#------------------------------------------------------------------------------
#$Date: 2019-11-24 12:53:08 +0200 (Sun, 24 Nov 2019) $
#$Revision: 237947 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/35/00/4350025.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4350025
loop_
_publ_author_name
'Litvinova, Yulia M.'
'Gayfulin, Yakov M.'
'van Leusen, Jan'
'Samsonenko, Denis G.'
'Lazarenko, Vladimir A.'
'Zubavichus, Yan V.'
'Kögerler, Paul'
'Mironov, Yuri V.'
_publ_section_title
;
 Metal--organic frameworks based on polynuclear lanthanide complexes and
 octahedral rhenium clusters
;
_journal_issue                   6
_journal_name_full               'Inorganic Chemistry Frontiers'
_journal_page_first              1518
_journal_paper_doi               10.1039/C9QI00339H
_journal_volume                  6
_journal_year                    2019
_chemical_formula_sum            'C30 H42 Eu4 N10 O23 Re6 S8'
_chemical_formula_weight         2892.25
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2019-03-20 deposited with the CCDC.	2019-05-06 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 110.984(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   22.6868(15)
_cell_length_b                   12.4553(11)
_cell_length_c                   23.6524(17)
_cell_measurement_reflns_used    3200
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      25.0
_cell_measurement_theta_min      3.50
_cell_volume                     6240.2(8)
_computing_cell_refinement       'iMosflm (Battye et al., 2011)'
_computing_data_collection       'Marccd (Doyle, 2011)'
_computing_data_reduction        'iMosflm (Battye et al., 2011)'
_computing_molecular_graphics    'ShelXle (Hübschle, 2011)'
_computing_publication_material  'CIFTAB (Sheldrick, 2015)'
_computing_structure_refinement  'SHELXL-2018 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT-2018 (Sheldrick, 2015)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Rayonix SX-165 CCD'
_diffrn_measurement_method       'φ scan'
_diffrn_radiation_monochromator  'Double Crystal Monochromator'
_diffrn_radiation_source         synchrotron
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.80246
_diffrn_reflns_av_R_equivalents  0.0705
_diffrn_reflns_av_unetI/netI     0.0564
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            72220
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        28.500
_diffrn_reflns_theta_max         29.691
_diffrn_reflns_theta_min         3.248
_diffrn_source                   synchrotron
_exptl_absorpt_coefficient_mu    21.733
_exptl_absorpt_correction_T_max  0.200
_exptl_absorpt_correction_T_min  0.100
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Scala (Evans, 2006)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    3.079
_exptl_crystal_description       block
_exptl_crystal_F_000             5224
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.08
_refine_diff_density_max         3.802
_refine_diff_density_min         -3.736
_refine_diff_density_rms         0.279
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.089
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     884
_refine_ls_number_reflns         12242
_refine_ls_number_restraints     501
_refine_ls_restrained_S_all      1.082
_refine_ls_R_factor_all          0.0373
_refine_ls_R_factor_gt           0.0363
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0170P)²+112.3000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0932
_refine_ls_wR_factor_ref         0.0940
_reflns_Friedel_coverage         0.000
_reflns_number_gt                11939
_reflns_number_total             12242
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9qi00339h2.cif
_cod_data_source_block           li83eu
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4350025
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.074
_shelx_estimated_absorpt_t_max   0.275
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.31003(2) 1.09221(2) 0.57275(2) 0.00947(8) Uani 1 1 d . . . . .
Re2 Re 0.33129(2) 1.29625(2) 0.58872(2) 0.00996(8) Uani 1 1 d . . . . .
Re3 Re 0.23167(2) 1.33736(3) 0.49415(2) 0.01053(8) Uani 1 1 d . . . . .
Re4 Re 0.21068(2) 1.13223(3) 0.47795(2) 0.01015(8) Uani 1 1 d . . . . .
Re5 Re 0.31955(2) 1.21079(3) 0.48535(2) 0.01028(8) Uani 1 1 d . . . . .
Re6 Re 0.22242(2) 1.21922(3) 0.58133(2) 0.00951(8) Uani 1 1 d . . . . .
S1 S 0.40756(9) 1.17313(17) 0.57652(9) 0.0135(4) Uani 1 1 d . . . . .
S2 S 0.33525(10) 1.40002(16) 0.50460(9) 0.0146(4) Uani 1 1 d . . . . .
S3 S 0.22371(10) 1.24704(17) 0.40155(8) 0.0157(4) Uani 1 1 d . . . . .
S4 S 0.29622(10) 1.02166(16) 0.47395(9) 0.0148(4) Uani 1 1 d . . . . .
S5 S 0.31837(10) 1.18252(17) 0.66511(8) 0.0143(4) Uani 1 1 d . . . . .
S6 S 0.24674(10) 1.40751(16) 0.59332(9) 0.0143(4) Uani 1 1 d . . . . .
S7 S 0.13447(9) 1.25523(17) 0.49001(9) 0.0146(4) Uani 1 1 d . . . . .
S8 S 0.20613(9) 1.02998(16) 0.56255(9) 0.0136(4) Uani 1 1 d . . . . .
C1 C 0.3543(4) 0.9546(7) 0.6221(4) 0.0153(16) Uani 1 1 d . . . . .
N1 N 0.3769(4) 0.8829(6) 0.6535(3) 0.0189(15) Uani 1 1 d . . . . .
C2 C 0.4005(4) 1.3860(7) 0.6536(4) 0.0170(17) Uani 1 1 d . . . . .
N2 N 0.4393(4) 1.4321(6) 0.6915(3) 0.0202(16) Uani 1 1 d . . . . .
C3 C 0.1852(4) 1.4792(7) 0.4502(4) 0.0181(17) Uani 1 1 d . . . . .
N3 N 0.1594(3) 1.5547(6) 0.4264(3) 0.0203(16) Uani 1 1 d . . . . .
C4 C 0.1403(4) 1.0384(7) 0.4141(4) 0.0164(17) Uani 1 1 d . . . . .
N4 N 0.1008(4) 0.9919(6) 0.3784(3) 0.0213(16) Uani 1 1 d . . . . .
C5 C 0.3781(4) 1.2138(7) 0.4318(4) 0.0183(18) Uani 1 1 d . . . . .
N5 N 0.4094(4) 1.2217(7) 0.4037(4) 0.0260(18) Uani 1 1 d . . . . .
C6 C 0.1661(4) 1.2283(7) 0.6361(4) 0.0166(17) Uani 1 1 d . . . . .
N6 N 0.1364(4) 1.2348(7) 0.6671(3) 0.0244(17) Uani 1 1 d . . . . .
Eu1 Eu 0.40533(2) 0.76799(4) 0.74721(2) 0.01656(10) Uani 1 1 d . . . . .
Eu2 Eu 0.51201(2) 0.53444(3) 0.77940(2) 0.01204(9) Uani 1 1 d . . . . .
Eu3 Eu 0.53711(2) 0.75535(3) 0.67604(2) 0.01426(9) Uani 1 1 d . . . . .
Eu4 Eu 0.58660(2) 0.81062(4) 0.84417(2) 0.01742(10) Uani 1 1 d D . . . .
O1 O 0.4594(3) 0.6588(5) 0.6989(2) 0.0143(12) Uani 1 1 d . . . . .
