#------------------------------------------------------------------------------
#$Date: 2017-06-17 05:26:40 +0300 (Sat, 17 Jun 2017) $
#$Revision: 197908 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/04/33/7043383.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7043383
loop_
_publ_author_name
'Yue, Cheng-Yang'
'Lei, Xiao-Wu'
'Lu, Xinxiu'
'Li, Yan'
'Wei, Jun-Chao'
'Wang, Wei'
'Yin, Yun-Dong'
'Wang, Ning'
_publ_section_title
;
 Comparison Studies of Hybrid Lead Halide [MPb2X7]2-- (M = Cu, Ag; X = Br,
 I) Chains: Band Structures and Visible Light Driven Photocatalytic
 Properties
;
_journal_name_full               'Dalton Trans.'
_journal_paper_doi               10.1039/C7DT00820A
_journal_year                    2017
_chemical_formula_moiety         C30N6H24CoAgPb2I7
_chemical_formula_sum            'C30 H24 Ag Co I7 N6 Pb2'
_chemical_formula_weight         1938.05
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2017-05-04 deposited with the CCDC.
2017-06-16 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 109.246(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.3592(17)
_cell_length_b                   13.6112(17)
_cell_length_c                   25.065(3)
_cell_measurement_reflns_used    9962
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      26.72
_cell_measurement_theta_min      2.16
_cell_volume                     4303.0(9)
_computing_cell_refinement       'APEX2 Software Suite (Bruker,2005)'
_computing_data_collection       'APEX2 Software Suite (Bruker,2005)'
_computing_data_reduction        'APEX2 Software Suite (Bruker,2005)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Bruker SMART CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0466
_diffrn_reflns_av_unetI/netI     0.0386
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            49370
_diffrn_reflns_theta_full        27.62
_diffrn_reflns_theta_max         27.62
_diffrn_reflns_theta_min         1.61
_exptl_absorpt_coefficient_mu    13.680
_exptl_absorpt_correction_T_max  0.2334
_exptl_absorpt_correction_T_min  0.2334
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.992
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3419
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.267
_refine_diff_density_min         -1.356
_refine_diff_density_rms         0.166
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     424
_refine_ls_number_reflns         9908
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.007
_refine_ls_R_factor_all          0.0565
_refine_ls_R_factor_gt           0.0334
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0344P)²+5.4922P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0693
_refine_ls_wR_factor_ref         0.0760
_reflns_number_gt                7433
_reflns_number_total             9908
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c7dt00820a2.cif
_cod_data_source_block           C30N6H24CoAgPb2I7
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7043383
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Co1 Co 0.42067(7) -0.54676(6) -0.19631(3) 0.02950(18) Uani 1 1 d .
N1 N 0.2922(4) -0.4726(4) -0.1820(2) 0.0367(12) Uani 1 1 d .
N2 N 0.4905(4) -0.4108(4) -0.1608(2) 0.0344(12) Uani 1 1 d .
N3 N 0.3964(4) -0.4945(4) -0.2790(2) 0.0364(12) Uani 1 1 d .
N4 N 0.5586(4) -0.5963(4) -0.2135(2) 0.0363(12) Uani 1 1 d .
N5 N 0.3350(4) -0.6808(4) -0.2197(2) 0.0359(12) Uani 1 1 d .
N6 N 0.4579(4) -0.6192(4) -0.1183(2) 0.0360(12) Uani 1 1 d .
C1 C 0.1954(5) -0.5087(5) -0.1915(3) 0.0449(17) Uani 1 1 d .
H1 H 0.1800 -0.5705 -0.2079 0.054 Uiso 1 1 calc R
C2 C 0.1171(6) -0.4594(6) -0.1783(3) 0.055(2) Uani 1 1 d .
H2 H 0.0497 -0.4864 -0.1865 0.066 Uiso 1 1 calc R
C3 C 0.1409(7) -0.3692(6) -0.1529(4) 0.061(2) Uani 1 1 d .
