0.0187(18) Uani 1 1 d . . .
C34 C 0.4535(3) 0.7754(3) 0.1103(2) 0.024(2) Uani 1 1 d . . .
H34 H 0.4600 0.7750 0.1349 0.029 Uiso 1 1 calc R U .
C35 C 0.4892(4) 0.7748(4) 0.0904(3) 0.039(3) Uani 1 1 d . . .
H35 H 0.5198 0.7755 0.1013 0.047 Uiso 1 1 calc R U .
C36 C 0.4797(4) 0.7732(4) 0.0545(3) 0.041(3) Uani 1 1 d . . .
H36 H 0.5036 0.7723 0.0405 0.049 Uiso 1 1 calc R U .
C37 C 0.4343(4) 0.7731(4) 0.0394(3) 0.044(3) Uani 1 1 d . . .
H37 H 0.4274 0.7721 0.0149 0.053 Uiso 1 1 calc R U .
C38 C 0.3986(3) 0.7745(4) 0.0598(2) 0.028(2) Uani 1 1 d . . .
H38 H 0.3678 0.7739 0.0493 0.033 Uiso 1 1 calc R U .
C39 C 0.3268(3) 0.8235(3) 0.1018(2) 0.0204(19) Uani 1 1 d . . .
C40 C 0.3450(3) 0.8614(3) 0.0871(2) 0.0208(19) Uani 1 1 d . . .
H40 H 0.3767 0.8634 0.0858 0.025 Uiso 1 1 calc R U .
C41 C 0.3158(4) 0.8957(3) 0.0744(3) 0.029(2) Uani 1 1 d . . .
H41 H 0.3282 0.9218 0.0649 0.035 Uiso 1 1 calc R U .
C42 C 0.2700(4) 0.8934(4) 0.0750(3) 0.035(2) Uani 1 1 d . . .
H42 H 0.2509 0.9175 0.0658 0.042 Uiso 1 1 calc R U .
C43 C 0.2516(4) 0.8564(4) 0.0891(3) 0.031(2) Uani 1 1 d . . .
H43 H 0.2198 0.8548 0.0899 0.037 Uiso 1 1 calc R U .
C44 C 0.2798(3) 0.8209(3) 0.1022(2) 0.0219(19) Uani 1 1 d . . .
H44 H 0.2670 0.7949 0.1115 0.026 Uiso 1 1 calc R U .
C45 C 0.0379(3) 0.6388(3) 0.0948(2) 0.024(2) Uani 1 1 d . . .
C46 C -0.0016(3) 0.6398(4) 0.1092(3) 0.031(2) Uani 1 1 d . . .
H46 H -0.0004 0.6383 0.1337 0.038 Uiso 1 1 calc R U .
C47 C -0.0431(4) 0.6430(4) 0.0889(3) 0.041(3) Uani 1 1 d . . .
H47 H -0.0703 0.6428 0.0995 0.050 Uiso 1 1 calc R U .
C48 C -0.0455(4) 0.6465(4) 0.0528(3) 0.046(3) Uani 1 1 d . . .
H48 H -0.0742 0.6495 0.0388 0.055 Uiso 1 1 calc R U .
C49 C -0.0052(4) 0.6456(5) 0.0372(3) 0.052(4) Uani 1 1 d . . .
H49 H -0.0064 0.6473 0.0128 0.063 Uiso 1 1 calc R U .
C50 C 0.0364(4) 0.6422(5) 0.0585(3) 0.044(3) Uani 1 1 d . . .
H50 H 0.0638 0.6421 0.0484 0.053 Uiso 1 1 calc R U .
C51 C 0.1218(3) 0.5893(3) 0.1017(2) 0.0199(19) Uani 1 1 d . . .
C52 C 0.0984(4) 0.5528(3) 0.0849(2) 0.027(2) Uani 1 1 d . . .
H52 H 0.0661 0.5523 0.0821 0.032 Uiso 1 1 calc R U .
C53 C 0.1223(4) 0.5174(3) 0.0722(2) 0.031(2) Uani 1 1 d . . .
H53 H 0.1060 0.4927 0.0609 0.037 Uiso 1 1 calc R U .
C54 C 0.1692(4) 0.5176(3) 0.0756(2) 0.028(2) Uani 1 1 d . . .
H54 H 0.1854 0.4929 0.0676 0.033 Uiso 1 1 calc R U .
C55 C 0.1924(4) 0.5553(4) 0.0912(3) 0.033(2) Uani 1 1 d . . .
H55 H 0.2246 0.5564 0.0931 0.040 Uiso 1 1 calc R U .
C56 C 0.1694(3) 0.5905(3) 0.1038(2) 0.022(2) Uani 1 1 d . . .
H56 H 0.1857 0.6158 0.1140 0.027 Uiso 1 1 calc R U .
C57 C 0.0812(3) 0.6145(3) 0.1620(2) 0.0147(17) Uani 1 1 d . . .
C58 C 0.0654(3) 0.5695(3) 0.1649(2) 0.0197(19) Uani 1 1 d . . .
H58 H 0.0622 0.5507 0.1449 0.024 Uiso 1 1 calc R U .
C59 C 0.0548(3) 0.5523(3) 0.1952(3) 0.024(2) Uani 1 1 d . . .
H59 H 0.0440 0.5221 0.1959 0.028 Uiso 1 1 calc R U .
C60 C 0.0595(3) 0.5785(3) 0.2253(2) 0.024(2) Uani 1 1 d . . .
H60 H 0.0524 0.5664 0.2465 0.028 Uiso 1 1 calc R U .
C61 C 0.0749(3) 0.6229(3) 0.2235(2) 0.0214(19) Uani 1 1 d . . .
H61 H 0.0783 0.6409 0.2439 0.026 Uiso 1 1 calc R U .
C62 C 0.0852(3) 0.6413(3) 0.1928(2) 0.0147(17) Uani 1 1 d . . .
C63 C 0.1253(3) 0.7160(3) 0.2348(2) 0.0150(17) Uani 1 1 d . . .
C64 C 0.1593(3) 0.6904(3) 0.2539(2) 0.0211(19) Uani 1 1 d . . .
H64 H 0.1698 0.6636 0.2441 0.025 Uiso 1 1 calc R U .
C65 C 0.1779(3) 0.7036(3) 0.2871(2) 0.026(2) Uani 1 1 d . . .
H65 H 0.2008 0.6857 0.2999 0.032 Uiso 1 1 calc R U .
C66 C 0.1631(3) 0.7426(3) 0.3016(2) 0.024(2) Uani 1 1 d . . .
H66 H 0.1756 0.7515 0.3243 0.029 Uiso 1 1 calc R U .
C67 C 0.1298(3) 0.7687(3) 0.2826(2) 0.023(2) Uani 1 1 d . . .
H67 H 0.1195 0.7955 0.2924 0.028 Uiso 1 1 calc R U .
C68 C 0.1112(3) 0.7560(3) 0.2494(2) 0.0197(19) Uani 1 1 d . . .
H68 H 0.0889 0.7745 0.2365 0.024 Uiso 1 1 calc R U .
C69 C 0.0506(3) 0.7297(3) 0.1811(2) 0.0181(18) Uani 1 1 d . . .
C70 C 0.0161(3) 0.7207(3) 0.2016(2) 0.0188(18) Uani 1 1 d . . .
H70 H 0.0219 0.7007 0.2207 0.023 Uiso 1 1 calc R U .
C71 C -0.0268(3) 0.7408(3) 0.1942(3) 0.024(2) Uani 1 1 d . . .
H71 H -0.0497 0.7347 0.2084 0.028 Uiso 1 1 calc R U .
C72 C -0.0356(3) 0.7697(3) 0.1661(3) 0.027(2) Uani 1 1 d . . .
H72 H -0.0650 0.7827 0.1604 0.032 Uiso 1 1 calc R U .
C73 C -0.0010(3) 0.7795(3) 0.1461(2) 0.0218(19) Uani 1 1 d . . .
H73 H -0.0067 0.7999 0.1272 0.026 Uiso 1 1 calc R U .
C74 C 0.0415(3) 0.7598(3) 0.1536(2) 0.0196(19) Uani 1 1 d . . .
C75 C 0.1110(3) 0.8253(3) 0.1493(2) 0.0197(19) Uani 1 1 d . . .
C76 C 0.0852(3) 0.8569(3) 0.1645(2) 0.024(2) Uani 1 1 d . . .
H76 H 0.0538 0.8514 0.1649 0.028 Uiso 1 1 calc R U .
C77 C 0.1044(4) 0.8964(3) 0.1791(2) 0.031(2) Uani 1 1 d . . .
H77 H 0.0858 0.9186 0.1878 0.038 Uiso 1 1 calc R U .
C78 C 0.1504(4) 0.9032(3) 0.1808(3) 0.031(2) Uani 1 1 d . . .
H78 H 0.1641 0.9289 0.1925 0.037 Uiso 1 1 calc R U .
C79 C 0.1770(4) 0.8721(4) 0.1653(3) 0.034(2) Uani 1 1 d . . .
H79 H 0.2083 0.8780 0.1648 0.041 Uiso 1 1 calc R U .
C80 C 0.1582(3) 0.8333(3) 0.1508(3) 0.026(2) Uani 1 1 d . . .
H80 H 0.1769 0.8115 0.1416 0.032 Uiso 1 1 calc R U .
C81 C 0.0561(3) 0.7957(4) 0.0870(2) 0.029(2) Uani 1 1 d . . .
C82 C 0.0542(4) 0.8413(4) 0.0777(3) 0.038(3) Uani 1 1 d . . .
H82 H 0.0694 0.8635 0.0926 0.046 Uiso 1 1 calc R U .
C83 C 0.0289(4) 0.8537(6) 0.0454(3) 0.057(4) Uani 1 1 d . . .
H83 H 0.0277 0.8846 0.0386 0.068 Uiso 1 1 calc R U .
C84 C 0.0061(5) 0.8219(7) 0.0241(3) 0.066(5) Uani 1 1 d . . .
H84 H -0.0117 0.8306 0.0031 0.080 Uiso 1 1 calc R U .
C85 C 0.0096(4) 0.7776(6) 0.0336(3) 0.055(4) Uani 1 1 d . . .
H85 H -0.0053 0.7554 0.0186 0.066 Uiso 1 1 calc R U .
C86 C 0.0339(3) 0.7642(5) 0.0644(3) 0.038(3) Uani 1 1 d . . .
H86 H 0.0355 0.7330 0.0703 0.046 Uiso 1 1 calc R U .
C87 C 0.8417(3) 0.8088(3) 0.1023(2) 0.0176(18) Uani 1 1 d . . .
C88 C 0.8384(3) 0.7618(3) 0.1026(2) 0.025(2) Uani 1 1 d . . .
H88 H 0.8138 0.7476 0.1116 0.030 Uiso 1 1 calc R U .
C89 C 0.8715(4) 0.7358(3) 0.0894(3) 0.031(2) Uani 1 1 d . . .
H89 H 0.8696 0.7037 0.0898 0.037 Uiso 1 1 calc R U .
C90 C 0.9068(4) 0.7567(4) 0.0760(3) 0.034(2) Uani 1 1 d . . .
H90 H 0.9297 0.7389 0.0677 0.041 Uiso 1 1 calc R U .
C91 C 0.9090(3) 0.8030(3) 0.0745(3) 0.027(2) Uani 1 1 d . . .
H91 H 0.9327 0.8171 0.0643 0.033 Uiso 1 1 calc R U .
C92 C 0.8765(3) 0.8293(3) 0.0880(2) 0.023(2) Uani 1 1 d . . .