H1 H 0.429469 0.621504 0.662419 0.017 Uiso 1 1 calc R U . . .
O2 O 0.4948(3) 0.6956(5) 0.8276(2) 0.0136(11) Uani 1 1 d . . . . .
H2 H 0.486068 0.681293 0.865484 0.016 Uiso 1 1 calc R U . . .
O3 O 0.5043(3) 0.8483(5) 0.7471(3) 0.0180(12) Uani 1 1 d . . . . .
H3 H 0.499750 0.927043 0.738471 0.022 Uiso 1 1 calc R U . . .
O4 O 0.5825(3) 0.6722(5) 0.7754(3) 0.0148(12) Uani 1 1 d . . . . .
H4 H 0.625507 0.642787 0.782191 0.018 Uiso 1 1 calc R U . . .
O1M O 0.3234(5) 0.6654(9) 0.6589(5) 0.069(3) Uani 1 1 d D U . . .
O2M O 0.5220(5) 0.3376(8) 0.8069(5) 0.070(3) Uani 1 1 d . U . . .
O3M O 0.4514(4) 0.7321(9) 0.5792(4) 0.051(2) Uani 1 1 d . U . . .
O4M O 0.5185(4) 0.9424(6) 0.6396(4) 0.0392(19) Uani 1 1 d . . . . .
O5M O 0.6910(5) 0.7226(10) 0.8866(5) 0.034(2) Uani 0.708(10) 1 d D U P A 1
O5M' O 0.6969(8) 0.769(2) 0.8627(12) 0.024(3) Uani 0.292(10) 1 d D U P A 2
O6M O 0.6041(4) 0.7266(6) 0.9408(3) 0.0355(18) Uani 1 1 d . . . . .
O1A O 0.1146(5) 1.0688(8) 0.7398(4) 0.053(2) Uani 1 1 d . U . . .
O2A O 0.0595(5) 0.9585(9) 0.6704(5) 0.060(2) Uani 1 1 d . U . . .
C1A C 0.1086(7) 0.9971(11) 0.7053(6) 0.048(2) Uani 1 1 d . U . . .
C2A C 0.1723(6) 0.9452(10) 0.7077(6) 0.043(2) Uani 1 1 d . U . . .
C3A C 0.2274(6) 1.0023(10) 0.7288(5) 0.039(2) Uani 1 1 d . U . . .
H3A H 0.227015 1.075163 0.740499 0.046 Uiso 1 1 calc R U . . .
C4A C 0.2845(6) 0.9532(9) 0.7332(5) 0.035(2) Uani 1 1 d . U . . .
H4A H 0.321917 0.995353 0.746673 0.042 Uiso 1 1 calc R U . . .
C5A C 0.1741(6) 0.8424(11) 0.6892(7) 0.050(3) Uani 1 1 d . U . . .
H5A H 0.136375 0.802060 0.671571 0.060 Uiso 1 1 calc R U . . .
C6A C 0.2341(6) 0.7969(11) 0.6969(6) 0.046(3) Uani 1 1 d . U . . .
H6A H 0.235624 0.724162 0.685352 0.056 Uiso 1 1 calc R U . . .
N1A N 0.2890(4) 0.8517(7) 0.7196(4) 0.0311(18) Uani 1 1 d . U . . .
O1B O 0.4223(3) 0.9261(6) 0.8072(3) 0.0300(16) Uani 1 1 d . . . . .
O2B O 0.5228(3) 0.9376(7) 0.8682(3) 0.0381(19) Uani 1 1 d . . . . .
C1B C 0.4658(5) 0.9593(8) 0.8530(5) 0.028(2) Uani 1 1 d . U . . .
C2B C 0.4477(5) 1.0314(10) 0.8948(5) 0.037(2) Uani 1 1 d . U . . .
C3B C 0.3855(5) 1.0392(10) 0.8912(5) 0.038(2) Uani 1 1 d . U . . .
H3B H 0.352958 1.000883 0.861206 0.045 Uiso 1 1 calc R U . . .
C4B C 0.3722(6) 1.1044(11) 0.9327(6) 0.043(2) Uani 1 1 d . U . . .
H4B H 0.329640 1.109378 0.930556 0.051 Uiso 1 1 calc R U . . .
C5B C 0.4929(6) 1.0903(13) 0.9380(7) 0.059(3) Uani 1 1 d . U . . .
H5B H 0.535639 1.087708 0.940504 0.071 Uiso 1 1 calc R U . . .
C6B C 0.4762(7) 1.1526(14) 0.9775(8) 0.068(3) Uani 1 1 d . U . . .
H6B H 0.508226 1.191812 1.007545 0.082 Uiso 1 1 calc R U . . .
N1B N 0.4162(5) 1.1607(10) 0.9755(5) 0.054(3) Uani 1 1 d . U . . .
O1C O 0.5746(4) 0.4574(6) 0.7296(4) 0.0354(17) Uani 1 1 d . U . . .
O2C O 0.5658(4) 0.5784(6) 0.6561(4) 0.0379(18) Uani 1 1 d . U . . .
C1C C 0.5817(6) 0.4894(10) 0.6825(6) 0.041(2) Uani 1 1 d D U . . .
C2C C 0.6251(6) 0.4205(11) 0.6612(6) 0.045(3) Uani 0.708(10) 1 d D U P A 1
C3C C 0.6354(8) 0.3136(13) 0.6814(8) 0.047(3) Uani 0.708(10) 1 d D U P A 1
H3C H 0.617054 0.285493 0.708613 0.056 Uiso 0.708(10) 1 calc R U P A 1
C4C C 0.6730(9) 0.2514(15) 0.6600(9) 0.052(3) Uani 0.708(10) 1 d D U P A 1
H4C H 0.677779 0.177634 0.670997 0.062 Uiso 0.708(10) 1 calc R U P A 1
C5C C 0.6543(9) 0.4607(15) 0.6224(9) 0.049(3) Uani 0.708(10) 1 d D U P A 1
H5C H 0.647634 0.532639 0.608186 0.059 Uiso 0.708(10) 1 calc R U P A 1
C6C C 0.6928(9) 0.3925(13) 0.6054(9) 0.048(3) Uani 0.708(10) 1 d D U P A 1
H6C H 0.712900 0.419281 0.579242 0.058 Uiso 0.708(10) 1 calc R U P A 1
N1C N 0.7036(8) 0.2891(11) 0.6242(7) 0.049(3) Uani 0.708(10) 1 d D U P A 1
C2C' C 0.6031(9) 0.401(2) 0.6495(10) 0.049(3) Uani 0.292(10) 1 d D U P A 2
C3C' C 0.5959(19) 0.290(2) 0.6555(18) 0.051(4) Uani 0.292(10) 1 d D U P A 2
H3C' H 0.578120 0.266569 0.684066 0.061 Uiso 0.292(10) 1 calc R U P A 2
C4C' C 0.6133(19) 0.215(3) 0.6222(18) 0.053(4) Uani 0.292(10) 1 d D U P A 2
H4C' H 0.603572 0.140926 0.624341 0.064 Uiso 0.292(10) 1 calc R U P A 2
C5C' C 0.633(2) 0.437(3) 0.6102(18) 0.049(4) Uani 0.292(10) 1 d D U P A 2
H5C' H 0.638946 0.510878 0.603669 0.059 Uiso 0.292(10) 1 calc R U P A 2
C6C' C 0.652(2) 0.355(3) 0.582(2) 0.053(4) Uani 0.292(10) 1 d D U P A 2
H6C' H 0.673867 0.376628 0.555977 0.064 Uiso 0.292(10) 1 calc R U P A 2
N1C' N 0.6447(18) 0.248(3) 0.5861(17) 0.056(4) Uani 0.292(10) 1 d D U P A 2
O1D O 0.6359(3) 0.8341(6) 0.7245(3) 0.0281(15) Uani 1 1 d D U . . .
