#------------------------------------------------------------------------------
#$Date: 2016-03-24 02:15:46 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179565 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/34/4503440.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4503440
loop_
_publ_author_name
'Qi, Yan'
'Che, Yunxia'
'Luo, Feng'
'Batten, Stuart R.'
'Liu, Yang'
'Zheng, Jimin'
_publ_section_title
;
 A Variety of 1D to 3D Metal−Organic Coordination Architectures
 Assembled with
 1,1′-(2,2′-Oxybis(ethane-2,1-diyl))bis(1H-imidazole)
;
_journal_issue                   5
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              1654
_journal_paper_doi               10.1021/cg7011217
_journal_volume                  8
_journal_year                    2008
_chemical_formula_sum            'C19 H18 Co2 N4 O8'
_chemical_formula_weight         548.23
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.27(3)
_cell_angle_beta                 95.99(3)
_cell_angle_gamma                117.55(3)
_cell_formula_units_Z            2
_cell_length_a                   10.650(2)
_cell_length_b                   10.969(2)
_cell_length_c                   11.246(2)
_cell_measurement_reflns_used    7289
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.52
_cell_measurement_theta_min      3.26
_cell_volume                     1024.9(7)
_computing_cell_refinement       'RAXIS-RAPID Auto(Rigaku, 2004)'
_computing_data_collection       'RAXIS-RAPID Auto(Rigaku, 2004)'
_computing_data_reduction        'CrystalStructure(Rigaku/MSC, 2004)'
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 2001)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'rigaku r-axis rapid IP area detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0593
_diffrn_reflns_av_sigmaI/netI    0.0807
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            10197
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.27
_diffrn_source                   'rotating anode'
_exptl_absorpt_coefficient_mu    1.676
_exptl_absorpt_correction_T_max  0.9091
_exptl_absorpt_correction_T_min  0.7468
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.777
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             556
_exptl_crystal_size_max          0.19
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.06
_refine_diff_density_max         0.587
_refine_diff_density_min         -0.632
_refine_diff_density_rms         0.106
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     302
_refine_ls_number_reflns         4655
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.021
_refine_ls_R_factor_all          0.0740
_refine_ls_R_factor_gt           0.0456
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0294P)²+1.0713P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0905
_refine_ls_wR_factor_ref         0.1010
_reflns_number_gt                3372
_reflns_number_total             4655
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg7011217-file005.cif
_cod_data_source_block           shelxl
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_hydrogen_treatment' value 'refu' changed to
'refU' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        1024.8(4)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4503440
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.6627(4) 0.7169(4) 0.4583(4) 0.0164(7) Uani 1 1 d .
C2 C 0.7502(4) 0.6400(4) 0.4404(3) 0.0152(7) Uani 1 1 d .
C3 C 0.6772(4) 0.4861(4) 0.4178(4) 0.0192(7) Uani 1 1 d .
H3 H 0.5811 0.4384 0.4231 0.023 Uiso 1 1 calc R
C4 C 0.7464(4) 0.4036(4) 0.3877(4) 0.0172(7) Uani 1 1 d .
C5 C 0.8874(3) 0.4731(4) 0.3731(3) 0.0154(7) Uani 1 1 d .
H5 H 0.9318 0.4164 0.3472 0.019 Uiso 1 1 calc R
C6 C 0.9618(3) 0.6271(4) 0.3973(3) 0.0150(7) Uani 1 1 d .
C7 C 0.8954(4) 0.7117(4) 0.4353(3) 0.0157(7) Uani 1 1 d .
H7 H 0.9480 0.8165 0.4575 0.019 Uiso 1 1 calc R
C8 C 0.6663(4) 0.2401(4) 0.3715(4) 0.0170(7) Uani 1 1 d .
C9 C 1.1153(4) 0.7017(4) 0.3814(3) 0.0163(7) Uani 1 1 d .
C10 C 0.8409(4) 1.0982(5) 0.8639(4) 0.0330(10) Uani 1 1 d .
H10 H 0.9110 1.0936 0.8228 0.040 Uiso 1 1 calc R
C11 C 0.6435(5) 1.0861(5) 0.8978(4) 0.0355(10) Uani 1 1 d .
H11 H 0.5487 1.0710 0.8835 0.043 Uiso 1 1 calc R
C12 C 0.7364(5) 1.1323(5) 1.0179(4) 0.0359(10) Uani 1 1 d .
H12 H 0.7182 1.1547 1.0999 0.043 Uiso 1 1 calc R
C13 C 0.9986(4) 1.1913(5) 1.0950(4) 0.0348(10) Uani 1 1 d .