H3 H 0.0902 -0.3350 -0.1423 0.073 Uiso 1 1 calc R
C4 C 0.2398(6) -0.3295(6) -0.1430(3) 0.0532(19) Uani 1 1 d .
H4 H 0.2559 -0.2673 -0.1272 0.064 Uiso 1 1 calc R
C5 C 0.3151(5) -0.3834(4) -0.1571(3) 0.0342(14) Uani 1 1 d .
C6 C 0.4255(5) -0.3482(4) -0.1464(2) 0.0349(14) Uani 1 1 d .
C7 C 0.4627(6) -0.2588(5) -0.1211(3) 0.0499(18) Uani 1 1 d .
H7 H 0.4172 -0.2152 -0.1121 0.060 Uiso 1 1 calc R
C8 C 0.5678(7) -0.2355(5) -0.1095(3) 0.058(2) Uani 1 1 d .
H8 H 0.5942 -0.1764 -0.0919 0.070 Uiso 1 1 calc R
C9 C 0.6328(6) -0.2988(6) -0.1239(3) 0.0522(19) Uani 1 1 d .
H9 H 0.7041 -0.2841 -0.1163 0.063 Uiso 1 1 calc R
C10 C 0.5909(6) -0.3852(5) -0.1497(3) 0.0462(17) Uani 1 1 d .
H10 H 0.6354 -0.4282 -0.1601 0.055 Uiso 1 1 calc R
C11 C 0.3096(6) -0.4465(5) -0.3109(3) 0.0431(16) Uani 1 1 d .
H11 H 0.2546 -0.4366 -0.2964 0.052 Uiso 1 1 calc R
C12 C 0.2983(6) -0.4114(5) -0.3635(3) 0.0483(18) Uani 1 1 d .
H12 H 0.2368 -0.3786 -0.3845 0.058 Uiso 1 1 calc R
C13 C 0.3792(7) -0.4255(6) -0.3849(3) 0.056(2) Uani 1 1 d .
H13 H 0.3742 -0.4020 -0.4205 0.067 Uiso 1 1 calc R
C14 C 0.4673(6) -0.4746(5) -0.3527(3) 0.0518(19) Uani 1 1 d .
H14 H 0.5227 -0.4851 -0.3667 0.062 Uiso 1 1 calc R
C15 C 0.4757(5) -0.5093(4) -0.2994(3) 0.0340(14) Uani 1 1 d .
C16 C 0.5668(5) -0.5650(4) -0.2629(3) 0.0335(14) Uani 1 1 d .
C17 C 0.6576(6) -0.5859(6) -0.2764(3) 0.0496(18) Uani 1 1 d .
H17 H 0.6633 -0.5636 -0.3104 0.060 Uiso 1 1 calc R
C18 C 0.7381(6) -0.6386(6) -0.2403(4) 0.060(2) Uani 1 1 d .
H18 H 0.7991 -0.6519 -0.2491 0.071 Uiso 1 1 calc R
C19 C 0.7285(6) -0.6716(5) -0.1910(3) 0.0521(19) Uani 1 1 d .
H19 H 0.7821 -0.7087 -0.1661 0.062 Uiso 1 1 calc R
C20 C 0.6375(6) -0.6491(5) -0.1787(3) 0.0474(18) Uani 1 1 d .
H20 H 0.6311 -0.6716 -0.1449 0.057 Uiso 1 1 calc R
C21 C 0.2694(6) -0.7033(5) -0.2711(3) 0.0500(18) Uani 1 1 d .
H21 H 0.2677 -0.6630 -0.3013 0.060 Uiso 1 1 calc R
C22 C 0.2040(7) -0.7844(6) -0.2810(4) 0.061(2) Uani 1 1 d .
H22 H 0.1585 -0.7986 -0.3172 0.073 Uiso 1 1 calc R
C23 C 0.2077(7) -0.8427(6) -0.2367(4) 0.071(3) Uani 1 1 d .