H92 H 0.8783 0.8614 0.0873 0.028 Uiso 1 1 calc R U .
C93 C 0.7930(3) 0.8926(3) 0.0961(2) 0.0171(18) Uani 1 1 d . . .
C94 C 0.7855(4) 0.8894(4) 0.0592(2) 0.030(2) Uani 1 1 d . . .
H94 H 0.7841 0.8605 0.0484 0.036 Uiso 1 1 calc R U .
C95 C 0.7805(4) 0.9275(4) 0.0392(3) 0.045(3) Uani 1 1 d . . .
H95 H 0.7752 0.9249 0.0146 0.054 Uiso 1 1 calc R U .
C96 C 0.7830(4) 0.9698(4) 0.0546(3) 0.044(3) Uani 1 1 d . . .
H96 H 0.7794 0.9962 0.0406 0.052 Uiso 1 1 calc R U .
C97 C 0.7906(4) 0.9736(4) 0.0900(3) 0.039(3) Uani 1 1 d . . .
H97 H 0.7928 1.0027 0.1004 0.046 Uiso 1 1 calc R U .
C98 C 0.7952(3) 0.9355(3) 0.1105(2) 0.025(2) Uani 1 1 d . . .
H98 H 0.7999 0.9387 0.1350 0.030 Uiso 1 1 calc R U .
C99 C 0.8274(3) 0.8607(3) 0.1636(2) 0.0135(17) Uani 1 1 d . . .
C100 C 0.8722(3) 0.8769(3) 0.1651(2) 0.0209(19) Uani 1 1 d . . .
H100 H 0.8870 0.8771 0.1449 0.025 Uiso 1 1 calc R U .
C101 C 0.8949(3) 0.8929(3) 0.1969(2) 0.025(2) Uani 1 1 d . . .
H101 H 0.9252 0.9036 0.1980 0.030 Uiso 1 1 calc R U .
C102 C 0.8740(3) 0.8933(3) 0.2261(3) 0.025(2) Uani 1 1 d . . .
H102 H 0.8894 0.9049 0.2472 0.031 Uiso 1 1 calc R U .
C103 C 0.8304(3) 0.8769(3) 0.2248(2) 0.0211(19) Uani 1 1 d . . .
H103 H 0.8164 0.8766 0.2454 0.025 Uiso 1 1 calc R U .
C104 C 0.8059(3) 0.8604(3) 0.1938(2) 0.0124(16) Uani 1 1 d . . .
C105 C 0.7384(3) 0.8284(3) 0.2359(2) 0.0154(17) Uani 1 1 d . . .
C106 C 0.7681(3) 0.7975(3) 0.2549(2) 0.025(2) Uani 1 1 d . . .
H106 H 0.7935 0.7861 0.2451 0.030 Uiso 1 1 calc R U .
C107 C 0.7604(3) 0.7836(3) 0.2878(2) 0.028(2) Uani 1 1 d . . .
H107 H 0.7794 0.7614 0.3000 0.034 Uiso 1 1 calc R U .
C108 C 0.7246(4) 0.8025(3) 0.3027(2) 0.026(2) Uani 1 1 d . . .
H108 H 0.7209 0.7954 0.3260 0.031 Uiso 1 1 calc R U .
C109 C 0.6947(3) 0.8315(3) 0.2838(2) 0.023(2) Uani 1 1 d . . .
H109 H 0.6692 0.8426 0.2936 0.028 Uiso 1 1 calc R U .
C110 C 0.7013(3) 0.8451(3) 0.2503(2) 0.0169(18) Uani 1 1 d . . .
H110 H 0.6807 0.8654 0.2376 0.020 Uiso 1 1 calc R U .
C111 C 0.7154(3) 0.8941(3) 0.1818(2) 0.0138(17) Uani 1 1 d . . .
C112 C 0.7272(3) 0.9319(3) 0.2021(2) 0.0186(18) Uani 1 1 d . . .
H112 H 0.7503 0.9296 0.2215 0.022 Uiso 1 1 calc R U .
C113 C 0.7061(3) 0.9723(3) 0.1947(3) 0.026(2) Uani 1 1 d . . .
H113 H 0.7146 0.9977 0.2091 0.032 Uiso 1 1 calc R U .
C114 C 0.6728(3) 0.9772(3) 0.1670(3) 0.024(2) Uani 1 1 d . . .
H114 H 0.6588 1.0057 0.1617 0.029 Uiso 1 1 calc R U .
C115 C 0.6600(3) 0.9391(3) 0.1467(2) 0.0204(19) Uani 1 1 d . . .
H115 H 0.6366 0.9419 0.1276 0.025 Uiso 1 1 calc R U .
C116 C 0.6805(3) 0.8974(3) 0.1537(2) 0.0182(18) Uani 1 1 d . . .
C117 C 0.6138(3) 0.8279(3) 0.1505(2) 0.0183(18) Uani 1 1 d . . .
C118 C 0.5853(3) 0.8567(3) 0.1655(2) 0.026(2) Uani 1 1 d . . .
H118 H 0.5907 0.8883 0.1657 0.031 Uiso 1 1 calc R U .
C119 C 0.5487(3) 0.8397(3) 0.1803(2) 0.026(2) Uani 1 1 d . . .
H119 H 0.5286 0.8599 0.1897 0.031 Uiso 1 1 calc R U .
C120 C 0.5416(3) 0.7934(4) 0.1816(3) 0.029(2) Uani 1 1 d . . .
H120 H 0.5170 0.7818 0.1923 0.034 Uiso 1 1 calc R U .
C121 C 0.5706(3) 0.7641(4) 0.1672(3) 0.030(2) Uani 1 1 d . . .
H121 H 0.5657 0.7323 0.1678 0.036 Uiso 1 1 calc R U .
C122 C 0.6065(3) 0.7812(3) 0.1519(3) 0.026(2) Uani 1 1 d . . .
H122 H 0.6264 0.7610 0.1422 0.031 Uiso 1 1 calc R U .
C123 C 0.6343(3) 0.8707(3) 0.0880(2) 0.0208(19) Uani 1 1 d . . .
C124 C 0.5878(3) 0.8737(3) 0.0788(2) 0.025(2) Uani 1 1 d . . .
H124 H 0.5680 0.8627 0.0941 0.030 Uiso 1 1 calc R U .
C125 C 0.5695(4) 0.8929(4) 0.0468(3) 0.038(3) Uani 1 1 d . . .
H125 H 0.5375 0.8954 0.0409 0.046 Uiso 1 1 calc R U .
C126 C 0.5982(5) 0.9077(4) 0.0245(3) 0.043(3) Uani 1 1 d . . .
H126 H 0.5860 0.9204 0.0028 0.052 Uiso 1 1 calc R U .
C127 C 0.6448(4) 0.9045(4) 0.0334(3) 0.037(3) Uani 1 1 d . . .
H127 H 0.6645 0.9151 0.0178 0.045 Uiso 1 1 calc R U .
C128 C 0.6630(4) 0.8859(3) 0.0650(3) 0.031(2) Uani 1 1 d . . .
H128 H 0.6950 0.8836 0.0708 0.037 Uiso 1 1 calc R U .
C129 C 0.8114(4) 0.5413(3) 0.0873(3) 0.030(2) Uani 1 1 d . . .
C130 C 0.7755(4) 0.5233(3) 0.0642(3) 0.036(3) Uani 1 1 d . . .
H130 H 0.7454 0.5238 0.0699 0.043 Uiso 1 1 calc R U .
C131 C 0.7845(6) 0.5046(4) 0.0327(3) 0.055(4) Uani 1 1 d . . .
H131 H 0.7601 0.4926 0.0171 0.065 Uiso 1 1 calc R U .
C132 C 0.8264(6) 0.5032(4) 0.0243(3) 0.052(3) Uani 1 1 d . U .
H132 H 0.8315 0.4900 0.0029 0.062 Uiso 1 1 calc R U .
C133 C 0.8637(6) 0.5210(4) 0.0466(3) 0.061(4) Uani 1 1 d . . .
H133 H 0.8935 0.5198 0.0404 0.073 Uiso 1 1 calc R U .
C134 C 0.8559(4) 0.5403(3) 0.0780(3) 0.037(3) Uani 1 1 d . . .
H134 H 0.8805 0.5528 0.0931 0.044 Uiso 1 1 calc R U .
C135 C 0.8516(3) 0.5857(3) 0.1494(2) 0.0211(19) Uani 1 1 d . . .
C136 C 0.8851(3) 0.5568(3) 0.1650(3) 0.027(2) Uani 1 1 d . . .
H136 H 0.8796 0.5251 0.1651 0.033 Uiso 1 1 calc R U .
C137 C 0.9266(3) 0.5738(3) 0.1807(3) 0.028(2) Uani 1 1 d . . .
H137 H 0.9495 0.5538 0.1911 0.034 Uiso 1 1 calc R U .
C138 C 0.9344(3) 0.6200(4) 0.1810(3) 0.030(2) Uani 1 1 d . . .
H138 H 0.9629 0.6317 0.1910 0.037 Uiso 1 1 calc R U .
C139 C 0.9007(4) 0.6490(4) 0.1667(3) 0.034(2) Uani 1 1 d . . .
H139 H 0.9057 0.6807 0.1677 0.041 Uiso 1 1 calc R U .
C140 C 0.8592(3) 0.6321(3) 0.1507(3) 0.027(2) Uani 1 1 d . . .
H140 H 0.8362 0.6523 0.1408 0.033 Uiso 1 1 calc R U .
C141 C 0.7866(3) 0.5151(3) 0.1532(2) 0.0186(18) Uani 1 1 d . . .
C142 C 0.8044(3) 0.4735(3) 0.1457(2) 0.023(2) Uani 1 1 d . . .
H142 H 0.8209 0.4706 0.1265 0.027 Uiso 1 1 calc R U .
C143 C 0.7983(3) 0.4361(3) 0.1660(2) 0.025(2) Uani 1 1 d . . .
H143 H 0.8103 0.4076 0.1606 0.030 Uiso 1 1 calc R U .
C144 C 0.7745(3) 0.4404(3) 0.1943(3) 0.028(2) Uani 1 1 d . . .
H144 H 0.7713 0.4152 0.2089 0.034 Uiso 1 1 calc R U .
C145 C 0.7553(3) 0.4817(3) 0.2010(2) 0.0179(18) Uani 1 1 d . . .
H145 H 0.7380 0.4842 0.2198 0.022 Uiso 1 1 calc R U .
C146 C 0.7610(3) 0.5195(3) 0.1808(2) 0.0165(18) Uani 1 1 d . . .
C147 C 0.7566(3) 0.5853(3) 0.2348(2) 0.0166(18) Uani 1 1 d . . .
C148 C 0.7987(3) 0.5682(3) 0.2490(2) 0.0183(18) Uani 1 1 d . . .
H148 H 0.8146 0.5477 0.2362 0.022 Uiso 1 1 calc R U .
C149 C 0.8173(3) 0.5815(3) 0.2823(2) 0.023(2) Uani 1 1 d . . .
H149 H 0.8458 0.5694 0.2922 0.028 Uiso 1 1 calc R U .
C150 C 0.7948(3) 0.6119(3) 0.3008(2) 0.024(2) Uani 1 1 d . . .
H150 H 0.8081 0.6211 0.3233 0.029 Uiso 1 1 calc R U .
C151 C 0.7534(3) 0.6292(3) 0.2869(2) 0.029(2) Uani 1 1 d . . .
H151 H 0.7376 0.6497 0.2998 0.034 Uiso 1 1 calc R U .
C152 C 0.7347(3) 0.6161(3) 0.2535(2) 0.022(2) Uani 1 1 d . . .
