#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:27:26 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179920 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/15/7021581.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7021581
loop_
_publ_author_name
'Goswami, Soumyabrata'
'Adhikary, Amit'
'Jena, Himanshu Sekhar'
'Konar, Sanjit'
_publ_section_title
;
 Lanthanide based coordination polymers chill, relax under magnetic field
 and also fluoresce.
;
_journal_issue                   27
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9813
_journal_page_last               9817
_journal_paper_doi               10.1039/c3dt51195b
_journal_volume                  42
_journal_year                    2013
_chemical_formula_moiety         'C10 H4 Dy Na O17 '
_chemical_formula_sum            'C10 H4 Dy Na O17'
_chemical_formula_weight         581.62
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 113.127(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   6.7395(5)
_cell_length_b                   15.8784(14)
_cell_length_c                   8.0974(6)
_cell_measurement_reflns_used    3853
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      26.50
_cell_measurement_theta_min      2.57
_cell_volume                     796.89(11)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  APEX-II
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0367
_diffrn_reflns_av_unetI/netI     0.0207
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            7314
_diffrn_reflns_theta_full        27.44
_diffrn_reflns_theta_max         27.44
_diffrn_reflns_theta_min         2.57
_exptl_absorpt_coefficient_mu    4.815
_exptl_absorpt_correction_T_max  0.260
_exptl_absorpt_correction_T_min  0.144
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   multi-scan
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    2.407
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             554
_exptl_crystal_size_max          0.43
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.747
_refine_diff_density_min         -0.836
_refine_diff_density_rms         0.084
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     142
_refine_ls_number_reflns         1900
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.064
_refine_ls_R_factor_all          0.0162
_refine_ls_R_factor_gt           0.0160
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0005P)²+2.0100P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0353
_refine_ls_wR_factor_ref         0.0354
_reflns_number_gt                1891
_reflns_number_total             1900
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3dt51195b.txt
_cod_data_source_block           Complex3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               7021581
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.16085(2) 0.2500 0.03867(2) 0.00929(5) Uani 1 2 d S
O1 O 0.4431(3) 0.15611(12) 0.1889(2) 0.0161(4) Uani 1 1 d .
O2 O 0.8338(3) 0.14021(14) 0.5002(3) 0.0266(5) Uani 1 1 d .
O3 O 0.8793(3) -0.03476(11) 0.6267(2) 0.0167(4) Uani 1 1 d .
O4 O 0.5438(3) -0.13332(16) 0.3498(3) 0.0316(5) Uani 1 1 d .
O5 O 0.2858(3) -0.01786(11) 0.0595(2) 0.0148(3) Uani 1 1 d .
O10 O 0.2292(4) 0.2500 0.3744(4) 0.0223(6) Uani 1 2 d S
O9 O -0.0635(3) 0.34720(11) 0.1243(2) 0.0133(3) Uani 1 1 d .
O7 O 0.1119(3) 0.37429(12) -0.1452(2) 0.0155(4) Uani 1 1 d .
H7 H 0.2044 0.4092 -0.0913 0.023 Uiso 1 1 calc R
O8 O -0.1859(4) 0.2500 -0.2030(4) 0.0291(7) Uani 1 2 d S
H8 H -0.2562 0.2098 -0.1922 0.044 Uiso 0.50 1 calc PR
O6 O 0.4193(4) 0.2500 -0.0998(3) 0.0163(5) Uani 1 2 d S
H6 H 0.4447 0.2014 -0.1194 0.024 Uiso 0.50 1 calc PR
C1 C 0.5225(4) 0.08498(16) 0.2585(3) 0.0134(5) Uani 1 1 d .
C2 C 0.7217(4) 0.08080(18) 0.4240(3) 0.0194(5) Uani 1 1 d .
C3 C 0.7451(4) -0.00757(18) 0.4818(4) 0.0205(6) Uani 1 1 d .
C4 C 0.5730(5) -0.0569(2) 0.3429(4) 0.0349(8) Uani 1 1 d .
C5 C 0.4421(4) 0.00156(17) 0.2009(3) 0.0163(5) Uani 1 1 d .
