#------------------------------------------------------------------------------
#$Date: 2016-03-25 11:39:42 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179801 $
#$URL: svn://www.crystallography.net/cod/cif/7/00/97/7009716.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7009716
loop_
_publ_author_name
'Haupt, Hans-Jürgen'
'Seewald, Oliver'
'Flörke, Ulrich'
'Buß, Volker'
'Weyhermüller, Thomas'
_publ_section_title
;
 Diastereomeric metallatetrahedron complexes of the type
 Re2(AgPR3)2(μ-PCy2)(CO)7Z (R = Et and Ph;
 Z = (−)- and (+)-camphanate): synthesis,
 structure and CD data
;
_journal_issue                   16
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2837
_journal_paper_doi               10.1039/b003013i
_journal_year                    2000
_chemical_formula_moiety         'C65 H65 Ag2 O11 P3 Re2 * CHCl3'
_chemical_formula_sum            'C66 H66 Ag2 Cl3 O11 P3 Re2'
_chemical_formula_weight         1822.59
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                98.26(1)
_cell_angle_beta                 100.47(2)
_cell_angle_gamma                101.69(2)
_cell_formula_units_Z            2
_cell_length_a                   14.723(8)
_cell_length_b                   16.244(4)
_cell_length_c                   16.665(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.385
_cell_measurement_theta_min      5.068
_cell_volume                     3770(2)
_computing_cell_refinement       'Siemens XSCANS'
_computing_data_collection       'Siemens XSCANS'
_computing_data_reduction        'Siemens XSCANS'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'Siemens SHELXTL'
_computing_structure_solution    'Siemens SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device       'Siemens P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0766
_diffrn_reflns_av_sigmaI/netI    0.1301
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            13788
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         2.61
_diffrn_standards_decay_%        10
_diffrn_standards_interval_count 397
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.933
_exptl_absorpt_correction_T_max  0.903
_exptl_absorpt_correction_T_min  0.746
_exptl_absorpt_correction_type   gaussian
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.606
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       block
_exptl_crystal_F_000             1780
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.078
_refine_diff_density_min         -1.089
_refine_diff_density_rms         0.217
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.009
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     765
_refine_ls_number_reflns         13221
_refine_ls_number_restraints     1314
_refine_ls_restrained_S_all      0.967
_refine_ls_R_factor_all          0.1678
_refine_ls_R_factor_gt           0.0782
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1423P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2070
_refine_ls_wR_factor_ref         0.2909
_reflns_number_gt                5349
_reflns_number_total             13221
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b003013i.txt
_cod_data_source_block           II
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7009716
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Re1 Re 0.31411(6) 0.36617(5) 0.27490(5) 0.0611(3) Uani 1 1 d U . .
Re2 Re 0.11001(6) 0.23000(5) 0.24546(5) 0.0587(3) Uani 1 1 d U . .
Ag1 Ag 0.18194(11) 0.29730(10) 0.11015(8) 0.0656(4) Uani 1 1 d U . .
Ag2 Ag 0.27600(11) 0.18906(10) 0.18268(9) 0.0667(4) Uani 1 1 d U . .
P1 P 0.1344(4) 0.3111(3) -0.0335(3) 0.0618(13) Uani 1 1 d U . .
P2 P 0.3641(4) 0.1047(4) 0.1069(3) 0.0666(13) Uani 1 1 d U . .
P3 P 0.1845(4) 0.3564(3) 0.3520(3) 0.0585(12) Uani 1 1 d U . .
O1 O 0.4520(13) 0.5166(12) 0.4000(11) 0.119(6) Uani 1 1 d U . .
C1 C 0.3997(16) 0.4595(15) 0.3516(14) 0.080(5) Uani 1 1 d U . .
O2 O 0.4626(12) 0.3661(12) 0.1642(11) 0.115(6) Uani 1 1 d U . .
C2 C 0.4042(15) 0.3617(15) 0.2031(13) 0.079(4) Uani 1 1 d U . .
O3 O 0.4003(11) 0.2510(11) 0.3851(10) 0.098(5) Uani 1 1 d U . .