H152 H 0.7065 0.6286 0.2435 0.027 Uiso 1 1 calc R U .
C153 C 0.6751(3) 0.5530(3) 0.1924(2) 0.0171(18) Uani 1 1 d . . .
C154 C 0.6609(3) 0.5373(3) 0.2232(2) 0.0164(17) Uani 1 1 d . . .
H154 H 0.6819 0.5376 0.2438 0.020 Uiso 1 1 calc R U .
C155 C 0.6179(3) 0.5215(3) 0.2248(2) 0.023(2) Uani 1 1 d . . .
H155 H 0.6098 0.5102 0.2460 0.028 Uiso 1 1 calc R U .
C156 C 0.5858(3) 0.5223(3) 0.1947(2) 0.025(2) Uani 1 1 d . . .
H156 H 0.5557 0.5119 0.1956 0.030 Uiso 1 1 calc R U .
C157 C 0.5981(3) 0.5379(3) 0.1643(2) 0.0194(19) Uani 1 1 d . . .
H157 H 0.5762 0.5385 0.1442 0.023 Uiso 1 1 calc R U .
C158 C 0.6429(3) 0.5532(3) 0.1623(2) 0.0174(18) Uani 1 1 d . . .
C159 C 0.6560(3) 0.5223(3) 0.0945(2) 0.0212(19) Uani 1 1 d . . .
C160 C 0.6588(4) 0.4798(3) 0.1091(3) 0.033(2) Uani 1 1 d . . .
H160 H 0.6609 0.4766 0.1336 0.039 Uiso 1 1 calc R U .
C161 C 0.6584(4) 0.4410(4) 0.0882(3) 0.042(3) Uani 1 1 d . . .
H161 H 0.6593 0.4118 0.0984 0.050 Uiso 1 1 calc R U .
C162 C 0.6567(4) 0.4456(4) 0.0524(3) 0.048(3) Uani 1 1 d . . .
H162 H 0.6579 0.4196 0.0382 0.057 Uiso 1 1 calc R U .
C163 C 0.6533(5) 0.4877(4) 0.0381(3) 0.053(4) Uani 1 1 d . . .
H163 H 0.6512 0.4908 0.0136 0.064 Uiso 1 1 calc R U .
C164 C 0.6527(5) 0.5259(4) 0.0582(3) 0.047(3) Uani 1 1 d . . .
H164 H 0.6502 0.5548 0.0475 0.056 Uiso 1 1 calc R U .
C165 C 0.6070(3) 0.6047(3) 0.1014(2) 0.0197(19) Uani 1 1 d . . .
C166 C 0.6088(3) 0.6517(3) 0.1038(2) 0.024(2) Uani 1 1 d . . .
H166 H 0.6358 0.6662 0.1141 0.028 Uiso 1 1 calc R U .
C167 C 0.5708(3) 0.6772(3) 0.0910(3) 0.029(2) Uani 1 1 d . . .
H167 H 0.5719 0.7092 0.0929 0.035 Uiso 1 1 calc R U .
C168 C 0.5318(4) 0.6565(4) 0.0757(3) 0.034(2) Uani 1 1 d . . .
H168 H 0.5060 0.6742 0.0673 0.041 Uiso 1 1 calc R U .
C169 C 0.5301(3) 0.6100(4) 0.0725(3) 0.032(2) Uani 1 1 d . . .
H169 H 0.5031 0.5956 0.0620 0.038 Uiso 1 1 calc R U .
C170 C 0.5681(3) 0.5842(3) 0.0848(3) 0.028(2) Uani 1 1 d . . .
H170 H 0.5673 0.5523 0.0819 0.034 Uiso 1 1 calc R U .
Ag1 Ag 0.32126(2) 0.70618(2) 0.13383(2) 0.01709(16) Uani 1 1 d . . .
Ag2 Ag 0.13769(2) 0.70763(2) 0.13338(2) 0.01820(16) Uani 1 1 d . . .
Ag3 Ag 0.72961(2) 0.79858(2) 0.13430(2) 0.01796(16) Uani 1 1 d . . .
Ag4 Ag 0.73094(2) 0.61499(2) 0.13303(2) 0.01776(16) Uani 1 1 d . . .
B1 B 0.0000 0.4567(7) 0.2500 0.066(7) Uani 1 2 d S T P
B2 B 0.0000 0.9577(9) 0.2500 0.067(7) Uani 1 2 d S T P
F1 F -0.0291(5) 0.4840(4) 0.2295(4) 0.145(6) Uani 1 1 d . . .
F2 F 0.0227(4) 0.4302(4) 0.2302(3) 0.133(5) Uani 1 1 d . . .
F3 F -0.0293(4) 0.9844(4) 0.2297(4) 0.132(6) Uani 1 1 d . . .
F4 F 0.0242(4) 0.9329(5) 0.2306(4) 0.140(6) Uani 1 1 d . . .
C1 C 0.2485(3) 0.7060(3) 0.1302(2) 0.0215(12) Uani 1 1 d . . .
C2 C 0.7294(3) 0.7259(3) 0.1302(2) 0.0221(12) Uani 1 1 d . . .
P1 P 0.36939(7) 0.63879(7) 0.12845(6) 0.0159(4) Uani 1 1 d . . .
P2 P 0.37347(7) 0.71368(7) 0.19095(5) 0.0126(4) Uani 1 1 d . . .
P3 P 0.36174(7) 0.77698(7) 0.12110(5) 0.0145(4) Uani 1 1 d . . .
P4 P 0.09408(8) 0.63630(8) 0.12067(6) 0.0165(5) Uani 1 1 d . . .
P5 P 0.10530(7) 0.70020(7) 0.19041(5) 0.0141(4) Uani 1 1 d . . .
P6 P 0.08733(8) 0.77500(8) 0.12753(6) 0.0176(5) Uani 1 1 d . . .
P7 P 0.79827(8) 0.84097(7) 0.12156(5) 0.0145(4) Uani 1 1 d . . .
P8 P 0.74681(7) 0.84075(7) 0.19128(5) 0.0124(4) Uani 1 1 d . . .
P9 P 0.66127(8) 0.84721(7) 0.12851(5) 0.0151(4) Uani 1 1 d . . .
P10 P 0.79731(8) 0.56534(7) 0.12751(6) 0.0178(5) Uani 1 1 d . . .
P11 P 0.73313(7) 0.57253(7) 0.18999(5) 0.0146(4) Uani 1 1 d . . .
P12 P 0.65741(8) 0.57351(7) 0.12024(6) 0.0168(5) Uani 1 1 d . . .
F15 F 0.4782(5) 0.4979(4) 0.1249(4) 0.070(2) Uani 0.5 1 d D . P
F10 F 0.0185(4) 0.4569(5) 0.1245(4) 0.073(2) Uani 0.5 1 d D U P
F11 F -0.0262(5) 0.3992(4) 0.1007(4) 0.073(2) Uani 0.5 1 d D U P
F14 F 0.4172(4) 0.4571(5) 0.1013(4) 0.070(2) Uani 0.5 1 d D U P
B11 B -0.0243(4) 0.4448(5) 0.1084(4) 0.073(2) Uani 0.5 1 d D U P
B10 B 0.4642(5) 0.4577(4) 0.1083(4) 0.070(2) Uani 0.5 1 d D U P
F12 F -0.0632(5) 0.4543(5) 0.1233(4) 0.073(2) Uani 0.5 1 d D U P
F13 F -0.0289(5) 0.4673(5) 0.0773(3) 0.073(2) Uani 0.5 1 d D U P
F16 F 0.4762(5) 0.4156(4) 0.1227(4) 0.070(2) Uani 0.5 1 d D U P
F17 F 0.4813(5) 0.4594(5) 0.0771(3) 0.070(2) Uani 0.5 1 d D . P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 N1 Ag2 175.0(8) . .
C2 N2 Ag4 175.7(8) . .
C8 C3 C4 119.6(9) . .
C8 C3 P1 123.2(8) . .
C4 C3 P1 117.2(7) . .
C5 C4 C3 119.7(11) . .
C5 C4 H4 120.2 . .
C3 C4 H4 120.2 . .
C6 C5 C4 120.8(12) . .
C6 C5 H5 119.6 . .
C4 C5 H5 119.6 . .
C5 C6 C7 120.9(10) . .
C5 C6 H6 119.5 . .
C7 C6 H6 119.5 . .
C6 C7 C8 119.7(11) . .
C6 C7 H7 120.1 . .
C8 C7 H7 120.1 . .
C7 C8 C3 119.3(11) . .
C7 C8 H8 120.3 . .
C3 C8 H8 120.3 . .
C10 C9 C14 119.6(8) . .
C10 C9 P1 118.2(7) . .
C14 C9 P1 122.2(7) . .
C9 C10 C11 120.3(10) . .
C9 C10 H10 119.9 . .
C11 C10 H10 119.9 . .
C10 C11 C12 119.5(10) . .
C10 C11 H11 120.2 . .
C12 C11 H11 120.2 . .
C13 C12 C11 120.4(9) . .
C13 C12 H12 119.8 . .
C11 C12 H12 119.8 . .
C14 C13 C12 120.3(9) . .
C14 C13 H13 119.9 . .
C12 C13 H13 119.9 . .
C13 C14 C9 119.8(9) . .
C13 C14 H14 120.1 . .
C9 C14 H14 120.1 . .
C20 C15 C16 119.8(8) . .
C20 C15 P1 119.9(6) . .
C16 C15 P1 120.3(6) . .
C17 C16 C15 120.3(8) . .
C17 C16 H16 119.8 . .
C15 C16 H16 119.8 . .
C16 C17 C18 120.3(9) . .
C16 C17 H17 119.8 . .
C18 C17 H17 119.8 . .
C17 C18 C19 120.0(8) . .
C17 C18 H18 120.0 . .
C19 C18 H18 120.0 . .
C18 C19 C20 120.6(8) . .
C18 C19 H19 119.7 . .
C20 C19 H19 119.7 . .
C15 C20 C19 118.9(8) . .
C15 C20 P2 122.0(6) . .
C19 C20 P2 119.1(6) . .
C26 C21 C22 119.1(8) . .
C26 C21 P2 119.5(6) . .
C22 C21 P2 121.1(7) . .
C23 C22 C21 119.4(9) . .
C23 C22 H22 120.3 . .
C21 C22 H22 120.3 . .
C24 C23 C22 121.4(9) . .
C24 C23 H23 119.3 . .
C22 C23 H23 119.3 . .
C23 C24 C25 119.8(8) . .
C23 C24 H24 120.1 . .
C25 C24 H24 120.1 . .
C24 C25 C26 118.8(9) . .
C24 C25 H25 120.6 . .
C26 C25 H25 120.6 . .
C21 C26 C25 121.4(9) . .
C21 C26 H26 119.3 . .
C25 C26 H26 119.3 . .
C28 C27 C32 118.5(8) . .
C28 C27 P2 121.8(6) . .
C32 C27 P2 119.6(6) . .
C29 C28 C27 121.4(8) . .
C29 C28 H28 119.3 . .
C27 C28 H28 119.3 . .
C28 C29 C30 119.1(8) . .
C28 C29 H29 120.5 . .
C30 C29 H29 120.5 . .
C31 C30 C29 119.9(8) . .
C31 C30 H30 120.0 . .
C29 C30 H30 120.0 . .
C30 C31 C32 121.8(8) . .
C30 C31 H31 119.1 . .
C32 C31 H31 119.1 . .
C31 C32 C27 119.2(8) . .
C31 C32 P3 119.4(6) . .
C27 C32 P3 121.4(6) . .
C38 C33 C34 120.3(8) . .
