#------------------------------------------------------------------------------
#$Date: 2016-03-24 03:26:43 +0200 (Thu, 24 Mar 2016) $
#$Revision: 179631 $
#$URL: svn://www.crystallography.net/cod/cif/4/50/95/4509564.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided the Crystal Eye server at
# http://wwmm.ch.cam.ac.uk/crystaleye/, created by Nick Day at the
# Peter Murray-Rust laboratory.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_4509564
loop_
_publ_author_name
'Meng, Jing-Xin'
'Lu, Ying'
'Li, Yang-Guang'
'Fu, Hai'
'Wang, En-Bo'
_publ_section_title
;
 Base-Directed Self-Assembly of Octamolybdate-Based Frameworks Decorated
 by Flexible N-Containing Ligands
;
_journal_issue                   9
_journal_name_full               'Crystal Growth & Design'
_journal_page_first              4116
_journal_paper_doi               10.1021/cg900352e
_journal_volume                  9
_journal_year                    2009
_chemical_formula_sum            'C26 H30 Cu2 Mo4 N4 O14'
_chemical_formula_weight         1133.38
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                94.38(3)
_cell_angle_beta                 110.47(3)
_cell_angle_gamma                103.46(3)
_cell_formula_units_Z            2
_cell_length_a                   10.615(2)
_cell_length_b                   13.366(3)
_cell_length_c                   13.440(3)
_cell_measurement_reflns_used    12303
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.00
_cell_measurement_theta_min      2.99
_cell_volume                     1711.1(8)
_computing_cell_refinement       'RAPID AUTO'
_computing_data_collection       'RAPID AUTO'
_computing_data_reduction        'RAPID AUTO'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 0.01
_diffrn_measured_fraction_theta_full 0.947
_diffrn_measured_fraction_theta_max 0.947
_diffrn_measurement_device_type  'Rigaku RAXIS RAPID IP'
_diffrn_measurement_method       Oscillation
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rotation anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0719
_diffrn_reflns_av_sigmaI/netI    0.0999
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            12303
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.99
_exptl_absorpt_coefficient_mu    2.713
_exptl_absorpt_correction_T_max  0.648
_exptl_absorpt_correction_T_min  0.556
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'ABSCOR by T.Higashi    8 March, 1995'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.200
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1104
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.16
_refine_diff_density_max         1.892
_refine_diff_density_min         -3.157
_refine_diff_density_rms         0.310
_refine_ls_extinction_coef       0.0022(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     452
_refine_ls_number_reflns         5719
_refine_ls_number_restraints     48
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.1070
_refine_ls_R_factor_gt           0.0663
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1103P)²+36.1672P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1621
_refine_ls_wR_factor_ref         0.2296
_reflns_number_gt                3730
_reflns_number_total             5719
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg900352esup2.cif
_cod_data_source_block           k
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        1711.1(6)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4509564
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Mo1 Mo 0.17119(12) 0.99831(10) -0.00162(10) 0.0215(4) Uani 1 1 d .
Mo2 Mo 0.14574(13) 1.16171(10) 0.24207(11) 0.0240(4) Uani 1 1 d .
Mo3 Mo -0.08316(13) 0.74503(10) -0.00918(10) 0.0239(4) Uani 1 1 d .
Mo4 Mo 0.07177(12) 0.90294(10) 0.23311(10) 0.0228(4) Uani 1 1 d .
Cu1 Cu 0.5587(2) 1.13885(17) 0.07953(17) 0.0368(5) Uani 1 1 d .
Cu2 Cu 0.1571(2) 0.54709(17) 0.06437(16) 0.0366(5) Uani 1 1 d .
O1 O 0.1859(10) 0.8316(9) 0.2767(9) 0.033(3) Uani 1 1 d .
O2 O 0.1853(10) 1.1195(8) 0.0686(9) 0.030(2) Uani 1 1 d .
O3 O 0.3323(10) 0.9942(8) -0.0008(8) 0.027(2) Uani 1 1 d U
O4 O -0.0864(10) 0.8026(8) 0.1193(7) 0.023(2) Uani 1 1 d U
O5 O 0.3057(11) 1.2489(9) 0.2921(9) 0.032(3) Uani 1 1 d .
O6 O 0.0445(10) 1.2285(8) 0.1365(8) 0.027(2) Uani 1 1 d .
O7 O 0.0089(11) 0.9140(9) 0.3340(8) 0.031(2) Uani 1 1 d .
O8 O 0.0776(12) 1.1758(9) 0.3381(10) 0.040(3) Uani 1 1 d .