C3 C 0.3648(14) 0.2891(14) 0.3416(12) 0.069(4) Uani 1 1 d U . .
O4 O 0.2304(12) 0.4971(10) 0.1856(9) 0.097(5) Uani 1 1 d U . .
C4 C 0.2571(15) 0.4447(13) 0.2133(12) 0.069(3) Uani 1 1 d U . .
O5 O -0.0696(11) 0.1601(12) 0.3028(10) 0.106(5) Uani 1 1 d U . .
C5 C -0.0008(16) 0.1852(14) 0.2821(13) 0.078(5) Uani 1 1 d U . .
O6 O 0.0464(12) 0.0766(11) 0.0982(10) 0.101(5) Uani 1 1 d U . .
C6 C 0.0738(16) 0.1326(14) 0.1504(13) 0.072(4) Uani 1 1 d U . .
C7 C 0.0364(14) 0.2955(13) 0.1883(12) 0.064(3) Uani 1 1 d U . .
O7 O -0.0152(10) 0.3323(10) 0.1609(9) 0.086(4) Uani 1 1 d U . .
O8 O 0.1785(10) 0.1612(9) 0.3355(8) 0.070(3) Uani 1 1 d U . .
O9 O 0.2298(13) 0.0696(10) 0.2541(9) 0.097(4) Uani 1 1 d U . .
O10 O 0.2455(11) 0.1028(10) 0.4698(8) 0.089(4) Uani 1 1 d U . .
O11 O 0.2389(17) 0.0743(13) 0.5963(10) 0.144(8) Uani 1 1 d U . .
C11 C 0.0120(14) 0.3204(10) -0.0638(10) 0.065(4) Uani 1 1 d DU . .
C12 C -0.0201(14) 0.3752(12) -0.0154(12) 0.083(5) Uani 1 1 d DU . .
H12 H 0.0210 0.4088 0.0324 0.100 Uiso 1 1 calc R . .
C13 C -0.1117(16) 0.3836(14) -0.0339(15) 0.107(7) Uani 1 1 d DU . .
H13 H -0.1317 0.4228 0.0011 0.128 Uiso 1 1 calc R . .
C14 C -0.1759(18) 0.3334(14) -0.1053(13) 0.100(6) Uani 1 1 d DU . .
H14 H -0.2387 0.3378 -0.1188 0.120 Uiso 1 1 calc R . .
C15 C -0.1395(17) 0.2757(18) -0.1554(17) 0.129(8) Uani 1 1 d DU . .
H15 H -0.1781 0.2414 -0.2040 0.154 Uiso 1 1 calc R . .
C16 C -0.0475(15) 0.2711(15) -0.1317(14) 0.098(6) Uani 1 1 d DU . .
H16 H -0.0250 0.2317 -0.1643 0.117 Uiso 1 1 calc R . .
C21 C 0.2069(13) 0.4056(12) -0.0591(10) 0.069(4) Uani 1 1 d DU . .
C22 C 0.1696(15) 0.4435(11) -0.1227(11) 0.087(6) Uani 1 1 d DU . .
H22 H 0.1066 0.4238 -0.1513 0.104 Uiso 1 1 calc R . .
C23 C 0.2289(17) 0.5110(13) -0.1419(13) 0.102(7) Uani 1 1 d DU . .
H23 H 0.2052 0.5370 -0.1847 0.123 Uiso 1 1 calc R . .
C24 C 0.3209(16) 0.5414(16) -0.1008(14) 0.111(8) Uani 1 1 d DU . .
H24 H 0.3597 0.5865 -0.1160 0.134 Uiso 1 1 calc R . .
C25 C 0.3553(17) 0.5050(15) -0.0372(17) 0.116(8) Uani 1 1 d DU . .
H25 H 0.4171 0.5278 -0.0068 0.140 Uiso 1 1 calc R . .
C26 C 0.3015(15) 0.4362(13) -0.0168(13) 0.091(6) Uani 1 1 d DU . .
H26 H 0.3273 0.4098 0.0248 0.109 Uiso 1 1 calc R . .
C31 C 0.1464(12) 0.2204(11) -0.1043(10) 0.064(4) Uani 1 1 d DU . .