C38 C33 P3 118.1(7) . .
C34 C33 P3 121.5(7) . .
C33 C34 C35 121.4(9) . .
C33 C34 H34 119.3 . .
C35 C34 H34 119.3 . .
C36 C35 C34 119.3(10) . .
C36 C35 H35 120.3 . .
C34 C35 H35 120.3 . .
C35 C36 C37 118.7(10) . .
C35 C36 H36 120.6 . .
C37 C36 H36 120.6 . .
C36 C37 C38 121.2(10) . .
C36 C37 H37 119.4 . .
C38 C37 H37 119.4 . .
C33 C38 C37 119.0(9) . .
C33 C38 H38 120.5 . .
C37 C38 H38 120.5 . .
C40 C39 C44 119.3(8) . .
C40 C39 P3 122.9(7) . .
C44 C39 P3 117.8(7) . .
C41 C40 C39 118.5(9) . .
C41 C40 H40 120.7 . .
C39 C40 H40 120.7 . .
C42 C41 C40 122.4(10) . .
C42 C41 H41 118.8 . .
C40 C41 H41 118.8 . .
C41 C42 C43 119.8(10) . .
C41 C42 H42 120.1 . .
C43 C42 H42 120.1 . .
C42 C43 C44 119.8(10) . .
C42 C43 H43 120.1 . .
C44 C43 H43 120.1 . .
C43 C44 C39 120.3(9) . .
C43 C44 H44 119.9 . .
C39 C44 H44 119.9 . .
C46 C45 C50 119.6(9) . .
C46 C45 P4 122.9(7) . .
C50 C45 P4 117.4(8) . .
C45 C46 C47 121.3(10) . .
C45 C46 H46 119.3 . .
C47 C46 H46 119.3 . .
C46 C47 C48 120.1(11) . .
C46 C47 H47 120.0 . .
C48 C47 H47 120.0 . .
C47 C48 C49 119.7(10) . .
C47 C48 H48 120.2 . .
C49 C48 H48 120.2 . .
C50 C49 C48 118.9(11) . .
C50 C49 H49 120.6 . .
C48 C49 H49 120.6 . .
C49 C50 C45 120.4(11) . .
C49 C50 H50 119.8 . .
C45 C50 H50 119.8 . .
C52 C51 C56 118.7(8) . .
C52 C51 P4 123.7(7) . .
C56 C51 P4 117.5(7) . .
C53 C52 C51 120.2(10) . .
C53 C52 H52 119.9 . .
C51 C52 H52 119.9 . .
C54 C53 C52 121.1(9) . .
C54 C53 H53 119.5 . .
C52 C53 H53 119.5 . .
C53 C54 C55 118.3(9) . .
C53 C54 H54 120.8 . .
C55 C54 H54 120.8 . .
C56 C55 C54 121.3(10) . .
C56 C55 H55 119.3 . .
C54 C55 H55 119.3 . .
C55 C56 C51 120.3(9) . .
C55 C56 H56 119.8 . .
C51 C56 H56 119.8 . .
C58 C57 C62 116.6(8) . .
C58 C57 P4 120.7(6) . .
C62 C57 P4 122.7(6) . .
C59 C58 C57 122.4(8) . .
C59 C58 H58 118.8 . .
C57 C58 H58 118.8 . .
C58 C59 C60 120.7(8) . .
C58 C59 H59 119.7 . .
C60 C59 H59 119.7 . .
C61 C60 C59 118.6(9) . .
C61 C60 H60 120.7 . .
C59 C60 H60 120.7 . .
C62 C61 C60 121.7(8) . .
C62 C61 H61 119.1 . .
C60 C61 H61 119.1 . .
C61 C62 C57 120.0(8) . .
C61 C62 P5 121.7(6) . .
C57 C62 P5 118.2(6) . .
C64 C63 C68 118.4(8) . .
C64 C63 P5 119.4(6) . .
C68 C63 P5 121.8(7) . .
C65 C64 C63 120.8(8) . .
C65 C64 H64 119.6 . .
C63 C64 H64 119.6 . .
C66 C65 C64 120.3(9) . .
C66 C65 H65 119.8 . .
C64 C65 H65 119.8 . .
C65 C66 C67 119.3(8) . .
C65 C66 H66 120.4 . .
C67 C66 H66 120.4 . .
C66 C67 C68 120.9(9) . .
C66 C67 H67 119.5 . .
C68 C67 H67 119.5 . .
C67 C68 C63 120.2(9) . .
C67 C68 H68 119.9 . .
C63 C68 H68 119.9 . .
C74 C69 C70 118.5(8) . .
C74 C69 P5 122.1(7) . .
C70 C69 P5 119.4(7) . .
C71 C70 C69 121.0(9) . .
C71 C70 H70 119.5 . .
C69 C70 H70 119.5 . .
C72 C71 C70 119.8(8) . .
C72 C71 H71 120.1 . .
C70 C71 H71 120.1 . .
C71 C72 C73 119.4(8) . .
C71 C72 H72 120.3 . .
C73 C72 H72 120.3 . .
C74 C73 C72 120.8(9) . .
C74 C73 H73 119.6 . .
C72 C73 H73 119.6 . .
C73 C74 C69 120.5(8) . .
C73 C74 P6 119.8(7) . .
C69 C74 P6 119.6(7) . .
C76 C75 C80 118.0(9) . .
C76 C75 P6 123.5(7) . .
C80 C75 P6 118.5(7) . .
C77 C76 C75 121.4(9) . .
C77 C76 H76 119.3 . .
C75 C76 H76 119.3 . .
C78 C77 C76 119.7(10) . .
C78 C77 H77 120.2 . .
C76 C77 H77 120.2 . .
C77 C78 C79 119.8(10) . .
C77 C78 H78 120.1 . .
C79 C78 H78 120.1 . .
C80 C79 C78 120.5(10) . .
C80 C79 H79 119.7 . .
C78 C79 H79 119.7 . .
C79 C80 C75 120.3(9) . .
C79 C80 H80 119.8 . .
C75 C80 H80 119.8 . .
C86 C81 C82 119.0(10) . .
C86 C81 P6 117.9(9) . .
C82 C81 P6 123.1(8) . .
C81 C82 C83 118.5(12) . .
C81 C82 H82 120.8 . .
C83 C82 H82 120.8 . .
C84 C83 C82 121.0(14) . .
C84 C83 H83 119.5 . .
C82 C83 H83 119.5 . .
C85 C84 C83 118.8(11) . .
C85 C84 H84 120.6 . .
C83 C84 H84 120.6 . .
C84 C85 C86 121.8(13) . .
C84 C85 H85 119.1 . .
C86 C85 H85 119.1 . .
C85 C86 C81 120.7(13) . .
C85 C86 H86 119.6 . .
C81 C86 H86 119.6 . .
C92 C87 C88 120.0(8) . .
C92 C87 P7 122.7(7) . .
C88 C87 P7 117.3(7) . .
C89 C88 C87 119.6(9) . .
C89 C88 H88 120.2 . .
C87 C88 H88 120.2 . .
C90 C89 C88 119.8(9) . .
C90 C89 H89 120.1 . .
C88 C89 H89 120.1 . .
C91 C90 C89 120.4(9) . .
C91 C90 H90 119.8 . .
C89 C90 H90 119.8 . .
C90 C91 C92 120.2(9) . .
C90 C91 H91 119.9 . .
C92 C91 H91 119.9 . .
C87 C92 C91 119.9(9) . .
C87 C92 H92 120.1 . .
C91 C92 H92 120.1 . .
C98 C93 C94 117.4(8) . .
C98 C93 P7 123.6(7) . .
C94 C93 P7 119.0(7) . .
C95 C94 C93 120.7(10) . .
C95 C94 H94 119.6 . .
C93 C94 H94 119.6 . .
C94 C95 C96 120.1(10) . .
C94 C95 H95 119.9 . .
C96 C95 H95 119.9 . .
C97 C96 C95 120.1(10) . .
C97 C96 H96 119.9 . .
C95 C96 H96 119.9 . .
C96 C97 C98 120.4(10) . .
C96 C97 H97 119.8 . .
C98 C97 H97 119.8 . .
C97 C98 C93 121.3(9) . .
C97 C98 H98 119.4 . .
C93 C98 H98 119.4 . .
C100 C99 C104 119.9(7) . .
C100 C99 P7 118.3(6) . .
C104 C99 P7 121.8(6) . .
C99 C100 C101 119.3(8) . .
C99 C100 H100 120.3 . .
C101 C100 H100 120.3 . .
C102 C101 C100 121.0(9) . .
C102 C101 H101 119.5 . .
C100 C101 H101 119.5 . .
C101 C102 C103 119.7(9) . .
C101 C102 H102 120.1 . .
C103 C102 H102 120.1 . .
C102 C103 C104 121.9(8) . .
C102 C103 H103 119.0 . .
C104 C103 H103 119.0 . .
C99 C104 C103 118.0(7) . .
C99 C104 P8 119.5(6) . .
C103 C104 P8 122.4(6) . .
C110 C105 C106 119.4(8) . .
C110 C105 P8 121.9(7) . .
C106 C105 P8 118.4(7) . .
C107 C106 C105 120.5(9) . .
C107 C106 H106 119.8 . .
C105 C106 H106 119.8 . .
C108 C107 C106 119.4(9) . .
C108 C107 H107 120.3 . .
C106 C107 H107 120.3 . .
C109 C108 C107 120.1(8) . .
C109 C108 H108 119.9 . .
C107 C108 H108 119.9 . .
C108 C109 C110 121.0(9) . .
C108 C109 H109 119.5 . .
C110 C109 H109 119.5 . .
C105 C110 C109 119.3(9) . .
C105 C110 H110 120.3 . .
C109 C110 H110 120.3 . .
C112 C111 C116 119.5(8) . .
C112 C111 P8 119.5(6) . .
C116 C111 P8 121.0(6) . .
C113 C112 C111 120.7(9) . .
C113 C112 H112 119.6 . .
C111 C112 H112 119.6 . .
C112 C113 C114 121.6(9) . .
C112 C113 H113 119.2 . .
C114 C113 H113 119.2 . .
C113 C114 C115 118.2(8) . .
C113 C114 H114 120.9 . .
C115 C114 H114 120.9 . .
C116 C115 C114 121.7(9) . .
C116 C115 H115 119.1 . .
C114 C115 H115 119.1 . .
C115 C116 C111 118.3(8) . .
C115 C116 P9 121.3(7) . .
C111 C116 P9 120.4(7) . .
C118 C117 C122 118.9(8) . .
C118 C117 P9 123.9(7) . .
C122 C117 P9 117.2(7) . .
C117 C118 C119 120.7(9) . .
C117 C118 H118 119.7 . .
C119 C118 H118 119.7 . .
C118 C119 C120 120.2(10) . .
C118 C119 H119 119.9 . .
C120 C119 H119 119.9 . .
C121 C120 C119 119.7(9) . .
C121 C120 H120 120.1 . .
C119 C120 H120 120.1 . .
C122 C121 C120 119.9(10) . .
C122 C121 H121 120.1 . .
C120 C121 H121 120.1 . .
C121 C122 C117 120.6(9) . .
C121 C122 H122 119.7 . .
C117 C122 H122 119.7 . .
C124 C123 C128 119.2(9) . .
C124 C123 P9 124.2(7) . .
C128 C123 P9 116.6(7) . .
C123 C124 C125 120.7(10) . .
C123 C124 H124 119.7 . .
C125 C124 H124 119.7 . .
C126 C125 C124 119.4(11) . .
C126 C125 H125 120.3 . .
C124 C125 H125 120.3 . .
