#------------------------------------------------------------------------------
#$Date: 2016-03-25 23:05:32 +0200 (Fri, 25 Mar 2016) $
#$Revision: 180025 $
#$URL: svn://www.crystallography.net/cod/cif/7/03/19/7031984.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7031984
loop_
_publ_author_name
'Reis, Samira G.'
'Del Águila-Sánchez, Miguel A'
'Guedes, Guilherme P.'
'Ferreira, Glaucio B.'
'Novak, Miguel A.'
'Speziali, Nivaldo L.'
'López-Ortiz, Fernando'
'Vaz, Maria G. F.'
_publ_section_title
;
 Synthesis, crystal structures and magnetic behaviour of four coordination
 compounds constructed with a phosphinic amide-TEMPO radical and
 [M(hfac)2] (M = Cu(II), Co(II) and Mn(II)).
;
_journal_issue                   39
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              14889
_journal_page_last               14901
_journal_paper_doi               10.1039/c4dt01444h
_journal_volume                  43
_journal_year                    2014
_chemical_absolute_configuration unk
_chemical_formula_moiety         'C31 H30 Co F12 N2 O6 P'
_chemical_formula_sum            'C31 H30 Co F12 N2 O6 P'
_chemical_formula_weight         844.47
_space_group_IT_number           110
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  'I 4bw -2c'
_symmetry_space_group_name_H-M   'I 41 c d'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2014-02-25T09:24:50-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   28.414(4)
_cell_length_b                   28.414(4)
_cell_length_c                   18.162(4)
_cell_measurement_temperature    293(2)
_cell_volume                     14663(4)
_computing_cell_refinement       'DIRAX (Duisenberg, 1992)'
_computing_data_collection       'COLLECT (Enraf-Nonius, 1997-2000.)'
_computing_data_reduction        'EVALCCD (Duisenberg, 2003)'
_computing_molecular_graphics
;
Ortep-3 for Windows: L. J. Farrugia, J. Appl. Cryst (1997), 30, 565
;
_computing_publication_material
'WinGX publication routines (Farrugia, 1999) and PublCIF'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker-Nonius Kappa-CCD'
_diffrn_measurement_method       ' φ-ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0658
_diffrn_reflns_av_unetI/netI     0.0363
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -33
_diffrn_reflns_limit_k_max       33
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            56145
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         3.16
_exptl_absorpt_coefficient_mu    0.616
_exptl_absorpt_correction_T_max  0.826
_exptl_absorpt_correction_T_min  0.806
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
SADABS, Bruker Analytical X-ray Systems,Inc., Madison WI, 1997.
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.53
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             6848
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.35
_exptl_crystal_size_min          0.31
_refine_diff_density_max         0.535
_refine_diff_density_min         -0.42
_refine_diff_density_rms         0.07
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.02(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.121
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     479
_refine_ls_number_reflns         6429
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.121
_refine_ls_R_factor_all          0.0826
_refine_ls_R_factor_gt           0.0528
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0476P)²+55.2655P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1211
_refine_ls_wR_factor_ref         0.1466
_reflns_number_gt                5066
_reflns_number_total             6469
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c4dt01444h2.cif
_cod_data_source_block           sad
_cod_depositor_comments
'Adding full bibliography for 7031981--7031984.cif.'
_cod_original_cell_volume        14663(5)
_cod_original_sg_symbol_H-M      'I 41 cd'
_cod_database_code               7031984
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'-y, x+1/2, z+1/4'
'y+1/2, -x, z+3/4'
'x, -y, z+1/2'
'-x+1/2, y+1/2, z'
'-y, -x+1/2, z+3/4'
'y+1/2, x, z+1/4'
'x+1/2, y+1/2, z+1/2'
'-x+1, -y+1, z+1'
'-y+1/2, x+1, z+3/4'
'y+1, -x+1/2, z+5/4'
'x+1/2, -y+1/2, z+1'
'-x+1, y+1, z+1/2'
'-y+1/2, -x+1, z+5/4'
'y+1, x+1/2, z+3/4'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C8 C 0.4424(2) 0.2733(2) 0.9741(3) 0.0447(13) Uani 1 1 d . . .
H8 H 0.4303 0.2411 0.9701 0.054 Uiso 1 1 calc R . .
C3 C 0.4222(3) 0.3011(3) 1.1792(4) 0.0630(18) Uani 1 1 d . . .