C32 C 0.1832(12) 0.2302(13) -0.1752(11) 0.081(5) Uani 1 1 d DU . .
H32 H 0.2021 0.2850 -0.1858 0.097 Uiso 1 1 calc R . .
C33 C 0.1925(15) 0.1611(15) -0.2300(12) 0.102(6) Uani 1 1 d DU . .
H33 H 0.2171 0.1699 -0.2765 0.122 Uiso 1 1 calc R . .
C34 C 0.1639(15) 0.0763(15) -0.2145(14) 0.095(6) Uani 1 1 d DU . .
H34 H 0.1708 0.0293 -0.2500 0.114 Uiso 1 1 calc R . .
C35 C 0.1246(17) 0.0654(13) -0.1434(14) 0.095(6) Uani 1 1 d DU . .
H35 H 0.1029 0.0109 -0.1329 0.114 Uiso 1 1 calc R . .
C36 C 0.1194(12) 0.1374(11) -0.0900(12) 0.067(4) Uani 1 1 d DU . .
H36 H 0.0968 0.1298 -0.0423 0.081 Uiso 1 1 calc R . .
C41 C 0.2915(13) 0.0106(13) 0.0319(11) 0.073(4) Uani 1 1 d DU . .
C42 C 0.3087(12) -0.0125(12) -0.0467(12) 0.077(5) Uani 1 1 d DU . .
H42 H 0.3562 0.0230 -0.0642 0.092 Uiso 1 1 calc R . .
C43 C 0.2581(16) -0.0848(14) -0.0971(14) 0.106(7) Uani 1 1 d DU . .
H43 H 0.2727 -0.0994 -0.1485 0.128 Uiso 1 1 calc R . .
C44 C 0.1846(15) -0.1389(16) -0.0759(15) 0.104(7) Uani 1 1 d DU . .
H44 H 0.1470 -0.1872 -0.1130 0.124 Uiso 1 1 calc R . .
C45 C 0.1697(16) -0.1176(15) 0.0033(16) 0.107(7) Uani 1 1 d DU . .
H45 H 0.1227 -0.1538 0.0206 0.128 Uiso 1 1 calc R . .
C46 C 0.2205(14) -0.0470(15) 0.0550(14) 0.098(6) Uani 1 1 d DU . .
H46 H 0.2088 -0.0352 0.1079 0.117 Uiso 1 1 calc R . .
C51 C 0.4484(14) 0.0613(11) 0.1745(11) 0.078(5) Uani 1 1 d DU . .
C52 C 0.4874(14) 0.1061(14) 0.2535(13) 0.099(7) Uani 1 1 d DU . .
H52 H 0.4698 0.1558 0.2729 0.118 Uiso 1 1 calc R . .
C53 C 0.5551(17) 0.0752(17) 0.3048(15) 0.122(8) Uani 1 1 d DU . .
H53 H 0.5813 0.1041 0.3591 0.146 Uiso 1 1 calc R . .
C54 C 0.5818(18) 0.0046(14) 0.2760(14) 0.102(7) Uani 1 1 d DU . .
H54 H 0.6282 -0.0133 0.3102 0.122 Uiso 1 1 calc R . .
C55 C 0.5438(18) -0.0405(15) 0.1999(15) 0.110(7) Uani 1 1 d DU . .
H55 H 0.5632 -0.0895 0.1815 0.132 Uiso 1 1 calc R . .
C56 C 0.4736(15) -0.0133(14) 0.1473(13) 0.090(6) Uani 1 1 d DU . .
H56 H 0.4447 -0.0456 0.0947 0.108 Uiso 1 1 calc R . .
C61 C 0.4365(12) 0.1669(12) 0.0456(10) 0.066(4) Uani 1 1 d DU . .
C62 C 0.5320(13) 0.1733(11) 0.0567(11) 0.080(5) Uani 1 1 d DU . .
H62 H 0.5612 0.1447 0.0946 0.096 Uiso 1 1 calc R . .
C63 C 0.5860(14) 0.2212(12) 0.0131(12) 0.081(5) Uani 1 1 d DU . .
