#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:24:26 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179629 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/93/4509330.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4509330
loop_
_publ_author_name
'Li, Zuo-Xi'
'Xu, Yao'
'Zuo, Yi'
'Li, Lei'
'Pan, Qinhe'
'Hu, Tong-Liang'
'Bu, Xian-He'
_publ_section_title
;
 Varying Ligand Backbones for Modulating the Interpenetration of
 Coordination Polymers Based on Homoleptic Cobalt(II) Nodes
;
_journal_issue                   9
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              3904
_journal_paper_doi               10.1021/cg801250g
_journal_volume                  9
_journal_year                    2009
_chemical_formula_sum            'C38 H32 Cl8 Co N12 O8'
_chemical_formula_weight         1127.29
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 111.81(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   8.0960(16)
_cell_length_b                   21.507(4)
_cell_length_c                   13.935(5)
_cell_measurement_reflns_used    6897
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      27.9524
_cell_measurement_theta_min      1.8369
_cell_volume                     2252.7(11)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0382
_diffrn_reflns_av_sigmaI/netI    0.0295
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            22716
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         1.84
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_exptl_absorpt_coefficient_mu    0.922
_exptl_absorpt_correction_T_max  0.871
_exptl_absorpt_correction_T_min  0.832
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   CrystalClear
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.662
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1142
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.490
_refine_diff_density_min         -0.526
_refine_diff_density_rms         0.065
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     336
_refine_ls_number_reflns         3971
_refine_ls_number_restraints     20
_refine_ls_restrained_S_all      1.139
_refine_ls_R_factor_all          0.0419
_refine_ls_R_factor_gt           0.0393
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0318P)²+3.9612P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0879
_refine_ls_wR_factor_ref         0.0896
_reflns_number_gt                3762
_reflns_number_total             3980
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg801250gsup1.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        2252.7(10)
_cod_original_sg_symbol_H-M      p21/c
_cod_database_code               4509330
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 1.0000 0.5000 0.5000 0.00925(13) Uani 1 2 d S . .
N1 N 0.7604(3) 0.54506(10) 0.39994(16) 0.0135(4) Uani 1 1 d . . .
N2 N 0.5732(3) 0.61258(10) 0.29665(17) 0.0172(5) Uani 1 1 d . . .
N5 N 0.9460(3) 0.52862(10) 0.63624(15) 0.0122(4) Uani 1 1 d . . .
N6 N 0.9356(3) 0.53108(10) 0.79280(16) 0.0140(4) Uani 1 1 d . . .
N4 N 0.1486(3) 0.91560(9) 0.01008(16) 0.0128(4) Uani 1 1 d . . .
N3 N 0.3062(3) 0.83074(10) 0.07222(17) 0.0174(5) Uani 1 1 d . . .
C1 C 0.7411(3) 0.60195(12) 0.3635(2) 0.0165(5) Uani 1 1 d . . .
H1A H 0.8317 0.6314 0.3814 0.020 Uiso 1 1 calc R . .
C2 C 0.5940(3) 0.51780(13) 0.3547(2) 0.0173(6) Uani 1 1 d . . .
H2A H 0.5660 0.4773 0.3667 0.021 Uiso 1 1 calc R . .
C3 C 0.4788(4) 0.55866(13) 0.2906(2) 0.0198(6) Uani 1 1 d . . .
H3A H 0.3596 0.5517 0.2505 0.024 Uiso 1 1 calc R . .
C4 C 0.5062(4) 0.66929(12) 0.2420(2) 0.0180(6) Uani 1 1 d . . .
C9 C 0.3348(4) 0.68828(13) 0.2265(2) 0.0208(6) Uani 1 1 d . . .
H9A H 0.2645 0.6649 0.2527 0.025 Uiso 1 1 calc R . .
C5 C 0.6134(4) 0.70385(13) 0.2045(2) 0.0209(6) Uani 1 1 d . . .
H5A H 0.7280 0.6905 0.2148 0.025 Uiso 1 1 calc R . .