H13A H 1.0597 1.3040 1.1407 0.042 Uiso 1 1 calc R
H13B H 1.0554 1.1545 1.0484 0.042 Uiso 1 1 calc R
C14 C 0.0304(4) -0.1349(5) -0.1997(4) 0.0313(9) Uani 1 1 d .
H14A H 0.0768 -0.1807 -0.2543 0.038 Uiso 1 1 calc R
H14B H -0.0636 -0.1663 -0.2590 0.038 Uiso 1 1 calc R
C15 C 0.1770(5) 0.0890(5) -0.2244(4) 0.0322(9) Uani 1 1 d .
H15A H 0.1004 0.0954 -0.2716 0.039 Uiso 1 1 calc R
H15B H 0.1969 0.0205 -0.2908 0.039 Uiso 1 1 calc R
C16 C 0.3176(5) 0.2476(5) -0.1441(5) 0.0396(11) Uani 1 1 d .
H16A H 0.3909 0.2396 -0.0941 0.048 Uiso 1 1 calc R
H16B H 0.3587 0.2842 -0.2060 0.048 Uiso 1 1 calc R
C17 C 0.3515(4) 0.4332(4) 0.0861(4) 0.0256(8) Uani 1 1 d .
H17 H 0.4102 0.4135 0.1339 0.031 Uiso 1 1 calc R
C18 C 0.2268(6) 0.5247(6) 0.0391(5) 0.0446(12) Uani 1 1 d .
H18 H 0.1821 0.5816 0.0481 0.054 Uiso 1 1 calc R
C19 C 0.2146(7) 0.4199(7) -0.0804(5) 0.0578(15) Uani 1 1 d .
H19 H 0.1619 0.3927 -0.1666 0.069 Uiso 1 1 calc R
Co1 Co 0.37490(5) 0.67809(5) 0.34729(5) 0.01656(13) Uani 1 1 d .
Co2 Co 0.62141(5) 0.99046(5) 0.59170(5) 0.01493(12) Uani 1 1 d .
H7A H 0.550(5) 0.926(5) 0.337(4) 0.055(16) Uiso 1 1 d D
N1 N 0.7092(3) 1.0645(4) 0.7995(3) 0.0261(7) Uani 1 1 d .
N2 N 0.8616(4) 1.1395(4) 0.9950(3) 0.0293(8) Uani 1 1 d .
N3 N 0.2948(4) 0.3628(4) -0.0486(3) 0.0328(8) Uani 1 1 d .
N4 N 0.3139(3) 0.5340(4) 0.1432(3) 0.0242(7) Uani 1 1 d .
O1 O 0.5267(3) 0.6254(3) 0.3824(3) 0.0242(6) Uani 1 1 d .
O2 O 0.7253(3) 0.8572(3) 0.5373(3) 0.0250(6) Uani 1 1 d .
O3 O 0.5693(2) 0.2111(3) 0.4330(2) 0.0187(5) Uani 1 1 d .
O4 O 0.6961(3) 0.1467(3) 0.3036(3) 0.0266(6) Uani 1 1 d .
O5 O 1.1631(3) 0.6131(3) 0.3362(3) 0.0233(6) Uani 1 1 d .
O6 O 1.1799(3) 0.8412(3) 0.4109(3) 0.0257(6) Uani 1 1 d .
O7 O 0.4974(3) 0.8974(3) 0.3843(3) 0.0179(5) Uani 1 1 d D
O8 O 0.1269(3) 0.0300(3) -0.1334(3) 0.0336(7) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O2 C1 O1 126.4(3) . .
O2 C1 C2 120.5(3) . .
O1 C1 C2 113.0(3) . .
C7 C2 C3 119.3(3) . .
C7 C2 C1 122.7(3) . .
C3 C2 C1 117.8(3) . .
C4 C3 C2 120.7(3) . .
C4 C3 H3 119.6 . .
C2 C3 H3 119.6 . .
C3 C4 C5 119.3(3) . .
C3 C4 C8 118.9(3) . .
C5 C4 C8 121.8(3) . .
C6 C5 C4 120.2(3) . .
C6 C5 H5 119.9 . .
C4 C5 H5 119.9 . .
C7 C6 C5 120.0(3) . .
C7 C6 C9 120.2(3) . .
C5 C6 C9 119.8(3) . .
C6 C7 C2 120.2(3) . .
C6 C7 H7 119.9 . .
C2 C7 H7 119.9 . .