H3A H 0.4416 0.3286 1.1751 0.094 Uiso 1 1 calc R . .
H3B H 0.4295 0.2849 1.2242 0.094 Uiso 1 1 calc R . .
H3C H 0.3897 0.3102 1.1794 0.094 Uiso 1 1 calc R . .
F4 F 0.5456(2) 0.0333(2) 0.6154(5) 0.143(3) Uani 1 1 d . . .
C2 C 0.4011(2) 0.2248(2) 1.1185(4) 0.0594(17) Uani 1 1 d . . .
H2A H 0.4076 0.2049 1.077 0.089 Uiso 1 1 calc R . .
H2B H 0.3685 0.2337 1.1181 0.089 Uiso 1 1 calc R . .
H2C H 0.408 0.2081 1.1632 0.089 Uiso 1 1 calc R . .
F1 F 0.3552(2) 0.1049(4) 0.7091(5) 0.181(4) Uani 1 1 d . . .
C5 C 0.5059(3) 0.1897(3) 1.0355(4) 0.070(2) Uani 1 1 d . . .
H5A H 0.5156 0.1721 1.0781 0.105 Uiso 1 1 calc R . .
H5B H 0.5249 0.1808 0.9941 0.105 Uiso 1 1 calc R . .
H5C H 0.4734 0.183 1.025 0.105 Uiso 1 1 calc R . .
F3 F 0.38306(19) 0.0599(2) 0.6333(6) 0.189(5) Uani 1 1 d . . .
F5 F 0.5882(2) 0.0910(3) 0.6098(6) 0.174(4) Uani 1 1 d . . .
C6 C 0.5631(2) 0.2530(3) 1.0682(5) 0.075(2) Uani 1 1 d . . .
H6A H 0.5663 0.286 1.0782 0.113 Uiso 1 1 calc R . .
H6B H 0.5826 0.2446 1.0271 0.113 Uiso 1 1 calc R . .
H6C H 0.5727 0.2353 1.1107 0.113 Uiso 1 1 calc R . .
F6 F 0.5829(3) 0.0572(3) 0.7061(5) 0.182(4) Uani 1 1 d . . .
F2 F 0.3674(3) 0.1272(4) 0.6108(7) 0.224(6) Uani 1 1 d . . .
H2 H 0.434(2) 0.326(2) 0.909(3) 0.044(19) Uiso 1 1 d . . .
Co1 Co 0.49279(2) 0.19010(2) 0.75784(5) 0.04118(19) Uani 1 1 d . . .
P1 P 0.41515(5) 0.27176(5) 0.83132(8) 0.0391(3) Uani 1 1 d . . .
O4 O 0.53295(14) 0.14148(14) 0.7008(2) 0.0498(10) Uani 1 1 d . . .
O2 O 0.44782(14) 0.23214(13) 0.8140(2) 0.0468(10) Uani 1 1 d . . .
O1 O 0.50021(15) 0.24480(13) 1.1796(2) 0.0480(9) Uani 1 1 d . . .
C1 C 0.4316(2) 0.2686(2) 1.1141(3) 0.0492(15) Uani 1 1 d . . .
O5 O 0.49482(14) 0.13800(14) 0.8421(3) 0.0514(10) Uani 1 1 d . . .
O6 O 0.55340(14) 0.21580(13) 0.8054(2) 0.0474(10) Uani 1 1 d . . .
O3 O 0.43489(13) 0.15733(14) 0.7097(2) 0.0497(10) Uani 1 1 d . . .
C30 C 0.5823(2) 0.1914(2) 0.8420(4) 0.0465(14) Uani 1 1 d . . .
N2 N 0.4292(2) 0.2991(2) 0.9078(3) 0.0521(13) Uani 1 1 d . . .
C4 C 0.5117(2) 0.2418(2) 1.0503(3) 0.0487(14) Uani 1 1 d . . .
N1 N 0.48275(16) 0.25475(16) 1.1165(3) 0.0409(11) Uani 1 1 d . . .
C9 C 0.4221(2) 0.2952(2) 1.0415(3) 0.0515(15) Uani 1 1 d . . .
H9A H 0.3884 0.298 1.035 0.062 Uiso 1 1 calc R . .
H9B H 0.4347 0.3268 1.0462 0.062 Uiso 1 1 calc R . .