H23 H 0.1644 -0.8978 -0.2424 0.085 Uiso 1 1 calc R
C24 C 0.2751(6) -0.8210(5) -0.1834(4) 0.060(2) Uani 1 1 d .
H24 H 0.2774 -0.8608 -0.1528 0.072 Uiso 1 1 calc R
C25 C 0.3393(5) -0.7390(4) -0.1760(3) 0.0369(15) Uani 1 1 d .
C26 C 0.4142(5) -0.7093(4) -0.1205(3) 0.0344(14) Uani 1 1 d .
C27 C 0.4417(6) -0.7694(5) -0.0729(3) 0.0507(19) Uani 1 1 d .
H27 H 0.4123 -0.8318 -0.0747 0.061 Uiso 1 1 calc R
C28 C 0.5130(7) -0.7352(6) -0.0232(3) 0.057(2) Uani 1 1 d .
H28 H 0.5332 -0.7749 0.0087 0.068 Uiso 1 1 calc R
C29 C 0.5539(6) -0.6433(6) -0.0209(3) 0.052(2) Uani 1 1 d .
H29 H 0.6007 -0.6188 0.0127 0.063 Uiso 1 1 calc R
C30 C 0.5250(5) -0.5876(5) -0.0689(3) 0.0438(16) Uani 1 1 d .
H30 H 0.5534 -0.5249 -0.0672 0.053 Uiso 1 1 calc R
Pb1 Pb -0.09695(2) -0.535774(19) -0.430442(12) 0.04139(7) Uani 1 1 d .
Pb2 Pb -0.05199(2) -0.200165(19) -0.477569(13) 0.04295(8) Uani 1 1 d .
I1 I -0.03840(5) -0.60882(4) -0.31353(2) 0.06534(16) Uani 1 1 d .
I2 I -0.01168(5) -0.32472(4) -0.37080(2) 0.05858(14) Uani 1 1 d .
I3 I -0.25821(4) -0.09858(3) -0.46833(2) 0.04942(13) Uani 1 1 d .
I4 I -0.33127(4) -0.52803(3) -0.44464(2) 0.04879(12) Uani 1 1 d .
I5 I -0.13993(4) -0.38184(3) -0.55302(2) 0.04809(12) Uani 1 1 d .
I6 I 0.08480(4) 0.01933(4) -0.41065(2) 0.04840(12) Uani 1 1 d .
I7 I -0.17466(3) -0.75236(3) -0.50270(2) 0.04204(11) Uani 1 1 d .
Ag1 Ag -0.13287(5) -0.95221(4) -0.48692(3) 0.0690(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N6 Co1 N3 170.1(2) . .
N6 Co1 N1 91.2(2) . .
N3 Co1 N1 97.8(2) . .
N6 Co1 N5 78.1(2) . .
N3 Co1 N5 97.1(2) . .
N1 Co1 N5 93.6(2) . .
N6 Co1 N2 94.7(2) . .
N3 Co1 N2 91.3(2) . .
N1 Co1 N2 77.5(2) . .
N5 Co1 N2 168.55(19) . .
N6 Co1 N4 94.8(2) . .
N3 Co1 N4 76.8(2) . .
N1 Co1 N4 170.0(2) . .
N5 Co1 N4 95.5(2) . .
N2 Co1 N4 94.0(2) . .
C1 N1 C5 118.2(6) . .
C1 N1 Co1 126.0(5) . .
C5 N1 Co1 115.6(4) . .
C10 N2 C6 118.4(6) . .
C10 N2 Co1 126.1(5) . .
C6 N2 Co1 115.4(4) . .
C15 N3 C11 119.1(6) . .
C15 N3 Co1 116.1(4) . .
C11 N3 Co1 124.8(4) . .
C20 N4 C16 119.0(6) . .
C20 N4 Co1 125.9(5) . .
C16 N4 Co1 114.9(4) . .
C21 N5 C25 119.5(6) . .
C21 N5 Co1 125.8(5) . .
C25 N5 Co1 114.1(4) . .
C30 N6 C26 118.6(6) . .