O4 C8 O3 125.1(3) . .
O4 C8 C4 120.2(3) . .
O3 C8 C4 114.7(3) . .
O6 C9 O5 126.5(3) . .
O6 C9 C6 117.1(3) . .
O5 C9 C6 116.3(3) . .
N1 C10 N2 112.2(3) . .
N1 C10 H10 123.9 . .
N2 C10 H10 123.9 . .
C12 C11 N1 110.2(4) . .
C12 C11 H11 124.9 . .
N1 C11 H11 124.9 . .
C11 C12 N2 106.2(4) . .
C11 C12 H12 126.9 . .
N2 C12 H12 126.9 . .
N2 C13 C14 113.6(3) . 2_666
N2 C13 H13A 108.8 . .
C14 C13 H13A 108.8 2_666 .
N2 C13 H13B 108.8 . .
C14 C13 H13B 108.8 2_666 .
H13A C13 H13B 107.7 . .
O8 C14 C13 109.3(3) . 2_666
O8 C14 H14A 109.8 . .
C13 C14 H14A 109.8 2_666 .
O8 C14 H14B 109.8 . .
C13 C14 H14B 109.8 2_666 .
H14A C14 H14B 108.3 . .
O8 C15 C16 108.2(4) . .
O8 C15 H15A 110.1 . .
C16 C15 H15A 110.1 . .
O8 C15 H15B 110.1 . .
C16 C15 H15B 110.1 . .
H15A C15 H15B 108.4 . .
N3 C16 C15 113.7(3) . .
N3 C16 H16A 108.8 . .
C15 C16 H16A 108.8 . .
N3 C16 H16B 108.8 . .
C15 C16 H16B 108.8 . .
H16A C16 H16B 107.7 . .
N4 C17 N3 111.7(4) . .
N4 C17 H17 124.1 . .
N3 C17 H17 124.1 . .
N4 C18 C19 109.9(4) . .
N4 C18 H18 125.0 . .
C19 C18 H18 125.0 . .
N3 C19 C18 106.1(4) . .
N3 C19 H19 126.9 . .
C18 C19 H19 126.9 . .
O7 Co1 O1 103.84(11) . .
O7 Co1 O5 111.29(11) . 1_455
O1 Co1 O5 142.29(11) . 1_455
O7 Co1 N4 109.16(12) . .
O1 Co1 N4 88.26(12) . .
O5 Co1 N4 92.75(12) 1_455 .
O7 Co1 O3 81.61(10) . 2_666
O1 Co1 O3 84.95(10) . 2_666
O5 Co1 O3 86.96(11) 1_455 2_666
N4 Co1 O3 168.43(11) . 2_666
O6 Co2 O3 168.10(10) 2_776 2_666
O6 Co2 O7 100.07(10) 2_776 2_676
O3 Co2 O7 90.02(9) 2_666 2_676
O6 Co2 N1 93.31(13) 2_776 .
O3 Co2 N1 91.90(12) 2_666 .
O7 Co2 N1 95.83(12) 2_676 .
O6 Co2 O7 95.42(11) 2_776 .
O3 Co2 O7 80.09(11) 2_666 .
O7 Co2 O7 79.71(10) 2_676 .
N1 Co2 O7 170.77(10) . .
O6 Co2 O2 81.36(10) 2_776 .
O3 Co2 O2 87.78(9) 2_666 .
O7 Co2 O2 172.00(10) 2_676 .
N1 Co2 O2 91.93(12) . .
O7 Co2 O2 92.33(10) . .
C10 N1 C11 104.2(3) . .
C10 N1 Co2 127.1(3) . .
C11 N1 Co2 128.7(3) . .
C10 N2 C12 107.2(3) . .
C10 N2 C13 125.5(3) . .
C12 N2 C13 127.2(3) . .
C17 N3 C19 107.0(4) . .
C17 N3 C16 126.3(4) . .
C19 N3 C16 126.7(4) . .
C17 N4 C18 105.2(3) . .
C17 N4 Co1 128.0(3) . .
C18 N4 Co1 126.8(3) . .
C1 O1 Co1 128.1(2) . .
C1 O2 Co2 127.5(2) . .
C8 O3 Co2 134.8(2) . 2_666
C8 O3 Co1 124.3(2) . 2_666
Co2 O3 Co1 92.32(10) 2_666 2_666
C9 O5 Co1 126.9(2) . 1_655
C9 O6 Co2 137.8(2) . 2_776
Co1 O7 Co2 113.74(11) . 2_676
Co1 O7 Co2 96.78(11) . .