H63 H 0.6510 0.2250 0.0212 0.098 Uiso 1 1 calc R . .
C64 C 0.5420(15) 0.2644(15) -0.0439(14) 0.096(6) Uani 1 1 d DU . .
H64 H 0.5768 0.2968 -0.0746 0.115 Uiso 1 1 calc R . .
C65 C 0.4427(16) 0.2574(15) -0.0533(14) 0.098(6) Uani 1 1 d DU . .
H65 H 0.4122 0.2867 -0.0896 0.118 Uiso 1 1 calc R . .
C66 C 0.3912(15) 0.2077(14) -0.0093(12) 0.086(5) Uani 1 1 d DU . .
H66 H 0.3259 0.2021 -0.0170 0.103 Uiso 1 1 calc R . .
C71 C 0.1277(11) 0.4450(10) 0.3494(12) 0.067(4) Uani 1 1 d DU . .
H71 H 0.1091 0.4455 0.2899 0.080 Uiso 1 1 calc R . .
C72 C 0.1872(12) 0.5348(9) 0.3854(12) 0.075(5) Uani 1 1 d DU . .
H72A H 0.2465 0.5417 0.3668 0.091 Uiso 1 1 calc R . .
H72B H 0.2023 0.5418 0.4455 0.091 Uiso 1 1 calc R . .
C73 C 0.1385(13) 0.6049(11) 0.3612(14) 0.092(6) Uani 1 1 d DU . .
H73A H 0.1785 0.6603 0.3894 0.111 Uiso 1 1 calc R . .
H73B H 0.1308 0.6029 0.3019 0.111 Uiso 1 1 calc R . .
C74 C 0.0424(14) 0.5948(12) 0.3836(17) 0.115(7) Uani 1 1 d DU . .
H74A H 0.0094 0.6342 0.3591 0.137 Uiso 1 1 calc R . .
H74B H 0.0511 0.6096 0.4435 0.137 Uiso 1 1 calc R . .
C75 C -0.0185(13) 0.5037(12) 0.3534(17) 0.114(7) Uani 1 1 d DU . .
H75A H -0.0383 0.4934 0.2934 0.137 Uiso 1 1 calc R . .
H75B H -0.0752 0.4983 0.3760 0.137 Uiso 1 1 calc R . .
C76 C 0.0334(12) 0.4354(13) 0.3784(15) 0.095(6) Uani 1 1 d DU . .
H76A H -0.0068 0.3791 0.3540 0.113 Uiso 1 1 calc R . .
H76B H 0.0460 0.4406 0.4384 0.113 Uiso 1 1 calc R . .
C81 C 0.2108(12) 0.3391(11) 0.4599(9) 0.069(4) Uani 1 1 d DU . .
H81 H 0.2486 0.2959 0.4572 0.083 Uiso 1 1 calc R . .
C82 C 0.2774(16) 0.4143(13) 0.5217(10) 0.099(7) Uani 1 1 d DU . .
H82A H 0.2459 0.4612 0.5279 0.119 Uiso 1 1 calc R . .
H82B H 0.3334 0.4336 0.5004 0.119 Uiso 1 1 calc R . .
C83 C 0.3077(16) 0.3912(18) 0.6071(11) 0.124(8) Uani 1 1 d DU . .
H83A H 0.3490 0.3520 0.6029 0.149 Uiso 1 1 calc R . .
H83B H 0.3435 0.4426 0.6463 0.149 Uiso 1 1 calc R . .
C84 C 0.2227(15) 0.3503(15) 0.6394(11) 0.110(7) Uani 1 1 d DU . .
H84A H 0.2452 0.3316 0.6906 0.132 Uiso 1 1 calc R . .
H84B H 0.1871 0.3928 0.6521 0.132 Uiso 1 1 calc R . .
C85 C 0.1574(15) 0.2746(13) 0.5779(10) 0.095(6) Uani 1 1 d DU . .
H85A H 0.1010 0.2550 0.5988 0.114 Uiso 1 1 calc R . .
H85B H 0.1894 0.2281 0.5722 0.114 Uiso 1 1 calc R . .
