#------------------------------------------------------------------------------
#$Date: 2016-03-25 22:59:02 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180021 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/15/7031500.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7031500
loop_
_publ_author_name
'Pajerowski, Daniel M.'
'Li, Quan'
'Hyun, Jason'
'Dennis, Cindi L.'
'Phelan, Daniel'
'Yan, Pengfei'
'Chen, Peng'
'Li, Guangming'
_publ_section_title
;
 Chloride-bridged, defect-dicubane {Ln4} core clusters: syntheses, crystal
 structures and magnetic properties.
;
_journal_issue                   31
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              11973
_journal_page_last               11980
_journal_paper_doi               10.1039/c4dt01329h
_journal_volume                  43
_journal_year                    2014
_chemical_formula_moiety         'C12 H50 Cl6 Dy4 O14, 2(C H4 O), 4(Cl) '
_chemical_formula_sum            'C14 H58 Cl10 Dy4 O16'
_chemical_formula_weight         1487.10
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                87.55(3)
_cell_angle_beta                 86.14(3)
_cell_angle_gamma                62.66(3)
_cell_formula_units_Z            1
_cell_length_a                   10.328(2)
_cell_length_b                   10.653(2)
_cell_length_c                   11.639(2)
_cell_measurement_reflns_used    11167
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.51
_cell_volume                     1134.8(5)
_computing_cell_refinement       'Bruker FRAMBO'
_computing_data_collection       'Bruker FRAMBO'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0431
_diffrn_reflns_av_unetI/netI     0.0551
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            11167
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.51
_exptl_absorpt_coefficient_mu    7.146
_exptl_absorpt_correction_T_max  0.395
_exptl_absorpt_correction_T_min  0.180
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs(Sheldrick,1996)
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.176
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             704
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.13
_refine_diff_density_max         4.026
_refine_diff_density_min         -1.585
_refine_diff_density_rms         0.224
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     210
_refine_ls_number_reflns         5203
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.0468
_refine_ls_R_factor_gt           0.0423
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0470P)²+7.1137P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1070
_refine_ls_wR_factor_ref         0.1098
_reflns_number_gt                4620
_reflns_number_total             5203
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt01329h1.cif
_cod_data_source_block           c
_cod_depositor_comments
'Adding full bibliography for 7031499--7031501.cif.'
_cod_original_cell_volume        1134.8(4)
_cod_database_code               7031500
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy -0.04465(3) 0.38007(3) 0.42843(3) 0.02175(10) Uani 1 1 d .
Dy2 Dy -0.16791(3) 0.44726(3) 0.75864(3) 0.02464(10) Uani 1 1 d .
C1 C -0.4588(12) 0.7465(12) 0.6698(13) 0.084(4) Uani 1 1 d .
H1A H -0.5618 0.8023 0.6859 0.127 Uiso 1 1 calc R
H1B H -0.4413 0.7150 0.5916 0.127 Uiso 1 1 calc R
H1C H -0.4099 0.8027 0.6806 0.127 Uiso 1 1 calc R
C1M C 0.377(2) -0.0431(19) 0.1094(17) 0.122(6) Uani 1 1 d .
H1M1 H 0.4313 0.0071 0.1219 0.183 Uiso 1 1 calc R
H1M2 H 0.2742 0.0212 0.1142 0.183 Uiso 1 1 calc R
H1M3 H 0.4036 -0.0847 0.0344 0.183 Uiso 1 1 calc R
C2 C -0.2689(16) 0.6194(13) 1.0277(10) 0.082(4) Uani 1 1 d .
H2A H -0.2718 0.5953 1.1079 0.124 Uiso 1 1 calc R
H2B H -0.3652 0.6857 1.0064 0.124 Uiso 1 1 calc R
H2C H -0.2042 0.6611 1.0139 0.124 Uiso 1 1 calc R
C3 C 0.0624(12) 0.1557(11) 0.9201(9) 0.063(3) Uani 1 1 d .