O9 O 0.1093(10) 0.8976(8) 0.0631(8) 0.026(2) Uani 1 1 d .
O10 O 0.0241(11) 0.6657(9) 0.0330(9) 0.034(3) Uani 1 1 d .
O11 O 0.2009(9) 1.0373(8) 0.2591(8) 0.023(2) Uani 1 1 d .
O12 O -0.2461(11) 0.6619(8) -0.0619(9) 0.031(2) Uani 1 1 d .
O13 O -0.0544(9) 1.0169(7) 0.1346(7) 0.019(2) Uani 1 1 d U
N1 N 0.6065(13) 1.0911(12) 0.2146(10) 0.034(3) Uani 1 1 d .
N2 N 0.5255(13) 1.2001(10) -0.0458(11) 0.031(3) Uani 1 1 d .
N3 N 0.1590(14) 0.5327(11) 0.2043(10) 0.032(3) Uani 1 1 d .
N4 N 0.2066(13) 0.5571(10) -0.0592(11) 0.031(3) Uani 1 1 d .
C1 C 0.7260(17) 1.0637(14) 0.2561(15) 0.039(4) Uani 1 1 d .
H1A H 0.7951 1.0843 0.2284 0.047 Uiso 1 1 calc R
C2 C 0.7489(15) 1.0082(15) 0.3353(15) 0.043(5) Uani 1 1 d .
H2A H 0.8324 0.9897 0.3598 0.051 Uiso 1 1 calc R
C3 C 0.6515(16) 0.9767(13) 0.3834(12) 0.031(4) Uani 1 1 d U
C4 C 0.5310(17) 1.0073(15) 0.3406(15) 0.042(4) Uani 1 1 d .
H4A H 0.4618 0.9893 0.3686 0.050 Uiso 1 1 calc R
C5 C 0.5103(16) 1.0631(14) 0.2587(12) 0.033(4) Uani 1 1 d .
H5A H 0.4275 1.0823 0.2324 0.039 Uiso 1 1 calc R
C6 C 0.6744(17) 0.9131(13) 0.4711(12) 0.032(4) Uani 1 1 d U
H6A H 0.6719 0.9520 0.5340 0.039 Uiso 1 1 calc R
H6B H 0.7673 0.9035 0.4905 0.039 Uiso 1 1 calc R
C7 C 0.6146(14) 1.2102(11) -0.0980(12) 0.027(3) Uani 1 1 d .
H7A H 0.7011 1.1982 -0.0639 0.032 Uiso 1 1 calc R
C8 C 0.5842(18) 1.2377(13) -0.2003(13) 0.035(4) Uani 1 1 d .
H8A H 0.6481 1.2426 -0.2338 0.042 Uiso 1 1 calc R
C9 C 0.4605(17) 1.2567(13) -0.2489(13) 0.035(4) Uani 1 1 d U
C10 C 0.3653(17) 1.2484(14) -0.2005(16) 0.044(5) Uani 1 1 d .
H10A H 0.2787 1.2601 -0.2350 0.053 Uiso 1 1 calc R
C11 C 0.4020(16) 1.2217(13) -0.0978(16) 0.038(4) Uani 1 1 d .
H11A H 0.3394 1.2185 -0.0633 0.045 Uiso 1 1 calc R
C12 C 0.418(2) 1.2786(18) -0.3663(15) 0.053(5) Uani 1 1 d .
H12A H 0.3217 1.2813 -0.3925 0.063 Uiso 1 1 calc R
H12B H 0.4763 1.3463 -0.3665 0.063 Uiso 1 1 calc R
C13 C 0.433(2) 1.1959(19) -0.4426(18) 0.064(7) Uani 1 1 d .
H13A H 0.5264 1.1871 -0.4105 0.077 Uiso 1 1 calc R
H13B H 0.4263 1.2221 -0.5091 0.077 Uiso 1 1 calc R
C14 C 0.1038(17) 0.5897(12) 0.2557(12) 0.029(4) Uani 1 1 d .
H14A H 0.0540 0.6325 0.2176 0.035 Uiso 1 1 calc R
C15 C 0.1162(19) 0.5887(14) 0.3621(14) 0.043(4) Uani 1 1 d .
H15A H 0.0764 0.6304 0.3934 0.051 Uiso 1 1 calc R
C16 C 0.1877(18) 0.5256(13) 0.4203(14) 0.036(4) Uani 1 1 d .
C17 C 0.244(2) 0.4682(14) 0.3685(15) 0.045(5) Uani 1 1 d .
