#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:22:12 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179627 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/91/4509120.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4509120
loop_
_publ_author_name
'Luo, Feng'
'Che, Yun-xia'
'Zheng, Ji-min'
_publ_section_title
;
 Trinuclear Cobalt Based Porous Coordination Polymers Showing Unique
 Topological and Magnetic Variety upon Different Dicarboxylate-like
 Ligands
;
_journal_issue                   2
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              1066
_journal_paper_doi               10.1021/cg800895g
_journal_volume                  9
_journal_year                    2009
_chemical_formula_sum            'C66.5 H66.5 Co3 N3.5 O19.5'
_chemical_formula_weight         1403.55
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 92.096(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.550(10)
_cell_length_b                   14.187(7)
_cell_length_c                   25.681(12)
_cell_measurement_reflns_used    14353
_cell_measurement_temperature    294(2)
_cell_measurement_theta_max      25.00
_cell_measurement_theta_min      1.44
_cell_volume                     8210(7)
_computing_cell_refinement       'rapid auto'
_computing_data_collection       'rapid auto'
_computing_data_reduction        'rapid auto'
_computing_molecular_graphics    'SHELXTL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXTL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      294(2)
_diffrn_measured_fraction_theta_full 0.975
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'rigaku r-axis rapid IP area detector'
_diffrn_measurement_method       oscillation
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1710
_diffrn_reflns_av_sigmaI/netI    0.2491
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            44282
_diffrn_reflns_theta_full        26.43
_diffrn_reflns_theta_max         26.43
_diffrn_reflns_theta_min         1.44
_exptl_absorpt_coefficient_mu    0.653
_exptl_absorpt_correction_T_max  0.9316
_exptl_absorpt_correction_T_min  0.9084
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Purple
_exptl_crystal_density_diffrn    1.045
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             2660
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.11
_refine_diff_density_max         3.461
_refine_diff_density_min         -1.348
_refine_diff_density_rms         0.343
_refine_ls_extinction_coef       0.15880(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.462
_refine_ls_hydrogen_treatment    refU
_refine_ls_matrix_type           full
_refine_ls_number_parameters     653
_refine_ls_number_reflns         16476
_refine_ls_number_restraints     7
_refine_ls_restrained_S_all      1.462
_refine_ls_R_factor_all          0.3233
_refine_ls_R_factor_gt           0.2256
_refine_ls_shift/su_max          0.024
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.2000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.4838
_refine_ls_wR_factor_ref         0.5282
_reflns_number_gt                6910
_reflns_number_total             16476
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg800895gsup1.cif
_cod_data_source_block           3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from
2011-04-26.

'_refine_ls_hydrogen_treatment' value 'refu' changed to
'refU' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P2/c
_cod_database_code               4509120
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C -0.027996(8) 0.704146(14) 0.061763(7) 0.09560(7) Uani 1 1 d .
C2 C -0.130949(2) 0.689241(4) 0.023231(3) 0.13467(10) Uani 1 1 d G
H2 H -0.1160 0.6647 -0.0072 0.162 Uiso 1 1 calc R
C3 C -0.191597(2) 0.704139(4) 0.026728(3) 0.09111(7) Uani 1 1 d G
H3 H -0.2172 0.6896 -0.0014 0.109 Uiso 1 1 calc R
C4 C -0.214013(2) 0.740755(5) 0.072197(3) 0.07859(7) Uani 1 1 d G
C5 C -0.175782(3) 0.762474(7) 0.114170(3) 0.14151(11) Uani 1 1 d G
H5 H -0.1908 0.7870 0.1446 0.170 Uiso 1 1 calc R
C6 C -0.115134(3) 0.747576(7) 0.110674(3) 0.10450(7) Uani 1 1 d G
H6 H -0.0896 0.7621 0.1388 0.125 Uiso 1 1 calc R
C7 C -0.092717(2) 0.710960(5) 0.065204(3) 0.18750(9) Uani 1 1 d G
C8 C -0.403721(3) 0.789912(8) 0.067334(5) 0.12762(7) Uani 1 1 d GD
C9 C -0.370584(2) 0.808180(6) 0.023876(5) 0.10064(7) Uani 1 1 d G
H9 H -0.3891 0.8313 -0.0064 0.121 Uiso 1 1 calc R
C10 C -0.309764(2) 0.791852(5) 0.025740(4) 0.10906(9) Uani 1 1 d G
H10 H -0.2876 0.8041 -0.0033 0.131 Uiso 1 1 calc R
C11 C -0.282082(2) 0.757261(6) 0.071062(4) 0.10033(8) Uani 1 1 d G
C12 C -0.315219(3) 0.738994(8) 0.114522(4) 0.20641(11) Uani 1 1 d G
H12 H -0.2967 0.7158 0.1448 0.248 Uiso 1 1 calc R
C13 C -0.376038(3) 0.755319(9) 0.112659(5) 0.23679(12) Uani 1 1 d G
H13 H -0.3982 0.7431 0.1417 0.284 Uiso 1 1 calc R
C14 C -0.471837(4) 0.788161(16) 0.065865(10) 0.17370(10) Uani 1 1 d D
C15 C 0.154580(6) 0.825639(11) 0.016286(5) 0.05741(5) Uani 1 1 d .