Na1 Na 0.7776(2) 0.2500 0.27530(18) 0.0109(3) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Dy1 O1 78.92(9) 4_565 .
O1 Dy1 O8 139.32(5) 4_565 .
O1 Dy1 O8 139.32(5) . .
O1 Dy1 O6 69.78(6) 4_565 .
O1 Dy1 O6 69.78(6) . .
O8 Dy1 O6 105.79(10) . .
O1 Dy1 O7 136.50(6) 4_565 4_565
O1 Dy1 O7 71.75(6) . 4_565
O8 Dy1 O7 69.02(6) . 4_565
O6 Dy1 O7 70.28(5) . 4_565
O1 Dy1 O7 71.75(6) 4_565 .
O1 Dy1 O7 136.50(6) . .
O8 Dy1 O7 69.02(6) . .
O6 Dy1 O7 70.28(5) . .
O7 Dy1 O7 109.58(9) 4_565 .
O1 Dy1 O9 136.09(6) 4_565 4_565
O1 Dy1 O9 85.28(6) . 4_565
O8 Dy1 O9 73.56(7) . 4_565
O6 Dy1 O9 140.50(4) . 4_565
O7 Dy1 O9 73.08(6) 4_565 4_565
O7 Dy1 O9 137.81(6) . 4_565
O1 Dy1 O9 85.28(6) 4_565 .
O1 Dy1 O9 136.09(6) . .
O8 Dy1 O9 73.56(7) . .
O6 Dy1 O9 140.50(4) . .
O7 Dy1 O9 137.81(6) 4_565 .
O7 Dy1 O9 73.08(6) . .
O9 Dy1 O9 78.32(8) 4_565 .
O1 Dy1 O10 71.34(6) 4_565 .
O1 Dy1 O10 71.34(6) . .
O8 Dy1 O10 125.29(10) . .
O6 Dy1 O10 128.93(9) . .
O7 Dy1 O10 125.15(4) 4_565 .
O7 Dy1 O10 125.15(4) . .
O9 Dy1 O10 64.80(6) 4_565 .
O9 Dy1 O10 64.80(6) . .
O1 Dy1 Na1 108.32(5) 4_565 1_455
O1 Dy1 Na1 108.32(5) . 1_455
O8 Dy1 Na1 76.78(8) . 1_455
O6 Dy1 Na1 177.43(6) . 1_455
O7 Dy1 Na1 110.98(4) 4_565 1_455
O7 Dy1 Na1 110.98(4) . 1_455
O9 Dy1 Na1 39.87(4) 4_565 1_455
O9 Dy1 Na1 39.87(4) . 1_455
O10 Dy1 Na1 48.51(6) . 1_455
O1 Dy1 Na1 40.67(5) 4_565 .
O1 Dy1 Na1 40.67(5) . .
O8 Dy1 Na1 158.44(8) . .
O6 Dy1 Na1 52.65(6) . .
O7 Dy1 Na1 99.61(4) 4_565 .
O7 Dy1 Na1 99.61(4) . .
O9 Dy1 Na1 121.90(4) 4_565 .
O9 Dy1 Na1 121.90(4) . .
O10 Dy1 Na1 76.28(6) . .
Na1 Dy1 Na1 124.78(4) 1_455 .
C1 O1 Dy1 154.34(16) . .
C1 O1 Na1 102.85(14) . .
Dy1 O1 Na1 102.67(7) . .
C2 O2 Na1 106.98(17) . .
Dy1 O10 Na1 88.51(9) . 1_455
Dy1 O9 Na1 100.57(7) . 1_455
Dy1 O7 H7 109.5 . .
Dy1 O8 H8 109.5 . .
Dy1 O6 H6 109.5 . .
O1 C1 C5 129.1(2) . .
O1 C1 C2 120.8(2) . .
C5 C1 C2 110.2(2) . .
O1 C1 Na1 53.44(12) . .
C5 C1 Na1 157.31(17) . .
C2 C1 Na1 73.05(15) . .
O2 C2 C3 127.8(2) . .
O2 C2 C1 126.0(3) . .
C3 C2 C1 106.1(2) . .