C86 C 0.1281(12) 0.2974(13) 0.4931(10) 0.080(5) Uani 1 1 d DU . .
H86A H 0.0930 0.2458 0.4541 0.096 Uiso 1 1 calc R . .
H86B H 0.0860 0.3359 0.4971 0.096 Uiso 1 1 calc R . .
C90 C 0.2099(16) 0.0965(14) 0.3220(12) 0.074(4) Uani 1 1 d U . .
C91 C 0.2306(17) 0.0470(14) 0.3902(12) 0.077(4) Uani 1 1 d U . .
C92 C 0.311(2) 0.0031(17) 0.3890(16) 0.111(6) Uani 1 1 d U . .
H92A H 0.3729 0.0430 0.4073 0.133 Uiso 1 1 calc R . .
H92B H 0.3067 -0.0307 0.3349 0.133 Uiso 1 1 calc R . .
C93 C 0.288(2) -0.0564(18) 0.4574(17) 0.124(7) Uani 1 1 d U . .
H93A H 0.2832 -0.1161 0.4355 0.148 Uiso 1 1 calc R . .
H93B H 0.3369 -0.0384 0.5080 0.148 Uiso 1 1 calc R . .
C94 C 0.197(2) -0.0435(16) 0.4729(14) 0.101(5) Uani 1 1 d U . .
C95 C 0.225(2) 0.0446(17) 0.5215(14) 0.098(6) Uani 1 1 d U . .
C96 C 0.151(2) -0.0282(16) 0.3937(14) 0.096(5) Uani 1 1 d U . .
C97 C 0.128(3) -0.1047(16) 0.3202(17) 0.172(12) Uani 1 1 d U . .
H97A H 0.1852 -0.1239 0.3166 0.258 Uiso 1 1 calc R . .
H97B H 0.1050 -0.0869 0.2695 0.258 Uiso 1 1 calc R . .
H97C H 0.0810 -0.1505 0.3291 0.258 Uiso 1 1 calc R . .
C98 C 0.0597(19) -0.0004(19) 0.3955(19) 0.135(9) Uani 1 1 d U . .
H98A H 0.0328 0.0081 0.3412 0.203 Uiso 1 1 calc R . .
H98B H 0.0724 0.0522 0.4347 0.203 Uiso 1 1 calc R . .
H98C H 0.0157 -0.0437 0.4117 0.203 Uiso 1 1 calc R . .
C99 C 0.149(2) -0.1090(19) 0.5192(18) 0.150(10) Uani 1 1 d U . .
H99A H 0.1335 -0.1652 0.4856 0.226 Uiso 1 1 calc R . .
H99B H 0.0912 -0.0949 0.5303 0.226 Uiso 1 1 calc R . .
H99C H 0.1909 -0.1079 0.5707 0.226 Uiso 1 1 calc R . .
C100 C 0.365(5) 0.694(5) -0.244(5) 0.26(3) Uiso 0.78(2) 1 d PU . .
Cl1 Cl 0.2239(17) 0.7057(15) -0.3950(15) 0.294(13) Uiso 0.78(2) 1 d PU . .
Cl2 Cl 0.244(2) 0.7030(18) -0.2464(18) 0.348(15) Uiso 0.78(2) 1 d PU . .
Cl3 Cl 0.355(2) 0.6358(19) -0.3276(19) 0.350(16) Uiso 0.78(2) 1 d PU . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Re1 C2 91.8(10) . . ?
C1 Re1 C3 88.2(9) . . ?
C2 Re1 C3 93.2(9) . . ?
C1 Re1 C4 91.3(9) . . ?
C2 Re1 C4 90.9(9) . . ?
C3 Re1 C4 175.9(8) . . ?
C1 Re1 P3 95.8(7) . . ?
C2 Re1 P3 172.3(7) . . ?
C3 Re1 P3 87.5(6) . . ?
C4 Re1 P3 88.5(6) . . ?
C1 Re1 Ag2 148.5(7) . . ?
C2 Re1 Ag2 71.7(7) . . ?
C3 Re1 Ag2 66.8(6) . . ?
C4 Re1 Ag2 114.9(6) . . ?