C16 C 0.154912(2) 0.876577(4) -0.035917(2) 0.05994(5) Uani 1 1 d G
C17 C 0.202757(2) 0.933581(4) -0.047620(2) 0.09686(7) Uani 1 1 d G
H17 H 0.2348 0.9393 -0.0240 0.116 Uiso 1 1 calc R
C18 C 0.202709(3) 0.982092(4) -0.094647(2) 0.09030(6) Uani 1 1 d G
H18 H 0.2347 1.0202 -0.1025 0.108 Uiso 1 1 calc R
C19 C 0.154817(3) 0.973601(4) -0.129970(2) 0.07878(6) Uani 1 1 d G
C20 C 0.106972(3) 0.916598(5) -0.118267(2) 0.09232(7) Uani 1 1 d G
H20 H 0.0749 0.9109 -0.1419 0.111 Uiso 1 1 calc R
C21 C 0.107019(2) 0.868086(4) -0.071241(2) 0.06992(6) Uani 1 1 d G
H21 H 0.0750 0.8299 -0.0634 0.084 Uiso 1 1 calc R
C22 C 0.156093(4) 1.029248(5) -0.178371(2) 0.09202(6) Uani 1 1 d G
C23 C 0.209738(4) 1.038401(6) -0.206364(2) 0.11442(8) Uani 1 1 d G
H23 H 0.2440 1.0107 -0.1921 0.137 Uiso 1 1 calc R
C24 C 0.213749(5) 1.084229(7) -0.251766(3) 0.12068(9) Uani 1 1 d G
H24 H 0.2500 1.0901 -0.2675 0.145 Uiso 1 1 calc R
C25 C 0.159985(6) 1.124572(7) -0.275844(3) 0.06976(6) Uani 1 1 d G
C26 C 0.106385(5) 1.109745(7) -0.251718(3) 0.08034(6) Uani 1 1 d G
H26 H 0.0717 1.1328 -0.2678 0.096 Uiso 1 1 calc R
C27 C 0.102472(4) 1.060371(6) -0.203059(2) 0.10418(8) Uani 1 1 d G
H27 H 0.0660 1.0493 -0.1884 0.125 Uiso 1 1 calc R
C28 C 0.161088(6) 1.178592(11) -0.326726(6) 0.05922(5) Uani 1 1 d .
C29 C 0.350768(6) 0.928233(9) 0.104540(6) 0.05107(5) Uani 1 1 d .
C30 C 0.321819(2) 1.024922(3) 0.111731(2) 0.05549(5) Uani 1 1 d G
C31 C 0.355689(2) 1.104325(3) 0.123871(2) 0.09461(8) Uani 1 1 d G
H31 H 0.3964 1.0987 0.1299 0.114 Uiso 1 1 calc R
C32 C 0.328641(2) 1.192091(3) 0.126932(2) 0.08922(7) Uani 1 1 d G
H32 H 0.3513 1.2452 0.1351 0.107 Uiso 1 1 calc R
C33 C 0.267723(2) 1.200455(3) 0.117853(2) 0.07496(6) Uani 1 1 d G
C34 C 0.233852(2) 1.121053(3) 0.105714(3) 0.07244(6) Uani 1 1 d G
H34 H 0.1931 1.1266 0.0996 0.087 Uiso 1 1 calc R
C35 C 0.260900(2) 1.033286(3) 0.102652(2) 0.08098(7) Uani 1 1 d G
H35 H 0.2382 0.9802 0.0945 0.097 Uiso 1 1 calc R
C36 C 0.240046(3) 1.298720(3) 0.116108(3) 0.05751(5) Uani 1 1 d G
C37 C 0.272299(3) 1.376026(3) 0.101841(3) 0.06758(6) Uani 1 1 d G
H37 H 0.3123 1.3685 0.0953 0.081 Uiso 1 1 calc R
C38 C 0.246562(4) 1.467063(3) 0.096714(4) 0.07006(6) Uani 1 1 d G
H38 H 0.2687 1.5185 0.0862 0.084 Uiso 1 1 calc R
C39 C 0.189020(4) 1.476215(4) 0.107648(4) 0.04782(4) Uani 1 1 d G
C40 C 0.158251(3) 1.397014(4) 0.122805(5) 0.08477(7) Uani 1 1 d G
H40 H 0.1185 1.4044 0.1303 0.102 Uiso 1 1 calc R
C41 C 0.181960(3) 1.308936(4) 0.127480(4) 0.08757(7) Uani 1 1 d G
H41 H 0.1594 1.2580 0.1380 0.105 Uiso 1 1 calc R
C42 C 0.157663(6) 1.569777(9) 0.101677(6) 0.04774(5) Uani 1 1 d .
C43 C 0.354673(6) 0.669853(10) 0.171238(5) 0.04686(4) Uani 1 1 d .
C44 C 0.354876(2) 0.616513(4) 0.223151(2) 0.05762(5) Uani 1 1 d G
C45 C 0.405466(2) 0.608800(4) 0.255447(2) 0.06893(6) Uani 1 1 d G
H45 H 0.4409 0.6359 0.2456 0.083 Uiso 1 1 calc R
C46 C 0.403089(3) 0.560606(4) 0.302449(2) 0.07325(6) Uani 1 1 d G
H46 H 0.4369 0.5554 0.3241 0.088 Uiso 1 1 calc R
C47 C 0.350121(3) 0.520125(4) 0.317155(2) 0.08665(6) Uani 1 1 d G
C48 C 0.299531(3) 0.527838(4) 0.284860(2) 0.10177(7) Uani 1 1 d G
H48 H 0.2641 0.5008 0.2947 0.122 Uiso 1 1 calc R
C49 C 0.301908(2) 0.576031(4) 0.237857(2) 0.09263(7) Uani 1 1 d G
H49 H 0.2681 0.5812 0.2162 0.111 Uiso 1 1 calc R
C50 C 0.348252(4) 0.465386(5) 0.367130(2) 0.07817(6) Uani 1 1 d G
C51 C 0.297646(4) 0.468800(6) 0.396758(2) 0.10489(7) Uani 1 1 d G
H51 H 0.2641 0.5016 0.3849 0.126 Uiso 1 1 calc R
C52 C 0.298608(5) 0.422568(7) 0.443828(2) 0.09170(6) Uani 1 1 d G
H52 H 0.2653 0.4269 0.4641 0.110 Uiso 1 1 calc R
C53 C 0.345997(5) 0.370289(7) 0.462647(2) 0.06560(5) Uani 1 1 d G
C54 C 0.391807(5) 0.364813(6) 0.431015(3) 0.07875(6) Uani 1 1 d G
H54 H 0.4240 0.3278 0.4417 0.094 Uiso 1 1 calc R
C55 C 0.394613(4) 0.411137(5) 0.382715(2) 0.08724(6) Uani 1 1 d G
H55 H 0.4275 0.4045 0.3622 0.105 Uiso 1 1 calc R
C56 C 0.342082(6) 0.315415(10) 0.513034(5) 0.06747(5) Uani 1 1 d .