H3A H 0.1633 0.0865 0.9159 0.095 Uiso 1 1 calc R
H3B H 0.0020 0.1090 0.9195 0.095 Uiso 1 1 calc R
H3C H 0.0411 0.2080 0.9900 0.095 Uiso 1 1 calc R
C4 C 0.2573(13) 0.0466(10) 0.4053(11) 0.069(3) Uani 1 1 d .
H4A H 0.3268 -0.0228 0.4545 0.104 Uiso 1 1 calc R
H4B H 0.3077 0.0768 0.3470 0.104 Uiso 1 1 calc R
H4C H 0.2045 0.0060 0.3694 0.104 Uiso 1 1 calc R
C5 C -0.0978(14) 0.0919(10) 0.3418(11) 0.064(3) Uani 1 1 d .
H5A H -0.1418 0.0694 0.2811 0.095 Uiso 1 1 calc R
H5B H -0.1440 0.0854 0.4146 0.095 Uiso 1 1 calc R
H5C H 0.0044 0.0266 0.3412 0.095 Uiso 1 1 calc R
C6 C -0.4101(9) 0.5550(10) 0.3665(10) 0.056(2) Uani 1 1 d .
H6A H -0.4080 0.4746 0.4085 0.084 Uiso 1 1 calc R
H6B H -0.4437 0.5580 0.2910 0.084 Uiso 1 1 calc R
H6C H -0.4750 0.6398 0.4066 0.084 Uiso 1 1 calc R
O1 O -0.4053(6) 0.6289(6) 0.7448(6) 0.0439(13) Uani 1 1 d .
H2O1 H -0.4400 0.6584 0.8122 0.053 Uiso 1 1 d R
O2 O -0.2185(9) 0.4966(7) 0.9616(5) 0.0571(18) Uani 1 1 d .
H1O2 H -0.1529 0.4283 0.9974 0.069 Uiso 1 1 d R
O3 O -0.2995(7) 0.3311(7) 0.8451(5) 0.0517(16) Uani 1 1 d .
H1O3 H -0.3192 0.2629 0.8615 0.062 Uiso 1 1 d R
O4 O -0.1152(7) 0.2306(6) 0.3250(5) 0.0399(12) Uani 1 1 d .
H1O4 H -0.1888 0.2853 0.2877 0.048 Uiso 1 1 d R
O5 O 0.1592(6) 0.1634(5) 0.4709(6) 0.0432(13) Uani 1 1 d .
H1O5 H 0.1811 0.1575 0.5407 0.052 Uiso 1 1 d R
O6 O -0.2676(5) 0.5439(6) 0.3567(5) 0.0384(12) Uani 1 1 d .
H2O6 H -0.2711 0.6249 0.3462 0.046 Uiso 1 1 d R
O7 O 0.0340(6) 0.2492(6) 0.8244(5) 0.0447(14) Uani 1 1 d .
H2O7 H 0.1085 0.2315 0.7796 0.054 Uiso 1 1 d R
O1M O 0.4063(10) -0.1469(10) 0.1912(8) 0.083(3) Uani 1 1 d .
H223 H 0.4929 -0.2001 0.2136 0.099 Uiso 1 1 d R
Cl1 Cl -0.3100(3) 0.2995(3) 0.11167(19) 0.0521(5) Uani 1 1 d .
Cl2 Cl 0.3248(2) 0.1485(2) 0.6863(2) 0.0482(5) Uani 1 1 d .
Cl3 Cl 0.0703(3) 0.3577(2) 0.19997(17) 0.0473(5) Uani 1 1 d .
Cl4 Cl -0.2017(2) 0.2917(2) 0.58946(16) 0.0361(4) Uani 1 1 d .
Cl5 Cl -0.0094(5) 0.5835(5) 0.3836(4) 0.0466(9) Uani 0.50 1 d P
Cl6 Cl 0.1347(5) 0.4595(4) 0.4164(4) 0.0466(9) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O6 Dy1 Cl6 113.51(17) . .
O6 Dy1 O5 161.1(2) . .
Cl6 Dy1 O5 81.69(18) . .