O2D O 0.6389(6) 0.9414(10) 0.8019(5) 0.038(3) Uani 0.708(10) 1 d D U P A 1
O2D' O 0.6223(14) 0.9477(15) 0.7885(12) 0.034(4) Uani 0.292(10) 1 d D U P A 2
C1D C 0.6545(5) 0.9148(7) 0.7581(4) 0.0255(18) Uani 1 1 d D U . . .
C2D C 0.7037(4) 0.9829(8) 0.7466(4) 0.0215(17) Uani 1 1 d . U . . .
C3D C 0.7260(5) 0.9548(8) 0.7011(4) 0.0243(18) Uani 1 1 d . U . . .
H3D H 0.709409 0.893856 0.676380 0.029 Uiso 1 1 calc R U . . .
C4D C 0.7720(5) 1.0155(9) 0.6921(5) 0.033(2) Uani 1 1 d . U . . .
H4D H 0.786745 0.995745 0.660698 0.040 Uiso 1 1 calc R U . . .
C5D C 0.7292(6) 1.0695(10) 0.7820(6) 0.042(2) Uani 1 1 d . U . . .
H5D H 0.715561 1.089509 0.814048 0.051 Uiso 1 1 calc R U . . .
C6D C 0.7751(7) 1.1275(11) 0.7703(7) 0.055(3) Uani 1 1 d . U . . .
H6D H 0.792259 1.188502 0.794736 0.066 Uiso 1 1 calc R U . . .
N1D N 0.7972(6) 1.1026(9) 0.7261(5) 0.050(2) Uani 1 1 d . U . . .
O1W O 0.4866(5) 1.0774(7) 0.7200(4) 0.049(2) Uani 1 1 d . . . . .
O2W O 0.5784(6) 1.1387(11) 0.8277(6) 0.043(3) Uani 0.6 1 d . . P . .
O3W O 0.5093(10) 0.5962(13) 0.9493(6) 0.045(4) Uani 0.5 1 d . . P . .
O4W O 0.2335(17) 0.780(3) 0.5195(18) 0.020(4) Uani 0.2 1 d . U P . .
O5W O 0.2401(16) 0.783(2) 0.4915(16) 0.020(4) Uani 0.2 1 d . U P . .
O6W O 0.3314(11) 0.6569(18) 0.5510(8) 0.033(5) Uani 0.3 1 d D U P . .
O7W O 0.2476(17) 0.751(3) 0.5380(15) 0.020(4) Uani 0.2 1 d . U P . .
O9W O 0.0068(12) 0.8818(19) 0.5654(10) 0.068(6) Uani 0.5 1 d . U P . .
O10W O 0.5416(19) 0.256(3) 0.5310(17) 0.052(9) Uani 0.25 1 d . U P . .
O11W O 0.496(3) 0.426(5) 0.546(2) 0.086(15) Uani 0.25 1 d . U P . .
O12W O 0.479(2) 0.525(4) 0.5373(19) 0.065(11) Uani 0.25 1 d . U P . .
O13W O 0.536(2) 1.011(3) 0.5331(18) 0.053(9) Uani 0.25 1 d . U P . .
O14W O 0.575(2) 0.048(3) 0.5670(18) 0.055(9) Uani 0.25 1 d . U P . .
O15W O 0.5474(17) 0.053(3) 0.4850(15) 0.046(8) Uani 0.25 1 d . U P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0050 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0090 0.0040 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0150 0.0080 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1500 0.1580 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu 0.0280 4.6530 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.6850 8.6400 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Re2 Re1 Re4 89.786(13) . .
Re2 Re1 Re5 59.769(12) . .
Re2 Re1 Re6 59.990(12) . .
Re4 Re1 Re5 60.001(12) . .
Re4 Re1 Re6 59.984(12) . .
Re6 Re1 Re5 89.992(14) . .
S1 Re1 Re2 57.46(5) . .
S1 Re1 Re4 117.04(5) . .
S1 Re1 Re5 57.06(5) . .
S1 Re1 Re6 117.41(5) . .
S1 Re1 S4 89.26(7) . .
S1 Re1 S8 173.16(7) . .
S4 Re1 Re2 116.88(5) . .
S4 Re1 Re4 57.40(5) . .
S4 Re1 Re5 57.15(5) . .
S4 Re1 Re6 117.34(5) . .
S4 Re1 S8 90.16(7) . .
S5 Re1 Re2 57.19(5) . .
S5 Re1 Re4 117.17(5) . .
S5 Re1 Re5 116.92(5) . .
S5 Re1 Re6 57.24(5) . .
S5 Re1 S1 89.90(7) . .
S5 Re1 S4 173.03(7) . .
S5 Re1 S8 89.85(7) . .
S8 Re1 Re2 117.05(5) . .
S8 Re1 Re4 57.29(5) . .
S8 Re1 Re5 117.25(5) . .
S8 Re1 Re6 57.10(5) . .
C1 Re1 Re2 133.5(2) . .
C1 Re1 Re4 136.6(2) . .
C1 Re1 Re5 137.5(2) . .
C1 Re1 Re6 132.4(2) . .
C1 Re1 S1 94.0(2) . .
C1 Re1 S4 96.3(2) . .
C1 Re1 S5 90.6(2) . .
C1 Re1 S8 92.8(2) . .
Re1 Re2 Re3 90.497(13) . .
Re1 Re2 Re5 60.549(12) . .
Re1 Re2 Re6 60.295(12) . .
Re5 Re2 Re3 60.329(12) . .
Re5 Re2 Re6 90.618(14) . .
Re6 Re2 Re3 60.113(12) . .
S1 Re2 Re1 57.40(5) . .
S1 Re2 Re3 117.62(5) . .
S1 Re2 Re5 57.33(5) . .
S1 Re2 Re6 117.65(5) . .
S2 Re2 Re1 117.89(5) . .
S2 Re2 Re3 57.30(5) . .
S2 Re2 Re5 57.38(5) . .
S2 Re2 Re6 117.39(5) . .
S2 Re2 S1 90.10(7) . .
S5 Re2 Re1 57.50(5) . .
S5 Re2 Re3 117.53(5) . .
S5 Re2 Re5 118.02(5) . .
S5 Re2 Re6 57.44(5) . .
S5 Re2 S1 90.06(7) . .
S5 Re2 S2 173.98(7) . .
S5 Re2 S6 89.53(7) . .
S6 Re2 Re1 117.60(5) . .
S6 Re2 Re3 57.48(5) . .
S6 Re2 Re5 117.78(5) . .
S6 Re2 Re6 57.32(5) . .
S6 Re2 S1 173.91(7) . .
S6 Re2 S2 89.68(7) . .
C2 Re2 Re1 133.3(2) . .