Co1 Co 0.091617(1) 0.716760(1) 0.092755(1) 0.04074(1) Uani 1 1 d .
Co2 Co 0.414710(1) 0.782776(1) 0.095608(1) 0.04115(1) Uani 1 1 d .
Co3 Co 0.253030(1) 0.749871(1) 0.095268(1) 0.03915(1) Uani 1 1 d .
O1 O 0.320625(4) 0.856767(7) 0.097415(4) 0.06758(4) Uani 1 1 d .
O2 O 0.405728(4) 0.925366(7) 0.107569(4) 0.06578(4) Uani 1 1 d .
O3 O 0.185768(5) 1.640408(6) 0.091115(4) 0.06374(4) Uani 1 1 d .
O4 O 0.102956(5) 1.575889(7) 0.104281(5) 0.08000(4) Uani 1 1 d .
O5 O 0.208877(5) 1.196296(10) -0.342041(4) 0.11453(5) Uani 1 1 d .
O6 O 0.112126(4) 1.207930(8) -0.343381(4) 0.06839(4) Uani 1 1 d .
O7 O 0.198102(5) 0.836728(8) 0.046986(4) 0.09210(4) Uani 1 1 d .
O8 O 0.109298(4) 0.779490(7) 0.025488(3) 0.06091(3) Uani 1 1 d .
O9 O 0.004307(5) 0.733388(8) 0.097057(4) 0.07234(4) Uani 1 1 d .
O10 O -0.008388(7) 0.655960(13) 0.024123(7) 0.18090(8) Uani 1 1 d .
O11 O 0.399452(4) 0.711184(7) 0.161312(3) 0.05555(3) Uani 1 1 d .
O12 O 0.307857(5) 0.663865(8) 0.143395(4) 0.09457(4) Uani 1 1 d .
O13 O 0.391700(5) 0.279157(8) 0.527053(4) 0.06894(4) Uani 1 1 d .
O14 O 0.296267(5) 0.310913(10) 0.533301(4) 0.11658(5) Uani 1 1 d .
O15 O -0.499073(4) 0.765996(9) 0.097200(5) 0.10458(5) Uani 1 1 d .
O16 O -0.491951(8) 0.851496(17) 0.027680(9) 0.21454(12) Uani 1 1 d .
C57 C 0.464698(7) 0.305058(7) 0.122200(4) 0.21349(17) Uani 1 1 d D
H57A H 0.5005 0.2730 0.1135 0.320 Uiso 1 1 calc R
H57B H 0.4347 0.2596 0.1299 0.320 Uiso 1 1 calc R
H57C H 0.4724 0.3443 0.1521 0.320 Uiso 1 1 calc R
C58 C 0.427387(9) 0.474773(5) 0.076332(9) 0.7709(6) Uani 1 1 d D
H58A H 0.4629 0.5110 0.0725 1.156 Uiso 1 1 calc R
H58B H 0.4102 0.4900 0.1089 1.156 Uiso 1 1 calc R
H58C H 0.3996 0.4893 0.0483 1.156 Uiso 1 1 calc R
N1 N 0.442725(7) 0.367406(6) 0.075133(5) 0.4003(2) Uani 1 1 d D
H1A H 0.4704 0.3612 0.0510 0.480 Uiso 1 1 calc R
H1B H 0.4099 0.3387 0.0619 0.480 Uiso 1 1 calc R
O18 O 0.446209(16) 0.91686(3) 0.928141(13) 0.4437(3) Uani 1 1 d .
C63 C 0.392345(18) 0.94930(2) 0.968616(11) 0.3618(2) Uani 1 1 d .
H63A H 0.4085 0.9919 0.9945 0.543 Uiso 1 1 calc R
H63B H 0.3770 0.8944 0.9854 0.543 Uiso 1 1 calc R
H63C H 0.3609 0.9800 0.9489 0.543 Uiso 1 1 calc R
C59 C 0.042538(8) 0.192967(5) 0.101005(9) 0.22681(19) Uani 1 1 d D
H59A H 0.0208 0.1863 0.1322 0.340 Uiso 1 1 calc R
H59B H 0.0182 0.2241 0.0748 0.340 Uiso 1 1 calc R
H59C H 0.0776 0.2297 0.1083 0.340 Uiso 1 1 calc R
O17 O 0.888104(17) 0.44146(2) 0.035447(10) 0.3435(2) Uani 1 1 d .
C62 C 0.948275(13) 0.40665(2) 0.069787(10) 0.35955(14) Uani 1 1 d .
H62A H 0.9827 0.4149 0.0493 0.539 Uiso 1 1 calc R
H62B H 0.9443 0.3413 0.0788 0.539 Uiso 1 1 calc R
H62C H 0.9525 0.4437 0.1010 0.539 Uiso 1 1 calc R
N2 N 0.060477(7) 0.093638(6) 0.080986(6) 0.4234(3) Uani 1 1 d D
H2A H 0.0914 0.1035 0.0605 0.508 Uiso 1 1 calc R
H2B H 0.0302 0.0749 0.0596 0.508 Uiso 1 1 calc R
C60 C 0.077615(10) 0.005487(6) 0.114746(7) 0.5262(3) Uani 1 1 d D
H60A H 0.0435 -0.0343 0.1179 0.789 Uiso 1 1 calc R
H60B H 0.0914 0.0255 0.1488 0.789 Uiso 1 1 calc R
H60C H 0.1085 -0.0290 0.0984 0.789 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O9 C1 O10 122.22(3) . .