C6 C 0.5481(4) 0.75850(13) 0.1516(2) 0.0203(6) Uani 1 1 d . . .
H6A H 0.6199 0.7829 0.1278 0.024 Uiso 1 1 calc R . .
C13 C 1.0116(3) 0.50526(12) 0.73051(19) 0.0142(5) Uani 1 1 d . . .
H13A H 1.0993 0.4748 0.7516 0.017 Uiso 1 1 calc R . .
C14 C 0.8224(4) 0.57231(12) 0.6389(2) 0.0175(6) Uani 1 1 d . . .
H14A H 0.7538 0.5966 0.5831 0.021 Uiso 1 1 calc R . .
C15 C 0.8156(4) 0.57469(13) 0.7341(2) 0.0189(6) Uani 1 1 d . . .
H15A H 0.7443 0.6006 0.7558 0.023 Uiso 1 1 calc R . .
C16 C 0.9690(3) 0.51518(12) 0.89857(19) 0.0150(5) Uani 1 1 d . . .
C17 C 1.0253(3) 0.45564(12) 0.9344(2) 0.0167(5) Uani 1 1 d . . .
H17A H 1.0419 0.4261 0.8901 0.020 Uiso 1 1 calc R . .
C18 C 0.9431(4) 0.55964(13) 0.9637(2) 0.0175(5) Uani 1 1 d . . .
H18A H 0.9049 0.5994 0.9392 0.021 Uiso 1 1 calc R . .
C10 C 0.1849(3) 0.87145(12) 0.0806(2) 0.0163(5) Uani 1 1 d . . .
H10A H 0.1334 0.8686 0.1300 0.020 Uiso 1 1 calc R . .
C12 C 0.2533(4) 0.90206(13) -0.0462(2) 0.0214(6) Uani 1 1 d . . .
H12A H 0.2565 0.9254 -0.1017 0.026 Uiso 1 1 calc R . .
C11 C 0.3503(4) 0.85023(14) -0.0096(2) 0.0231(6) Uani 1 1 d . . .
H11A H 0.4302 0.8315 -0.0343 0.028 Uiso 1 1 calc R . .
C7 C 0.3757(4) 0.77666(12) 0.1342(2) 0.0176(6) Uani 1 1 d . . .
C8 C 0.2687(4) 0.74233(13) 0.1715(2) 0.0206(6) Uani 1 1 d . . .
H8A H 0.1533 0.7553 0.1599 0.025 Uiso 1 1 calc R . .
Cl1 Cl 0.80448(10) 0.76059(4) 0.48113(7) 0.0366(2) Uani 1 1 d D . .
Cl2 Cl 0.43259(12) 0.91529(5) 0.33567(6) 0.0427(2) Uani 1 1 d . . .
Cl3 Cl 0.43543(13) 0.93030(4) 0.54096(7) 0.0424(2) Uani 1 1 d . . .
Cl4 Cl 0.23018(12) 0.83091(4) 0.41183(8) 0.0449(2) Uani 1 1 d . . .
C19 C 0.4241(4) 0.87562(15) 0.4448(2) 0.0307(7) Uani 1 1 d . . .
H19A H 0.5273 0.8479 0.4715 0.037 Uiso 1 1 calc R . .
O1 O 0.8403(6) 0.81478(19) 0.5464(3) 0.0305(10) Uani 0.765(6) 1 d PD A 1
O3 O 0.8543(4) 0.70643(14) 0.5542(3) 0.0525(12) Uani 0.765(6) 1 d PD A 1
O4 O 0.6165(4) 0.75478(17) 0.4270(2) 0.0365(9) Uani 0.765(6) 1 d PD A 1
O2 O 0.9051(7) 0.7574(3) 0.4202(4) 0.069(2) Uani 0.765(6) 1 d PD A 1
O3' O 0.7164(16) 0.8047(4) 0.3855(6) 0.060(4) Uani 0.235(6) 1 d PD A 2
O4' O 0.6850(13) 0.7149(4) 0.4698(8) 0.042(3) Uani 0.235(6) 1 d PD A 2
O2' O 0.9540(15) 0.7397(7) 0.4545(12) 0.052(5) Uani 0.235(6) 1 d PD A 2
O1' O 0.8595(19) 0.8000(5) 0.5649(7) 0.031(5) Uiso 0.235(6) 1 d PD A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Co1 N1 180.0 3_766 .