C2 Re2 Re3 136.2(2) . .
C2 Re2 Re5 135.3(2) . .
C2 Re2 Re6 134.0(2) . .
C2 Re2 S1 92.6(2) . .
C2 Re2 S2 94.6(2) . .
C2 Re2 S5 91.5(2) . .
C2 Re2 S6 93.4(2) . .
Re2 Re3 Re4 89.436(13) . .
Re2 Re3 Re5 59.700(12) . .
Re2 Re3 Re6 59.903(12) . .
Re4 Re3 Re5 59.967(13) . .
Re6 Re3 Re4 59.932(12) . .
Re6 Re3 Re5 90.130(14) . .
S2 Re3 Re2 57.22(5) . .
S2 Re3 Re4 117.04(5) . .
S2 Re3 Re5 57.12(5) . .
S2 Re3 Re6 117.10(5) . .
S2 Re3 S3 89.84(7) . .
S2 Re3 S6 89.40(7) . .
S3 Re3 Re2 116.69(5) . .
S3 Re3 Re4 57.17(5) . .
S3 Re3 Re5 57.05(5) . .
S3 Re3 Re6 117.06(5) . .
S6 Re3 Re2 57.12(5) . .
S6 Re3 Re4 117.00(5) . .
S6 Re3 Re5 116.79(5) . .
S6 Re3 Re6 57.14(5) . .
S6 Re3 S3 172.66(7) . .
S7 Re3 Re2 117.01(5) . .
S7 Re3 Re4 57.23(5) . .
S7 Re3 Re5 117.16(5) . .
S7 Re3 Re6 57.17(5) . .
S7 Re3 S2 172.98(7) . .
S7 Re3 S3 89.73(7) . .
S7 Re3 S6 90.13(7) . .
C3 Re3 Re2 135.3(2) . .
C3 Re3 Re4 135.3(2) . .
C3 Re3 Re5 136.2(2) . .
C3 Re3 Re6 133.7(2) . .
C3 Re3 S2 94.4(2) . .
C3 Re3 S3 94.6(2) . .
C3 Re3 S6 92.7(2) . .
C3 Re3 S7 92.7(2) . .
Re1 Re4 Re3 90.281(13) . .
Re1 Re4 Re5 60.310(12) . .
Re1 Re4 Re6 60.178(12) . .
Re3 Re4 Re5 60.129(12) . .
Re6 Re4 Re3 60.033(12) . .
Re6 Re4 Re5 90.282(14) . .
S3 Re4 Re1 117.46(5) . .
S3 Re4 Re3 57.41(5) . .
S3 Re4 Re5 57.18(5) . .
S3 Re4 Re6 117.41(5) . .
S3 Re4 S4 89.59(7) . .
S3 Re4 S8 173.59(7) . .
S4 Re4 Re1 57.42(5) . .
S4 Re4 Re3 117.36(5) . .
S4 Re4 Re5 57.27(5) . .
S4 Re4 Re6 117.56(5) . .
S7 Re4 Re1 117.34(5) . .
S7 Re4 Re3 57.17(5) . .
S7 Re4 Re5 117.27(5) . .
S7 Re4 Re6 57.19(5) . .
S7 Re4 S3 89.85(7) . .
S7 Re4 S4 173.42(7) . .
S7 Re4 S8 89.53(7) . .
S8 Re4 Re1 57.47(5) . .
S8 Re4 Re3 117.23(5) . .
S8 Re4 Re5 117.74(5) . .
S8 Re4 Re6 57.22(5) . .
S8 Re4 S4 90.30(7) . .
C4 Re4 Re1 135.3(2) . .
C4 Re4 Re3 134.4(2) . .
C4 Re4 Re5 135.3(2) . .
C4 Re4 Re6 134.4(2) . .
C4 Re4 S3 93.2(2) . .
C4 Re4 S4 94.0(2) . .
C4 Re4 S7 92.6(2) . .
C4 Re4 S8 93.2(2) . .
Re2 Re5 Re1 59.683(13) . .
Re2 Re5 Re3 59.971(12) . .
Re2 Re5 Re4 89.556(14) . .
Re3 Re5 Re1 89.792(14) . .
Re4 Re5 Re1 59.689(12) . .
Re4 Re5 Re3 59.904(13) . .
S1 Re5 Re1 57.11(5) . .
S1 Re5 Re2 57.44(5) . .
S1 Re5 Re3 117.37(5) . .
S1 Re5 Re4 116.77(5) . .
S1 Re5 S2 90.13(7) . .
S1 Re5 S3 173.07(7) . .
S1 Re5 S4 89.33(7) . .
S2 Re5 Re1 116.97(5) . .
S2 Re5 Re2 57.33(5) . .
S2 Re5 Re3 57.15(5) . .
S2 Re5 Re4 117.00(5) . .
S2 Re5 S3 90.05(7) . .
S2 Re5 S4 172.95(7) . .
S3 Re5 Re1 116.89(5) . .
S3 Re5 Re2 117.26(5) . .
S3 Re5 Re3 57.35(5) . .
S3 Re5 Re4 57.23(5) . .
S3 Re5 S4 89.64(7) . .
S4 Re5 Re1 57.20(5) . .
S4 Re5 Re2 116.85(5) . .
S4 Re5 Re3 117.17(5) . .
S4 Re5 Re4 57.30(5) . .
C5 Re5 Re1 136.3(2) . .
C5 Re5 Re2 132.5(2) . .
C5 Re5 Re3 133.7(2) . .
C5 Re5 Re4 137.9(2) . .
C5 Re5 S1 92.4(2) . .
C5 Re5 S2 90.8(2) . .
C5 Re5 S3 94.5(2) . .
C5 Re5 S4 96.3(2) . .
Re2 Re6 Re1 59.714(13) . .
Re2 Re6 Re3 59.984(12) . .
Re2 Re6 Re4 89.542(14) . .
Re3 Re6 Re1 90.086(14) . .
Re4 Re6 Re1 59.838(12) . .
Re4 Re6 Re3 60.036(13) . .
S5 Re6 Re1 57.18(5) . .
S5 Re6 Re2 57.07(5) . .
S5 Re6 Re3 117.03(5) . .
S5 Re6 Re4 116.96(5) . .
S6 Re6 Re1 116.92(5) . .
S6 Re6 Re2 57.23(5) . .
S6 Re6 Re3 57.40(5) . .
S6 Re6 Re4 117.37(5) . .
S6 Re6 S5 89.22(7) . .
S7 Re6 Re1 117.08(5) . .
S7 Re6 Re2 117.12(5) . .
S7 Re6 Re3 57.19(5) . .
S7 Re6 Re4 57.27(5) . .
S7 Re6 S5 172.93(7) . .
S7 Re6 S6 90.32(7) . .
S7 Re6 S8 89.64(7) . .
S8 Re6 Re1 57.37(5) . .
S8 Re6 Re2 117.04(5) . .
S8 Re6 Re3 117.33(5) . .
S8 Re6 Re4 57.32(5) . .
S8 Re6 S5 89.99(7) . .
S8 Re6 S6 173.25(7) . .
C6 Re6 Re1 136.2(2) . .
C6 Re6 Re2 134.8(2) . .
C6 Re6 Re3 133.7(2) . .
C6 Re6 Re4 135.6(2) . .
