#------------------------------------------------------------------------------
#$Date: 2016-03-25 16:03:25 +0200 (Fri, 25 Mar 2016) $
#$Revision: 179949 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/44/7024485.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7024485
loop_
_publ_author_name
'Wang, Siegfried M. J.'
'Zhao, Liang'
'Mak, Thomas C. W.'
_publ_section_title
;
 Coordination networks constructed with the multinuclear silver-ethynide
 supramolecular synthon 4-nitrophenyl-C[triple bond]C subset Ag(n) (n = 3,
 4, 5).
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2108
_journal_page_last               2121
_journal_paper_doi               10.1039/b917789b
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         'C19 H11 Ag4 F9 N3 O8'
_chemical_formula_sum            'C19 H11 Ag4 F9 N3 O8'
_chemical_formula_weight         1011.79
_chemical_name_common            'Compound 8'
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.8390(10)
_cell_angle_beta                 93.4210(10)
_cell_angle_gamma                96.3040(10)
_cell_formula_units_Z            2
_cell_length_a                   10.3159(8)
_cell_length_b                   11.0201(8)
_cell_length_c                   12.7685(9)
_cell_measurement_reflns_used    335
_cell_measurement_temperature    296(2)
_cell_volume                     1366.71(17)
_computing_cell_refinement       'BrukerAXS APEX2 Suite 2.1.4'
_computing_data_collection       'BrukerAXS APEX2 Suite 2.1.4'
_computing_data_reduction        'BrukerAXS APEX2 Suite 2.1.4'
_computing_molecular_graphics    'BrukerAXS APEX2 Suite 2.1.4'
_computing_publication_material  'BrukerAXS APEX2 Suite 2.1.4'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'BrukerAXS Kappa APEX2 CCD'
_diffrn_measurement_method       'Omega scan and Phi scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0247
_diffrn_reflns_av_sigmaI/netI    0.0129
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            42251
_diffrn_reflns_theta_full        25.51
_diffrn_reflns_theta_max         25.51
_diffrn_reflns_theta_min         2.00
_exptl_absorpt_coefficient_mu    2.934
_exptl_absorpt_correction_T_max  0.4731
_exptl_absorpt_correction_T_min  0.3585
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    2.459
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             958
_exptl_crystal_size_max          0.44
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.702
_refine_diff_density_min         -0.938
_refine_diff_density_rms         0.068
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     405
_refine_ls_number_reflns         5104
_refine_ls_number_restraints     24
_refine_ls_restrained_S_all      1.054
_refine_ls_R_factor_all          0.0203
_refine_ls_R_factor_gt           0.0185
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0121P)²+2.3897P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0411
_refine_ls_wR_factor_ref         0.0420
_reflns_number_gt                4800
_reflns_number_total             5104
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b917789b.txt
_cod_data_source_block           729719
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7024485
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.62224(2) 0.51594(2) 0.299486(17) 0.03022(6) Uani 1 1 d . . .
Ag2 Ag 0.59883(2) 0.413856(17) 0.493601(16) 0.02490(5) Uani 1 1 d . . .
Ag3 Ag 0.66170(2) 0.634838(19) 0.680169(16) 0.02830(5) Uani 1 1 d . . .
Ag4 Ag 0.87635(2) 0.54782(2) 0.512202(19) 0.03694(6) Uani 1 1 d . . .
C1 C 0.6574(2) 0.6147(2) 0.4968(2) 0.0228(5) Uani 1 1 d . . .
C2 C 0.6934(2) 0.7048(2) 0.4651(2) 0.0243(5) Uani 1 1 d . . .
C3 C 0.74395(16) 0.82274(12) 0.44639(15) 0.0258(5) Uani 1 1 d G . .
C4 C 0.84317(17) 0.82276(12) 0.37736(14) 0.0312(6) Uani 1 1 d G . .
H4 H 0.8710 0.7457 0.3382 0.037 Uiso 1 1 calc R . .
C5 C 0.90075(16) 0.93801(16) 0.36685(15) 0.0353(6) Uani 1 1 d G . .
H5 H 0.9671 0.9380 0.3207 0.042 Uiso 1 1 calc R . .
C6 C 0.85910(18) 1.05324(12) 0.42536(16) 0.0332(6) Uani 1 1 d G . .
C7 C 0.75988(18) 1.05322(12) 0.49438(15) 0.0366(7) Uani 1 1 d G . .
H7 H 0.7320 1.1303 0.5335 0.044 Uiso 1 1 calc R . .
C8 C 0.70230(16) 0.93797(15) 0.50490(14) 0.0337(6) Uani 1 1 d G . .