C125 C126 C127 120.3(10) . .
C125 C126 H126 119.9 . .
C127 C126 H126 119.9 . .
C128 C127 C126 120.4(11) . .
C128 C127 H127 119.8 . .
C126 C127 H127 119.8 . .
C127 C128 C123 120.0(10) . .
C127 C128 H128 120.0 . .
C123 C128 H128 120.0 . .
C130 C129 C134 119.0(10) . .
C130 C129 P10 117.2(9) . .
C134 C129 P10 123.8(8) . .
C131 C130 C129 119.6(12) . .
C131 C130 H130 120.2 . .
C129 C130 H130 120.2 . .
C132 C131 C130 121.2(13) . .
C132 C131 H131 119.4 . .
C130 C131 H131 119.4 . .
C131 C132 C133 121.2(12) . .
C131 C132 H132 119.4 . .
C133 C132 H132 119.4 . .
C134 C133 C132 119.0(14) . .
C134 C133 H133 120.5 . .
C132 C133 H133 120.5 . .
C133 C134 C129 120.0(13) . .
C133 C134 H134 120.0 . .
C129 C134 H134 120.0 . .
C136 C135 C140 119.2(9) . .
C136 C135 P10 122.6(7) . .
C140 C135 P10 118.3(7) . .
C135 C136 C137 120.5(9) . .
C135 C136 H136 119.7 . .
C137 C136 H136 119.7 . .
C138 C137 C136 119.8(9) . .
C138 C137 H137 120.1 . .
C136 C137 H137 120.1 . .
C139 C138 C137 120.0(9) . .
C139 C138 H138 120.0 . .
C137 C138 H138 120.0 . .
C138 C139 C140 120.5(9) . .
C138 C139 H139 119.8 . .
C140 C139 H139 119.8 . .
C135 C140 C139 120.0(9) . .
C135 C140 H140 120.0 . .
C139 C140 H140 120.0 . .
C142 C141 C146 120.2(8) . .
C142 C141 P10 120.4(7) . .
C146 C141 P10 119.4(6) . .
C141 C142 C143 120.4(9) . .
C141 C142 H142 119.8 . .
C143 C142 H142 119.8 . .
C142 C143 C144 119.9(8) . .
C142 C143 H143 120.0 . .
C144 C143 H143 120.0 . .
C145 C144 C143 119.5(9) . .
C145 C144 H144 120.3 . .
C143 C144 H144 120.3 . .
C146 C145 C144 121.3(9) . .
C146 C145 H145 119.4 . .
C144 C145 H145 119.4 . .
C145 C146 C141 118.6(8) . .
C145 C146 P11 119.2(7) . .
C141 C146 P11 122.2(6) . .
C152 C147 C148 119.3(8) . .
C152 C147 P11 119.5(6) . .
C148 C147 P11 120.8(7) . .
C147 C148 C149 119.4(9) . .
C147 C148 H148 120.3 . .
C149 C148 H148 120.3 . .
C150 C149 C148 120.6(9) . .
C150 C149 H149 119.7 . .
C148 C149 H149 119.7 . .
C151 C150 C149 120.4(9) . .
C151 C150 H150 119.8 . .
C149 C150 H150 119.8 . .
C150 C151 C152 119.1(9) . .
C150 C151 H151 120.4 . .
C152 C151 H151 120.4 . .
C147 C152 C151 121.2(9) . .
C147 C152 H152 119.4 . .
C151 C152 H152 119.4 . .
C154 C153 C158 117.5(8) . .
C154 C153 P11 122.7(6) . .
C158 C153 P11 119.7(7) . .
C155 C154 C153 122.8(8) . .
C155 C154 H154 118.6 . .
C153 C154 H154 118.6 . .
C154 C155 C156 119.2(8) . .
C154 C155 H155 120.4 . .
C156 C155 H155 120.4 . .
C157 C156 C155 119.9(8) . .
C157 C156 H156 120.1 . .
C155 C156 H156 120.1 . .
C156 C157 C158 121.1(8) . .
C156 C157 H157 119.4 . .
C158 C157 H157 119.4 . .
C153 C158 C157 119.4(8) . .
C153 C158 P12 121.7(7) . .
C157 C158 P12 119.0(6) . .
C160 C159 C164 118.4(9) . .
C160 C159 P12 122.6(7) . .
C164 C159 P12 119.0(7) . .
C159 C160 C161 120.6(10) . .
C159 C160 H160 119.7 . .
C161 C160 H160 119.7 . .
C162 C161 C160 119.7(11) . .
C162 C161 H161 120.1 . .
C160 C161 H161 120.1 . .
C163 C162 C161 119.2(10) . .
C163 C162 H162 120.4 . .
C161 C162 H162 120.4 . .
C162 C163 C164 121.7(11) . .
C162 C163 H163 119.2 . .
C164 C163 H163 119.2 . .
C163 C164 C159 120.3(11) . .
C163 C164 H164 119.9 . .
C159 C164 H164 119.9 . .
C170 C165 C166 119.3(8) . .
C170 C165 P12 123.7(7) . .
C166 C165 P12 117.0(7) . .
C167 C166 C165 119.6(9) . .
C167 C166 H166 120.2 . .
C165 C166 H166 120.2 . .
C168 C167 C166 120.6(10) . .
C168 C167 H167 119.7 . .
C166 C167 H167 119.7 . .
C167 C168 C169 120.1(10) . .
C167 C168 H168 119.9 . .
C169 C168 H168 119.9 . .
C168 C169 C170 119.6(10) . .
C168 C169 H169 120.2 . .
C170 C169 H169 120.2 . .
C165 C170 C169 120.7(9) . .
C165 C170 H170 119.7 . .
C169 C170 H170 119.7 . .
C1 Ag1 P1 125.4(3) . .
C1 Ag1 P3 119.7(3) . .
P1 Ag1 P3 111.11(7) . .
C1 Ag1 P2 123.3(2) . .
P1 Ag1 P2 81.52(7) . .
P3 Ag1 P2 81.18(7) . .
N1 Ag2 P6 125.3(2) . .
N1 Ag2 P4 119.1(2) . .
P6 Ag2 P4 111.77(8) . .
N1 Ag2 P5 123.0(2) . .
P6 Ag2 P5 81.78(7) . .
P4 Ag2 P5 81.58(7) . .
C2 Ag3 P9 125.4(3) . .
C2 Ag3 P7 118.8(3) . .
P9 Ag3 P7 111.77(7) . .
C2 Ag3 P8 123.6(2) . .
P9 Ag3 P8 82.05(7) . .
P7 Ag3 P8 81.44(7) . .
N2 Ag4 P10 125.4(2) . .
N2 Ag4 P12 119.1(2) . .
P10 Ag4 P12 111.96(8) . .
N2 Ag4 P11 122.7(2) . .
P10 Ag4 P11 81.62(7) . .
P12 Ag4 P11 81.48(7) . .
F2 B1 F2 109(2) . 2
F2 B1 F1 109.8(8) . .
F2 B1 F1 110.8(8) 2 .
F2 B1 F1 110.8(8) . 2
F2 B1 F1 109.8(8) 2 2
F1 B1 F1 107(2) . 2
F4 B2 F4 113(2) 2 .
F4 B2 F3 110.2(8) 2 2
F4 B2 F3 107.4(10) . 2
F4 B2 F3 107.4(10) 2 .
F4 B2 F3 110.2(8) . .
F3 B2 F3 108(2) 2 .
N1 C1 Ag1 175.2(8) . .
N2 C2 Ag3 175.6(8) . .
C3 P1 C9 105.0(4) . .
C3 P1 C15 103.8(4) . .
C9 P1 C15 102.1(4) . .
C3 P1 Ag1 124.1(3) . .
C9 P1 Ag1 115.3(3) . .
C15 P1 Ag1 103.7(3) . .
C21 P2 C27 104.9(4) . .
C21 P2 C20 104.2(4) . .
C27 P2 C20 100.7(4) . .
C21 P2 Ag1 133.7(3) . .
C27 P2 Ag1 106.8(3) . .
C20 P2 Ag1 102.1(3) . .
C39 P3 C33 102.2(4) . .
C39 P3 C32 104.6(4) . .
C33 P3 C32 102.8(4) . .
C39 P3 Ag1 116.9(3) . .
C33 P3 Ag1 121.7(3) . .
C32 P3 Ag1 106.6(3) . .
C51 P4 C57 104.3(4) . .
C51 P4 C45 103.6(4) . .
C57 P4 C45 102.7(4) . .
C51 P4 Ag2 118.4(3) . .
C57 P4 Ag2 106.8(3) . .
C45 P4 Ag2 119.1(3) . .
C63 P5 C69 103.6(4) . .
C63 P5 C62 105.2(4) . .
C69 P5 C62 100.1(4) . .
C63 P5 Ag2 134.1(3) . .
C69 P5 Ag2 102.3(3) . .
C62 P5 Ag2 106.7(3) . .
C75 P6 C81 104.5(5) . .
C75 P6 C74 102.2(4) . .
C81 P6 C74 103.1(4) . .
C75 P6 Ag2 115.2(3) . .
C81 P6 Ag2 125.4(3) . .
C74 P6 Ag2 103.4(3) . .
C93 P7 C87 103.1(4) . .
C93 P7 C99 102.4(4) . .
C87 P7 C99 104.7(4) . .
C93 P7 Ag3 121.1(3) . .
C87 P7 Ag3 117.1(3) . .
C99 P7 Ag3 106.4(3) . .
C105 P8 C104 105.2(4) . .
C105 P8 C111 103.4(4) . .
C104 P8 C111 101.1(4) . .
C105 P8 Ag3 134.2(3) . .
C104 P8 Ag3 106.4(3) . .
C111 P8 Ag3 102.0(3) . .
C123 P9 C116 103.1(4) . .
C123 P9 C117 104.3(4) . .
C116 P9 C117 102.0(4) . .
C123 P9 Ag3 124.5(3) . .
C116 P9 Ag3 103.3(3) . .
C117 P9 Ag3 116.6(3) . .
C129 P10 C135 104.0(5) . .
C129 P10 C141 103.2(4) . .
C135 P10 C141 102.6(4) . .
C129 P10 Ag4 125.4(3) . .
C135 P10 Ag4 115.2(3) . .
C141 P10 Ag4 103.6(3) . .
C153 P11 C147 105.0(4) . .
C153 P11 C146 101.0(4) . .
C147 P11 C146 103.7(4) . .
C153 P11 Ag4 106.5(3) . .
C147 P11 Ag4 133.8(3) . .
C146 P11 Ag4 102.4(3) . .
C159 P12 C165 104.0(4) . .
C159 P12 C158 103.1(4) . .
C165 P12 C158 104.2(4) . .
C159 P12 Ag4 118.5(3) . .
C165 P12 Ag4 118.7(3) . .
C158 P12 Ag4 106.5(3) . .
F13 B11 F11 106.6(10) . .
F13 B11 F10 104.6(9) . .
F11 B11 F10 111.1(10) . .
F13 B11 F12 106.2(10) . .
F11 B11 F12 106.1(9) . .
F10 B11 F12 121.3(11) . .
F17 B10 F14 107.9(10) . .
F17 B10 F15 104.8(9) . .
F14 B10 F15 109.5(10) . .
F17 B10 F16 106.4(9) . .
F14 B10 F16 105.4(9) . .
F15 B10 F16 122.1(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
N1 C1 1.149(12) .
N1 Ag2 2.164(8) .
N2 C2 1.131(12) .
N2 Ag4 2.155(7) .
C3 C8 1.394(14) .
C3 C4 1.403(14) .
C3 P1 1.818(9) .
C4 C5 1.371(15) .