H17A H 0.2949 0.4252 0.4056 0.055 Uiso 1 1 calc R
C18 C 0.2293(18) 0.4719(13) 0.2625(13) 0.037(4) Uani 1 1 d .
H18A H 0.2691 0.4309 0.2304 0.045 Uiso 1 1 calc R
C19 C 0.216(2) 0.5311(14) 0.5374(13) 0.042(4) Uani 1 1 d U
H19A H 0.2468 0.4713 0.5615 0.050 Uiso 1 1 calc R
H19B H 0.1297 0.5281 0.5489 0.050 Uiso 1 1 calc R
C20 C 0.330(2) 0.6337(18) 0.6058(16) 0.058(5) Uani 1 1 d U
H20A H 0.3972 0.6514 0.5721 0.070 Uiso 1 1 calc R
H20B H 0.2847 0.6895 0.6024 0.070 Uiso 1 1 calc R
C21 C 0.1650(16) 0.6189(13) -0.1300(12) 0.031(4) Uani 1 1 d .
H21A H 0.0951 0.6485 -0.1269 0.037 Uiso 1 1 calc R
C22 C 0.2203(18) 0.6420(15) -0.2085(15) 0.042(4) Uani 1 1 d .
H22A H 0.1861 0.6836 -0.2580 0.051 Uiso 1 1 calc R
C23 C 0.3279(18) 0.6005(15) -0.2102(15) 0.043(5) Uani 1 1 d .
C24 C 0.3664(18) 0.5336(14) -0.1405(15) 0.041(4) Uani 1 1 d .
H24A H 0.4338 0.5011 -0.1435 0.049 Uiso 1 1 calc R
C25 C 0.3063(19) 0.5146(14) -0.0668(15) 0.040(4) Uani 1 1 d .
H25A H 0.3359 0.4699 -0.0195 0.048 Uiso 1 1 calc R
C26 C 0.404(2) 0.6314(17) -0.2828(14) 0.056(6) Uani 1 1 d .
H26A H 0.4674 0.7006 -0.2507 0.067 Uiso 1 1 calc R
H26B H 0.4621 0.5845 -0.2809 0.067 Uiso 1 1 calc R
OW1 O 0.0299(18) 0.2482(12) 0.5304(11) 0.064(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O3 Mo1 O13 109.4(5) . 2_575
O3 Mo1 O2 109.8(5) . .
O13 Mo1 O2 108.7(4) 2_575 .
O3 Mo1 O9 109.6(5) . .
O13 Mo1 O9 110.5(5) 2_575 .
O2 Mo1 O9 108.7(5) . .
O5 Mo2 O8 104.9(6) . .
O5 Mo2 O6 101.3(5) . .
O8 Mo2 O6 101.3(5) . .
O5 Mo2 O11 99.0(5) . .
O8 Mo2 O11 104.3(5) . .
O6 Mo2 O11 141.8(4) . .
O5 Mo2 O13 162.9(4) . .
O8 Mo2 O13 91.7(5) . .
O6 Mo2 O13 79.2(4) . .
O11 Mo2 O13 72.2(4) . .
O12 Mo3 O10 104.2(5) . .
O12 Mo3 O4 99.1(5) . .
O10 Mo3 O4 102.0(5) . .
O12 Mo3 O6 102.4(5) . 2_575
O10 Mo3 O6 97.4(5) . 2_575
O4 Mo3 O6 146.4(5) . 2_575
O12 Mo3 O2 87.8(4) . 2_575
O10 Mo3 O2 167.1(5) . 2_575
O4 Mo3 O2 80.6(4) . 2_575
O6 Mo3 O2 74.8(4) 2_575 2_575
O12 Mo3 O9 163.6(4) . .
O10 Mo3 O9 91.7(5) . .
O4 Mo3 O9 73.1(4) . .
O6 Mo3 O9 79.2(4) 2_575 .
O2 Mo3 O9 76.8(3) 2_575 .
O1 Mo4 O7 103.8(5) . .
O1 Mo4 O11 99.5(5) . .
O7 Mo4 O11 102.4(5) . .
O1 Mo4 O4 102.4(5) . .
O7 Mo4 O4 102.2(5) . .
O11 Mo4 O4 141.9(4) . .
O1 Mo4 O13 162.6(5) . .
O7 Mo4 O13 92.9(4) . .
O11 Mo4 O13 71.8(3) . .
O4 Mo4 O13 78.3(4) . .
O1 Mo4 O9 89.4(4) . .
O7 Mo4 O9 166.0(4) . .
O11 Mo4 O9 79.7(4) . .
O4 Mo4 O9 69.8(4) . .
O13 Mo4 O9 74.5(3) . .