H8 H 0.6359 0.9380 0.5511 0.040 Uiso 1 1 calc R . .
C15 C 0.8005(3) 0.9286(3) 0.8416(2) 0.0345(6) Uani 1 1 d . . .
C16 C 0.8757(3) 1.0527(3) 0.9062(3) 0.0434(8) Uani 1 1 d . . .
H9 H 0.8251 1.0972 0.9642 0.052 Uiso 1 1 calc R . .
H10 H 0.8911 1.1054 0.8585 0.052 Uiso 1 1 calc R . .
C17 C 1.0081(3) 1.0349(3) 0.9583(3) 0.0436(8) Uani 1 1 d . . .
H11 H 1.0568 0.9871 0.9003 0.052 Uiso 1 1 calc R . .
H12 H 1.0588 1.1187 0.9938 0.052 Uiso 1 1 calc R . .
C18 C 0.6238(3) 0.6444(3) 0.0921(2) 0.0387(7) Uani 1 1 d . . .
C19 C 0.6188(5) 0.7013(3) 0.0036(3) 0.0606(11) Uani 1 1 d . . .
H13 H 0.6634 0.6534 -0.0561 0.091 Uiso 1 1 calc R . .
H14 H 0.6607 0.7888 0.0308 0.091 Uiso 1 1 calc R . .
H15 H 0.5291 0.6995 -0.0222 0.091 Uiso 1 1 calc R . .
C20 C 0.6618(3) 0.3742(3) 0.7226(2) 0.0296(6) Uani 1 1 d . . .
C21 C 0.7130(4) 0.2962(3) 0.7944(3) 0.0487(8) Uani 1 1 d D . .
C22 C 0.5979(3) 0.2182(3) 0.2626(2) 0.0318(6) Uani 1 1 d . A .
C23 C 0.6115(4) 0.0861(3) 0.1796(3) 0.0488(9) Uani 1 1 d D . .
C24 C 0.9705(3) 0.4520(2) 0.2754(2) 0.0288(6) Uani 1 1 d . . .
C25 C 0.9463(3) 0.4186(3) 0.1495(3) 0.0460(8) Uani 1 1 d D . .
F1 F 0.6537(3) 0.1790(3) 0.7661(2) 0.1013(11) Uani 1 1 d D . .
F2 F 0.7029(4) 0.3466(3) 0.8994(2) 0.1101(12) Uani 1 1 d D . .
F3 F 0.8378(3) 0.2854(3) 0.7831(3) 0.0993(10) Uani 1 1 d D . .
F4 F 0.7255(7) 0.0525(8) 0.1977(4) 0.099(3) Uani 0.712(11) 1 d PD A 1
F5 F 0.5174(8) 0.0037(5) 0.1754(8) 0.115(4) Uani 0.712(11) 1 d PD A 1
F6 F 0.6155(8) 0.0922(4) 0.0752(3) 0.0734(18) Uani 0.712(11) 1 d PD A 1
F7 F 0.5067(17) 0.0324(19) 0.1163(16) 0.127(12) Uani 0.288(11) 1 d PD A 2
F8 F 0.702(2) 0.0681(16) 0.133(3) 0.167(15) Uani 0.288(11) 1 d PD A 2
F9 F 0.614(2) -0.0106(9) 0.2338(9) 0.093(7) Uani 0.288(11) 1 d PD A 2
F10 F 0.9162(3) 0.5183(3) 0.12068(19) 0.0775(7) Uani 1 1 d D . .
F11 F 1.0477(3) 0.3798(3) 0.09675(18) 0.0813(8) Uani 1 1 d D . .
F12 F 0.8465(3) 0.3264(3) 0.10942(19) 0.0939(10) Uani 1 1 d D . .
N1 N 0.9259(3) 1.1724(3) 0.4201(3) 0.0458(7) Uani 1 1 d . . .
N2 N 0.7461(3) 0.8313(3) 0.7923(2) 0.0421(6) Uani 1 1 d . . .
N3 N 0.6283(3) 0.5995(3) 0.1606(2) 0.0453(7) Uani 1 1 d . . .
O1 O 0.9108(3) 1.2714(2) 0.4915(2) 0.0557(7) Uani 1 1 d . . .
O2 O 0.9973(3) 1.1688(3) 0.3466(3) 0.0761(9) Uani 1 1 d . . .
O3 O 0.6412(2) 0.31314(18) 0.62289(16) 0.0367(5) Uani 1 1 d . . .