C6 Re6 S5 94.1(2) . .
C6 Re6 S6 92.2(2) . .
C6 Re6 S7 92.9(2) . .
C6 Re6 S8 94.5(2) . .
Re1 S1 Re2 65.14(5) . .
Re5 S1 Re1 65.83(5) . .
Re5 S1 Re2 65.22(5) . .
Re2 S2 Re3 65.48(5) . .
Re2 S2 Re5 65.29(5) . .
Re5 S2 Re3 65.72(5) . .
Re4 S3 Re3 65.42(5) . .
Re5 S3 Re3 65.61(5) . .
Re5 S3 Re4 65.59(5) . .
Re4 S4 Re1 65.18(5) . .
Re5 S4 Re1 65.65(5) . .
Re5 S4 Re4 65.43(5) . .
Re1 S5 Re6 65.59(5) . .
Re2 S5 Re1 65.31(5) . .
Re2 S5 Re6 65.49(5) . .
Re2 S6 Re3 65.40(5) . .
Re2 S6 Re6 65.45(5) . .
Re6 S6 Re3 65.46(5) . .
Re3 S7 Re4 65.60(5) . .
Re6 S7 Re3 65.63(5) . .
Re6 S7 Re4 65.53(5) . .
Re4 S8 Re1 65.24(5) . .
Re6 S8 Re1 65.53(5) . .
Re6 S8 Re4 65.46(5) . .
N1 C1 Re1 173.5(7) . .
C1 N1 Eu1 156.6(7) . .
N2 C2 Re2 176.9(8) . .
C2 N2 Eu2 172.3(7) . 1_565
N3 C3 Re3 179.1(8) . .
C3 N3 Eu4 163.0(7) . 4_585
N4 C4 Re4 176.9(8) . .
C4 N4 Eu2 155.7(7) . 4_575
N5 C5 Re5 176.0(8) . .
C5 N5 Eu3 170.2(7) . 3_676
N6 C6 Re6 178.4(8) . .
C6 N6 Eu1 166.6(7) . 2_556
N1 Eu1 N6 137.5(3) . 2_546
N1 Eu1 Eu2 124.89(17) . .
N1 Eu1 Eu3 68.88(17) . .
N1 Eu1 Eu4 108.57(18) . .
N1 Eu1 O1M 71.7(3) . .
N1 Eu1 O1A 130.9(3) . 2_546
N1 Eu1 N1A 69.3(2) . .
N6 Eu1 Eu2 96.36(18) 2_546 .
N6 Eu1 Eu3 152.62(18) 2_546 .
N6 Eu1 Eu4 99.50(19) 2_546 .
N6 Eu1 O1M 101.4(3) 2_546 .
N6 Eu1 O1A 67.5(3) 2_546 2_546
N6 Eu1 N1A 69.2(3) 2_546 .
Eu2 Eu1 Eu3 60.798(11) . .
Eu2 Eu1 Eu4 61.149(12) . .
Eu3 Eu1 Eu4 57.414(11) . .
O1 Eu1 N1 85.1(2) . .
O1 Eu1 N6 133.5(2) . 2_546
O1 Eu1 Eu2 40.10(13) . .
O1 Eu1 Eu3 33.73(14) . .
O1 Eu1 Eu4 75.42(13) . .
O1 Eu1 O2 74.45(19) . .
O1 Eu1 O3 66.7(2) . .
O1 Eu1 O1M 71.0(3) . .
O1 Eu1 O1A 69.4(2) . 2_546
O1 Eu1 N1A 137.2(2) . .
O2 Eu1 N1 141.8(2) . .
O2 Eu1 N6 76.1(2) . 2_546
O2 Eu1 Eu2 40.09(14) . .
O2 Eu1 Eu3 76.55(14) . .
O2 Eu1 Eu4 35.45(14) . .
O2 Eu1 O3 68.9(2) . .
O2 Eu1 O1M 127.8(3) . .
O2 Eu1 O1A 71.2(3) . 2_546
O2 Eu1 N1A 144.4(2) . .
O3 Eu1 N1 73.4(2) . .
O3 Eu1 N6 131.6(2) . 2_546
O3 Eu1 Eu2 77.80(14) . .
O3 Eu1 Eu3 34.87(14) . .
O3 Eu1 Eu4 35.62(14) . .
O3 Eu1 O1M 126.4(3) . .
O3 Eu1 O1A 126.5(3) . 2_546
O3 Eu1 N1A 131.2(2) . .
O1M Eu1 Eu2 90.3(2) . .
O1M Eu1 Eu3 94.1(3) . .
O1M Eu1 Eu4 146.3(2) . .
O1M Eu1 N1A 68.7(3) . .
O1A Eu1 Eu2 48.8(2) 2_546 .
O1A Eu1 Eu3 101.9(2) 2_546 .
O1A Eu1 Eu4 104.6(2) 2_546 .
O1A Eu1 O1M 60.7(3) 2_546 .
O1A Eu1 N1A 101.8(3) 2_546 .
N1A Eu1 Eu2 150.5(2) . .
N1A Eu1 Eu3 137.99(18) . .
N1A Eu1 Eu4 144.4(2) . .
O1B Eu1 N1 89.5(3) . .
O1B Eu1 N6 71.8(3) . 2_546
O1B Eu1 Eu2 125.21(17) . .
O1B Eu1 Eu3 107.70(17) . .
O1B Eu1 Eu4 68.32(16) . .
O1B Eu1 O1 139.4(2) . .
O1B Eu1 O2 85.9(2) . .
O1B Eu1 O3 73.2(2) . .
O1B Eu1 O1M 144.0(3) . .
O1B Eu1 O1A 136.8(3) . 2_546
O1B Eu1 N1A 76.1(3) . .
N2 Eu2 N4 141.6(3) 1_545 4_676
N2 Eu2 Eu1 92.39(18) 1_545 .
N2 Eu2 O2M 71.9(3) 1_545 .
N2 Eu2 O1A 66.8(2) 1_545 2_546
N2 Eu2 O2A 81.7(3) 1_545 2_546
N2 Eu2 C1A 69.7(3) 1_545 2_546
N2 Eu2 C1C 70.6(3) 1_545 .
N4 Eu2 Eu1 123.08(18) 4_676 .
N4 Eu2 O2M 70.4(3) 4_676 .
N4 Eu2 O1A 127.8(3) 4_676 2_546
N4 Eu2 O2A 87.1(3) 4_676 2_546
N4 Eu2 C1A 109.8(3) 4_676 2_546
N4 Eu2 C1C 101.8(3) 4_676 .
O1 Eu2 N2 71.2(2) . 1_545
O1 Eu2 N4 145.8(2) . 4_676
O1 Eu2 Eu1 39.42(14) . .
O1 Eu2 O2M 143.1(3) . .
O1 Eu2 O1A 65.3(3) . 2_546
O1 Eu2 O2A 113.2(3) . 2_546
O1 Eu2 C1A 88.8(3) . 2_546
O1 Eu2 C1C 77.5(3) . .
O2 Eu2 N2 130.6(2) . 1_545
O2 Eu2 N4 83.1(2) . 4_676
O2 Eu2 Eu1 40.02(13) . .
O2 Eu2 O1 73.8(2) . .
O2 Eu2 O2M 134.6(3) . .