C17 C 0.3413(3) 0.2140(2) 0.7955(4) 0.0634(18) Uani 1 1 d . . .
H17 H 0.3614 0.2015 0.7603 0.076 Uiso 1 1 calc R . .
F11 F 0.6544(2) 0.1985(2) 0.9073(4) 0.138(3) Uani 1 1 d . . .
C28 C 0.5318(2) 0.1245(2) 0.8717(4) 0.0554(17) Uani 1 1 d . A .
C29 C 0.5758(2) 0.1473(2) 0.8740(4) 0.0599(18) Uani 1 1 d . . .
H29 H 0.6009 0.1326 0.8972 0.072 Uiso 1 1 calc R . .
F12 F 0.62690(19) 0.25927(18) 0.8647(5) 0.143(3) Uani 1 1 d . . .
C10 C 0.41372(19) 0.31804(19) 0.7641(3) 0.0436(13) Uani 1 1 d . . .
C31 C 0.6302(2) 0.2147(3) 0.8527(4) 0.0618(18) Uani 1 1 d . . .
C25 C 0.5188(2) 0.1032(2) 0.6745(4) 0.0512(16) Uani 1 1 d . . .
C11 C 0.4561(2) 0.3390(2) 0.7434(4) 0.0617(18) Uani 1 1 d . . .
H11 H 0.4842 0.3291 0.7645 0.074 Uiso 1 1 calc R . .
C16 C 0.3563(2) 0.2494(2) 0.8410(4) 0.0489(14) Uani 1 1 d . . .
C13 C 0.4153(3) 0.3888(3) 0.6608(4) 0.075(2) Uani 1 1 d . . .
H13 H 0.416 0.4126 0.6256 0.09 Uiso 1 1 calc R . .
F10 F 0.6565(2) 0.2098(3) 0.7962(4) 0.171(4) Uani 1 1 d . . .
C26 C 0.5578(3) 0.0704(3) 0.6515(6) 0.085(3) Uani 1 1 d . . .
C22 C 0.3864(3) 0.0993(4) 0.6596(7) 0.096(3) Uani 1 1 d . . .
C21 C 0.3252(2) 0.2687(3) 0.8920(5) 0.074(2) Uani 1 1 d . . .
H21 H 0.3353 0.2931 0.9223 0.089 Uiso 1 1 calc R . .
C24 C 0.4724(2) 0.0884(2) 0.6662(5) 0.065(2) Uani 1 1 d . . .
H24 H 0.4667 0.058 0.6494 0.078 Uiso 1 1 calc R . .
C15 C 0.3724(3) 0.3330(3) 0.7323(4) 0.0641(19) Uani 1 1 d . . .
H15 H 0.344 0.3192 0.7453 0.077 Uiso 1 1 calc R . .
C7 C 0.4959(2) 0.2709(2) 0.9841(3) 0.0526(16) Uani 1 1 d . . .
H7A H 0.5097 0.2576 0.9399 0.063 Uiso 1 1 calc R . .
H7B H 0.5079 0.3027 0.9894 0.063 Uiso 1 1 calc R . .
C19 C 0.2655(3) 0.2157(4) 0.8507(7) 0.096(3) Uani 1 1 d . . .
H19 H 0.2347 0.2045 0.8528 0.116 Uiso 1 1 calc R . .
C23 C 0.4339(2) 0.1173(3) 0.6821(4) 0.0620(18) Uani 1 1 d . . .
C20 C 0.2796(3) 0.2521(4) 0.8982(6) 0.090(3) Uani 1 1 d . . .
H20 H 0.2589 0.2646 0.9327 0.108 Uiso 1 1 calc R . .
C12 C 0.4562(4) 0.3741(3) 0.6919(5) 0.084(3) Uani 1 1 d . . .
H12 H 0.4845 0.388 0.6782 0.101 Uiso 1 1 calc R . .
C27 C 0.5292(3) 0.0753(4) 0.9054(7) 0.112(4) Uani 1 1 d . . .
C18 C 0.2956(3) 0.1969(3) 0.8026(6) 0.084(3) Uani 1 1 d . . .
H18 H 0.2859 0.1718 0.7732 0.101 Uiso 1 1 calc R . .
C14 C 0.3736(4) 0.3694(3) 0.6798(5) 0.084(3) Uani 1 1 d . . .