O9 C1 C7 120.18(3) . .
O10 C1 C7 116.968(18) . .
C3 C2 C7 120.0 . .
C3 C2 H2 120.0 . .
C7 C2 H2 120.0 . .
C2 C3 C4 120.0 . .
C2 C3 H3 120.0 . .
C4 C3 H3 120.0 . .
C3 C4 C5 120.0 . .
C3 C4 C11 115.5 . .
C5 C4 C11 124.5 . .
C6 C5 C4 120.0 . .
C6 C5 H5 120.0 . .
C4 C5 H5 120.0 . .
C7 C6 C5 120.0 . .
C7 C6 H6 120.0 . .
C5 C6 H6 120.0 . .
C6 C7 C2 120.0 . .
C6 C7 C1 117.9 . .
C2 C7 C1 121.9 . .
C9 C8 C13 120.0 . .
C9 C8 C14 123.4 . .
C13 C8 C14 115.7 . .
C8 C9 C10 120.0 . .
C8 C9 H9 120.0 . .
C10 C9 H9 120.0 . .
C11 C10 C9 120.0 . .
C11 C10 H10 120.0 . .
C9 C10 H10 120.0 . .
C10 C11 C12 120.0 . .
C10 C11 C4 118.9 . .
C12 C11 C4 121.1 . .
C13 C12 C11 120.0 . .
C13 C12 H12 120.0 . .
C11 C12 H12 120.0 . .
C12 C13 C8 120.0 . .
C12 C13 H13 120.0 . .
C8 C13 H13 120.0 . .
O15 C14 O16 122.29(3) . .
O15 C14 C8 125.71(3) . .
O16 C14 C8 107.844(19) . .
O8 C15 O7 125.43(3) . .
O8 C15 C16 116.600(17) . .
O7 C15 C16 117.89(2) . .
C17 C16 C21 120.0 . .
C17 C16 C15 119.7 . .
C21 C16 C15 120.3 . .
C18 C17 C16 120.0 . .
C18 C17 H17 120.0 . .
C16 C17 H17 120.0 . .
C17 C18 C19 120.0 . .
C17 C18 H18 120.0 . .
C19 C18 H18 120.0 . .
C20 C19 C18 120.0 . .
C20 C19 C22 122.2 . .
C18 C19 C22 117.7 . .
C21 C20 C19 120.0 . .
C21 C20 H20 120.0 . .
C19 C20 H20 120.0 . .
C20 C21 C16 120.0 . .
C20 C21 H21 120.0 . .
C16 C21 H21 120.0 . .
C27 C22 C23 118.0 . .
C27 C22 C19 120.2 . .
C23 C22 C19 120.9 . .
C24 C23 C22 124.3 . .
C24 C23 H23 117.8 . .
C22 C23 H23 117.8 . .
C23 C24 C25 118.5 . .
C23 C24 H24 120.7 . .
C25 C24 H24 120.7 . .
C26 C25 C24 118.3 . .
C26 C25 C28 120.1 . .
C24 C25 C28 121.6 . .
C25 C26 C27 122.8 . .
C25 C26 H26 118.6 . .
C27 C26 H26 118.6 . .
C22 C27 C26 117.6 . .
C22 C27 H27 121.2 . .
C26 C27 H27 121.2 . .
O5 C28 O6 128.43(3) . .
O5 C28 C25 115.859(18) . .
O6 C28 C25 115.10(2) . .
O1 C29 O2 121.86(2) . .
O1 C29 C30 121.32(3) . .
O2 C29 C30 116.802(17) . .
C31 C30 C35 120.0 . .
C31 C30 C29 121.3 . .
C35 C30 C29 118.6 . .
C32 C31 C30 120.0 . .
C32 C31 H31 120.0 . .
C30 C31 H31 120.0 . .
C31 C32 C33 120.0 . .
C31 C32 H32 120.0 . .
C33 C32 H32 120.0 . .
C34 C33 C32 120.0 . .
C34 C33 C36 120.8 . .
C32 C33 C36 118.9 . .
C33 C34 C35 120.0 . .
C33 C34 H34 120.0 . .
C35 C34 H34 120.0 . .
C34 C35 C30 120.0 . .
C34 C35 H35 120.0 . .
C30 C35 H35 120.0 . .
C41 C36 C37 119.7 . .
C41 C36 C33 119.1 . .
C37 C36 C33 121.1 . .
C36 C37 C38 122.2 . .
C36 C37 H37 118.9 . .
C38 C37 H37 118.9 . .
C39 C38 C37 117.6 . .
C39 C38 H38 121.2 . .
C37 C38 H38 121.2 . .
C38 C39 C40 118.6 . .
C38 C39 C42 121.1 . .
C40 C39 C42 120.3 . .
C41 C40 C39 124.8 . .
C41 C40 H40 117.6 . .
C39 C40 H40 117.6 . .
C36 C41 C40 117.2 . .
C36 C41 H41 121.4 . .
C40 C41 H41 121.4 . .
O3 C42 O4 118.66(2) . .
O3 C42 C39 119.94(3) . .
O4 C42 C39 121.266(16) . .
O11 C43 O12 127.36(3) . .
O11 C43 C44 116.685(17) . .
O12 C43 C44 115.94(2) . .
C45 C44 C49 120.0 . .
C45 C44 C43 122.3 . .