C4 H4 0.9500 .
C5 C6 1.358(18) .
C5 H5 0.9500 .
C6 C7 1.380(18) .
C6 H6 0.9500 .
C7 C8 1.395(15) .
C7 H7 0.9500 .
C8 H8 0.9500 .
C9 C10 1.376(13) .
C9 C14 1.418(13) .
C9 P1 1.827(9) .
C10 C11 1.392(13) .
C10 H10 0.9500 .
C11 C12 1.397(16) .
C11 H11 0.9500 .
C12 C13 1.378(15) .
C12 H12 0.9500 .
C13 C14 1.374(13) .
C13 H13 0.9500 .
C14 H14 0.9500 .
C15 C20 1.386(12) .
C15 C16 1.415(12) .
C15 P1 1.841(9) .
C16 C17 1.379(13) .
C16 H16 0.9500 .
C17 C18 1.382(14) .
C17 H17 0.9500 .
C18 C19 1.390(13) .
C18 H18 0.9500 .
C19 C20 1.416(12) .
C19 H19 0.9500 .
C20 P2 1.839(9) .
C21 C26 1.389(13) .
C21 C22 1.406(12) .
C21 P2 1.821(8) .
C22 C23 1.391(13) .
C22 H22 0.9500 .
C23 C24 1.382(14) .
C23 H23 0.9500 .
C24 C25 1.402(14) .
C24 H24 0.9500 .
C25 C26 1.403(13) .
C25 H25 0.9500 .
C26 H26 0.9500 .
C27 C28 1.401(12) .
C27 C32 1.407(11) .
C27 P2 1.834(9) .
C28 C29 1.375(13) .
C28 H28 0.9500 .
C29 C30 1.415(13) .
C29 H29 0.9500 .
C30 C31 1.350(13) .
C30 H30 0.9500 .
C31 C32 1.392(12) .
C31 H31 0.9500 .
C32 P3 1.856(9) .
C33 C38 1.365(13) .
C33 C34 1.381(13) .
C33 P3 1.831(9) .
C34 C35 1.392(14) .
C34 H34 0.9500 .
C35 C36 1.390(16) .
C35 H35 0.9500 .
C36 C37 1.397(17) .
C36 H36 0.9500 .
C37 C38 1.408(14) .
C37 H37 0.9500 .
C38 H38 0.9500 .
C39 C40 1.397(13) .
C39 C44 1.400(13) .
C39 P3 1.826(9) .
C40 C41 1.382(13) .
C40 H40 0.9500 .
C41 C42 1.367(15) .
C41 H41 0.9500 .
C42 C43 1.370(15) .
C42 H42 0.9500 .
C43 C44 1.395(13) .
C43 H43 0.9500 .
C44 H44 0.9500 .
C45 C46 1.365(14) .
C45 C50 1.411(14) .
C45 P4 1.832(9) .
C46 C47 1.376(15) .
C46 H46 0.9500 .
C47 C48 1.405(17) .
C47 H47 0.9500 .
C48 C49 1.409(18) .
C48 H48 0.9500 .
C49 C50 1.396(16) .
C49 H49 0.9500 .
C50 H50 0.9500 .
C51 C52 1.399(13) .
C51 C56 1.404(13) .
C51 P4 1.821(9) .
C52 C53 1.392(14) .
C52 H52 0.9500 .
C53 C54 1.383(15) .
C53 H53 0.9500 .
C54 C55 1.406(14) .
C54 H54 0.9500 .
C55 C56 1.369(13) .
C55 H55 0.9500 .
C56 H56 0.9500 .
C57 C58 1.421(12) .
C57 C62 1.429(11) .
C57 P4 1.821(9) .
C58 C59 1.359(13) .
C58 H58 0.9500 .
C59 C60 1.398(13) .
C59 H59 0.9500 .
C60 C61 1.393(13) .
C60 H60 0.9500 .
C61 C62 1.385(12) .
C61 H61 0.9500 .
C62 P5 1.847(8) .
C63 C64 1.394(13) .
C63 C68 1.401(12) .
C63 P5 1.811(8) .
C64 C65 1.395(13) .
C64 H64 0.9500 .
C65 C66 1.379(13) .
C65 H65 0.9500 .
C66 C67 1.389(14) .
C66 H66 0.9500 .
C67 C68 1.388(13) .
C67 H67 0.9500 .
C68 H68 0.9500 .
C69 C74 1.393(13) .
C69 C70 1.401(12) .
C69 P5 1.837(9) .
C70 C71 1.400(13) .
C70 H70 0.9500 .
C71 C72 1.384(14) .
C71 H71 0.9500 .
C72 C73 1.399(13) .
C72 H72 0.9500 .
C73 C74 1.386(13) .
C73 H73 0.9500 .
C74 P6 1.855(9) .
C75 C76 1.388(13) .
C75 C80 1.414(13) .
C75 P6 1.809(9) .
C76 C77 1.387(14) .
C76 H76 0.9500 .
C77 C78 1.371(15) .
C77 H77 0.9500 .
C78 C79 1.400(15) .
C78 H78 0.9500 .
C79 C80 1.364(14) .
C79 H79 0.9500 .
C80 H80 0.9500 .
C81 C86 1.385(15) .
C81 C82 1.395(16) .
C81 P6 1.827(10) .
C82 C83 1.424(15) .
C82 H82 0.9500 .
C83 C84 1.37(2) .
C83 H83 0.9500 .
C84 C85 1.36(2) .
C84 H84 0.9500 .
C85 C86 1.371(17) .
C85 H85 0.9500 .
C86 H86 0.9500 .
C87 C92 1.375(13) .
C87 C88 1.393(13) .
C87 P7 1.840(9) .
C88 C89 1.397(14) .
C88 H88 0.9500 .
C89 C90 1.378(15) .
C89 H89 0.9500 .
C90 C91 1.372(15) .
C90 H90 0.9500 .
C91 C92 1.396(13) .
C91 H91 0.9500 .
C92 H92 0.9500 .
C93 C98 1.385(13) .
C93 C94 1.427(13) .
C93 P7 1.815(8) .
C94 C95 1.366(15) .
C94 H94 0.9500 .
C95 C96 1.386(17) .
C95 H95 0.9500 .
C96 C97 1.370(16) .
C96 H96 0.9500 .
C97 C98 1.379(14) .
C97 H97 0.9500 .
C98 H98 0.9500 .
C99 C100 1.406(12) .
C99 C104 1.409(12) .
C99 P7 1.843(8) .
C100 C101 1.409(13) .
C100 H100 0.9500 .
C101 C102 1.363(14) .
C101 H101 0.9500 .
C102 C103 1.376(13) .
C102 H102 0.9500 .
C103 C104 1.410(12) .
C103 H103 0.9500 .
C104 P8 1.837(8) .
C105 C110 1.391(12) .
C105 C106 1.408(13) .
C105 P8 1.823(8) .
C106 C107 1.394(13) .
C106 H106 0.9500 .
C107 C108 1.392(14) .
C107 H107 0.9500 .
C108 C109 1.377(14) .
C108 H108 0.9500 .
C109 C110 1.401(12) .
C109 H109 0.9500 .
C110 H110 0.9500 .
C111 C112 1.387(12) .
C111 C116 1.408(12) .
C111 P8 1.846(9) .
C112 C113 1.363(13) .
C112 H112 0.9500 .
C113 C114 1.371(14) .
C113 H113 0.9500 .
C114 C115 1.400(12) .
C114 H114 0.9500 .
C115 C116 1.386(12) .
C115 H115 0.9500 .
C116 P9 1.829(9) .
C117 C118 1.383(13) .
C117 C122 1.403(13) .
C117 P9 1.833(9) .
C118 C119 1.387(13) .
C118 H118 0.9500 .
C119 C120 1.389(14) .
C119 H119 0.9500 .
C120 C121 1.391(15) .
C120 H120 0.9500 .
C121 C122 1.384(14) .
C121 H121 0.9500 .
C122 H122 0.9500 .
C123 C124 1.382(13) .
C123 C128 1.389(14) .
C123 P9 1.811(9) .
C124 C125 1.407(14) .
C124 H124 0.9500 .
C125 C126 1.367(18) .
C125 H125 0.9500 .
C126 C127 1.386(18) .
C126 H126 0.9500 .
C127 C128 1.388(14) .
C127 H127 0.9500 .
C128 H128 0.9500 .
C129 C130 1.404(15) .
C129 C134 1.414(16) .
C129 P10 1.819(10) .
C130 C131 1.402(16) .
C130 H130 0.9500 .
C131 C132 1.33(2) .
C131 H131 0.9500 .
C132 C133 1.41(2) .
C132 H132 0.9500 .
C133 C134 1.393(16) .
C133 H133 0.9500 .
C134 H134 0.9500 .
C135 C136 1.390(13) .
C135 C140 1.392(13) .
C135 P10 1.822(10) .
C136 C137 1.395(14) .
C136 H136 0.9500 .
C137 C138 1.386(14) .
C137 H137 0.9500 .
C138 C139 1.378(15) .
C138 H138 0.9500 .
C139 C140 1.395(14) .
C139 H139 0.9500 .
C140 H140 0.9500 .
C141 C142 1.384(12) .
C141 C146 1.404(13) .
C141 P10 1.841(9) .
C142 C143 1.386(13) .
C142 H142 0.9500 .
C143 C144 1.390(14) .
C143 H143 0.9500 .
C144 C145 1.388(13) .
C144 H144 0.9500 .
C145 C146 1.388(12) .
C145 H145 0.9500 .
C146 P11 1.831(9) .
C147 C152 1.380(13) .
C147 C148 1.393(12) .
C147 P11 1.829(8) .
C148 C149 1.395(13) .
C148 H148 0.9500 .
C149 C150 1.381(14) .
C149 H149 0.9500 .
C150 C151 1.375(14) .
C150 H150 0.9500 .
C151 C152 1.399(13) .
C151 H151 0.9500 .
C152 H152 0.9500 .
C153 C154 1.403(12) .
C153 C158 1.412(12) .
C153 P11 1.829(9) .
C154 C155 1.367(12) .
C154 H154 0.9500 .
C155 C156 1.408(13) .
C155 H155 0.9500 .
C156 C157 1.364(13) .
C156 H156 0.9500 .
C157 C158 1.417(12) .
C157 H157 0.9500 .
C158 P12 1.846(9) .
C159 C160 1.379(14) .
C159 C164 1.408(14) .
C159 P12 1.814(9) .
C160 C161 1.406(14) .
C160 H160 0.9500 .
C161 C162 1.393(18) .
C161 H161 0.9500 .
C162 C163 1.364(18) .
C162 H162 0.9500 .
C163 C164 1.374(15) .
C163 H163 0.9500 .
C164 H164 0.9500 .
C165 C170 1.385(13) .
C165 C166 1.394(13) .
C165 P12 1.826(9) .
C166 C167 1.395(14) .
C166 H166 0.9500 .
C167 C168 1.374(15) .
C167 H167 0.9500 .
C168 C169 1.383(15) .
C168 H168 0.9500 .
C169 C170 1.393(14) .
C169 H169 0.9500 .
C170 H170 0.9500 .
Ag1 C1 2.144(9) .
Ag1 P1 2.477(2) .
Ag1 P3 2.496(2) .
Ag1 P2 2.546(2) .
Ag2 P6 2.483(2) .
Ag2 P4 2.490(2) .
Ag2 P5 2.542(2) .
Ag3 C2 2.154(9) .
Ag3 P9 2.473(2) .
Ag3 P7 2.497(2) .
Ag3 P8 2.537(2) .
Ag4 P10 2.489(2) .