O2 Eu2 O1A 67.4(2) . 2_546
O2 Eu2 O2A 81.3(3) . 2_546
O2 Eu2 C1A 75.9(3) . 2_546
O2 Eu2 C1C 132.6(3) . .
O4 Eu2 N2 126.2(2) . 1_545
O4 Eu2 N4 78.7(2) . 4_676
O4 Eu2 Eu1 79.80(14) . .
O4 Eu2 O1 69.76(19) . .
O4 Eu2 O2 69.00(19) . .
O4 Eu2 O2M 135.5(3) . .
O4 Eu2 O1A 123.7(2) . 2_546
O4 Eu2 O2A 148.2(3) . 2_546
O4 Eu2 C1A 142.6(3) . 2_546
O4 Eu2 C1C 66.0(3) . .
O2M Eu2 Eu1 144.2(3) . .
O2M Eu2 O1A 100.6(3) . 2_546
O2M Eu2 C1A 79.4(4) . 2_546
O2M Eu2 C1C 89.6(4) . .
O1A Eu2 Eu1 44.0(2) 2_546 .
O1A Eu2 C1A 23.8(3) 2_546 2_546
O1A Eu2 C1C 130.1(3) 2_546 .
O2A Eu2 Eu1 84.7(3) 2_546 .
O2A Eu2 O2M 61.7(4) 2_546 .
O2A Eu2 O1A 47.9(3) 2_546 2_546
O2A Eu2 C1A 24.5(4) 2_546 2_546
O2A Eu2 C1C 145.5(3) 2_546 .
C1A Eu2 Eu1 64.9(3) 2_546 .
C1A Eu2 C1C 140.3(3) 2_546 .
O1C Eu2 N2 73.2(3) . 1_545
O1C Eu2 N4 89.2(3) . 4_676
O1C Eu2 Eu1 133.6(2) . .
O1C Eu2 O1 94.8(3) . .
O1C Eu2 O2 143.8(2) . .
O1C Eu2 O4 74.8(2) . .
O1C Eu2 O2M 73.6(4) . .
O1C Eu2 O1A 139.2(3) . 2_546
O1C Eu2 O2A 133.7(3) . 2_546
O1C Eu2 C1A 139.3(3) . 2_546
O1C Eu2 C1C 17.6(3) . .
C1C Eu2 Eu1 116.0(2) . .
N5 Eu3 Eu1 158.85(19) 3_676 .
N5 Eu3 Eu2 138.76(19) 3_676 .
N5 Eu3 Eu4 134.59(19) 3_676 .
Eu2 Eu3 Eu1 56.532(11) . .
Eu4 Eu3 Eu1 61.795(11) . .
Eu4 Eu3 Eu2 61.294(12) . .
O1 Eu3 N5 143.8(2) . 3_676
O1 Eu3 Eu1 34.19(15) . .
O1 Eu3 Eu2 36.53(14) . .
O1 Eu3 Eu4 79.44(14) . .
O1 Eu3 O3 68.6(2) . .
O1 Eu3 O4 69.72(19) . .
O1 Eu3 O3M 75.1(3) . .
O1 Eu3 O4M 120.9(2) . .
O1 Eu3 O2C 81.6(3) . .
O3 Eu3 N5 143.9(3) . 3_676
O3 Eu3 Eu1 36.41(15) . .
O3 Eu3 Eu2 75.15(15) . .
O3 Eu3 Eu4 38.44(15) . .
O3 Eu3 O4 69.8(2) . .
O3 Eu3 O3M 112.2(3) . .
O3 Eu3 O4M 74.2(2) . .
O3 Eu3 O2C 140.0(2) . .
O4 Eu3 N5 127.0(2) . 3_676
O4 Eu3 Eu1 74.14(13) . .
O4 Eu3 Eu2 36.04(14) . .
O4 Eu3 Eu4 36.86(14) . .
O4 Eu3 O4M 134.4(2) . .
O3M Eu3 N5 75.7(3) . 3_676
O3M Eu3 Eu1 86.2(2) . .
O3M Eu3 Eu2 105.2(2) . .
O3M Eu3 Eu4 147.8(2) . .
O3M Eu3 O4 141.0(3) . .
O3M Eu3 O4M 78.7(3) . .
O4M Eu3 N5 73.1(3) . 3_676
O4M Eu3 Eu1 92.87(18) . .
O4M Eu3 Eu2 148.14(17) . .
O4M Eu3 Eu4 98.29(19) . .
O2C Eu3 N5 74.2(3) . 3_676
O2C Eu3 Eu1 115.1(2) . .
O2C Eu3 Eu2 65.2(2) . .
O2C Eu3 Eu4 112.02(19) . .
O2C Eu3 O4 75.4(2) . .
O2C Eu3 O3M 83.5(3) . .
O2C Eu3 O4M 145.7(3) . .
O1D Eu3 N5 72.2(3) . 3_676
O1D Eu3 Eu1 121.13(18) . .
O1D Eu3 Eu2 108.77(18) . .
O1D Eu3 Eu4 62.41(18) . .
O1D Eu3 O1 140.2(2) . .
O1D Eu3 O3 86.4(2) . .
O1D Eu3 O4 72.9(2) . .
O1D Eu3 O3M 144.6(3) . .
O1D Eu3 O4M 77.8(3) . .
O1D Eu3 O2C 101.7(3) . .
N3 Eu4 Eu3 139.26(17) 4_686 .
N3 Eu4 C1D 84.0(2) 4_686 .
O2 Eu4 N3 139.5(2) . 4_686
O2 Eu4 Eu3 79.05(13) . .
O2 Eu4 O5M 116.3(3) . .
O2 Eu4 O2D' 138.2(8) . .
O2 Eu4 C1D 134.94(19) . .
O3 Eu4 N3 129.6(2) . 4_686
O3 Eu4 Eu3 37.31(14) . .
O3 Eu4 O2 68.9(2) . .
O3 Eu4 O5M 140.2(3) . .
O3 Eu4 O5M' 127.0(6) . .
O3 Eu4 O2D 78.8(3) . .
O3 Eu4 O2D' 69.5(8) . .
O3 Eu4 C1D 72.9(2) . .
O4 Eu4 N3 146.3(2) . 4_686
O4 Eu4 Eu3 38.41(14) . .
O4 Eu4 O2 68.8(2) . .
O4 Eu4 O3 70.2(2) . .
O4 Eu4 O5M 75.5(3) . .
O4 Eu4 O5M' 75.7(6) . .
O4 Eu4 O6M 106.8(2) . .
O4 Eu4 O2D 96.4(3) . .
O4 Eu4 O2D' 94.4(5) . .
O4 Eu4 C1D 76.61(19) . .
O5M Eu4 N3 74.2(3) . 4_686
O5M Eu4 Eu3 103.0(3) . .
O5M Eu4 C1D 80.2(4) . .
O5M' Eu4 Eu3 92.8(6) . .
O5M' Eu4 O2 131.9(6) . .
O5M' Eu4 O2D' 74.2(9) . .
O5M' Eu4 C1D 60.5(7) . .
O6M Eu4 N3 74.4(3) . 4_686
O6M Eu4 Eu3 143.28(18) . .
O6M Eu4 O2 74.9(2) . .
O6M Eu4 O3 142.1(2) . .