O2 C2 Na1 50.46(14) . .
C3 C2 Na1 163.82(19) . .
C1 C2 Na1 79.08(15) . .
O3 C3 C2 125.4(2) . .
O3 C3 C4 126.4(3) . .
C2 C3 C4 108.0(2) . .
O4 C4 C5 126.8(3) . .
O4 C4 C3 125.2(3) . .
C5 C4 C3 108.0(3) . .
O5 C5 C1 126.7(2) . .
O5 C5 C4 126.1(3) . .
C1 C5 C4 107.1(2) . .
O2 Na1 O2 91.15(11) 4_565 .
O2 Na1 O9 148.08(8) 4_565 4_665
O2 Na1 O9 87.28(6) . 4_665
O2 Na1 O9 87.28(6) 4_565 1_655
O2 Na1 O9 148.08(8) . 1_655
O9 Na1 O9 77.72(9) 4_665 1_655
O2 Na1 O1 118.79(8) 4_565 .
O2 Na1 O1 69.51(6) . .
O9 Na1 O1 90.41(6) 4_665 .
O9 Na1 O1 137.54(8) 1_655 .
O2 Na1 O1 69.51(6) 4_565 4_565
O2 Na1 O1 118.79(8) . 4_565
O9 Na1 O1 137.54(8) 4_665 4_565
O9 Na1 O1 90.41(6) 1_655 4_565
O1 Na1 O1 71.22(8) . 4_565
O2 Na1 O10 87.37(7) 4_565 1_655
O2 Na1 O10 87.37(7) . 1_655
O9 Na1 O10 60.71(6) 4_665 1_655
O9 Na1 O10 60.71(6) 1_655 1_655
O1 Na1 O10 144.29(4) . 1_655
O1 Na1 O10 144.29(4) 4_565 1_655
O2 Na1 C2 22.57(7) 4_565 4_565
O2 Na1 C2 110.13(9) . 4_565
O9 Na1 C2 154.27(8) 4_665 4_565
O9 Na1 C2 77.72(7) 1_655 4_565
O1 Na1 C2 113.06(8) . 4_565
O1 Na1 C2 50.07(6) 4_565 4_565
O10 Na1 C2 100.11(6) 1_655 4_565
O2 Na1 C2 110.13(9) 4_565 .
O2 Na1 C2 22.57(7) . .
O9 Na1 C2 77.72(7) 4_665 .
O9 Na1 C2 154.27(8) 1_655 .
O1 Na1 C2 50.07(6) . .
O1 Na1 C2 113.06(8) 4_565 .
O10 Na1 C2 100.11(6) 1_655 .
C2 Na1 C2 125.10(11) 4_565 .
O2 Na1 C1 123.76(8) 4_565 .
O2 Na1 C1 49.57(7) . .
O9 Na1 C1 77.92(6) 4_665 .
O9 Na1 C1 148.06(8) 1_655 .
O1 Na1 C1 23.71(6) . .
O1 Na1 C1 93.80(7) 4_565 .
O10 Na1 C1 121.88(5) 1_655 .
C2 Na1 C1 127.76(8) 4_565 .
C2 Na1 C1 27.87(6) . .
O2 Na1 C1 49.57(7) 4_565 4_565
O2 Na1 C1 123.76(8) . 4_565
O9 Na1 C1 148.06(8) 4_665 4_565
O9 Na1 C1 77.92(6) 1_655 4_565
O1 Na1 C1 93.80(7) . 4_565
O1 Na1 C1 23.71(6) 4_565 4_565
O10 Na1 C1 121.88(5) 1_655 4_565
C2 Na1 C1 27.87(6) 4_565 4_565
C2 Na1 C1 127.76(8) . 4_565
C1 Na1 C1 114.95(10) . 4_565
O2 Na1 Dy1 116.27(6) 4_565 1_655
O2 Na1 Dy1 116.27(6) . 1_655
O9 Na1 Dy1 39.56(5) 4_665 1_655
O9 Na1 Dy1 39.56(5) 1_655 1_655
O1 Na1 Dy1 124.48(5) . 1_655
O1 Na1 Dy1 124.48(5) 4_565 1_655
O10 Na1 Dy1 42.98(6) 1_655 1_655
C2 Na1 Dy1 114.77(6) 4_565 1_655
C2 Na1 Dy1 114.77(6) . 1_655
C1 Na1 Dy1 117.08(5) . 1_655
C1 Na1 Dy1 117.08(5) 4_565 1_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O1 2.3459(17) 4_565
Dy1 O1 2.3459(17) .