N1 Co1 N4 90.56(8) 3_766 2_645
N1 Co1 N4 89.44(8) . 2_645
N1 Co1 N4 89.44(8) 3_766 4_676
N1 Co1 N4 90.56(8) . 4_676
N4 Co1 N4 180.0 2_645 4_676
N1 Co1 N5 89.25(8) 3_766 .
N1 Co1 N5 90.75(8) . .
N4 Co1 N5 90.40(8) 2_645 .
N4 Co1 N5 89.60(8) 4_676 .
N1 Co1 N5 90.75(8) 3_766 3_766
N1 Co1 N5 89.25(8) . 3_766
N4 Co1 N5 89.60(8) 2_645 3_766
N4 Co1 N5 90.40(8) 4_676 3_766
N5 Co1 N5 180.00(4) . 3_766
C1 N1 C2 105.2(2) . .
C1 N1 Co1 128.31(18) . .
C2 N1 Co1 126.39(17) . .
C1 N2 C3 107.1(2) . .
C1 N2 C4 126.6(2) . .
C3 N2 C4 126.4(2) . .
C13 N5 C14 105.1(2) . .
C13 N5 Co1 128.32(17) . .
C14 N5 Co1 126.43(17) . .
C13 N6 C15 106.6(2) . .
C13 N6 C16 127.0(2) . .
C15 N6 C16 126.4(2) . .
C10 N4 C12 104.9(2) . .
C10 N4 Co1 128.35(17) . 2_655
C12 N4 Co1 125.85(17) . 2_655
C10 N3 C11 107.0(2) . .
C10 N3 C7 127.5(2) . .
C11 N3 C7 125.5(2) . .
N1 C1 N2 111.7(2) . .
N1 C1 H1A 124.1 . .
N2 C1 H1A 124.1 . .
C3 C2 N1 110.0(2) . .
C3 C2 H2A 125.0 . .
N1 C2 H2A 125.0 . .
C2 C3 N2 106.1(2) . .
C2 C3 H3A 127.0 . .
N2 C3 H3A 127.0 . .
C9 C4 C5 121.0(2) . .
C9 C4 N2 119.6(2) . .
C5 C4 N2 119.4(2) . .
C4 C9 C8 119.5(3) . .
C4 C9 H9A 120.2 . .
C8 C9 H9A 120.2 . .
C6 C5 C4 119.2(3) . .
C6 C5 H5A 120.4 . .
C4 C5 H5A 120.4 . .
C7 C6 C5 119.6(3) . .
C7 C6 H6A 120.2 . .
C5 C6 H6A 120.2 . .
N5 C13 N6 111.8(2) . .
N5 C13 H13A 124.1 . .
N6 C13 H13A 124.1 . .
C15 C14 N5 110.3(2) . .
C15 C14 H14A 124.9 . .
N5 C14 H14A 124.9 . .
C14 C15 N6 106.3(2) . .
C14 C15 H15A 126.8 . .
N6 C15 H15A 126.8 . .
C18 C16 C17 120.6(2) . .
C18 C16 N6 119.4(2) . .
C17 C16 N6 120.0(2) . .
C18 C17 C16 119.9(2) 3_767 .
C18 C17 H17A 120.0 3_767 .
C16 C17 H17A 120.0 . .
C17 C18 C16 119.5(3) 3_767 .
C17 C18 H18A 120.3 3_767 .
C16 C18 H18A 120.3 . .
N4 C10 N3 111.7(2) . .
N4 C10 H10A 124.1 . .
N3 C10 H10A 124.1 . .