C49 C44 C43 117.7 . .
C46 C45 C44 120.0 . .
C46 C45 H45 120.0 . .
C44 C45 H45 120.0 . .
C45 C46 C47 120.0 . .
C45 C46 H46 120.0 . .
C47 C46 H46 120.0 . .
C48 C47 C46 120.0 . .
C48 C47 C50 120.2 . .
C46 C47 C50 119.8 . .
C47 C48 C49 120.0 . .
C47 C48 H48 120.0 . .
C49 C48 H48 120.0 . .
C48 C49 C44 120.0 . .
C48 C49 H49 120.0 . .
C44 C49 H49 120.0 . .
C55 C50 C51 119.9 . .
C55 C50 C47 120.2 . .
C51 C50 C47 119.8 . .
C52 C51 C50 118.4 . .
C52 C51 H51 120.8 . .
C50 C51 H51 120.8 . .
C53 C52 C51 123.6 . .
C53 C52 H52 118.2 . .
C51 C52 H52 118.2 . .
C54 C53 C52 115.2 . .
C54 C53 C56 123.9 . .
C52 C53 C56 120.6 . .
C53 C54 C55 124.6 . .
C53 C54 H54 117.7 . .
C55 C54 H54 117.7 . .
C50 C55 C54 118.0 . .
C50 C55 H55 121.0 . .
C54 C55 H55 121.0 . .
O14 C56 O13 129.14(3) . .
O14 C56 C53 119.051(19) . .
O13 C56 C53 111.81(2) . .
O9 Co1 O8 102.974(11) . .
O9 Co1 O6 95.212(14) . 4_576
O8 Co1 O6 115.12(3) . 4_576
O9 Co1 O4 103.158(5) . 1_545
O8 Co1 O4 122.386(11) . 1_545
O6 Co1 O4 112.44(2) 4_576 1_545
O9 Co1 O3 159.703(11) . 1_545
O8 Co1 O3 88.917(17) . 1_545
O6 Co1 O3 94.468(19) 4_576 1_545
O4 Co1 O3 56.592(12) 1_545 1_545
O15 Co2 O11 96.972(12) 1_655 .
O15 Co2 O13 100.877(13) 1_655 4_565
O11 Co2 O13 117.77(3) . 4_565
O15 Co2 O2 102.685(5) 1_655 .
O11 Co2 O2 110.53(2) . .
O13 Co2 O2 122.325(11) 4_565 .
O15 Co2 O1 160.542(12) 1_655 .
O11 Co2 O1 91.521(18) . .
O13 Co2 O1 90.466(18) 4_565 .
O2 Co2 O1 57.876(12) . .
O5 Co3 O14 177.194(6) 4_576 4_565
O5 Co3 O12 92.64(3) 4_576 .
O14 Co3 O12 85.83(3) 4_565 .
O5 Co3 O7 87.31(3) 4_576 .
O14 Co3 O7 94.23(3) 4_565 .
O12 Co3 O7 179.799(5) . .
O5 Co3 O1 94.62(2) 4_576 .
O14 Co3 O1 87.73(2) 4_565 .
O12 Co3 O1 89.61(3) . .
O7 Co3 O1 90.20(3) . .
O5 Co3 O3 86.97(2) 4_576 1_545
O14 Co3 O3 90.69(2) 4_565 1_545
O12 Co3 O3 90.49(3) . 1_545
O7 Co3 O3 89.70(3) . 1_545
O1 Co3 O3 178.405(4) . 1_545
C29 O1 Co3 166.515(10) . .
C29 O1 Co2 82.98(3) . .
Co3 O1 Co2 108.76(3) . .
C29 O2 Co2 97.271(9) . .
C42 O3 Co3 160.617(12) . 1_565
C42 O3 Co1 84.22(3) . 1_565
Co3 O3 Co1 107.16(4) 1_565 1_565
C42 O4 Co1 100.408(9) . 1_565
C28 O5 Co3 143.503(12) . 4_575
C28 O6 Co1 129.690(13) . 4_575
C15 O7 Co3 136.70(2) . .
C15 O8 Co1 126.214(13) . .
C1 O9 Co1 119.05(2) . .
C43 O11 Co2 126.512(13) . .
C43 O12 Co3 139.31(2) . .
C56 O13 Co2 128.212(12) . 4_566
C56 O14 Co3 143.533(13) . 4_566
C14 O15 Co2 122.82(2) . 1_455
N1 C57 H57A 109.5 . .
N1 C57 H57B 109.5 . .
H57A C57 H57B 109.5 . .
N1 C57 H57C 109.5 . .
H57A C57 H57C 109.5 . .
H57B C57 H57C 109.5 . .
N1 C58 H58A 109.5 . .
N1 C58 H58B 109.5 . .
H58A C58 H58B 109.5 . .
N1 C58 H58C 109.5 . .
H58A C58 H58C 109.5 . .
H58B C58 H58C 109.5 . .
C58 N1 C57 126.89(2) . .
C58 N1 H1A 105.6 . .
C57 N1 H1A 105.6 . .
C58 N1 H1B 105.6 . .
C57 N1 H1B 105.6 . .
H1A N1 H1B 106.1 . .
O18 C63 H63A 109.5 . .
O18 C63 H63B 109.5 . .
H63A C63 H63B 109.5 . .
O18 C63 H63C 109.5 . .
H63A C63 H63C 109.5 . .
H63B C63 H63C 109.5 . .
N2 C59 H59A 109.5 . .
N2 C59 H59B 109.5 . .
H59A C59 H59B 109.5 . .
N2 C59 H59C 109.5 . .
H59A C59 H59C 109.5 . .
H59B C59 H59C 109.5 . .
O17 C62 H62A 109.5 . .
O17 C62 H62B 109.5 . .
H62A C62 H62B 109.5 . .