O6M Eu4 O5M 67.3(4) . .
O6M Eu4 O5M' 85.9(7) . .
O6M Eu4 O2D 137.8(3) . .
O6M Eu4 O2D' 146.3(8) . .
O6M Eu4 C1D 144.7(3) . .
O2B Eu4 N3 70.9(2) . 4_686
O2B Eu4 Eu3 113.57(19) . .
O2B Eu4 O2 82.5(2) . .
O2B Eu4 O3 76.5(2) . .
O2B Eu4 O4 141.9(2) . .
O2B Eu4 O5M 141.7(3) . .
O2B Eu4 O5M' 141.4(6) . .
O2B Eu4 O6M 88.3(3) . .
O2B Eu4 O2D 94.7(4) . .
O2B Eu4 O2D' 90.7(4) . .
O2B Eu4 C1D 110.9(3) . .
O2D Eu4 N3 67.0(3) . 4_686
O2D Eu4 Eu3 72.2(2) . .
O2D Eu4 O2 147.3(3) . .
O2D Eu4 O5M 85.8(4) . .
O2D Eu4 C1D 19.8(2) . .
O2D' Eu4 Eu3 66.1(7) . .
O2D' Eu4 C1D 20.4(3) . .
C1D Eu4 Eu3 56.00(13) . .
Eu1 O1 Eu2 100.5(2) . .
Eu1 O1 H1 111.9 . .
Eu2 O1 H1 111.9 . .
Eu3 O1 Eu1 112.1(2) . .
Eu3 O1 Eu2 108.0(2) . .
Eu3 O1 H1 111.9 . .
Eu1 O2 Eu2 99.9(2) . .
Eu1 O2 Eu4 109.7(2) . .
Eu1 O2 H2 113.1 . .
Eu2 O2 Eu4 106.9(2) . .
Eu2 O2 H2 113.1 . .
Eu4 O2 H2 113.1 . .
Eu1 O3 H3 111.8 . .
Eu3 O3 Eu1 108.7(2) . .
Eu3 O3 Eu4 104.2(2) . .
Eu3 O3 H3 111.8 . .
Eu4 O3 Eu1 108.3(2) . .
Eu4 O3 H3 111.8 . .
Eu2 O4 Eu3 106.8(2) . .
Eu2 O4 H4 111.2 . .
Eu3 O4 H4 111.2 . .
Eu4 O4 Eu2 111.3(2) . .
Eu4 O4 Eu3 104.7(2) . .
Eu4 O4 H4 111.2 . .
Eu1 O1A Eu2 87.3(3) 2_556 2_556
C1A O1A Eu1 146.2(8) . 2_556
C1A O1A Eu2 85.1(9) . 2_556
C1A O2A Eu2 96.9(9) . 2_556
O1A C1A Eu2 71.1(8) . 2_556
O1A C1A O2A 127.9(14) . .
O1A C1A C2A 114.2(13) . .
O2A C1A Eu2 58.6(8) . 2_556
O2A C1A C2A 117.9(13) . .
C2A C1A Eu2 162.5(8) . 2_556
C3A C2A C1A 120.7(12) . .
C5A C2A C1A 120.8(13) . .
C5A C2A C3A 118.5(12) . .
C2A C3A H3A 120.0 . .
C2A C3A C4A 120.1(12) . .
C4A C3A H3A 120.0 . .
C3A C4A H4A 118.3 . .
N1A C4A C3A 123.3(12) . .
N1A C4A H4A 118.3 . .
C2A C5A H5A 120.9 . .
C2A C5A C6A 118.1(13) . .
C6A C5A H5A 120.9 . .
C5A C6A H6A 118.3 . .
N1A C6A C5A 123.5(12) . .
N1A C6A H6A 118.3 . .
C4A N1A Eu1 117.8(8) . .
C4A N1A C6A 116.2(10) . .
C6A N1A Eu1 125.8(7) . .
C1B O1B Eu1 134.7(7) . .
C1B O2B Eu4 138.2(7) . .
O1B C1B C2B 117.0(9) . .
O2B C1B O1B 126.6(9) . .
O2B C1B C2B 116.3(9) . .
C3B C2B C1B 121.0(9) . .
C5B C2B C1B 120.2(10) . .
C5B C2B C3B 118.8(10) . .
C2B C3B H3B 120.9 . .
C2B C3B C4B 118.2(10) . .
C4B C3B H3B 120.9 . .
C3B C4B H4B 118.4 . .
N1B C4B C3B 123.3(11) . .
N1B C4B H4B 118.4 . .
C2B C5B H5B 120.2 . .
C6B C5B C2B 119.7(12) . .
C6B C5B H5B 120.2 . .
C5B C6B H6B 118.6 . .
N1B C6B C5B 122.8(12) . .
N1B C6B H6B 118.6 . .
C4B N1B C6B 117.2(10) . .
C1C O1C Eu2 127.6(8) . .
C1C O2C Eu3 139.7(7) . .
O1C C1C Eu2 34.7(5) . .
O1C C1C O2C 128.2(11) . .
O1C C1C C2C 114.8(11) . .
O1C C1C C2C' 113.2(16) . .
O2C C1C Eu2 94.1(7) . .
O2C C1C C2C 115.9(11) . .
O2C C1C C2C' 117.9(15) . .
C2C C1C Eu2 149.6(8) . .
C2C' C1C Eu2 143.7(15) . .
C3C C2C C1C 118.1(12) . .
C5C C2C C1C 121.9(12) . .
C5C C2C C3C 120.0(15) . .
C2C C3C H3C 121.3 . .
C4C C3C C2C 117.3(15) . .
C4C C3C H3C 121.3 . .
C3C C4C H4C 118.1 . .
N1C C4C C3C 123.9(16) . .
N1C C4C H4C 118.1 . .
C2C C5C H5C 121.0 . .
C6C C5C C2C 118.0(16) . .
C6C C5C H5C 121.0 . .
C5C C6C H6C 118.4 . .
N1C C6C C5C 123.2(16) . .
N1C C6C H6C 118.4 . .
C6C N1C C4C 117.5(16) . .
C3C' C2C' C1C 126(3) . .
C3C' C2C' C5C' 119(3) . .
C5C' C2C' C1C 115(2) . .
C2C' C3C' H3C' 118.3 . .
C4C' C3C' C2C' 123(3) . .
C4C' C3C' H3C' 118.3 . .
C3C' C4C' H4C' 120.8 . .
N1C' C4C' C3C' 118(4) . .
N1C' C4C' H4C' 120.8 . .
C2C' C5C' H5C' 123.2 . .
C6C' C5C' C2C' 114(3) . .
C6C' C5C' H5C' 123.2 . .
C5C' C6C' H6C' 115.7 . .
N1C' C6C' C5C' 129(4) . .
N1C' C6C' H6C' 115.7 . .
C4C' N1C' C6C' 117(4) . .
C1D O1D Eu3 133.7(6) . .
C1D O2D Eu4 119.1(8) . .
C1D O2D' Eu4 116.6(12) . .
O1D C1D Eu4 87.1(6) . .
O1D C1D O2D' 119.2(15) . .
O1D C1D C2D 116.0(7) . .
O2D C1D Eu4 41.1(6) . .
O2D C1D O1D 127.1(10) . .