N2 Cu1 N1 173.8(6) . .
N3 Cu2 N4 164.0(6) . .
N3 Cu2 O10 96.5(5) . .
N4 Cu2 O10 96.7(5) . .
Mo1 O2 Mo3 130.9(6) . 2_575
Mo3 O4 Mo4 124.9(5) . .
Mo2 O6 Mo3 123.8(5) . 2_575
Mo1 O9 Mo3 130.1(5) . .
Mo1 O9 Mo4 131.9(5) . .
Mo3 O9 Mo4 88.5(3) . .
Mo3 O10 Cu2 171.8(6) . .
Mo2 O11 Mo4 123.3(5) . .
Mo1 O13 Mo2 129.8(5) 2_575 .
Mo1 O13 Mo4 132.7(5) 2_575 .
Mo2 O13 Mo4 87.3(3) . .
C1 N1 C5 117.5(14) . .
C1 N1 Cu1 120.3(11) . .
C5 N1 Cu1 120.7(10) . .
C7 N2 C11 115.8(14) . .
C7 N2 Cu1 121.2(10) . .
C11 N2 Cu1 122.2(11) . .
C18 N3 C14 115.6(13) . .
C18 N3 Cu2 121.0(11) . .
C14 N3 Cu2 123.0(11) . .
C21 N4 C25 116.6(14) . .
C21 N4 Cu2 123.4(11) . .
C25 N4 Cu2 119.1(11) . .
C2 C1 N1 122.3(15) . .
C2 C1 H1A 118.8 . .
N1 C1 H1A 118.8 . .
C1 C2 C3 122.2(14) . .
C1 C2 H2A 118.9 . .
C3 C2 H2A 118.9 . .
C4 C3 C2 114.2(15) . .
C4 C3 C6 122.8(16) . .
C2 C3 C6 123.0(14) . .
C5 C4 C3 122.0(16) . .
C5 C4 H4A 119.0 . .
C3 C4 H4A 119.0 . .
N1 C5 C4 121.7(14) . .
N1 C5 H5A 119.2 . .
C4 C5 H5A 119.2 . .
C3 C6 C13 114.9(14) . 2_675
C3 C6 H6A 108.5 . .
C13 C6 H6A 108.5 2_675 .
C3 C6 H6B 108.5 . .
C13 C6 H6B 108.5 2_675 .
H6A C6 H6B 107.5 . .
N2 C7 C8 123.7(14) . .
N2 C7 H7A 118.1 . .
C8 C7 H7A 118.1 . .
C9 C8 C7 118.3(16) . .
C9 C8 H8A 120.9 . .
C7 C8 H8A 120.9 . .
C8 C9 C10 121.1(16) . .
C8 C9 C12 119.6(16) . .
C10 C9 C12 119.0(15) . .
C9 C10 C11 118.0(14) . .
C9 C10 H10A 121.0 . .
C11 C10 H10A 121.0 . .
N2 C11 C10 123.0(15) . .
N2 C11 H11A 118.5 . .
C10 C11 H11A 118.5 . .
C13 C12 C9 112.7(15) . .
C13 C12 H12A 109.1 . .
C9 C12 H12A 109.1 . .
C13 C12 H12B 109.1 . .
C9 C12 H12B 109.1 . .
H12A C12 H12B 107.8 . .
C12 C13 C6 116.3(17) . 2_675
C12 C13 H13A 108.2 . .
C6 C13 H13A 108.2 2_675 .
C12 C13 H13B 108.2 . .
C6 C13 H13B 108.2 2_675 .
H13A C13 H13B 107.4 . .
N3 C14 C15 124.3(15) . .
N3 C14 H14A 117.8 . .
C15 C14 H14A 117.8 . .
C16 C15 C14 119.4(17) . .
C16 C15 H15A 120.3 . .
C14 C15 H15A 120.3 . .
C17 C16 C15 116.4(16) . .
C17 C16 C19 122.6(16) . .
C15 C16 C19 120.6(16) . .
C16 C17 C18 122.0(16) . .
C16 C17 H17A 119.0 . .
C18 C17 H17A 119.0 . .
N3 C18 C17 122.2(15) . .
N3 C18 H18A 118.9 . .
C17 C18 H18A 118.9 . .
C16 C19 C20 111.7(15) . .
C16 C19 H19A 109.3 . .
C20 C19 H19A 109.3 . .
C16 C19 H19B 109.3 . .
C20 C19 H19B 109.3 . .
H19A C19 H19B 107.9 . .
C26 C20 C19 116.6(18) 1_556 .