O17 C62 H62C 109.5 . .
H62A C62 H62C 109.5 . .
H62B C62 H62C 109.5 . .
C59 N2 C60 127.06(3) . .
C59 N2 H2A 105.5 . .
C60 N2 H2A 105.5 . .
C59 N2 H2B 105.5 . .
C60 N2 H2B 105.5 . .
H2A N2 H2B 106.1 . .
N2 C60 H60A 109.5 . .
N2 C60 H60B 109.5 . .
H60A C60 H60B 109.5 . .
N2 C60 H60C 109.5 . .
H60A C60 H60C 109.5 . .
H60B C60 H60C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 O9 1.2149(4) .
C1 O10 1.2761(5) .
C1 C7 1.4685 .
C2 C3 1.3900 .
C2 C7 1.3900 .
C2 H2 0.9300 .
C3 C4 1.3900 .
C3 H3 0.9300 .
C4 C5 1.3900 .
C4 C11 1.5519 .
C5 C6 1.3900 .
C5 H5 0.9300 .
C6 C7 1.3900 .
C6 H6 0.9300 .
C8 C9 1.3900 .
C8 C13 1.3901 .
C8 C14 1.5353 .
C9 C10 1.3900 .
C9 H9 0.9300 .
C10 C11 1.3900 .
C10 H10 0.9300 .
C11 C12 1.3900 .
C12 C13 1.3900 .
C12 H12 0.9300 .
C13 H13 0.9300 .
C14 O15 1.0769(4) .
C14 O16 1.3936(5) .
C15 O8 1.2429(5) .
C15 O7 1.2462(4) .
C15 C16 1.5232 .
C16 C17 1.3900 .
C16 C21 1.3900 .
C17 C18 1.3900 .
C17 H17 0.9300 .
C18 C19 1.3900 .
C18 H18 0.9300 .
C19 C20 1.3900 .
C19 C22 1.4737 .
C20 C21 1.3900 .
C20 H20 0.9300 .
C21 H21 0.9300 .
C22 C27 1.4152 .
C22 C23 1.4355 .
C23 C24 1.3409 .
C23 H23 0.9300 .
C24 C25 1.4577 .
C24 H24 0.9300 .
C25 C26 1.3942 .
C25 C28 1.5159 .
C26 C27 1.4381 .
C26 H26 0.9300 .
C27 H27 0.9300 .
C28 O5 1.1875(5) .
C28 O6 1.2412(5) .
C29 O1 1.2306(5) .
C29 O2 1.2396(6) .
C29 C30 1.5332 .
C30 C31 1.3900 .
C30 C35 1.3900 .
C31 C32 1.3900 .
C31 H31 0.9300 .
C32 C33 1.3900 .
C32 H32 0.9300 .
C33 C34 1.3900 .
C33 C36 1.5274 .
C34 C35 1.3900 .
C34 H34 0.9300 .
C35 H35 0.9300 .
C36 C41 1.3601 .
C36 C37 1.3732 .
C37 C38 1.4201 .
C37 H37 0.9300 .
C38 C39 1.3439 .
C38 H38 0.9300 .
C39 C40 1.3839 .
C39 C42 1.5091 .
C40 C41 1.3627 .
C40 H40 0.9300 .
C41 H41 0.9300 .
C42 O3 1.2214(5) .
C42 O4 1.2409(6) .
C43 O11 1.2030(4) .
C43 O12 1.2561(5) .
C43 C44 1.5328 .
C44 C45 1.3900 .
C44 C49 1.3900 .
C45 C46 1.3900 .
C45 H45 0.9300 .
C46 C47 1.3900 .
C46 H46 0.9300 .
C47 C48 1.3900 .
C47 C50 1.5020 .
C48 C49 1.3900 .
C48 H48 0.9300 .
C49 H49 0.9300 .
C50 C55 1.3472 .
C50 C51 1.3954 .
C51 C52 1.3748 .
C51 H51 0.9300 .
C52 C53 1.3740 .
C52 H52 0.9300 .
C53 C54 1.3396 .
C53 C56 1.5155 .
C54 C55 1.4072 .
C54 H54 0.9300 .
C55 H55 0.9300 .
C56 O14 1.1754(5) .
C56 O13 1.2715(5) .
Co1 O9 1.9900(9) .
Co1 O8 1.9964(7) .
Co1 O6 1.9975(7) 4_576
Co1 O4 2.0351(10) 1_545
Co1 O3 2.3852(9) 1_545
Co2 O15 1.9577(8) 1_655
Co2 O11 2.0099(7) .
Co2 O13 2.0184(7) 4_565
Co2 O2 2.0572(10) .
Co2 O1 2.3691(9) .
Co3 O5 2.0697(7) 4_576
Co3 O14 2.0833(7) 4_565
Co3 O12 2.1055(6) .
Co3 O7 2.1161(6) .
Co3 O1 2.1495(7) .
Co3 O3 2.1707(7) 1_545
O3 Co3 2.1707(7) 1_565
O3 Co1 2.3852(9) 1_565
O4 Co1 2.0351(10) 1_565
O5 Co3 2.0697(7) 4_575
O6 Co1 1.9975(7) 4_575
O13 Co2 2.0184(7) 4_566
O14 Co3 2.0833(7) 4_566
O15 Co2 1.9577(9) 1_455
C57 N1 1.5637(5) .
C57 H57A 0.9600 .
C57 H57B 0.9600 .
C57 H57C 0.9600 .
C58 N1 1.5625(7) .
C58 H58A 0.9600 .
C58 H58B 0.9600 .
C58 H58C 0.9600 .
N1 H1A 0.9000 .
N1 H1B 0.9000 .
O18 C63 1.6911(7) .
C63 H63A 0.9600 .
C63 H63B 0.9600 .