O2D C1D C2D 116.7(8) . .
O2D' C1D Eu4 43.0(9) . .
O2D' C1D C2D 122.6(12) . .
C2D C1D Eu4 153.3(5) . .
C3D C2D C1D 120.0(8) . .
C5D C2D C1D 121.0(8) . .
C5D C2D C3D 118.9(9) . .
C2D C3D H3D 120.3 . .
C4D C3D C2D 119.5(9) . .
C4D C3D H3D 120.3 . .
C3D C4D H4D 118.8 . .
N1D C4D C3D 122.5(10) . .
N1D C4D H4D 118.8 . .
C2D C5D H5D 120.7 . .
C2D C5D C6D 118.6(10) . .
C6D C5D H5D 120.7 . .
C5D C6D H6D 118.2 . .
N1D C6D C5D 123.7(11) . .
N1D C6D H6D 118.2 . .
C6D N1D C4D 116.8(10) . .
O14W O13W O15W 97(4) 1_565 1_565
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 Re2 2.5892(5) .
Re1 Re4 2.5955(4) .
Re1 Re5 2.6117(4) .
Re1 Re6 2.6044(5) .
Re1 S1 2.404(2) .
Re1 S4 2.4097(19) .
Re1 S5 2.403(2) .
Re1 S8 2.410(2) .
Re1 C1 2.114(9) .
Re2 Re3 2.5986(4) .
Re2 Re5 2.5914(4) .
Re2 Re6 2.5964(5) .
Re2 S1 2.406(2) .
Re2 S2 2.401(2) .
Re2 S5 2.395(2) .
Re2 S6 2.400(2) .
Re2 C2 2.084(9) .
Re3 Re4 2.6020(5) .
Re3 Re5 2.6079(5) .
Re3 Re6 2.6019(4) .
Re3 S2 2.403(2) .
Re3 S3 2.411(2) .
Re3 S6 2.410(2) .
Re3 S7 2.401(2) .
Re3 C3 2.128(9) .
Re4 Re5 2.6037(5) .
Re4 Re6 2.5993(4) .
Re4 S3 2.404(2) .
Re4 S4 2.409(2) .
Re4 S7 2.402(2) .
Re4 S8 2.4051(19) .
Re4 C4 2.114(8) .
Re5 S1 2.4026(19) .
Re5 S2 2.403(2) .
Re5 S3 2.403(2) .
Re5 S4 2.408(2) .
Re5 C5 2.141(9) .
Re6 S5 2.405(2) .
Re6 S6 2.403(2) .
Re6 S7 2.4002(19) .
Re6 S8 2.403(2) .
Re6 C6 2.124(9) .
C1 N1 1.158(11) .
N1 Eu1 2.521(7) .
C2 N2 1.159(12) .
N2 Eu2 2.493(7) 1_565
C3 N3 1.143(12) .
N3 Eu4 2.650(7) 4_585
C4 N4 1.144(11) .
N4 Eu2 2.504(7) 4_575
C5 N5 1.135(12) .
N5 Eu3 2.599(8) 3_676
C6 N6 1.162(12) .
N6 Eu1 2.560(8) 2_556
Eu1 Eu2 3.6850(6) .
Eu1 Eu3 3.9243(6) .
Eu1 Eu4 3.9622(6) .
Eu1 O1 2.380(6) .
Eu1 O2 2.406(6) .
Eu1 O3 2.460(6) .
Eu1 O1M 2.583(11) .
Eu1 O1A 2.560(10) 2_546
Eu1 N1A 2.692(8) .
Eu1 O1B 2.377(7) .
Eu2 O1 2.414(6) .
Eu2 O2 2.409(6) .
Eu2 O4 2.370(6) .
Eu2 O2M 2.525(10) .
Eu2 O1A 2.775(11) 2_546
Eu2 O2A 2.513(10) 2_546
Eu2 C1A 2.923(14) 2_546
Eu2 O1C 2.350(7) .
Eu2 C1C 3.265(12) .
Eu3 Eu4 3.7883(6) .
Eu3 O1 2.351(6) .
Eu3 O3 2.369(6) .
Eu3 O4 2.433(6) .
Eu3 O3M 2.433(8) .
Eu3 O4M 2.467(8) .
Eu3 O2C 2.392(7) .
Eu3 O1D 2.336(6) .
Eu4 O2 2.441(6) .
Eu4 O3 2.430(6) .
Eu4 O4 2.350(6) .
Eu4 O5M 2.474(10) .
Eu4 O5M' 2.436(16) .
Eu4 O6M 2.413(8) .
Eu4 O2B 2.348(7) .
Eu4 O2D 2.430(10) .
Eu4 O2D' 2.464(17) .
Eu4 C1D 3.232(9) .
O1 H1 1.0000 .
O2 H2 1.0000 .
O3 H3 1.0000 .
O4 H4 1.0000 .
O1A C1A 1.184(17) .
O2A C1A 1.222(18) .
C1A C2A 1.565(18) .
C2A C3A 1.368(19) .
C2A C5A 1.359(19) .
C3A H3A 0.9500 .
C3A C4A 1.402(15) .
C4A H4A 0.9500 .
C4A N1A 1.317(15) .
C5A H5A 0.9500 .
C5A C6A 1.426(17) .
C6A H6A 0.9500 .
C6A N1A 1.351(17) .
O1B C1B 1.246(12) .
O2B C1B 1.242(12) .
C1B C2B 1.497(13) .
C2B C3B 1.385(15) .
C2B C5B 1.372(16) .
C3B H3B 0.9500 .
C3B C4B 1.388(15) .
C4B H4B 0.9500 .
C4B N1B 1.337(15) .
C5B H5B 0.9500 .
C5B C6B 1.367(17) .
C6B H6B 0.9500 .
C6B N1B 1.350(17) .
O1C C1C 1.247(14) .
O2C C1C 1.260(15) .
C1C C2C 1.522(18) .
C1C C2C' 1.523(19) .
C2C C3C 1.405(14) .
C2C C5C 1.403(14) .
C3C H3C 0.9500 .
C3C C4C 1.376(17) .
C4C H4C 0.9500 .
C4C N1C 1.357(15) .
C5C H5C 0.9500 .
C5C C6C 1.378(17) .
C6C H6C 0.9500 .
C6C N1C 1.356(15) .
C2C' C3C' 1.403(16) .
C2C' C5C' 1.403(16) .
C3C' H3C' 0.9500 .
C3C' C4C' 1.376(18) .
C4C' H4C' 0.9500 .
C4C' N1C' 1.357(17) .
C5C' H5C' 0.9500 .
C5C' C6C' 1.377(18) .
C6C' H6C' 0.9500 .
C6C' N1C' 1.357(17) .
O1D C1D 1.257(8) .
O2D C1D 1.254(9) .
O2D' C1D 1.261(10) .
C1D C2D 1.503(12) .
C2D C3D 1.387(12) .
C2D C5D 1.361(14) .
C3D H3D 0.9500 .
C3D C4D 1.365(14) .
C4D H4D 0.9500 .
C4D N1D 1.350(14) .
C5D H5D 0.9500 .
C5D C6D 1.374(17) .
C6D H6D 0.9500 .
C6D N1D 1.347(15) .
O13W O14W 1.06(5) 1_565
O13W O15W 1.36(5) 1_565