C11 C12 N4 110.6(2) . .
C11 C12 H12A 124.7 . .
N4 C12 H12A 124.7 . .
C12 C11 N3 105.7(2) . .
C12 C11 H11A 127.1 . .
N3 C11 H11A 127.1 . .
C8 C7 C6 121.2(2) . .
C8 C7 N3 120.1(2) . .
C6 C7 N3 118.7(2) . .
C7 C8 C9 119.3(3) . .
C7 C8 H8A 120.3 . .
C9 C8 H8A 120.3 . .
O2 Cl1 O4 115.2(3) . .
O2 Cl1 O1 113.7(3) . .
O4 Cl1 O1 109.2(2) . .
O2 Cl1 O3 107.9(3) . .
O4 Cl1 O3 104.8(2) . .
O1 Cl1 O3 105.0(2) . .
O4' Cl1 O3' 105.1(6) . .
O1' Cl1 O3' 104.4(5) . .
O2' Cl1 O3' 97.3(6) . .
O4' Cl1 O1' 122.8(7) . .
O4' Cl1 O2' 111.9(7) . .
O1' Cl1 O2' 111.5(7) . .
Cl4 C19 Cl3 110.76(18) . .
Cl4 C19 Cl2 110.94(18) . .
Cl3 C19 Cl2 108.97(18) . .
Cl4 C19 H19A 108.7 . .
Cl3 C19 H19A 108.7 . .
Cl2 C19 H19A 108.7 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 N1 2.153(2) 3_766
Co1 N1 2.153(2) .
Co1 N4 2.153(2) 2_645
Co1 N4 2.153(2) 4_676
Co1 N5 2.189(2) .
Co1 N5 2.189(2) 3_766
N1 C1 1.312(3) .
N1 C2 1.388(3) .
N2 C1 1.351(3) .
N2 C3 1.374(4) .
N2 C4 1.433(3) .
N5 C13 1.320(3) .
N5 C14 1.383(3) .
N6 C13 1.355(3) .
N6 C15 1.379(3) .
N6 C16 1.438(3) .
N4 C10 1.318(3) .
N4 C12 1.383(3) .
N4 Co1 2.153(2) 2_655
N3 C10 1.352(3) .
N3 C11 1.380(4) .
N3 C7 1.433(3) .
C1 H1A 0.9300 .
C2 C3 1.349(4) .
C2 H2A 0.9300 .
C3 H3A 0.9300 .
C4 C9 1.384(4) .
C4 C5 1.385(4) .
C9 C8 1.386(4) .
C9 H9A 0.9300 .
C5 C6 1.384(4) .
C5 H5A 0.9300 .
C6 C7 1.382(4) .
C6 H6A 0.9300 .
C13 H13A 0.9300 .
C14 C15 1.348(4) .
C14 H14A 0.9300 .
C15 H15A 0.9300 .
C16 C18 1.387(4) .
C16 C17 1.388(4) .
C17 C18 1.385(4) 3_767
C17 H17A 0.9300 .
C18 C17 1.385(4) 3_767
C18 H18A 0.9300 .
C10 H10A 0.9300 .
C12 C11 1.350(4) .
C12 H12A 0.9300 .
C11 H11A 0.9300 .
C7 C8 1.378(4) .
C8 H8A 0.9300 .
Cl1 O1' 1.376(7) .
Cl1 O2' 1.463(8) .
Cl1 O3' 1.574(7) .
Cl1 O4' 1.346(6) .
Cl1 O1 1.440(3) .
Cl1 O2 1.379(4) .
Cl1 O3 1.500(3) .
Cl1 O4 1.431(3) .
Cl2 C19 1.767(3) .
Cl3 C19 1.760(3) .
Cl4 C19 1.751(3) .
C19 H19A 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N1 Co1 N1 C1 -2(100) 3_766 .
N4 Co1 N1 C1 -177.3(2) 2_645 .
N4 Co1 N1 C1 2.7(2) 4_676 .
N5 Co1 N1 C1 92.3(2) . .