O4 O 0.6497(2) 0.48687(19) 0.77302(16) 0.0363(5) Uani 1 1 d . . .
O5 O 0.5606(2) 0.29760(19) 0.22110(16) 0.0371(5) Uani 1 1 d . . .
O6 O 0.6240(2) 0.2270(2) 0.36044(17) 0.0457(6) Uani 1 1 d . . .
O7 O 0.8752(2) 0.4866(2) 0.32651(17) 0.0443(5) Uani 1 1 d . . .
O8 O 1.0802(2) 0.4421(2) 0.31264(18) 0.0390(5) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N3 Ag1 O5 106.81(9) . .
N3 Ag1 C1 131.68(10) . .
O5 Ag1 C1 121.44(8) . .
N3 Ag1 C2 103.28(10) . .
O5 Ag1 C2 149.86(8) . .
C1 Ag1 C2 28.74(8) . .
N3 Ag1 Ag2 175.96(8) . .
O5 Ag1 Ag2 75.07(5) . .
C1 Ag1 Ag2 46.38(6) . .
C2 Ag1 Ag2 75.03(6) . .
N3 Ag1 Ag3 115.55(7) . 2_666
O5 Ag1 Ag3 55.87(5) . 2_666
C1 Ag1 Ag3 91.23(6) . 2_666
C2 Ag1 Ag3 111.66(6) . 2_666
Ag2 Ag1 Ag3 62.334(7) . 2_666
C1 Ag2 O6 128.56(9) . .
C1 Ag2 O3 130.68(8) . .
O6 Ag2 O3 87.78(7) . .
C1 Ag2 C1 106.89(7) . 2_666
O6 Ag2 C1 101.37(9) . 2_666
O3 Ag2 C1 94.27(8) . 2_666
C1 Ag2 Ag3 52.21(6) . .
O6 Ag2 Ag3 159.18(6) . .
O3 Ag2 Ag3 81.77(5) . .
C1 Ag2 Ag3 97.34(6) 2_666 .
C1 Ag2 Ag2 60.17(6) . 2_666
O6 Ag2 Ag2 130.77(6) . 2_666
O3 Ag2 Ag2 124.30(5) . 2_666
C1 Ag2 Ag2 46.72(5) 2_666 2_666
Ag3 Ag2 Ag2 69.491(9) . 2_666
C1 Ag2 Ag1 51.79(6) . .
O6 Ag2 Ag1 81.12(5) . .
O3 Ag2 Ag1 161.98(6) . .
C1 Ag2 Ag1 101.78(5) 2_666 .
Ag3 Ag2 Ag1 103.979(10) . .
Ag2 Ag2 Ag1 73.410(9) 2_666 .
C1 Ag2 Ag4 53.33(6) . .
O6 Ag2 Ag4 97.37(7) . .
O3 Ag2 Ag4 95.52(6) . .
C1 Ag2 Ag4 159.14(5) 2_666 .
Ag3 Ag2 Ag4 66.011(8) . .
Ag2 Ag2 Ag4 113.131(12) 2_666 .
Ag1 Ag2 Ag4 72.082(7) . .
C1 Ag2 Ag3 94.87(6) . 2_666
O6 Ag2 Ag3 77.07(6) . 2_666
O3 Ag2 Ag3 128.75(6) . 2_666
C1 Ag2 Ag3 43.82(5) 2_666 2_666
Ag3 Ag2 Ag3 123.365(8) . 2_666
Ag2 Ag2 Ag3 53.874(8) 2_666 2_666
Ag1 Ag2 Ag3 62.423(7) . 2_666
Ag4 Ag2 Ag3 134.499(9) . 2_666
N2 Ag3 C1 113.79(10) . .
N2 Ag3 O4 111.45(9) . .
C1 Ag3 O4 132.46(8) . .
N2 Ag3 Ag2 162.62(7) . .
C1 Ag3 Ag2 50.20(6) . .
O4 Ag3 Ag2 82.87(5) . .
N2 Ag3 Ag4 105.28(7) . .
C1 Ag3 Ag4 50.27(6) . .
O4 Ag3 Ag4 103.97(5) . .
Ag2 Ag3 Ag4 60.255(8) . .
N2 Ag3 Ag2 122.48(7) . 2_666
C1 Ag3 Ag2 53.34(6) . 2_666
O4 Ag3 Ag2 110.77(5) . 2_666
Ag2 Ag3 Ag2 56.635(8) . 2_666
Ag4 Ag3 Ag2 100.413(9) . 2_666
N2 Ag3 Ag1 124.24(7) . 2_666
C1 Ag3 Ag1 103.74(6) . 2_666
O4 Ag3 Ag1 59.72(5) . 2_666
Ag2 Ag3 Ag1 70.997(7) . 2_666
Ag4 Ag3 Ag1 130.480(9) . 2_666
Ag2 Ag3 Ag1 55.242(7) 2_666 2_666
O8 Ag4 O7 161.13(8) 2_766 .