Ag4 P12 2.496(2) .
Ag4 P11 2.541(2) .
B1 F2 1.341(16) .
B1 F2 1.341(16) 2
B1 F1 1.361(16) .
B1 F1 1.361(16) 2
B2 F4 1.330(18) 2
B2 F4 1.330(18) .
B2 F3 1.350(19) 2
B2 F3 1.350(19) .
F15 B10 1.392(10) .
F10 B11 1.387(10) .
F11 B11 1.381(10) .
F14 B10 1.383(10) .
B11 F13 1.375(10) .
B11 F12 1.389(10) .
B10 F17 1.377(10) .
B10 F16 1.393(10) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C8 C3 C4 C5 -1.2(15)
P1 C3 C4 C5 179.3(8)
C3 C4 C5 C6 0.2(17)
C4 C5 C6 C7 0.8(18)
C5 C6 C7 C8 -0.8(17)
C6 C7 C8 C3 -0.1(15)
C4 C3 C8 C7 1.1(14)
P1 C3 C8 C7 -179.4(8)
C14 C9 C10 C11 -0.4(14)
P1 C9 C10 C11 179.0(8)
C9 C10 C11 C12 -1.5(15)
C10 C11 C12 C13 1.7(15)
C11 C12 C13 C14 0.0(15)
C12 C13 C14 C9 -1.9(15)
C10 C9 C14 C13 2.1(14)
P1 C9 C14 C13 -177.3(7)
C20 C15 C16 C17 2.9(13)
P1 C15 C16 C17 -177.2(7)
C15 C16 C17 C18 -0.2(14)
C16 C17 C18 C19 -2.0(14)
C17 C18 C19 C20 1.4(13)
C16 C15 C20 C19 -3.4(12)
P1 C15 C20 C19 176.7(6)
C16 C15 C20 P2 174.1(7)
P1 C15 C20 P2 -5.7(10)
C18 C19 C20 C15 1.3(12)
C18 C19 C20 P2 -176.3(7)
C26 C21 C22 C23 -1.3(12)
P2 C21 C22 C23 -174.7(6)
C21 C22 C23 C24 0.3(13)
C22 C23 C24 C25 0.3(14)
C23 C24 C25 C26 0.1(14)
C22 C21 C26 C25 1.7(14)
P2 C21 C26 C25 175.2(7)
C24 C25 C26 C21 -1.1(15)
C32 C27 C28 C29 -0.4(13)
P2 C27 C28 C29 179.1(7)
C27 C28 C29 C30 0.6(14)
C28 C29 C30 C31 -1.0(14)
C29 C30 C31 C32 1.3(14)
C30 C31 C32 C27 -1.2(13)
C30 C31 C32 P3 -179.3(7)
C28 C27 C32 C31 0.7(12)
P2 C27 C32 C31 -178.9(7)
C28 C27 C32 P3 178.8(7)
P2 C27 C32 P3 -0.8(10)
C38 C33 C34 C35 3.8(15)
P3 C33 C34 C35 179.7(8)
C33 C34 C35 C36 -3.0(17)
C34 C35 C36 C37 1.2(18)
C35 C36 C37 C38 -0.1(19)
C34 C33 C38 C37 -2.7(15)
P3 C33 C38 C37 -178.7(8)
C36 C37 C38 C33 0.9(18)
C44 C39 C40 C41 1.9(13)
P3 C39 C40 C41 -177.3(7)
C39 C40 C41 C42 -1.5(15)
C40 C41 C42 C43 1.0(16)
C41 C42 C43 C44 -0.9(16)
C42 C43 C44 C39 1.3(15)
C40 C39 C44 C43 -1.9(14)
P3 C39 C44 C43 177.4(8)
C50 C45 C46 C47 1.5(16)
P4 C45 C46 C47 178.1(9)
C45 C46 C47 C48 -1.7(18)
C46 C47 C48 C49 1.7(19)
C47 C48 C49 C50 -1(2)
C48 C49 C50 C45 1(2)
C46 C45 C50 C49 -1.3(18)
P4 C45 C50 C49 -178.1(10)
C56 C51 C52 C53 3.4(14)
P4 C51 C52 C53 -177.7(7)
C51 C52 C53 C54 -0.6(15)
C52 C53 C54 C55 -2.1(15)
C53 C54 C55 C56 2.0(15)
C54 C55 C56 C51 0.8(15)
C52 C51 C56 C55 -3.5(14)
P4 C51 C56 C55 177.5(8)
C62 C57 C58 C59 -0.4(13)
P4 C57 C58 C59 -178.9(7)
C57 C58 C59 C60 -0.7(15)
C58 C59 C60 C61 0.7(14)
C59 C60 C61 C62 0.2(14)
C60 C61 C62 C57 -1.3(13)
C60 C61 C62 P5 179.7(7)
C58 C57 C62 C61 1.3(12)
P4 C57 C62 C61 179.8(7)
C58 C57 C62 P5 -179.6(6)
P4 C57 C62 P5 -1.1(10)
C68 C63 C64 C65 1.8(13)
P5 C63 C64 C65 175.0(7)
C63 C64 C65 C66 -0.5(14)
C64 C65 C66 C67 -0.4(14)
C65 C66 C67 C68 -0.1(14)
C66 C67 C68 C63 1.4(13)
C64 C63 C68 C67 -2.2(13)
P5 C63 C68 C67 -175.3(7)
C74 C69 C70 C71 1.2(13)
P5 C69 C70 C71 -176.8(7)
C69 C70 C71 C72 0.7(14)
C70 C71 C72 C73 -2.2(14)
C71 C72 C73 C74 1.7(14)
C72 C73 C74 C69 0.2(14)
C72 C73 C74 P6 -177.9(7)
C70 C69 C74 C73 -1.6(13)
P5 C69 C74 C73 176.3(7)
C70 C69 C74 P6 176.5(6)
P5 C69 C74 P6 -5.6(10)
C80 C75 C76 C77 3.3(13)
P6 C75 C76 C77 -176.0(7)
C75 C76 C77 C78 -4.6(14)
C76 C77 C78 C79 5.3(14)
C77 C78 C79 C80 -5.1(16)
C78 C79 C80 C75 4.0(16)
C76 C75 C80 C79 -3.1(14)
P6 C75 C80 C79 176.4(8)
C86 C81 C82 C83 0.9(15)
P6 C81 C82 C83 179.9(8)
C81 C82 C83 C84 1.0(17)
C82 C83 C84 C85 -2.5(19)
C83 C84 C85 C86 2.1(19)
C84 C85 C86 C81 -0.1(18)
C82 C81 C86 C85 -1.4(15)
P6 C81 C86 C85 179.6(8)
C92 C87 C88 C89 2.4(14)
P7 C87 C88 C89 -177.6(7)
C87 C88 C89 C90 -0.7(15)
C88 C89 C90 C91 -1.8(16)
C89 C90 C91 C92 2.6(16)
C88 C87 C92 C91 -1.5(14)
P7 C87 C92 C91 178.4(7)
C90 C91 C92 C87 -1.0(15)
C98 C93 C94 C95 -0.4(15)
P7 C93 C94 C95 178.6(9)
C93 C94 C95 C96 0.6(18)
C94 C95 C96 C97 0(2)
C95 C96 C97 C98 -1.0(19)
C96 C97 C98 C93 1.2(17)
C94 C93 C98 C97 -0.5(15)
P7 C93 C98 C97 -179.5(8)
C104 C99 C100 C101 -0.4(12)
P7 C99 C100 C101 179.0(7)
C99 C100 C101 C102 -0.6(14)
C100 C101 C102 C103 1.5(15)
C101 C102 C103 C104 -1.5(14)
C100 C99 C104 C103 0.4(12)
P7 C99 C104 C103 -178.9(6)
C100 C99 C104 P8 178.2(6)
P7 C99 C104 P8 -1.1(9)
C102 C103 C104 C99 0.6(13)
C102 C103 C104 P8 -177.2(7)
C110 C105 C106 C107 0.1(13)
P8 C105 C106 C107 -173.7(7)
C105 C106 C107 C108 -3.8(15)
C106 C107 C108 C109 6.0(15)
C107 C108 C109 C110 -4.5(14)
C106 C105 C110 C109 1.4(12)
P8 C105 C110 C109 174.9(6)
C108 C109 C110 C105 0.8(13)
C116 C111 C112 C113 -1.5(13)
P8 C111 C112 C113 176.8(7)
C111 C112 C113 C114 -0.4(14)
C112 C113 C114 C115 1.6(15)
C113 C114 C115 C116 -1.1(14)
C114 C115 C116 C111 -0.6(13)
C114 C115 C116 P9 176.5(7)
C112 C111 C116 C115 1.9(12)
P8 C111 C116 C115 -176.3(7)
C112 C111 C116 P9 -175.3(6)
P8 C111 C116 P9 6.5(10)
C122 C117 C118 C119 -2.9(14)
P9 C117 C118 C119 177.0(7)
C117 C118 C119 C120 2.8(15)
C118 C119 C120 C121 -1.5(15)
C119 C120 C121 C122 0.5(15)
C120 C121 C122 C117 -0.6(15)
C118 C117 C122 C121 1.7(14)
P9 C117 C122 C121 -178.1(8)
C128 C123 C124 C125 -1.5(14)
P9 C123 C124 C125 179.4(7)
C123 C124 C125 C126 1.4(15)
C124 C125 C126 C127 -0.8(16)
C125 C126 C127 C128 0.3(16)
C126 C127 C128 C123 -0.4(16)
C124 C123 C128 C127 1.0(14)
P9 C123 C128 C127 -179.8(8)
C134 C129 C130 C131 0.4(14)
P10 C129 C130 C131 179.7(8)
C129 C130 C131 C132 0.5(16)
C130 C131 C132 C133 -0.6(18)
C131 C132 C133 C134 0.0(18)
C132 C133 C134 C129 0.9(17)
C130 C129 C134 C133 -1.0(15)
P10 C129 C134 C133 179.7(8)
C140 C135 C136 C137 -2.7(14)
P10 C135 C136 C137 178.2(7)
C135 C136 C137 C138 0.8(15)
C136 C137 C138 C139 1.8(15)
C137 C138 C139 C140 -2.4(16)
C136 C135 C140 C139 2.1(15)
P10 C135 C140 C139 -178.9(8)
C138 C139 C140 C135 0.5(16)
C146 C141 C142 C143 -2.0(14)
P10 C141 C142 C143 176.8(7)
C141 C142 C143 C144 -0.5(15)
C142 C143 C144 C145 2.8(15)
C143 C144 C145 C146 -2.6(14)
C144 C145 C146 C141 0.1(13)
C144 C145 C146 P11 177.8(7)
C142 C141 C146 C145 2.2(13)
P10 C141 C146 C145 -176.6(6)
C142 C141 C146 P11 -175.4(7)
P10 C141 C146 P11 5.8(10)
C152 C147 C148 C149 1.9(12)
P11 C147 C148 C149 174.8(6)
C147 C148 C149 C150 -1.2(13)
C148 C149 C150 C151 0.9(13)
C149 C150 C151 C152 -1.2(14)
C148 C147 C152 C151 -2.3(14)
P11 C147 C152 C151 -175.3(7)
C150 C151 C152 C147 1.9(15)
C158 C153 C154 C155 1.4(13)
P11 C153 C154 C155 -178.1(7)
C153 C154 C155 C156 -2.1(14)