C26 C20 H20A 108.1 1_556 .
C19 C20 H20A 108.1 . .
C26 C20 H20B 108.1 1_556 .
C19 C20 H20B 108.1 . .
H20A C20 H20B 107.3 . .
N4 C21 C22 123.9(15) . .
N4 C21 H21A 118.0 . .
C22 C21 H21A 118.0 . .
C23 C22 C21 117.6(16) . .
C23 C22 H22A 121.2 . .
C21 C22 H22A 121.2 . .
C24 C23 C22 118.3(16) . .
C24 C23 C26 120.7(17) . .
C22 C23 C26 121.0(19) . .
C25 C24 C23 120.2(16) . .
C25 C24 H24A 119.9 . .
C23 C24 H24A 119.9 . .
N4 C25 C24 123.2(17) . .
N4 C25 H25A 118.4 . .
C24 C25 H25A 118.4 . .
C20 C26 C23 121.0(18) 1_554 .
C20 C26 H26A 107.1 1_554 .
C23 C26 H26A 107.1 . .
C20 C26 H26B 107.1 1_554 .
C23 C26 H26B 107.1 . .
H26A C26 H26B 106.8 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Mo1 O3 1.721(9) .
Mo1 O13 1.746(9) 2_575
Mo1 O2 1.759(11) .
Mo1 O9 1.779(10) .
Mo2 O5 1.689(11) .
Mo2 O8 1.705(11) .
Mo2 O6 1.881(10) .
Mo2 O11 1.891(9) .
Mo2 O13 2.421(9) .
Mo3 O12 1.690(11) .
Mo3 O10 1.716(10) .
Mo3 O4 1.851(9) .
Mo3 O6 1.934(10) 2_575
Mo3 O2 2.370(9) 2_575
Mo3 O9 2.376(10) .
Mo4 O1 1.688(10) .
Mo4 O7 1.719(10) .
Mo4 O11 1.911(10) .
Mo4 O4 1.949(9) .
Mo4 O13 2.426(9) .
Mo4 O9 2.452(10) .
Cu1 N2 1.887(14) .
Cu1 N1 1.909(14) .
Cu2 N3 1.899(13) .
Cu2 N4 1.915(13) .
Cu2 O10 2.327(10) .
O2 Mo3 2.370(9) 2_575
O6 Mo3 1.934(10) 2_575
O13 Mo1 1.746(9) 2_575
N1 C1 1.344(19) .
N1 C5 1.35(2) .
N2 C7 1.35(2) .
N2 C11 1.362(19) .
N3 C18 1.34(2) .
N3 C14 1.346(19) .
N4 C21 1.33(2) .
N4 C25 1.34(2) .
C1 C2 1.33(2) .
C1 H1A 0.9300 .
C2 C3 1.40(2) .
C2 H2A 0.9300 .
C3 C4 1.38(2) .
C3 C6 1.49(2) .
C4 C5 1.36(2) .
C4 H4A 0.9300 .
C5 H5A 0.9300 .
C6 C13 1.55(3) 2_675
C6 H6A 0.9700 .
C6 H6B 0.9700 .
C7 C8 1.40(2) .
C7 H7A 0.9300 .
C8 C9 1.34(2) .
C8 H8A 0.9300 .
C9 C10 1.37(3) .
C9 C12 1.55(2) .
C10 C11 1.40(3) .
C10 H10A 0.9300 .
C11 H11A 0.9300 .
C12 C13 1.52(3) .
C12 H12A 0.9700 .
C12 H12B 0.9700 .
C13 C6 1.55(3) 2_675
C13 H13A 0.9700 .
C13 H13B 0.9700 .
C14 C15 1.39(2) .
C14 H14A 0.9300 .
C15 C16 1.37(2) .
C15 H15A 0.9300 .
C16 C17 1.37(2) .
C16 C19 1.49(2) .
C17 C18 1.38(2) .
C17 H17A 0.9300 .
C18 H18A 0.9300 .
C19 C20 1.56(3) .
C19 H19A 0.9700 .
C19 H19B 0.9700 .
C20 C26 1.43(3) 1_556
C20 H20A 0.9700 .
C20 H20B 0.9700 .
C21 C22 1.40(2) .
C21 H21A 0.9300 .
C22 C23 1.39(2) .
C22 H22A 0.9300 .
C23 C24 1.37(3) .
C23 C26 1.50(2) .
C24 C25 1.36(2) .
C24 H24A 0.9300 .
C25 H25A 0.9300 .
C26 C20 1.43(3) 1_554
C26 H26A 0.9700 .
C26 H26B 0.9700 .