Co2 O7 Co2 100.29(10) 2_676 .
Co1 O7 H7A 123(3) . .
Co2 O7 H7A 106(4) 2_676 .
Co2 O7 H7A 115(3) . .
C15 O8 C14 112.2(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O2 1.240(4) .
C1 O1 1.269(4) .
C1 C2 1.505(4) .
C2 C7 1.392(4) .
C2 C3 1.398(5) .
C3 C4 1.386(5) .
C3 H3 0.9300 .
C4 C5 1.395(4) .
C4 C8 1.515(4) .
C5 C6 1.392(4) .
C5 H5 0.9300 .
C6 C7 1.388(4) .
C6 C9 1.517(4) .
C7 H7 0.9300 .
C8 O4 1.232(4) .
C8 O3 1.285(4) .
C9 O6 1.239(4) .
C9 O5 1.271(4) .
C10 N1 1.319(5) .
C10 N2 1.335(5) .
C10 H10 0.9300 .
C11 C12 1.349(6) .
C11 N1 1.376(5) .
C11 H11 0.9300 .
C12 N2 1.356(5) .
C12 H12 0.9300 .
C13 N2 1.464(5) .
C13 C14 1.515(6) 2_666
C13 H13A 0.9700 .
C13 H13B 0.9700 .
C14 O8 1.423(5) .
C14 C13 1.515(5) 2_666
C14 H14A 0.9700 .
C14 H14B 0.9700 .
C15 O8 1.423(5) .
C15 C16 1.501(6) .
C15 H15A 0.9700 .
C15 H15B 0.9700 .
C16 N3 1.471(5) .
C16 H16A 0.9700 .
C16 H16B 0.9700 .
C17 N4 1.320(5) .
C17 N3 1.337(5) .
C17 H17 0.9300 .
C18 N4 1.357(6) .
C18 C19 1.360(6) .
C18 H18 0.9300 .
C19 N3 1.357(6) .
C19 H19 0.9300 .
Co1 O7 1.979(2) .
Co1 O1 2.000(3) .
Co1 O5 2.000(2) 1_455
Co1 N4 2.073(3) .
Co1 O3 2.187(3) 2_666
Co2 O6 2.080(2) 2_776
Co2 O3 2.091(2) 2_666
Co2 O7 2.112(2) 2_676
Co2 N1 2.112(3) .
Co2 O7 2.146(3) .
Co2 O2 2.174(2) .
O3 Co2 2.091(2) 2_666
O3 Co1 2.187(3) 2_666
O5 Co1 2.000(2) 1_655
O6 Co2 2.080(2) 2_776
O7 Co2 2.112(2) 2_676
O7 H7A 0.842(10) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O2 C1 C2 C7 -39.9(5) . .
O1 C1 C2 C7 137.6(3) . .
O2 C1 C2 C3 145.0(3) . .
O1 C1 C2 C3 -37.5(4) . .
C7 C2 C3 C4 -1.5(5) . .
C1 C2 C3 C4 173.8(3) . .
C2 C3 C4 C5 -3.2(5) . .
C2 C3 C4 C8 176.7(3) . .
C3 C4 C5 C6 4.2(5) . .
C8 C4 C5 C6 -175.8(3) . .
C4 C5 C6 C7 -0.3(5) . .
C4 C5 C6 C9 179.9(3) . .
C5 C6 C7 C2 -4.4(5) . .
C9 C6 C7 C2 175.3(3) . .
C3 C2 C7 C6 5.3(5) . .
C1 C2 C7 C6 -169.7(3) . .
C3 C4 C8 O4 155.9(4) . .
C5 C4 C8 O4 -24.1(5) . .
C3 C4 C8 O3 -24.1(5) . .
C5 C4 C8 O3 155.9(3) . .
C7 C6 C9 O6 3.9(5) . .
C5 C6 C9 O6 -176.3(3) . .
C7 C6 C9 O5 -174.7(3) . .
C5 C6 C9 O5 5.1(5) . .
N1 C11 C12 N2 -0.1(5) . .
O8 C15 C16 N3 -64.6(5) . .
N4 C18 C19 N3 0.6(6) . .
N2 C10 N1 C11 -0.2(5) . .
N2 C10 N1 Co2 -179.2(3) . .
C12 C11 N1 C10 0.2(5) . .
C12 C11 N1 Co2 179.2(3) . .
O6 Co2 N1 C10 -45.7(4) 2_776 .
O3 Co2 N1 C10 123.6(4) 2_666 .