H14 H 0.3459 0.38 0.6584 0.101 Uiso 1 1 calc R . .
F7A F 0.5518(5) 0.0440(4) 0.8666(8) 0.121(2) Uani 0.5 1 d P A 1
F8A F 0.4999(6) 0.0852(4) 0.9707(9) 0.121(2) Uani 0.5 1 d P A 1
F9A F 0.5604(6) 0.0753(4) 0.9694(9) 0.121(2) Uani 0.5 1 d P A 1
F7B F 0.5027(6) 0.0457(3) 0.8680(8) 0.121(2) Uani 0.5 1 d P A 2
F8B F 0.4971(6) 0.0652(4) 0.9464(10) 0.121(2) Uani 0.5 1 d P A 2
F9B F 0.5687(6) 0.0594(4) 0.9338(10) 0.121(2) Uani 0.5 1 d P A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 C8 C9 111.6(5) . .
N2 C8 C7 112.0(5) . .
C9 C8 C7 107.7(5) . .
O2 Co1 O6 96.16(16) . .
O2 Co1 O4 173.62(16) . .
O6 Co1 O4 89.17(16) . .
O2 Co1 O3 88.65(16) . .
O6 Co1 O3 174.08(15) . .
O4 Co1 O3 85.83(16) . .
O2 Co1 O1 87.96(16) . 14_544
O6 Co1 O1 86.70(17) . 14_544
O4 Co1 O1 95.87(17) . 14_544
O3 Co1 O1 96.94(17) . 14_544
O2 Co1 O5 93.74(16) . .
O6 Co1 O5 85.58(16) . .
O4 Co1 O5 83.15(16) . .
O3 Co1 O5 90.68(17) . .
O1 Co1 O5 172.23(16) 14_544 .
O2 P1 N2 112.6(3) . .
O2 P1 C10 115.1(3) . .
N2 P1 C10 103.6(3) . .
O2 P1 C16 109.5(3) . .
N2 P1 C16 108.1(3) . .
C10 P1 C16 107.7(3) . .
C25 O4 Co1 126.3(4) . .
P1 O2 Co1 160.7(3) . .
N1 O1 Co1 143.1(3) . 14_545
N1 C1 C2 109.6(5) . .
N1 C1 C3 107.7(5) . .
C2 C1 C3 110.9(6) . .
N1 C1 C9 108.7(5) . .
C2 C1 C9 110.4(5) . .
C3 C1 C9 109.6(5) . .
C28 O5 Co1 123.3(4) . .
C30 O6 Co1 124.7(4) . .
C23 O3 Co1 126.5(4) . .
O6 C30 C29 128.7(6) . .
O6 C30 C31 114.1(5) . .
C29 C30 C31 117.2(6) . .
C8 N2 P1 121.6(5) . .
N1 C4 C5 108.7(5) . .
N1 C4 C7 109.6(5) . .
C5 C4 C7 111.0(6) . .
N1 C4 C6 107.6(5) . .
C5 C4 C6 110.2(6) . .
C7 C4 C6 109.7(6) . .
O1 N1 C4 116.7(4) . .
O1 N1 C1 117.2(5) . .
C4 N1 C1 124.8(5) . .
C8 C9 C1 115.4(5) . .
C16 C17 C18 119.4(7) . .
O5 C28 C29 128.6(6) . .
O5 C28 C27 114.4(7) . .
C29 C28 C27 116.9(7) . .
C30 C29 C28 121.3(6) . .
C15 C10 C11 119.4(6) . .
C15 C10 P1 122.1(5) . .
C11 C10 P1 118.5(5) . .
F10 C31 F12 106.7(8) . .
F10 C31 F11 105.5(7) . .
F12 C31 F11 105.0(7) . .
F10 C31 C30 111.8(6) . .
F12 C31 C30 112.5(6) . .
F11 C31 C30 114.7(6) . .
O4 C25 C24 127.4(6) . .
O4 C25 C26 113.9(6) . .
C24 C25 C26 118.7(6) . .
C12 C11 C10 119.9(7) . .
C17 C16 C21 119.6(6) . .
C17 C16 P1 119.3(5) . .
C21 C16 P1 121.0(5) . .
C14 C13 C12 121.2(7) . .
F6 C26 F5 102.4(9) . .
F6 C26 F4 107.6(9) . .
F5 C26 F4 104.6(9) . .