P3 Re1 Ag2 101.69(13) . . ?
C1 Re1 Ag1 149.9(6) . . ?
C2 Re1 Ag1 79.3(6) . . ?
C3 Re1 Ag1 120.7(6) . . ?
C4 Re1 Ag1 60.5(6) . . ?
P3 Re1 Ag1 93.78(13) . . ?
Ag2 Re1 Ag1 54.84(5) . . ?
C5 Re2 C7 86.0(9) . . ?
C5 Re2 C6 89.8(9) . . ?
C7 Re2 C6 93.2(9) . . ?
C5 Re2 O8 83.8(7) . . ?
C7 Re2 O8 166.6(6) . . ?
C6 Re2 O8 95.5(7) . . ?
C5 Re2 P3 101.9(7) . . ?
C7 Re2 P3 89.2(6) . . ?
C6 Re2 P3 168.2(6) . . ?
O8 Re2 P3 84.4(4) . . ?
C5 Re2 Ag1 144.7(7) . . ?
C7 Re2 Ag1 64.2(6) . . ?
C6 Re2 Ag1 74.4(6) . . ?
O8 Re2 Ag1 128.2(3) . . ?
P3 Re2 Ag1 96.38(12) . . ?
C5 Re2 Ag2 145.2(7) . . ?
C7 Re2 Ag2 119.1(6) . . ?
C6 Re2 Ag2 66.8(6) . . ?
O8 Re2 Ag2 73.9(3) . . ?
P3 Re2 Ag2 102.04(13) . . ?
Ag1 Re2 Ag2 55.14(5) . . ?
P1 Ag1 Ag2 132.29(14) . . ?
P1 Ag1 Re2 142.76(15) . . ?
Ag2 Ag1 Re2 63.66(5) . . ?
P1 Ag1 Re1 147.96(14) . . ?
Ag2 Ag1 Re1 62.10(5) . . ?
Re2 Ag1 Re1 67.12(4) . . ?
P2 Ag2 O9 89.6(3) . . ?
P2 Ag2 Ag1 121.38(14) . . ?
O9 Ag2 Ag1 134.3(4) . . ?
P2 Ag2 Re1 135.70(15) . . ?
O9 Ag2 Re1 118.9(3) . . ?
Ag1 Ag2 Re1 63.07(5) . . ?
P2 Ag2 Re2 157.53(15) . . ?
O9 Ag2 Re2 77.5(3) . . ?
Ag1 Ag2 Re2 61.21(5) . . ?
Re1 Ag2 Re2 66.61(4) . . ?
C31 P1 C11 106.5(8) . . ?
C31 P1 C21 105.6(7) . . ?
C11 P1 C21 105.0(8) . . ?
C31 P1 Ag1 111.6(5) . . ?
C11 P1 Ag1 114.4(6) . . ?
C21 P1 Ag1 113.0(5) . . ?
C41 P2 C51 103.8(8) . . ?
C41 P2 C61 104.6(8) . . ?
C51 P2 C61 105.2(8) . . ?
C41 P2 Ag2 115.4(6) . . ?
C51 P2 Ag2 113.5(6) . . ?
C61 P2 Ag2 113.2(6) . . ?
C71 P3 C81 108.6(9) . . ?
C71 P3 Re2 115.8(6) . . ?
C81 P3 Re2 116.5(6) . . ?
C71 P3 Re1 113.0(5) . . ?
C81 P3 Re1 118.0(6) . . ?
Re2 P3 Re1 83.21(15) . . ?
O1 C1 Re1 179(2) . . ?
O2 C2 Re1 174(2) . . ?
O3 C3 Re1 173(2) . . ?
O4 C4 Re1 171.9(19) . . ?
O5 C5 Re2 177(2) . . ?
O6 C6 Re2 174(2) . . ?
O7 C7 Re2 171.1(17) . . ?
C90 O8 Re2 129.0(12) . . ?
C90 O9 Ag2 110.5(13) . . ?
C95 O10 C91 102.2(17) . . ?
C12 C11 C16 119(2) . . ?
C12 C11 P1 119.3(14) . . ?