O7 Co2 N1 C10 -146.2(4) 2_676 .
O7 Co2 N1 C10 153.2(6) . .
O2 Co2 N1 C10 35.7(4) . .
O6 Co2 N1 C11 135.5(4) 2_776 .
O3 Co2 N1 C11 -55.2(4) 2_666 .
O7 Co2 N1 C11 35.1(4) 2_676 .
O7 Co2 N1 C11 -25.5(9) . .
O2 Co2 N1 C11 -143.0(4) . .
N1 C10 N2 C12 0.1(5) . .
N1 C10 N2 C13 -176.7(4) . .
C11 C12 N2 C10 0.0(5) . .
C11 C12 N2 C13 176.8(4) . .
C14 C13 N2 C10 -142.9(4) 2_666 .
C14 C13 N2 C12 40.9(6) 2_666 .
N4 C17 N3 C19 -0.8(5) . .
N4 C17 N3 C16 178.2(3) . .
C18 C19 N3 C17 0.1(6) . .
C18 C19 N3 C16 -178.8(4) . .
C15 C16 N3 C17 114.6(5) . .
C15 C16 N3 C19 -66.7(6) . .
N3 C17 N4 C18 1.1(5) . .
N3 C17 N4 Co1 -178.4(2) . .
C19 C18 N4 C17 -1.0(6) . .
C19 C18 N4 Co1 178.5(3) . .
O7 Co1 N4 C17 116.2(3) . .
O1 Co1 N4 C17 12.1(3) . .
O5 Co1 N4 C17 -130.2(3) 1_455 .
O3 Co1 N4 C17 -41.9(7) 2_666 .
O7 Co1 N4 C18 -63.3(4) . .
O1 Co1 N4 C18 -167.3(4) . .
O5 Co1 N4 C18 50.4(4) 1_455 .
O3 Co1 N4 C18 138.7(5) 2_666 .
O2 C1 O1 Co1 7.8(5) . .
C2 C1 O1 Co1 -169.5(2) . .
O7 Co1 O1 C1 25.1(3) . .
O5 Co1 O1 C1 -133.4(3) 1_455 .
N4 Co1 O1 C1 134.4(3) . .
O3 Co1 O1 C1 -55.0(3) 2_666 .
O1 C1 O2 Co2 7.7(5) . .
C2 C1 O2 Co2 -175.2(2) . .
O6 Co2 O2 C1 -142.9(3) 2_776 .
O3 Co2 O2 C1 32.2(3) 2_666 .
O7 Co2 O2 C1 -41.9(8) 2_676 .
N1 Co2 O2 C1 124.0(3) . .
O7 Co2 O2 C1 -47.8(3) . .
O4 C8 O3 Co2 -23.9(6) . 2_666
C4 C8 O3 Co2 156.2(2) . 2_666
O4 C8 O3 Co1 114.2(4) . 2_666
C4 C8 O3 Co1 -65.7(4) . 2_666
O6 C9 O5 Co1 18.9(5) . 1_655
C6 C9 O5 Co1 -162.7(2) . 1_655
O5 C9 O6 Co2 0.9(6) . 2_776
C6 C9 O6 Co2 -177.5(2) . 2_776
O1 Co1 O7 Co2 -164.40(12) . 2_676
O5 Co1 O7 Co2 1.64(16) 1_455 2_676
N4 Co1 O7 Co2 102.59(14) . 2_676
O3 Co1 O7 Co2 -81.75(13) 2_666 2_676
O1 Co1 O7 Co2 -59.99(11) . .
O5 Co1 O7 Co2 106.05(11) 1_455 .
N4 Co1 O7 Co2 -153.00(11) . .
O3 Co1 O7 Co2 22.65(9) 2_666 .
O6 Co2 O7 Co1 145.02(10) 2_776 .
O3 Co2 O7 Co1 -23.86(9) 2_666 .
O7 Co2 O7 Co1 -115.70(12) 2_676 .
N1 Co2 O7 Co1 -54.0(7) . .
O2 Co2 O7 Co1 63.48(10) . .
O6 Co2 O7 Co2 -99.29(10) 2_776 2_676
O3 Co2 O7 Co2 91.84(10) 2_666 2_676
O7 Co2 O7 Co2 0.0 2_676 2_676
N1 Co2 O7 Co2 61.7(7) . 2_676
O2 Co2 O7 Co2 179.18(9) . 2_676
C16 C15 O8 C14 -158.7(3) . .
C13 C14 O8 C15 171.1(3) 2_666 .