C30 N6 Co1 126.3(5) . .
C26 N6 Co1 115.0(4) . .
N1 C1 C2 123.4(7) . .
N1 C1 H1 118.3 . .
C2 C1 H1 118.3 . .
C1 C2 C3 118.1(7) . .
C1 C2 H2 120.9 . .
C3 C2 H2 120.9 . .
C4 C3 C2 119.9(7) . .
C4 C3 H3 120.1 . .
C2 C3 H3 120.1 . .
C3 C4 C5 118.9(7) . .
C3 C4 H4 120.5 . .
C5 C4 H4 120.5 . .
N1 C5 C4 121.4(6) . .
N1 C5 C6 115.6(5) . .
C4 C5 C6 123.0(6) . .
N2 C6 C7 120.7(6) . .
N2 C6 C5 115.8(5) . .
C7 C6 C5 123.4(6) . .
C8 C7 C6 119.2(7) . .
C8 C7 H7 120.4 . .
C6 C7 H7 120.4 . .
C9 C8 C7 119.8(7) . .
C9 C8 H8 120.1 . .
C7 C8 H8 120.1 . .
C8 C9 C10 118.3(7) . .
C8 C9 H9 120.9 . .
C10 C9 H9 120.9 . .
N2 C10 C9 123.6(7) . .
N2 C10 H10 118.2 . .
C9 C10 H10 118.2 . .
N3 C11 C12 123.0(7) . .
N3 C11 H11 118.5 . .
C12 C11 H11 118.5 . .
C11 C12 C13 118.6(7) . .
C11 C12 H12 120.7 . .
C13 C12 H12 120.7 . .
C14 C13 C12 118.5(7) . .
C14 C13 H13 120.8 . .
C12 C13 H13 120.8 . .
C13 C14 C15 121.2(7) . .
C13 C14 H14 119.4 . .
C15 C14 H14 119.4 . .
N3 C15 C14 119.6(6) . .
N3 C15 C16 116.1(5) . .
C14 C15 C16 124.2(6) . .
N4 C16 C17 120.0(6) . .
N4 C16 C15 115.7(5) . .
C17 C16 C15 124.3(6) . .
C18 C17 C16 120.4(7) . .
C18 C17 H17 119.8 . .
C16 C17 H17 119.8 . .
C19 C18 C17 119.3(7) . .
C19 C18 H18 120.4 . .
C17 C18 H18 120.4 . .
C18 C19 C20 118.9(7) . .
C18 C19 H19 120.5 . .
C20 C19 H19 120.5 . .
N4 C20 C19 122.3(7) . .
N4 C20 H20 118.8 . .
C19 C20 H20 118.8 . .
N5 C21 C22 122.3(7) . .
N5 C21 H21 118.9 . .
C22 C21 H21 118.9 . .
C23 C22 C21 118.2(8) . .
C23 C22 H22 120.9 . .
C21 C22 H22 120.9 . .
C22 C23 C24 120.5(8) . .
C22 C23 H23 119.7 . .
C24 C23 H23 119.7 . .
C23 C24 C25 118.7(8) . .
C23 C24 H24 120.6 . .
C25 C24 H24 120.6 . .
N5 C25 C24 120.8(7) . .
N5 C25 C26 116.2(6) . .
C24 C25 C26 123.0(6) . .
N6 C26 C27 120.7(6) . .
N6 C26 C25 115.8(5) . .
C27 C26 C25 123.5(6) . .
C28 C27 C26 119.0(7) . .
C28 C27 H27 120.5 . .
C26 C27 H27 120.5 . .
C29 C28 C27 120.0(7) . .
C29 C28 H28 120.0 . .
C27 C28 H28 120.0 . .
C28 C29 C30 118.7(7) . .
C28 C29 H29 120.6 . .
C30 C29 H29 120.6 . .
N6 C30 C29 123.1(7) . .
N6 C30 H30 118.5 . .
C29 C30 H30 118.5 . .
I1 Pb1 I4 93.083(18) . .