C63 H63C 0.9600 .
C59 N2 1.5585(7) .
C59 H59A 0.9600 .
C59 H59B 0.9600 .
C59 H59C 0.9600 .
O17 C62 1.6659(7) .
C62 H62A 0.9600 .
C62 H62B 0.9600 .
C62 H62C 0.9600 .
N2 C60 1.5622(6) .
N2 H2A 0.9000 .
N2 H2B 0.9000 .
C60 H60A 0.9600 .
C60 H60B 0.9600 .
C60 H60C 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C7 C2 C3 C4 0.0 . .
C2 C3 C4 C5 0.0 . .
C2 C3 C4 C11 178.2 . .
C3 C4 C5 C6 0.0 . .
C11 C4 C5 C6 -178.0 . .
C4 C5 C6 C7 0.0 . .
C5 C6 C7 C2 0.0 . .
C5 C6 C7 C1 174.8 . .
C3 C2 C7 C6 0.0 . .
C3 C2 C7 C1 -174.6 . .
O9 C1 C7 C6 -2.85(2) . .
O10 C1 C7 C6 168.218(14) . .
O9 C1 C7 C2 171.883(13) . .
O10 C1 C7 C2 -17.05(2) . .
C13 C8 C9 C10 0.0 . .
C14 C8 C9 C10 -168.3 . .
C8 C9 C10 C11 0.0 . .
C9 C10 C11 C12 0.0 . .
C9 C10 C11 C4 -179.3 . .
C3 C4 C11 C10 -39.1 . .
C5 C4 C11 C10 139.0 . .
C3 C4 C11 C12 141.5 . .
C5 C4 C11 C12 -40.4 . .
C10 C11 C12 C13 0.0 . .
C4 C11 C12 C13 179.3 . .
C11 C12 C13 C8 0.0 . .
C9 C8 C13 C12 0.0 . .
C14 C8 C13 C12 169.1 . .
C9 C8 C14 O15 171.910(19) . .
C13 C8 C14 O15 3.18(3) . .
C9 C8 C14 O16 -30.77(2) . .
C13 C8 C14 O16 160.499(15) . .
O8 C15 C16 C17 176.565(9) . .
O7 C15 C16 C17 -0.388(15) . .
O8 C15 C16 C21 -1.865(15) . .
O7 C15 C16 C21 -178.818(10) . .
C21 C16 C17 C18 0.0 . .
C15 C16 C17 C18 -178.4 . .
C16 C17 C18 C19 0.0 . .
C17 C18 C19 C20 0.0 . .
C17 C18 C19 C22 177.8 . .
C18 C19 C20 C21 0.0 . .
C22 C19 C20 C21 -177.7 . .
C19 C20 C21 C16 0.0 . .
C17 C16 C21 C20 0.0 . .
C15 C16 C21 C20 178.4 . .
C20 C19 C22 C27 27.9 . .
C18 C19 C22 C27 -149.9 . .
C20 C19 C22 C23 -140.7 . .
C18 C19 C22 C23 41.5 . .
C27 C22 C23 C24 8.1 . .
C19 C22 C23 C24 176.9 . .
C22 C23 C24 C25 -2.6 . .
C23 C24 C25 C26 -3.0 . .
C23 C24 C25 C28 179.1 . .
C24 C25 C26 C27 3.0 . .
C28 C25 C26 C27 -179.0 . .
C23 C22 C27 C26 -7.6 . .
C19 C22 C27 C26 -176.5 . .
C25 C26 C27 C22 2.4 . .
C26 C25 C28 O5 172.772(11) . .
C24 C25 C28 O5 -9.326(18) . .
C26 C25 C28 O6 1.009(15) . .
C24 C25 C28 O6 178.911(9) . .
O1 C29 C30 C31 174.839(11) . .
O2 C29 C30 C31 -3.396(15) . .
O1 C29 C30 C35 -9.155(16) . .
O2 C29 C30 C35 172.610(10) . .
C35 C30 C31 C32 0.0 . .
C29 C30 C31 C32 176.0 . .
C30 C31 C32 C33 0.0 . .
C31 C32 C33 C34 0.0 . .
C31 C32 C33 C36 -174.0 . .
C32 C33 C34 C35 0.0 . .
C36 C33 C34 C35 173.9 . .
C33 C34 C35 C30 0.0 . .
C31 C30 C35 C34 0.0 . .
C29 C30 C35 C34 -176.1 . .
C34 C33 C36 C41 31.4 . .
C32 C33 C36 C41 -154.7 . .
C34 C33 C36 C37 -146.7 . .
C32 C33 C36 C37 27.2 . .
C41 C36 C37 C38 -2.2 . .
C33 C36 C37 C38 175.9 . .
C36 C37 C38 C39 1.6 . .
C37 C38 C39 C40 -0.4 . .
C37 C38 C39 C42 -178.1 . .
C38 C39 C40 C41 -0.2 . .
C42 C39 C40 C41 177.5 . .
C37 C36 C41 C40 1.5 . .
C33 C36 C41 C40 -176.7 . .
C39 C40 C41 C36 -0.3 . .
C38 C39 C42 O3 -6.395(17) . .
C40 C39 C42 O3 175.935(10) . .
C38 C39 C42 O4 169.347(12) . .
C40 C39 C42 O4 -8.324(17) . .
O11 C43 C44 C45 -5.425(15) . .
O12 C43 C44 C45 173.309(9) . .
O11 C43 C44 C49 173.800(9) . .
O12 C43 C44 C49 -7.466(14) . .
C49 C44 C45 C46 0.0 . .
C43 C44 C45 C46 179.2 . .
C44 C45 C46 C47 0.0 . .
C45 C46 C47 C48 0.0 . .
C45 C46 C47 C50 178.0 . .
C46 C47 C48 C49 0.0 . .