O6 Dy1 Cl6 80.59(18) . 2_566
Cl6 Dy1 Cl6 81.25(16) . 2_566
O5 Dy1 Cl6 114.10(18) . 2_566
O6 Dy1 Cl5 117.98(18) . 2_566
Cl6 Dy1 Cl5 69.74(16) . 2_566
O5 Dy1 Cl5 77.01(18) . 2_566
Cl6 Dy1 Cl5 37.47(15) 2_566 2_566
O6 Dy1 Cl5 76.29(17) . .
Cl6 Dy1 Cl5 37.55(15) . .
O5 Dy1 Cl5 119.17(18) . .
Cl6 Dy1 Cl5 69.44(15) 2_566 .
Cl5 Dy1 Cl5 82.42(17) 2_566 .
O6 Dy1 O4 77.8(2) . .
Cl6 Dy1 O4 139.49(18) . .
O5 Dy1 O4 83.3(2) . .
Cl6 Dy1 O4 139.01(18) 2_566 .
Cl5 Dy1 O4 141.50(17) 2_566 .
Cl5 Dy1 O4 135.98(17) . .
O6 Dy1 Cl4 88.30(15) . .
Cl6 Dy1 Cl4 141.42(12) . .
O5 Dy1 Cl4 85.66(16) . .
Cl6 Dy1 Cl4 71.02(11) 2_566 .
Cl5 Dy1 Cl4 71.94(12) 2_566 .
Cl5 Dy1 Cl4 139.32(11) . .
O4 Dy1 Cl4 73.90(15) . .
O6 Dy1 Cl3 86.25(16) . .
Cl6 Dy1 Cl3 70.70(12) . .
O5 Dy1 Cl3 88.57(17) . .
Cl6 Dy1 Cl3 141.00(12) 2_566 .
Cl5 Dy1 Cl3 139.38(12) 2_566 .
Cl5 Dy1 Cl3 71.82(12) . .
O4 Dy1 Cl3 71.53(15) . .
Cl4 Dy1 Cl3 145.38(5) . .
O6 Dy1 Dy1 98.86(14) . 2_566
Cl6 Dy1 Dy1 40.77(11) . 2_566
O5 Dy1 Dy1 100.07(14) . 2_566
Cl6 Dy1 Dy1 40.48(11) 2_566 2_566
Cl5 Dy1 Dy1 41.25(11) 2_566 2_566
Cl5 Dy1 Dy1 41.17(11) . 2_566
O4 Dy1 Dy1 176.46(14) . 2_566
Cl4 Dy1 Dy1 107.37(4) . 2_566
Cl3 Dy1 Dy1 107.24(5) . 2_566
O6 Dy1 Dy2 96.64(15) . .
Cl6 Dy1 Dy2 99.58(11) . .
O5 Dy1 Dy2 91.54(16) . .
Cl6 Dy1 Dy2 31.67(11) 2_566 .
Cl5 Dy1 Dy2 31.75(11) 2_566 .
Cl5 Dy1 Dy2 99.66(11) . .
O4 Dy1 Dy2 118.25(14) . .
Cl4 Dy1 Dy2 44.35(4) . .
Cl3 Dy1 Dy2 170.17(4) . .
Dy1 Dy1 Dy2 63.06(2) 2_566 .
O6 Dy1 Dy2 91.38(14) . 2_566
Cl6 Dy1 Dy2 31.43(11) . 2_566
O5 Dy1 Dy2 97.57(16) . 2_566
Cl6 Dy1 Dy2 99.24(11) 2_566 2_566
Cl5 Dy1 Dy2 99.66(11) 2_566 2_566
Cl5 Dy1 Dy2 31.73(10) . 2_566
O4 Dy1 Dy2 115.62(14) . 2_566
Cl4 Dy1 Dy2 170.18(4) . 2_566
Cl3 Dy1 Dy2 44.30(4) . 2_566
Dy1 Dy1 Dy2 62.977(19) 2_566 2_566
Dy2 Dy1 Dy2 126.04(2) . 2_566
Cl5 Dy2 Cl6 38.78(15) 2_566 2_566
Cl5 Dy2 O7 77.54(19) 2_566 .