I1 Pb1 I2 84.452(18) . .
I4 Pb1 I2 102.351(16) . .
I1 Pb1 I7 99.776(17) . .
I4 Pb1 I7 81.212(13) . .
I2 Pb1 I7 174.386(15) . .
I1 Pb1 I5 93.187(17) . 3_544
I4 Pb1 I5 158.963(15) . 3_544
I2 Pb1 I5 98.231(16) . 3_544
I7 Pb1 I5 77.940(13) . 3_544
I1 Pb1 I5 163.636(17) . .
I4 Pb1 I5 90.660(15) . .
I2 Pb1 I5 79.185(15) . .
I7 Pb1 I5 96.537(15) . .
I5 Pb1 I5 88.943(13) 3_544 .
I2 Pb2 I5 90.781(18) . .
I2 Pb2 I3 94.857(17) . .
I5 Pb2 I3 103.274(16) . .
I2 Pb2 I7 96.733(16) . 3_544
I5 Pb2 I7 86.224(15) . 3_544
I3 Pb2 I7 164.909(15) . 3_544
I2 Pb2 Ag1 123.334(19) . 1_565
I5 Pb2 Ag1 132.570(19) . 1_565
I3 Pb2 Ag1 47.981(14) . 1_565
I7 Pb2 Ag1 117.060(15) 3_544 1_565
I2 Pb2 Ag1 127.243(19) . 3_544
I5 Pb2 Ag1 117.876(18) . 3_544
I3 Pb2 Ag1 117.230(17) . 3_544
I7 Pb2 Ag1 47.712(15) 3_544 3_544
Ag1 Pb2 Ag1 69.40(2) 1_565 3_544
I2 Pb2 I6 97.800(17) . .
I5 Pb2 I6 167.115(15) . .
I3 Pb2 I6 85.634(15) . .
I7 Pb2 I6 83.250(14) 3_544 .
Ag1 Pb2 I6 48.460(16) 1_565 .
Ag1 Pb2 I6 49.248(16) 3_544 .
I2 Pb2 I6 170.910(16) . 3_554
I5 Pb2 I6 98.302(17) . 3_554
I3 Pb2 I6 82.757(14) . 3_554
I7 Pb2 I6 84.292(13) 3_544 3_554
Ag1 Pb2 I6 49.187(16) 1_565 3_554
Ag1 Pb2 I6 48.031(16) 3_544 3_554
I6 Pb2 I6 73.311(16) . 3_554
Pb2 I2 Pb1 98.781(18) . .
Ag1 I3 Pb2 73.08(2) 1_565 .
Pb2 I5 Pb1 98.734(15) . 3_544
Pb2 I5 Pb1 91.253(17) . .
Pb1 I5 Pb1 91.057(13) 3_544 .
Ag1 I6 Ag1 85.87(2) 1_565 3_544
Ag1 I6 Pb2 64.244(17) 1_565 .
Ag1 I6 Pb2 64.363(16) 3_544 .
Ag1 I6 Pb2 64.373(17) 1_565 3_554
Ag1 I6 Pb2 63.351(17) 3_544 3_554
Pb2 I6 Pb2 106.689(15) . 3_554
Ag1 I7 Pb2 71.176(17) . 3_544
Ag1 I7 Pb1 138.86(2) . .
Pb2 I7 Pb1 96.582(14) 3_544 .
I3 Ag1 I7 129.10(3) 1_545 .
I3 Ag1 I6 108.87(3) 1_545 1_545
I7 Ag1 I6 109.37(3) . 1_545
I3 Ag1 I6 103.91(3) 1_545 3_544
I7 Ag1 I6 105.49(3) . 3_544
I6 Ag1 I6 94.13(2) 1_545 3_544
I3 Ag1 Pb2 58.935(17) 1_545 1_545
I7 Ag1 Pb2 171.37(3) . 1_545
I6 Ag1 Pb2 67.297(17) 1_545 1_545
I6 Ag1 Pb2 67.461(17) 3_544 1_545
I3 Ag1 Pb2 168.74(3) 1_545 3_544
I7 Ag1 Pb2 61.112(16) . 3_544
I6 Ag1 Pb2 67.596(19) 1_545 3_544
I6 Ag1 Pb2 66.389(18) 3_544 3_544
Pb2 Ag1 Pb2 110.603(19) 1_545 3_544
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Co1 N6 2.098(5) .