Dy1 O8 2.387(3) .
Dy1 O6 2.414(3) .
Dy1 O7 2.4154(18) 4_565
Dy1 O7 2.4154(18) .
Dy1 O9 2.4440(18) 4_565
Dy1 O9 2.4440(18) .
Dy1 O10 2.573(3) .
Dy1 Na1 3.7722(14) 1_455
Dy1 Na1 3.8332(13) .
O1 C1 1.282(3) .
O1 Na1 2.560(2) .
O2 C2 1.215(3) .
O2 Na1 2.441(2) .
O3 C3 1.244(3) .
O4 C4 1.233(4) .
O5 C5 1.252(3) .
O10 Na1 2.826(3) 1_455
O9 Na1 2.4599(19) 1_455
O7 H7 0.8200 .
O8 H8 0.8200 .
O6 H6 0.8200 .
C1 C5 1.438(4) .
C1 C2 1.479(3) .
C1 Na1 3.108(3) .
C2 C3 1.468(4) .
C2 Na1 3.027(3) .
C3 C4 1.484(4) .
C4 C5 1.472(4) .
Na1 O2 2.441(2) 4_565
Na1 O9 2.4599(19) 4_665
Na1 O9 2.4599(19) 1_655
Na1 O1 2.560(2) 4_565
Na1 O10 2.826(3) 1_655
Na1 C2 3.027(3) 4_565
Na1 C1 3.108(3) 4_565
Na1 Dy1 3.7722(14) 1_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 Dy1 O1 C1 157.3(4) 4_565 .
O8 Dy1 O1 C1 -39.5(4) . .
O6 Dy1 O1 C1 -130.4(4) . .
O7 Dy1 O1 C1 -55.3(4) 4_565 .
O7 Dy1 O1 C1 -154.8(4) . .
O9 Dy1 O1 C1 18.4(4) 4_565 .
O9 Dy1 O1 C1 86.2(4) . .
O10 Dy1 O1 C1 83.4(4) . .
Na1 Dy1 O1 C1 51.4(4) 1_455 .
Na1 Dy1 O1 C1 173.9(4) . .
O1 Dy1 O1 Na1 -16.65(9) 4_565 .
O8 Dy1 O1 Na1 146.64(13) . .
O6 Dy1 O1 Na1 55.70(7) . .
O7 Dy1 O1 Na1 130.80(8) 4_565 .
O7 Dy1 O1 Na1 31.28(12) . .
O9 Dy1 O1 Na1 -155.48(7) 4_565 .
O9 Dy1 O1 Na1 -87.73(10) . .
O10 Dy1 O1 Na1 -90.51(8) . .
Na1 Dy1 O1 Na1 -122.47(6) 1_455 .
O1 Dy1 O10 Na1 137.87(5) 4_565 1_455
O1 Dy1 O10 Na1 -137.87(5) . 1_455
O8 Dy1 O10 Na1 0.0 . 1_455
O6 Dy1 O10 Na1 180.0 . 1_455
O7 Dy1 O10 Na1 -87.81(6) 4_565 1_455
O7 Dy1 O10 Na1 87.81(6) . 1_455
O9 Dy1 O10 Na1 -44.26(5) 4_565 1_455
O9 Dy1 O10 Na1 44.26(5) . 1_455
Na1 Dy1 O10 Na1 180.0 . 1_455
O1 Dy1 O9 Na1 -126.21(7) 4_565 1_455
O1 Dy1 O9 Na1 -57.55(10) . 1_455
O8 Dy1 O9 Na1 88.93(8) . 1_455
O6 Dy1 O9 Na1 -176.02(10) . 1_455
O7 Dy1 O9 Na1 60.72(10) 4_565 1_455
O7 Dy1 O9 Na1 161.44(7) . 1_455
O9 Dy1 O9 Na1 12.83(8) 4_565 1_455
O10 Dy1 O9 Na1 -54.64(7) . 1_455
Na1 Dy1 O9 Na1 -107.64(6) . 1_455
Dy1 O1 C1 C5 34.8(5) . .