F6 C26 C25 112.3(8) . .
F5 C26 C25 112.1(7) . .
F4 C26 C25 116.7(7) . .
F3 C22 F1 109.7(10) . .
F3 C22 F2 105.1(11) . .
F1 C22 F2 96.7(9) . .
F3 C22 C23 119.2(8) . .
F1 C22 C23 113.0(9) . .
F2 C22 C23 110.4(9) . .
C20 C21 C16 120.9(8) . .
C25 C24 C23 122.8(6) . .
C10 C15 C14 119.5(7) . .
C4 C7 C8 114.2(5) . .
C18 C19 C20 120.9(8) . .
O3 C23 C24 127.1(6) . .
O3 C23 C22 116.2(6) . .
C24 C23 C22 116.6(6) . .
C21 C20 C19 117.9(8) . .
C13 C12 C11 120.4(8) . .
F8B C27 F7A 122.8(13) . .
F8B C27 F9B 108.5(13) . .
F7A C27 F9B 63.7(9) . .
F8B C27 F7B 74.8(11) . .
F7A C27 F7B 64.4(12) . .
F9B C27 F7B 118.1(13) . .
F8B C27 F9A 88.0(13) . .
F7A C27 F9A 97.4(10) . .
F7B C27 F9A 139.1(10) . .
F7A C27 F8A 147.3(10) . .
F9B C27 F8A 103.3(12) . .
F7B C27 F8A 102.4(11) . .
F9A C27 F8A 72.7(11) . .
F8B C27 C28 120.0(10) . .
F7A C27 C28 112.6(9) . .
F9B C27 C28 115.4(10) . .
F7B C27 C28 114.0(10) . .
F9A C27 C28 106.8(11) . .
F8A C27 C28 100.1(9) . .
C19 C18 C17 121.3(9) . .
C13 C14 C15 119.6(8) . .
C27 F8A F9A 53.3(9) . .
C27 F9A F8A 54.0(9) . .
C27 F7B F8B 49.5(8) . .
C27 F8B F7B 55.7(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C8 N2 1.459(8) .
C8 C9 1.490(8) .
C8 C7 1.532(8) .
C3 C1 1.523(9) .
F4 C26 1.290(9) .
C2 C1 1.517(9) .
F1 C22 1.271(12) .
C5 C4 1.514(10) .
F3 C22 1.222(10) .
F5 C26 1.289(11) .
C6 C4 1.528(9) .
F6 C26 1.279(11) .
F2 C22 1.306(14) .
Co1 O2 2.025(4) .
Co1 O6 2.060(4) .
Co1 O4 2.070(4) .
Co1 O3 2.083(4) .
Co1 O1 2.115(4) 14_544
Co1 O5 2.129(4) .
P1 O2 1.493(4) .
P1 N2 1.641(6) .
P1 C10 1.794(6) .
P1 C16 1.798(6) .
O4 C25 1.254(7) .
O1 N1 1.281(6) .
O1 Co1 2.115(4) 14_545
C1 N1 1.507(7) .
C1 C9 1.543(9) .
O5 C28 1.241(8) .
O6 C30 1.265(7) .
O3 C23 1.243(8) .
C30 C29 1.394(9) .
C30 C31 1.526(9) .
C4 N1 1.503(7) .
C4 C7 1.528(8) .
C17 C16 1.370(9) .
C17 C18 1.391(11) .
F11 C31 1.292(9) .
C28 C29 1.407(9) .
C28 C27 1.528(11) .
F12 C31 1.288(9) .
C10 C15 1.376(9) .
C10 C11 1.394(9) .
C31 F10 1.277(9) .
C25 C24 1.391(9) .
C25 C26 1.507(10) .
C11 C12 1.368(10) .
C16 C21 1.392(10) .
C13 C14 1.352(12) .
C13 C12 1.358(12) .
C22 C23 1.502(10) .
C21 C20 1.386(11) .
C24 C23 1.396(9) .
C15 C14 1.405(10) .
C19 C18 1.336(13) .
C19 C20 1.405(13) .
C27 F8B 1.211(18) .
C27 F7A 1.303(18) .
C27 F9B 1.318(18) .
C27 F7B 1.316(17) .
C27 F9A 1.46(2) .
C27 F8A 1.476(18) .
F8A F9A 1.74(2) .
F7B F8B 1.54(2) .