O8 Ag4 C1 106.64(8) 2_766 .
O7 Ag4 C1 89.96(8) . .
O8 Ag4 Ag4 83.23(5) 2_766 2_766
O7 Ag4 Ag4 79.86(5) . 2_766
C1 Ag4 Ag4 169.74(6) . 2_766
O8 Ag4 Ag2 93.93(5) 2_766 .
O7 Ag4 Ag2 91.22(6) . .
C1 Ag4 Ag2 46.11(6) . .
Ag4 Ag4 Ag2 132.103(15) 2_766 .
O8 Ag4 Ag3 61.35(5) 2_766 .
O7 Ag4 Ag3 134.38(5) . .
C1 Ag4 Ag3 45.29(6) . .
Ag4 Ag4 Ag3 144.419(13) 2_766 .
Ag2 Ag4 Ag3 53.734(7) . .
C2 C1 Ag2 159.9(2) . .
C2 C1 Ag3 121.9(2) . .
Ag2 C1 Ag3 77.59(8) . .
C2 C1 Ag1 78.76(17) . .
Ag2 C1 Ag1 81.83(8) . .
Ag3 C1 Ag1 159.33(12) . .
C2 C1 Ag4 95.54(18) . .
Ag2 C1 Ag4 80.56(8) . .
Ag3 C1 Ag4 84.44(8) . .
Ag1 C1 Ag4 94.15(9) . .
C2 C1 Ag2 111.74(19) . 2_666
Ag2 C1 Ag2 73.11(7) . 2_666
Ag3 C1 Ag2 82.84(8) . 2_666
Ag1 C1 Ag2 89.39(8) . 2_666
Ag4 C1 Ag2 152.65(11) . 2_666
C1 C2 C3 170.4(3) . .
C1 C2 Ag1 72.51(17) . .
C3 C2 Ag1 116.94(16) . .
C4 C3 C8 120.0 . .
C4 C3 C2 119.67(14) . .
C8 C3 C2 120.07(14) . .
C3 C4 C5 120.0 . .
C3 C4 H4 120.0 . .
C5 C4 H4 120.0 . .
C6 C5 C4 120.0 . .
C6 C5 H5 120.0 . .
C4 C5 H5 120.0 . .
C7 C6 C5 120.0 . .
C7 C6 N1 120.44(18) . .
C5 C6 N1 119.40(18) . .
C6 C7 C8 120.0 . .
C6 C7 H7 120.0 . .
C8 C7 H7 120.0 . .
C7 C8 C3 120.0 . .
C7 C8 H8 120.0 . .
C3 C8 H8 120.0 . .
N2 C15 C16 177.8(3) . .
C15 C16 C17 111.4(3) . .
C15 C16 H9 109.3 . .
C17 C16 H9 109.3 . .
C15 C16 H10 109.3 . .
C17 C16 H10 109.3 . .
H9 C16 H10 108.0 . .
C17 C17 C16 112.4(3) 2_777 .
C17 C17 H11 109.1 2_777 .
C16 C17 H11 109.1 . .
C17 C17 H12 109.1 2_777 .
C16 C17 H12 109.1 . .
H11 C17 H12 107.9 . .
N3 C18 C19 179.6(4) . .
C18 C19 H13 109.5 . .
C18 C19 H14 109.5 . .
H13 C19 H14 109.5 . .
C18 C19 H15 109.5 . .
H13 C19 H15 109.5 . .
H14 C19 H15 109.5 . .
O4 C20 O3 130.5(3) . .
O4 C20 C21 115.5(3) . .
O3 C20 C21 114.0(3) . .
F1 C21 F2 106.4(3) . .
F1 C21 F3 105.4(3) . .
F2 C21 F3 107.1(3) . .
F1 C21 C20 113.1(3) . .
F2 C21 C20 113.9(3) . .
F3 C21 C20 110.4(3) . .
O6 C22 O5 130.1(3) . .
O6 C22 C23 114.6(3) . .
O5 C22 C23 115.3(3) . .
F8 C23 F5 125.5(8) . .
F8 C23 F7 110.9(15) . .
F5 C23 F7 42.2(10) . .
F8 C23 F4 44(2) . .
F5 C23 F4 114.4(6) . .