C16 C11 P1 121.6(15) . . ?
C11 C12 C13 122(2) . . ?
C12 C13 C14 121(2) . . ?
C13 C14 C15 116(2) . . ?
C16 C15 C14 119(2) . . ?
C11 C16 C15 123(2) . . ?
C22 C21 C26 120(2) . . ?
C22 C21 P1 120.4(14) . . ?
C26 C21 P1 119.3(13) . . ?
C23 C22 C21 117.6(19) . . ?
C24 C23 C22 123(2) . . ?
C25 C24 C23 119(2) . . ?
C24 C25 C26 121(2) . . ?
C25 C26 C21 119(2) . . ?
C36 C31 C32 117.2(19) . . ?
C36 C31 P1 120.8(13) . . ?
C32 C31 P1 121.9(13) . . ?
C33 C32 C31 122.4(18) . . ?
C32 C33 C34 119.6(19) . . ?
C35 C34 C33 118(2) . . ?
C36 C35 C34 119.0(19) . . ?
C35 C36 C31 123.3(18) . . ?
C42 C41 C46 116(2) . . ?
C42 C41 P2 123.0(14) . . ?
C46 C41 P2 120.3(15) . . ?
C43 C42 C41 121(2) . . ?
C42 C43 C44 122(2) . . ?
C43 C44 C45 117(3) . . ?
C46 C45 C44 122(2) . . ?
C45 C46 C41 122(2) . . ?
C52 C51 C56 120(2) . . ?
C52 C51 P2 118.0(14) . . ?
C56 C51 P2 121.9(14) . . ?
C51 C52 C53 118.6(19) . . ?
C54 C53 C52 120(2) . . ?
C55 C54 C53 122(3) . . ?
C54 C55 C56 119(2) . . ?
C51 C56 C55 119.5(19) . . ?
C66 C61 C62 121(2) . . ?
C66 C61 P2 117.5(14) . . ?
C62 C61 P2 121.4(14) . . ?
C61 C62 C63 121.3(19) . . ?
C62 C63 C64 119.3(19) . . ?
C63 C64 C65 118(2) . . ?
C66 C65 C64 121(2) . . ?
C61 C66 C65 119.5(19) . . ?
C72 C71 C76 108.2(13) . . ?
C72 C71 P3 118.7(11) . . ?
C76 C71 P3 116.9(10) . . ?
C71 C72 C73 113.7(13) . . ?
C74 C73 C72 111.8(13) . . ?
C73 C74 C75 112.1(14) . . ?
C74 C75 C76 113.2(15) . . ?
C75 C76 C71 111.2(13) . . ?
C86 C81 C82 112.7(13) . . ?
C86 C81 P3 116.9(11) . . ?
C82 C81 P3 115.0(11) . . ?
C81 C82 C83 112.1(14) . . ?
C84 C83 C82 111.8(14) . . ?
C85 C84 C83 112.7(15) . . ?
C84 C85 C86 111.7(13) . . ?
C81 C86 C85 113.5(13) . . ?
O8 C90 O9 124.1(18) . . ?
O8 C90 C91 120.0(17) . . ?
O9 C90 C91 115.9(18) . . ?
O10 C91 C92 110.0(19) . . ?
O10 C91 C90 109.1(16) . . ?
C92 C91 C90 116.8(18) . . ?
O10 C91 C96 103.2(16) . . ?
C92 C91 C96 100.5(19) . . ?
C90 C91 C96 116(2) . . ?
C91 C92 C93 97.2(19) . . ?
C94 C93 C92 105(2) . . ?
C96 C94 C93 103(2) . . ?
C96 C94 C95 100(2) . . ?
C93 C94 C95 101(2) . . ?
C96 C94 C99 123(3) . . ?
C93 C94 C99 114(2) . . ?
C95 C94 C99 113(2) . . ?
O11 C95 O10 117(2) . . ?
O11 C95 C94 133(2) . . ?
O10 C95 C94 109.9(18) . . ?
C94 C96 C98 114(2) . . ?
C94 C96 C91 95(2) . . ?
C98 C96 C91 111(2) . . ?