C154 C155 C156 C157 1.2(14)
C155 C156 C157 C158 0.5(14)
C154 C153 C158 C157 0.3(12)
P11 C153 C158 C157 179.8(6)
C154 C153 C158 P12 179.5(6)
P11 C153 C158 P12 -1.0(10)
C156 C157 C158 C153 -1.2(13)
C156 C157 C158 P12 179.6(7)
C164 C159 C160 C161 0.1(16)
P12 C159 C160 C161 -178.8(9)
C159 C160 C161 C162 2.0(18)
C160 C161 C162 C163 -3.0(19)
C161 C162 C163 C164 2(2)
C162 C163 C164 C159 0(2)
C160 C159 C164 C163 -1.3(19)
P12 C159 C164 C163 177.6(11)
C170 C165 C166 C167 3.0(14)
P12 C165 C166 C167 -177.7(7)
C165 C166 C167 C168 -0.7(15)
C166 C167 C168 C169 -0.7(16)
C167 C168 C169 C170 -0.1(16)
C166 C165 C170 C169 -3.8(15)
P12 C165 C170 C169 176.9(8)
C168 C169 C170 C165 2.4(16)
C8 C3 P1 C9 -3.9(9)
C4 C3 P1 C9 175.6(8)
C8 C3 P1 C15 103.0(8)
C4 C3 P1 C15 -77.5(8)
C8 C3 P1 Ag1 -139.6(7)
C4 C3 P1 Ag1 39.9(9)
C10 C9 P1 C3 -105.2(8)
C14 C9 P1 C3 74.1(8)
C10 C9 P1 C15 146.7(7)
C14 C9 P1 C15 -33.9(8)
C10 C9 P1 Ag1 35.0(8)
C14 C9 P1 Ag1 -145.6(7)
C20 C15 P1 C3 158.4(7)
C16 C15 P1 C3 -21.5(8)
C20 C15 P1 C9 -92.6(7)
C16 C15 P1 C9 87.5(8)
C20 C15 P1 Ag1 27.6(7)
C16 C15 P1 Ag1 -152.3(7)
C26 C21 P2 C27 58.1(8)
C22 C21 P2 C27 -128.6(7)
C26 C21 P2 C20 163.5(7)
C22 C21 P2 C20 -23.3(8)
C26 C21 P2 Ag1 -73.8(8)
C22 C21 P2 Ag1 99.5(7)
C28 C27 P2 C21 20.2(8)
C32 C27 P2 C21 -160.3(7)
C28 C27 P2 C20 -87.8(8)
C32 C27 P2 C20 91.8(7)
C28 C27 P2 Ag1 165.9(7)
C32 C27 P2 Ag1 -14.5(7)
C15 C20 P2 C21 123.0(7)
C19 C20 P2 C21 -59.5(7)
C15 C20 P2 C27 -128.5(7)
C19 C20 P2 C27 49.1(7)
C15 C20 P2 Ag1 -18.6(7)
C19 C20 P2 Ag1 159.0(6)
C40 C39 P3 C33 -31.5(9)
C44 C39 P3 C33 149.2(7)
C40 C39 P3 C32 75.4(8)
C44 C39 P3 C32 -103.8(8)
C40 C39 P3 Ag1 -167.0(7)
C44 C39 P3 Ag1 13.8(8)
C38 C33 P3 C39 -53.0(8)
C34 C33 P3 C39 131.0(8)
C38 C33 P3 C32 -161.3(8)
C34 C33 P3 C32 22.7(9)
C38 C33 P3 Ag1 79.6(8)
C34 C33 P3 Ag1 -96.3(8)
C31 C32 P3 C39 -41.5(8)
C27 C32 P3 C39 140.4(7)
C31 C32 P3 C33 64.9(8)
C27 C32 P3 C33 -113.2(7)
C31 C32 P3 Ag1 -166.0(6)
C27 C32 P3 Ag1 16.0(7)
C52 C51 P4 C57 79.6(8)
C56 C51 P4 C57 -101.4(7)
C52 C51 P4 C45 -27.5(9)
C56 C51 P4 C45 151.5(7)
C52 C51 P4 Ag2 -161.9(7)
C56 C51 P4 Ag2 17.0(8)
C58 C57 P4 C51 -40.0(8)
C62 C57 P4 C51 141.6(7)
C58 C57 P4 C45 67.8(8)
C62 C57 P4 C45 -110.6(7)
C58 C57 P4 Ag2 -166.2(6)
C62 C57 P4 Ag2 15.4(8)
C46 C45 P4 C51 129.0(8)
C50 C45 P4 C51 -54.3(9)
C46 C45 P4 C57 20.7(9)
C50 C45 P4 C57 -162.6(9)
C46 C45 P4 Ag2 -96.9(9)
C50 C45 P4 Ag2 79.8(9)
C64 C63 P5 C69 162.0(7)
C68 C63 P5 C69 -25.0(8)
C64 C63 P5 C62 57.4(8)
C68 C63 P5 C62 -129.6(7)
C64 C63 P5 Ag2 -75.3(8)
C68 C63 P5 Ag2 97.7(7)
C74 C69 P5 C63 123.1(7)
C70 C69 P5 C63 -59.0(8)
C74 C69 P5 C62 -128.5(7)
C70 C69 P5 C62 49.5(7)
C74 C69 P5 Ag2 -18.7(7)
C70 C69 P5 Ag2 159.2(6)
C61 C62 P5 C63 19.1(8)
C57 C62 P5 C63 -160.0(7)
C61 C62 P5 C69 -88.2(8)
C57 C62 P5 C69 92.8(7)
C61 C62 P5 Ag2 165.6(7)
C57 C62 P5 Ag2 -13.5(7)
C76 C75 P6 C81 72.5(9)
C80 C75 P6 C81 -106.9(8)
C76 C75 P6 C74 -34.7(9)
C80 C75 P6 C74 145.9(7)
C76 C75 P6 Ag2 -146.0(7)
C80 C75 P6 Ag2 34.6(8)
C86 C81 P6 C75 179.9(8)
C82 C81 P6 C75 0.9(10)
C86 C81 P6 C74 -73.6(8)
C82 C81 P6 C74 107.4(9)
C86 C81 P6 Ag2 43.6(9)
C82 C81 P6 Ag2 -135.4(8)
C73 C74 P6 C75 85.5(8)
C69 C74 P6 C75 -92.6(7)
C73 C74 P6 C81 -22.7(8)
C69 C74 P6 C81 159.1(7)
C73 C74 P6 Ag2 -154.5(7)
C69 C74 P6 Ag2 27.3(7)
C98 C93 P7 C87 -129.5(8)
C94 C93 P7 C87 51.6(8)
C98 C93 P7 C99 -20.9(9)
C94 C93 P7 C99 160.2(7)
C98 C93 P7 Ag3 97.1(8)
C94 C93 P7 Ag3 -81.8(8)
C92 C87 P7 C93 31.5(8)
C88 C87 P7 C93 -148.5(7)
C92 C87 P7 C99 -75.2(8)
C88 C87 P7 C99 104.7(7)
C92 C87 P7 Ag3 167.2(6)
C88 C87 P7 Ag3 -12.9(8)
C100 C99 P7 C93 -65.7(7)
C104 C99 P7 C93 113.6(7)
C100 C99 P7 C87 41.5(7)
C104 C99 P7 C87 -139.2(7)
C100 C99 P7 Ag3 166.2(6)
C104 C99 P7 Ag3 -14.5(7)
C110 C105 P8 C104 130.2(7)
C106 C105 P8 C104 -56.2(8)
C110 C105 P8 C111 24.5(8)
C106 C105 P8 C111 -161.9(7)
C110 C105 P8 Ag3 -97.6(7)
C106 C105 P8 Ag3 76.0(8)
C99 C104 P8 C105 162.2(6)
C103 C104 P8 C105 -20.0(8)
C99 C104 P8 C111 -90.4(7)
C103 C104 P8 C111 87.4(7)
C99 C104 P8 Ag3 15.8(7)
C103 C104 P8 Ag3 -166.4(6)
C112 C111 P8 C105 58.6(7)
C116 C111 P8 C105 -123.1(7)
C112 C111 P8 C104 -50.1(7)
C116 C111 P8 C104 128.1(7)
C112 C111 P8 Ag3 -159.8(6)
C116 C111 P8 Ag3 18.5(7)
C124 C123 P9 C116 -103.6(8)
C128 C123 P9 C116 77.2(8)
C124 C123 P9 C117 2.6(9)
C128 C123 P9 C117 -176.6(7)
C124 C123 P9 Ag3 140.0(7)
C128 C123 P9 Ag3 -39.2(8)
C115 C116 P9 C123 23.8(8)
C111 C116 P9 C123 -159.1(7)
C115 C116 P9 C117 -84.2(8)
C111 C116 P9 C117 92.9(7)
C115 C116 P9 Ag3 154.4(7)
C111 C116 P9 Ag3 -28.5(7)
C118 C117 P9 C123 -73.3(8)
C122 C117 P9 C123 106.6(7)
C118 C117 P9 C116 33.7(9)
C122 C117 P9 C116 -146.4(7)
C118 C117 P9 Ag3 145.3(7)
C122 C117 P9 Ag3 -34.8(8)
C130 C129 P10 C135 -178.9(7)
C134 C129 P10 C135 0.4(9)
C130 C129 P10 C141 74.3(8)
C134 C129 P10 C141 -106.4(8)
C130 C129 P10 Ag4 -43.2(9)
C134 C129 P10 Ag4 136.1(7)
C136 C135 P10 C129 -74.0(8)
C140 C135 P10 C129 106.9(8)
C136 C135 P10 C141 33.2(9)
C140 C135 P10 C141 -145.9(8)
C136 C135 P10 Ag4 145.0(7)
C140 C135 P10 Ag4 -34.1(8)
C142 C141 P10 C129 21.7(9)
C146 C141 P10 C129 -159.5(7)
C142 C141 P10 C135 -86.1(8)
C146 C141 P10 C135 92.7(7)
C142 C141 P10 Ag4 153.7(7)
C146 C141 P10 Ag4 -27.5(7)
C154 C153 P11 C147 -19.4(8)
C158 C153 P11 C147 161.0(7)
C154 C153 P11 C146 88.2(7)
C158 C153 P11 C146 -91.4(7)
C154 C153 P11 Ag4 -165.2(6)
C158 C153 P11 Ag4 15.2(7)
C152 C147 P11 C153 -57.1(8)
C148 C147 P11 C153 130.0(7)
C152 C147 P11 C146 -162.7(7)
C148 C147 P11 C146 24.4(8)
C152 C147 P11 Ag4 74.6(8)
C148 C147 P11 Ag4 -98.3(7)
C145 C146 P11 C153 -49.1(7)
C141 C146 P11 C153 128.5(7)
C145 C146 P11 C147 59.5(7)
C141 C146 P11 C147 -122.9(7)
C145 C146 P11 Ag4 -158.9(6)
C141 C146 P11 Ag4 18.6(7)
C160 C159 P12 C165 -127.4(9)
C164 C159 P12 C165 53.7(10)
C160 C159 P12 C158 -18.9(9)
C164 C159 P12 C158 162.2(9)
C160 C159 P12 Ag4 98.3(8)
C164 C159 P12 Ag4 -80.6(9)
C170 C165 P12 C159 28.0(9)
C166 C165 P12 C159 -151.3(7)
C170 C165 P12 C158 -79.7(9)
C166 C165 P12 C158 101.0(8)
C170 C165 P12 Ag4 162.1(7)
C166 C165 P12 Ag4 -17.1(8)
C153 C158 P12 C159 111.3(7)
C157 C158 P12 C159 -69.5(8)
C153 C158 P12 C165 -140.4(7)
C157 C158 P12 C165 38.8(8)
C153 C158 P12 Ag4 -14.1(7)
C157 C158 P12 Ag4 165.1(6)