Na1 O1 C1 C5 -151.3(2) . .
Dy1 O1 C1 C2 -143.6(3) . .
Na1 O1 C1 C2 30.3(3) . .
Dy1 O1 C1 Na1 -173.9(4) . .
Na1 O2 C2 C3 159.4(2) . .
Na1 O2 C2 C1 -25.4(3) . .
O1 C1 C2 O2 -5.3(4) . .
C5 C1 C2 O2 176.0(3) . .
Na1 C1 C2 O2 19.7(3) . .
O1 C1 C2 C3 170.7(2) . .
C5 C1 C2 C3 -7.9(3) . .
Na1 C1 C2 C3 -164.2(2) . .
O1 C1 C2 Na1 -25.0(2) . .
C5 C1 C2 Na1 156.28(19) . .
O2 C2 C3 O3 4.6(5) . .
C1 C2 C3 O3 -171.3(2) . .
Na1 C2 C3 O3 82.0(7) . .
O2 C2 C3 C4 -178.9(3) . .
C1 C2 C3 C4 5.2(3) . .
Na1 C2 C3 C4 -101.5(7) . .
O3 C3 C4 O4 -2.6(5) . .
C2 C3 C4 O4 -179.0(3) . .
O3 C3 C4 C5 175.7(3) . .
C2 C3 C4 C5 -0.8(3) . .
O1 C1 C5 O5 6.9(4) . .
C2 C1 C5 O5 -174.6(2) . .
Na1 C1 C5 O5 -80.3(5) . .
O1 C1 C5 C4 -171.0(3) . .
C2 C1 C5 C4 7.5(3) . .
Na1 C1 C5 C4 101.7(5) . .
O4 C4 C5 O5 -3.8(5) . .
C3 C4 C5 O5 177.9(2) . .
O4 C4 C5 C1 174.1(3) . .
C3 C4 C5 C1 -4.1(3) . .
C2 O2 Na1 O2 148.04(16) . 4_565
C2 O2 Na1 O9 -63.86(18) . 4_665
C2 O2 Na1 O9 -125.25(19) . 1_655
C2 O2 Na1 O1 27.59(17) . .
C2 O2 Na1 O1 80.90(19) . 4_565
C2 O2 Na1 O10 -124.64(18) . 1_655
C2 O2 Na1 C2 135.5(2) . 4_565
C2 O2 Na1 C1 12.55(16) . .
C2 O2 Na1 C1 108.12(19) . 4_565
C2 O2 Na1 Dy1 -91.72(18) . 1_655
C1 O1 Na1 O2 -109.00(16) . 4_565
Dy1 O1 Na1 O2 68.29(10) . 4_565
C1 O1 Na1 O2 -29.43(15) . .
Dy1 O1 Na1 O2 147.87(9) . .
C1 O1 Na1 O9 57.52(15) . 4_665
Dy1 O1 Na1 O9 -125.18(7) . 4_665
C1 O1 Na1 O9 129.62(15) . 1_655
Dy1 O1 Na1 O9 -53.08(12) . 1_655
C1 O1 Na1 O1 -161.50(13) . 4_565
Dy1 O1 Na1 O1 15.79(9) . 4_565
C1 O1 Na1 O10 23.4(2) . 1_655
Dy1 O1 Na1 O10 -159.27(13) . 1_655
C1 O1 Na1 C2 -133.32(15) . 4_565
Dy1 O1 Na1 C2 43.97(10) . 4_565
C1 O1 Na1 C2 -16.02(15) . .
Dy1 O1 Na1 C2 161.27(11) . .
Dy1 O1 Na1 C1 177.30(19) . .