Cl6 Dy2 O7 116.28(19) 2_566 .
Cl5 Dy2 O1 120.71(19) 2_566 .
Cl6 Dy2 O1 81.94(19) 2_566 .
O7 Dy2 O1 161.7(2) . .
Cl5 Dy2 O3 140.8(2) 2_566 .
Cl6 Dy2 O3 140.16(19) 2_566 .
O7 Dy2 O3 83.6(2) . .
O1 Dy2 O3 80.7(2) . .
Cl5 Dy2 O2 139.9(2) 2_566 .
Cl6 Dy2 O2 143.16(19) 2_566 .
O7 Dy2 O2 82.5(2) . .
O1 Dy2 O2 83.2(3) . .
O3 Dy2 O2 69.0(2) . .
Cl5 Dy2 Cl3 73.96(12) 2_566 2_566
Cl6 Dy2 Cl3 72.35(12) 2_566 2_566
O7 Dy2 Cl3 96.73(17) . 2_566
O1 Dy2 Cl3 90.33(16) . 2_566
O3 Dy2 Cl3 142.91(16) . 2_566
O2 Dy2 Cl3 74.24(17) . 2_566
Cl5 Dy2 Cl4 73.89(12) 2_566 .
Cl6 Dy2 Cl4 72.75(12) 2_566 .
O7 Dy2 Cl4 91.43(16) . .
O1 Dy2 Cl4 92.67(16) . .
O3 Dy2 Cl4 72.59(16) . .
O2 Dy2 Cl4 141.56(17) . .
Cl3 Dy2 Cl4 144.16(6) 2_566 .
Cl5 Dy2 Dy1 33.06(11) 2_566 .
Cl6 Dy2 Dy1 32.75(11) 2_566 .
O7 Dy2 Dy1 95.29(16) . .
O1 Dy2 Dy1 100.24(16) . .
O3 Dy2 Dy1 117.76(15) . .
O2 Dy2 Dy1 172.71(17) . .
Cl3 Dy2 Dy1 99.20(5) 2_566 .
Cl4 Dy2 Dy1 45.17(4) . .
Cl5 Dy2 Dy1 33.10(11) 2_566 2_566
Cl6 Dy2 Dy1 32.29(11) 2_566 2_566
O7 Dy2 Dy1 97.93(16) . 2_566
O1 Dy2 Dy1 99.02(15) . 2_566
O3 Dy2 Dy1 171.63(15) . 2_566
O2 Dy2 Dy1 119.32(16) . 2_566
Cl3 Dy2 Dy1 45.26(4) 2_566 2_566
Cl4 Dy2 Dy1 99.10(4) . 2_566
Dy1 Dy2 Dy1 53.96(2) . 2_566
O1 C1 H1A 109.5 . .
O1 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
O1 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
O1M C1M H1M1 109.5 . .
O1M C1M H1M2 109.5 . .
H1M1 C1M H1M2 109.5 . .
O1M C1M H1M3 109.5 . .
H1M1 C1M H1M3 109.5 . .
H1M2 C1M H1M3 109.5 . .
O2 C2 H2A 109.5 . .
O2 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
O2 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
O7 C3 H3A 109.5 . .
O7 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
O7 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
O5 C4 H4A 109.5 . .
O5 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
O5 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
O4 C5 H5A 109.5 . .
O4 C5 H5B 109.5 . .
H5A C5 H5B 109.5 . .
O4 C5 H5C 109.5 . .
H5A C5 H5C 109.5 . .
H5B C5 H5C 109.5 . .
O6 C6 H6A 109.5 . .
O6 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
O6 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C1 O1 Dy2 129.5(6) . .
C1 O1 H2O1 107.4 . .
Dy2 O1 H2O1 108.3 . .
C2 O2 Dy2 134.4(7) . .
C2 O2 H1O2 108.7 . .
Dy2 O2 H1O2 107.5 . .
Dy2 O3 H1O3 157.2 . .
C5 O4 Dy1 134.3(6) . .