C50 C47 C48 C49 -178.0 . .
C47 C48 C49 C44 0.0 . .
C45 C44 C49 C48 0.0 . .
C43 C44 C49 C48 -179.2 . .
C48 C47 C50 C55 141.0 . .
C46 C47 C50 C55 -37.0 . .
C48 C47 C50 C51 -37.3 . .
C46 C47 C50 C51 144.7 . .
C55 C50 C51 C52 5.6 . .
C47 C50 C51 C52 -176.1 . .
C50 C51 C52 C53 -2.3 . .
C51 C52 C53 C54 -1.7 . .
C51 C52 C53 C56 -175.5 . .
C52 C53 C54 C55 2.7 . .
C56 C53 C54 C55 176.2 . .
C51 C50 C55 C54 -4.7 . .
C47 C50 C55 C54 177.1 . .
C53 C54 C55 C50 0.4 . .
C54 C53 C56 O14 -166.105(12) . .
C52 C53 C56 O14 7.068(17) . .
C54 C53 C56 O13 13.409(16) . .
C52 C53 C56 O13 -173.419(9) . .
O2 C29 O1 Co3 150.05(4) . .
C30 C29 O1 Co3 -28.10(5) . .
O2 C29 O1 Co2 -1.131(14) . .
C30 C29 O1 Co2 -179.276(12) . .
O5 Co3 O1 C29 -19.43(4) 4_576 .
O14 Co3 O1 C29 162.11(4) 4_565 .
O12 Co3 O1 C29 -112.04(5) . .
O7 Co3 O1 C29 67.89(5) . .
O3 Co3 O1 C29 154.50(13) 1_545 .
O5 Co3 O1 Co2 130.222(16) 4_576 .
O14 Co3 O1 Co2 -48.242(16) 4_565 .
O12 Co3 O1 Co2 37.604(18) . .
O7 Co3 O1 Co2 -142.465(18) . .
O3 Co3 O1 Co2 -55.85(15) 1_545 .
O15 Co2 O1 C29 -1.970(19) 1_655 .
O11 Co2 O1 C29 114.11(2) . .
O13 Co2 O1 C29 -128.095(14) 4_565 .
O2 Co2 O1 C29 0.683(8) . .
O15 Co2 O1 Co3 -175.151(13) 1_655 .
O11 Co2 O1 Co3 -59.067(18) . .
O13 Co2 O1 Co3 58.724(15) 4_565 .
O2 Co2 O1 Co3 -172.498(8) . .
O1 C29 O2 Co2 1.303(16) . .
C30 C29 O2 Co2 179.528(9) . .
O15 Co2 O2 C29 178.416(9) 1_655 .
O11 Co2 O2 C29 -79.042(17) . .
O13 Co2 O2 C29 66.618(16) 4_565 .
O1 Co2 O2 C29 -0.679(8) . .
O4 C42 O3 Co3 130.52(3) . 1_565
C39 C42 O3 Co3 -53.63(4) . 1_565
O4 C42 O3 Co1 3.244(13) . 1_565
C39 C42 O3 Co1 179.096(12) . 1_565
O3 C42 O4 Co1 -3.847(16) . 1_565
C39 C42 O4 Co1 -179.641(10) . 1_565
O6 C28 O5 Co3 -17.55(3) . 4_575
C25 C28 O5 Co3 171.984(14) . 4_575
O5 C28 O6 Co1 8.42(2) . 4_575
C25 C28 O6 Co1 178.948(8) . 4_575
O8 C15 O7 Co3 48.17(3) . .
C16 C15 O7 Co3 -135.173(16) . .
O5 Co3 O7 C15 -105.48(3) 4_576 .
O14 Co3 O7 C15 72.17(3) 4_565 .
O12 Co3 O7 C15 180(21) . .
O1 Co3 O7 C15 159.908(16) . .
O3 Co3 O7 C15 -18.499(16) 1_545 .
O7 C15 O8 Co1 3.67(2) . .
C16 C15 O8 Co1 -173.023(8) . .
O9 Co1 O8 C15 144.10(2) . .
O6 Co1 O8 C15 41.918(14) 4_576 .
O4 Co1 O8 C15 -100.90(3) 1_545 .
O3 Co1 O8 C15 -52.51(3) 1_545 .
O10 C1 O9 Co1 6.16(3) . .
C7 C1 O9 Co1 176.749(10) . .
O8 Co1 O9 C1 56.59(4) . .
O6 Co1 O9 C1 173.875(13) 4_576 .
O4 Co1 O9 C1 -71.60(3) 1_545 .
O3 Co1 O9 C1 -67.95(3) 1_545 .
O12 C43 O11 Co2 -1.32(2) . .
C44 C43 O11 Co2 177.245(7) . .
O15 Co2 O11 C43 -152.048(19) 1_655 .
O13 Co2 O11 C43 -45.833(14) 4_565 .
O2 Co2 O11 C43 101.57(2) . .
O1 Co2 O11 C43 45.49(3) . .
O11 C43 O12 Co3 -41.60(3) . .
C44 C43 O12 Co3 139.824(14) . .
O5 Co3 O12 C43 -82.55(3) 4_576 .
O14 Co3 O12 C43 99.81(3) 4_565 .
O7 Co3 O12 C43 -7.9(15) . .
O1 Co3 O12 C43 12.061(16) . .
O3 Co3 O12 C43 -169.531(16) 1_545 .
O14 C56 O13 Co2 -10.97(2) . 4_566
C53 C56 O13 Co2 169.582(9) . 4_566
O13 C56 O14 Co3 -4.08(3) . 4_566
C53 C56 O14 Co3 175.341(12) . 4_566
O16 C14 O15 Co2 16.82(3) . 1_455
C8 C14 O15 Co2 171.083(14) . 1_455