C1 O1 Na1 C1 -154.16(18) . 4_565
Dy1 O1 Na1 C1 23.14(8) . 4_565
C1 O1 Na1 Dy1 79.03(16) . 1_655
Dy1 O1 Na1 Dy1 -103.67(6) . 1_655
O2 C2 Na1 O2 -34.30(17) . 4_565
C3 C2 Na1 O2 -124.6(6) . 4_565
C1 C2 Na1 O2 124.98(15) . 4_565
C3 C2 Na1 O2 -90.3(7) . .
C1 C2 Na1 O2 159.3(3) . .
O2 C2 Na1 O9 113.41(18) . 4_665
C3 C2 Na1 O9 23.1(7) . 4_665
C1 C2 Na1 O9 -87.31(14) . 4_665
O2 C2 Na1 O9 95.8(2) . 1_655
C3 C2 Na1 O9 5.5(8) . 1_655
C1 C2 Na1 O9 -104.9(2) . 1_655
O2 C2 Na1 O1 -145.5(2) . .
C3 C2 Na1 O1 124.2(7) . .
C1 C2 Na1 O1 13.74(12) . .
O2 C2 Na1 O1 -109.87(18) . 4_565
C3 C2 Na1 O1 159.8(6) . 4_565
C1 C2 Na1 O1 49.41(16) . 4_565
O2 C2 Na1 O10 56.59(19) . 1_655
C3 C2 Na1 O10 -33.7(7) . 1_655
C1 C2 Na1 O10 -144.13(15) . 1_655
O2 C2 Na1 C2 -53.5(2) . 4_565
C3 C2 Na1 C2 -143.8(6) . 4_565
C1 C2 Na1 C2 105.80(16) . 4_565
O2 C2 Na1 C1 -159.3(3) . .
C3 C2 Na1 C1 110.4(7) . .
O2 C2 Na1 C1 -88.16(19) . 4_565
C3 C2 Na1 C1 -178.5(6) . 4_565
C1 C2 Na1 C1 71.12(17) . 4_565
O2 C2 Na1 Dy1 99.19(18) . 1_655
C3 C2 Na1 Dy1 8.9(7) . 1_655
C1 C2 Na1 Dy1 -101.53(14) . 1_655
O1 C1 Na1 O2 85.34(16) . 4_565
C5 C1 Na1 O2 -169.6(4) . 4_565
C2 C1 Na1 O2 -67.74(17) . 4_565
O1 C1 Na1 O2 142.80(18) . .
C5 C1 Na1 O2 -112.1(5) . .
C2 C1 Na1 O2 -10.28(14) . .
O1 C1 Na1 O9 -120.38(16) . 4_665
C5 C1 Na1 O9 -15.3(4) . 4_665
C2 C1 Na1 O9 86.55(15) . 4_665
O1 C1 Na1 O9 -79.4(2) . 1_655
C5 C1 Na1 O9 25.7(5) . 1_655
C2 C1 Na1 O9 127.54(17) . 1_655
C5 C1 Na1 O1 105.1(5) . .
C2 C1 Na1 O1 -153.1(2) . .
O1 C1 Na1 O1 17.52(13) . 4_565
C5 C1 Na1 O1 122.6(4) . 4_565
C2 C1 Na1 O1 -135.56(15) . 4_565
O1 C1 Na1 O10 -164.13(16) . 1_655
C5 C1 Na1 O10 -59.1(5) . 1_655
C2 C1 Na1 O10 42.79(17) . 1_655
O1 C1 Na1 C2 57.86(18) . 4_565
C5 C1 Na1 C2 162.9(4) . 4_565
C2 C1 Na1 C2 -95.21(18) . 4_565
O1 C1 Na1 C2 153.1(2) . .
C5 C1 Na1 C2 -101.9(5) . .
O1 C1 Na1 C1 28.7(2) . 4_565
C5 C1 Na1 C1 133.7(4) . 4_565
C2 C1 Na1 C1 -124.41(14) . 4_565
O1 C1 Na1 Dy1 -114.64(15) . 1_655
C5 C1 Na1 Dy1 -9.6(5) . 1_655
C2 C1 Na1 Dy1 92.28(15) . 1_655