Co1 N3 2.114(5) .
Co1 N1 2.122(5) .
Co1 N5 2.131(5) .
Co1 N2 2.131(5) .
Co1 N4 2.135(5) .
N1 C1 1.329(8) .
N1 C5 1.353(8) .
N2 C10 1.323(8) .
N2 C6 1.347(8) .
N3 C15 1.334(8) .
N3 C11 1.341(8) .
N4 C20 1.335(8) .
N4 C16 1.350(8) .
N5 C21 1.334(9) .
N5 C25 1.337(8) .
N6 C30 1.338(8) .
N6 C26 1.351(8) .
C1 C2 1.371(10) .
C1 H1 0.9300 .
C2 C3 1.372(11) .
C2 H2 0.9300 .
C3 C4 1.372(11) .
C3 H3 0.9300 .
C4 C5 1.381(9) .
C4 H4 0.9300 .
C5 C6 1.488(9) .
C6 C7 1.386(9) .
C7 C8 1.374(11) .
C7 H7 0.9300 .
C8 C9 1.354(11) .
C8 H8 0.9300 .
C9 C10 1.370(10) .
C9 H9 0.9300 .
C10 H10 0.9300 .
C11 C12 1.364(9) .
C11 H11 0.9300 .
C12 C13 1.368(11) .
C12 H12 0.9300 .
C13 C14 1.362(11) .
C13 H13 0.9300 .
C14 C15 1.385(9) .
C14 H14 0.9300 .
C15 C16 1.469(9) .
C16 C17 1.392(9) .
C17 C18 1.361(11) .
C17 H17 0.9300 .
C18 C19 1.358(11) .
C18 H18 0.9300 .
C19 C20 1.384(10) .
C19 H19 0.9300 .
C20 H20 0.9300 .
C21 C22 1.378(10) .
C21 H21 0.9300 .
C22 C23 1.351(12) .
C22 H22 0.9300 .
C23 C24 1.376(12) .
C23 H23 0.9300 .
C24 C25 1.383(9) .
C24 H24 0.9300 .
C25 C26 1.477(9) .
C26 C27 1.392(9) .
C27 C28 1.376(11) .
C27 H27 0.9300 .
C28 C29 1.358(11) .
C28 H28 0.9300 .
C29 C30 1.365(10) .
C29 H29 0.9300 .
C30 H30 0.9300 .
Pb1 I1 2.9456(7) .
Pb1 I4 3.0336(7) .
Pb1 I2 3.2653(7) .
Pb1 I7 3.4365(6) .
Pb1 I5 3.5084(7) 3_544
Pb1 I5 3.6050(7) .
Pb2 I2 3.0620(7) .
Pb2 I5 3.0994(6) .
Pb2 I3 3.1585(6) .
Pb2 I7 3.2889(6) 3_544
Pb2 Ag1 3.5279(8) 1_565
Pb2 Ag1 3.5554(7) 3_544
Pb2 I6 3.6135(6) .
Pb2 I6 3.6457(7) 3_554
I3 Ag1 2.7394(8) 1_565
I5 Pb1 3.5084(7) 3_544
I6 Ag1 2.9318(9) 1_565
I6 Ag1 2.9874(9) 3_544
I6 Pb2 3.6457(7) 3_554
I7 Ag1 2.7788(8) .
I7 Pb2 3.2889(6) 3_544
Ag1 I3 2.7393(8) 1_545
Ag1 I6 2.9318(9) 1_545
Ag1 I6 2.9874(9) 3_544
Ag1 Pb2 3.5278(8) 1_545
Ag1 Pb2 3.5554(7) 3_544