F7 C23 F4 135.5(8) . .
F8 C23 F6 58(2) . .
F5 C23 F6 105.9(5) . .
F7 C23 F6 66.4(12) . .
F4 C23 F6 101.6(4) . .
F8 C23 F9 99.1(15) . .
F5 C23 F9 55.7(7) . .
F7 C23 F9 95.5(11) . .
F4 C23 F9 63.6(8) . .
F6 C23 F9 137.3(5) . .
F8 C23 C22 122.2(7) . .
F5 C23 C22 112.2(4) . .
F7 C23 C22 113.6(7) . .
F4 C23 C22 110.7(4) . .
F6 C23 C22 111.5(3) . .
F9 C23 C22 111.2(5) . .
O8 C24 O7 128.6(3) . .
O8 C24 C25 116.7(3) . .
O7 C24 C25 114.7(2) . .
F11 C25 F12 107.3(3) . .
F11 C25 F10 106.6(3) . .
F12 C25 F10 106.4(3) . .
F11 C25 C24 113.7(3) . .
F12 C25 C24 110.8(3) . .
F10 C25 C24 111.6(3) . .
O2 N1 O1 123.7(3) . .
O2 N1 C6 118.4(3) . .
O1 N1 C6 118.0(3) . .
C15 N2 Ag3 172.1(3) . .
C18 N3 Ag1 175.6(3) . .
C20 O3 Ag2 121.34(17) . .
C20 O4 Ag3 118.95(17) . .
C22 O5 Ag1 122.65(18) . .
C22 O6 Ag2 118.64(18) . .
C24 O7 Ag4 124.56(18) . .
C24 O8 Ag4 121.89(19) . 2_766
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N3 2.235(3) .
Ag1 O5 2.304(2) .
Ag1 C1 2.406(3) .
Ag1 C2 2.474(3) .
Ag1 Ag2 3.0311(3) .
Ag1 Ag3 3.2702(4) 2_666
Ag2 C1 2.217(2) .
Ag2 O6 2.285(2) .
Ag2 O3 2.3003(18) .
Ag2 C1 2.642(2) 2_666
Ag2 Ag3 2.8179(3) .
Ag2 Ag2 2.9137(4) 2_666
Ag2 Ag4 3.0344(4) .
Ag2 Ag3 3.2675(3) 2_666
Ag3 N2 2.243(3) .
Ag3 C1 2.280(2) .
Ag3 O4 2.2885(19) .
Ag3 Ag4 3.1930(3) .
Ag3 Ag2 3.2675(3) 2_666
Ag3 Ag1 3.2702(4) 2_666
Ag4 O8 2.221(2) 2_766
Ag4 O7 2.256(2) .
Ag4 C1 2.467(2) .
Ag4 Ag4 2.8636(5) 2_766
C1 C2 1.213(4) .
C1 Ag2 2.642(2) 2_666
C2 C3 1.440(3) .
C3 C4 1.3900 .
C3 C8 1.3900 .
C4 C5 1.3900 .
C4 H4 0.9300 .
C5 C6 1.3900 .
C5 H5 0.9300 .
C6 C7 1.3900 .
C6 N1 1.437(3) .
C7 C8 1.3900 .
C7 H7 0.9300 .
C8 H8 0.9300 .
C15 N2 1.129(4) .
C15 C16 1.466(4) .
C16 C17 1.542(4) .
C16 H9 0.9700 .
C16 H10 0.9700 .
C17 C17 1.500(6) 2_777
C17 H11 0.9700 .
C17 H12 0.9700 .
C18 N3 1.130(4) .
C18 C19 1.452(4) .
C19 H13 0.9600 .
C19 H14 0.9600 .
C19 H15 0.9600 .
C20 O4 1.235(3) .
C20 O3 1.237(3) .
C20 C21 1.544(4) .
C21 F1 1.298(4) .
C21 F2 1.301(4) .
C21 F3 1.318(4) .
C22 O6 1.234(3) .
C22 O5 1.236(3) .
C22 C23 1.542(4) .
C23 F8 1.144(11) .
C23 F5 1.241(6) .
C23 F7 1.279(12) .
C23 F4 1.299(6) .
C23 F6 1.358(5) .
C23 F9 1.439(11) .
C24 O8 1.231(3) .
C24 O7 1.242(3) .
C24 C25 1.534(4) .
C25 F11 1.318(4) .
C25 F12 1.320(4) .
C25 F10 1.322(4) .
N1 O2 1.221(4) .
N1 O1 1.221(4) .
O8 Ag4 2.221(2) 2_766