N5 Co1 N1 C1 -87.7(2) 3_766 .
N1 Co1 N1 C2 174(100) 3_766 .
N4 Co1 N1 C2 -1.9(2) 2_645 .
N4 Co1 N1 C2 178.1(2) 4_676 .
N5 Co1 N1 C2 -92.3(2) . .
N5 Co1 N1 C2 87.7(2) 3_766 .
N1 Co1 N5 C13 -19.3(2) 3_766 .
N1 Co1 N5 C13 160.7(2) . .
N4 Co1 N5 C13 71.3(2) 2_645 .
N4 Co1 N5 C13 -108.7(2) 4_676 .
N5 Co1 N5 C13 -140(100) 3_766 .
N1 Co1 N5 C14 166.7(2) 3_766 .
N1 Co1 N5 C14 -13.3(2) . .
N4 Co1 N5 C14 -102.8(2) 2_645 .
N4 Co1 N5 C14 77.2(2) 4_676 .
N5 Co1 N5 C14 46(100) 3_766 .
C2 N1 C1 N2 -0.8(3) . .
Co1 N1 C1 N2 175.33(16) . .
C3 N2 C1 N1 0.4(3) . .
C4 N2 C1 N1 -179.5(2) . .
C1 N1 C2 C3 1.0(3) . .
Co1 N1 C2 C3 -175.26(18) . .
N1 C2 C3 N2 -0.8(3) . .
C1 N2 C3 C2 0.3(3) . .
C4 N2 C3 C2 -179.9(2) . .
C1 N2 C4 C9 -142.8(3) . .
C3 N2 C4 C9 37.4(4) . .
C1 N2 C4 C5 37.9(4) . .
C3 N2 C4 C5 -141.9(3) . .
C5 C4 C9 C8 0.7(4) . .
N2 C4 C9 C8 -178.5(2) . .
C9 C4 C5 C6 0.6(4) . .
N2 C4 C5 C6 179.8(2) . .
C4 C5 C6 C7 -2.0(4) . .
C14 N5 C13 N6 0.6(3) . .
Co1 N5 C13 N6 -174.43(16) . .
C15 N6 C13 N5 -1.1(3) . .
C16 N6 C13 N5 177.2(2) . .
C13 N5 C14 C15 0.1(3) . .
Co1 N5 C14 C15 175.30(18) . .
N5 C14 C15 N6 -0.8(3) . .
C13 N6 C15 C14 1.1(3) . .
C16 N6 C15 C14 -177.3(2) . .
C13 N6 C16 C18 153.2(3) . .
C15 N6 C16 C18 -28.7(4) . .
C13 N6 C16 C17 -27.2(4) . .
C15 N6 C16 C17 150.8(3) . .
C18 C16 C17 C18 -0.3(4) . 3_767
N6 C16 C17 C18 -179.8(2) . 3_767
C17 C16 C18 C17 0.3(4) . 3_767
N6 C16 C18 C17 179.8(2) . 3_767
C12 N4 C10 N3 -0.1(3) . .
Co1 N4 C10 N3 -169.47(17) 2_655 .
C11 N3 C10 N4 -0.1(3) . .
C7 N3 C10 N4 -179.1(2) . .
C10 N4 C12 C11 0.2(3) . .
Co1 N4 C12 C11 169.97(19) 2_655 .
N4 C12 C11 N3 -0.3(3) . .
C10 N3 C11 C12 0.2(3) . .
C7 N3 C11 C12 179.2(3) . .
C5 C6 C7 C8 2.1(4) . .
C5 C6 C7 N3 -175.1(2) . .
C10 N3 C7 C8 34.1(4) . .
C11 N3 C7 C8 -144.7(3) . .
C10 N3 C7 C6 -148.6(3) . .
C11 N3 C7 C6 32.6(4) . .
C6 C7 C8 C9 -0.7(4) . .
N3 C7 C8 C9 176.5(2) . .
C4 C9 C8 C7 -0.7(4) . .