C94 C96 C97 115(2) . . ?
C98 C96 C97 107(3) . . ?
C91 C96 C97 115(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Re1 C1 1.90(2) . ?
Re1 C2 1.95(2) . ?
Re1 C3 1.96(2) . ?
Re1 C4 1.97(2) . ?
Re1 P3 2.478(5) . ?
Re1 Re2 3.259(1) . ?
Re1 Ag2 2.9523(19) . ?
Re1 Ag1 2.9783(19) . ?
Re2 C5 1.89(2) . ?
Re2 C7 1.898(19) . ?
Re2 C6 1.98(2) . ?
Re2 O8 2.215(12) . ?
Re2 P3 2.430(5) . ?
Re2 Ag1 2.9169(17) . ?
Re2 Ag2 2.983(2) . ?
Ag1 P1 2.424(5) . ?
Ag1 Ag2 2.731(2) . ?
Ag2 P2 2.444(5) . ?
Ag2 O9 2.463(14) . ?
P1 C31 1.81(2) . ?
P1 C11 1.82(2) . ?
P1 C21 1.84(2) . ?
P2 C41 1.83(2) . ?
P2 C51 1.84(2) . ?
P2 C61 1.86(2) . ?
P3 C71 1.808(16) . ?
P3 C81 1.844(15) . ?
O1 C1 1.17(2) . ?
O2 C2 1.16(2) . ?
O3 C3 1.14(2) . ?
O4 C4 1.13(2) . ?
O5 C5 1.15(2) . ?
O6 C6 1.11(2) . ?
C7 O7 1.13(2) . ?
O8 C90 1.24(2) . ?
O9 C90 1.26(2) . ?
O10 C95 1.39(3) . ?
O10 C91 1.45(2) . ?
O11 C95 1.23(3) . ?
C11 C12 1.329(19) . ?
C11 C16 1.336(19) . ?
C12 C13 1.37(2) . ?
C13 C14 1.41(2) . ?
C14 C15 1.41(2) . ?
C15 C16 1.36(2) . ?
C21 C22 1.383(19) . ?
C21 C26 1.395(19) . ?
C22 C23 1.37(2) . ?
C23 C24 1.36(2) . ?
C24 C25 1.35(2) . ?
C25 C26 1.36(2) . ?
C31 C36 1.394(18) . ?
C31 C32 1.402(18) . ?
C32 C33 1.39(2) . ?
C33 C34 1.43(2) . ?
C34 C35 1.43(2) . ?
C35 C36 1.39(2) . ?
C41 C42 1.392(19) . ?
C41 C46 1.40(2) . ?
C42 C43 1.33(2) . ?
C43 C44 1.38(2) . ?
C44 C45 1.38(2) . ?
C45 C46 1.32(2) . ?
C51 C52 1.369(19) . ?
C51 C56 1.378(19) . ?
C52 C53 1.41(2) . ?
C53 C54 1.34(2) . ?
C54 C55 1.33(2) . ?
C55 C56 1.41(2) . ?
C61 C66 1.363(19) . ?
C61 C62 1.365(18) . ?
C62 C63 1.37(2) . ?
C63 C64 1.40(2) . ?
C64 C65 1.42(2) . ?
C65 C66 1.37(2) . ?
C71 C72 1.514(15) . ?
C71 C76 1.538(15) . ?
C72 C73 1.526(15) . ?
C73 C74 1.511(15) . ?
C74 C75 1.526(15) . ?
C75 C76 1.532(15) . ?
C81 C86 1.505(14) . ?
C81 C82 1.517(15) . ?
C82 C83 1.535(15) . ?
C83 C84 1.519(15) . ?
C84 C85 1.513(15) . ?
C85 C86 1.520(14) . ?
C90 C91 1.51(3) . ?
C91 C92 1.50(3) . ?
C91 C96 1.53(3) . ?
C92 C93 1.64(3) . ?
C93 C94 1.46(3) . ?
C94 C96 1.45(3) . ?
C94 C95 1.48(3) . ?
C94 C99 1.54(3) . ?
C96 C98 1.50(4) . ?
C96 C97 1.55(3) . ?