C5 O4 H1O4 114.7 . .
Dy1 O4 H1O4 106.8 . .
C4 O5 Dy1 134.4(7) . .
C4 O5 H1O5 113.1 . .
Dy1 O5 H1O5 112.3 . .
C6 O6 Dy1 132.9(5) . .
C6 O6 H2O6 110.8 . .
Dy1 O6 H2O6 111.6 . .
C3 O7 Dy2 135.9(6) . .
C3 O7 H2O7 113.8 . .
Dy2 O7 H2O7 110.2 . .
C1M O1M H223 123.1 . .
Dy2 Cl3 Dy1 90.43(6) 2_566 .
Dy2 Cl4 Dy1 90.47(5) . .
Cl6 Cl5 Dy2 70.7(2) . 2_566
Cl6 Cl5 Dy1 70.8(2) . 2_566
Dy2 Cl5 Dy1 115.19(18) 2_566 2_566
Cl6 Cl5 Dy1 70.2(2) . .
Dy2 Cl5 Dy1 115.18(18) 2_566 .
Dy1 Cl5 Dy1 97.58(17) 2_566 .
Cl5 Cl6 Dy2 70.5(2) . 2_566
Cl5 Cl6 Dy1 72.3(2) . .
Dy2 Cl6 Dy1 116.28(19) 2_566 .
Cl5 Cl6 Dy1 71.7(2) . 2_566
Dy2 Cl6 Dy1 115.58(18) 2_566 2_566
Dy1 Cl6 Dy1 98.75(16) . 2_566
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O6 2.343(5) .
Dy1 Cl6 2.358(4) .
Dy1 O5 2.363(5) .
Dy1 Cl6 2.372(4) 2_566
Dy1 Cl5 2.384(5) 2_566
Dy1 Cl5 2.388(5) .
Dy1 O4 2.421(5) .
Dy1 Cl4 2.8053(19) .
Dy1 Cl3 2.812(2) .
Dy1 Dy1 3.5903(10) 2_566
Dy1 Dy2 3.9552(11) .
Dy1 Dy2 3.9582(11) 2_566
Dy2 Cl5 2.300(4) 2_566
Dy2 Cl6 2.302(5) 2_566
Dy2 O7 2.329(6) .
Dy2 O1 2.335(5) .
Dy2 O3 2.377(6) .
Dy2 O2 2.412(6) .
Dy2 Cl3 2.765(2) 2_566
Dy2 Cl4 2.7651(19) .
Dy2 Dy1 3.9582(11) 2_566
C1 O1 1.405(12) .
C1 H1A 0.9600 .
C1 H1B 0.9600 .
C1 H1C 0.9600 .
C1M O1M 1.364(17) .
C1M H1M1 0.9600 .
C1M H1M2 0.9600 .
C1M H1M3 0.9600 .
C2 O2 1.408(12) .
C2 H2A 0.9600 .
C2 H2B 0.9600 .
C2 H2C 0.9600 .
C3 O7 1.414(11) .
C3 H3A 0.9600 .
C3 H3B 0.9600 .
C3 H3C 0.9600 .
C4 O5 1.406(10) .
C4 H4A 0.9600 .
C4 H4B 0.9600 .
C4 H4C 0.9600 .
C5 O4 1.410(11) .
C5 H5A 0.9600 .
C5 H5B 0.9600 .
C5 H5C 0.9600 .
C6 O6 1.419(9) .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
O1 H2O1 0.8499 .
O2 H1O2 0.8496 .
O3 H1O3 0.8500 .
O4 H1O4 0.8500 .
O5 H1O5 0.8494 .
O6 H2O6 0.8498 .
O7 H2O7 0.8490 .
O1M H223 0.8614 .
Cl3 Dy2 2.765(2) 2_566
Cl5 Cl6 1.528(6) .
Cl5 Dy2 2.300(4) 2_566
Cl5 Dy1 2.384(5) 2_566
Cl6 Dy2 2.302(5) 2_566
Cl6 Dy1 2.372(4) 2_566
