#------------------------------------------------------------------------------
#$Date: 2016-03-26 00:35:06 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180086 $
#$URL: svn://www.crystallography.net/cod/cif/7/05/32/7053206.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7053206
loop_
_publ_author_name
'Mei, Xuelan'
'Wang, Xiufeng'
'Wang, Juanjuan'
'Ma, Yue'
'Li, Licun'
'Liao, Daizheng'
_publ_section_title
;
 Dinuclear lanthanide complexes bridged by nitronyl nitroxide radical
 ligands with 2-phenolate groups: structure and magnetic properties
;
_journal_issue                   11
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              3620
_journal_paper_doi               10.1039/c3nj00739a
_journal_volume                  37
_journal_year                    2013
_chemical_formula_sum            'C46 H60 Dy2 N4 O14'
_chemical_formula_weight         1217.98
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                104.288(7)
_cell_angle_beta                 98.792(4)
_cell_angle_gamma                114.280(4)
_cell_formula_units_Z            1
_cell_length_a                   10.453(5)
_cell_length_b                   11.248(5)
_cell_length_c                   11.848(5)
_cell_measurement_reflns_used    4356
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      28.2
_cell_measurement_theta_min      1.9
_cell_volume                     1178.4(9)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_collection       'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_data_reduction        'CrystalClear (Rigaku/MSC Inc., 2005)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'profile data from ω-scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0429
_diffrn_reflns_av_sigmaI/netI    0.0662
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            9287
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         1.85
_exptl_absorpt_coefficient_mu    3.216
_exptl_absorpt_correction_T_max  0.6989
_exptl_absorpt_correction_T_min  0.5656
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   CrystalClear
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.716
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             608
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.742
_refine_diff_density_min         -1.097
_refine_diff_density_rms         0.138
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     306
_refine_ls_number_reflns         4135
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.062
_refine_ls_R_factor_all          0.0422
_refine_ls_R_factor_gt           0.0378
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0171P)²+0.7798P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0638
_refine_ls_wR_factor_ref         0.0657
_reflns_number_gt                3856
_reflns_number_total             4135
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3nj00739a.txt
_cod_data_source_block           Dy
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7053206
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Dy1 Dy 0.65494(2) 0.15782(2) 0.13775(2) 0.01582(8) Uani 1 1 d .
C1 C 0.8262(5) -0.0691(5) 0.3450(5) 0.0240(12) Uani 1 1 d .
H1A H 0.7610 -0.0910 0.3964 0.036 Uiso 1 1 calc R
H1B H 0.9247 -0.0482 0.3886 0.036 Uiso 1 1 calc R
H1C H 0.7887 -0.1489 0.2699 0.036 Uiso 1 1 calc R
C2 C 0.8329(5) 0.0551(5) 0.3142(4) 0.0165(11) Uani 1 1 d .
C3 C 0.9576(5) 0.1823(5) 0.3710(5) 0.0219(12) Uani 1 1 d .
H3 H 1.0349 0.1868 0.4286 0.026 Uiso 1 1 calc R
C4 C 0.9774(5) 0.3045(5) 0.3493(5) 0.0192(11) Uani 1 1 d .
C5 C 1.1205(5) 0.4347(5) 0.4171(5) 0.0347(15) Uani 1 1 d .
H5A H 1.1831 0.4518 0.3631 0.052 Uiso 1 1 calc R
H5B H 1.1701 0.4232 0.4877 0.052 Uiso 1 1 calc R
H5C H 1.1012 0.5137 0.4447 0.052 Uiso 1 1 calc R
C6 C 0.4678(6) 0.2791(6) 0.4560(5) 0.0308(13) Uani 1 1 d .
H6A H 0.4412 0.1872 0.4625 0.046 Uiso 1 1 calc R
H6B H 0.3813 0.2939 0.4468 0.046 Uiso 1 1 calc R
H6C H 0.5443 0.3506 0.5298 0.046 Uiso 1 1 calc R
C7 C 0.5246(5) 0.2876(5) 0.3459(5) 0.0240(12) Uani 1 1 d .
C8 C 0.5395(6) 0.3992(5) 0.3078(5) 0.0288(13) Uani 1 1 d .
H8 H 0.5121 0.4630 0.3521 0.035 Uiso 1 1 calc R
C9 C 0.5913(5) 0.4251(5) 0.2102(5) 0.0251(13) Uani 1 1 d .
C10 C 0.5897(6) 0.5463(5) 0.1772(6) 0.0356(16) Uani 1 1 d .
H10A H 0.6753 0.5897 0.1492 0.053 Uiso 1 1 calc R
H10B H 0.5927 0.6145 0.2487 0.053 Uiso 1 1 calc R
H10C H 0.5001 0.5130 0.1121 0.053 Uiso 1 1 calc R
C11 C 0.6946(5) -0.0832(4) -0.0491(4) 0.0126(10) Uani 1 1 d .
C12 C 0.7020(5) -0.1845(5) -0.0030(4) 0.0168(11) Uani 1 1 d .
H12 H 0.6422 -0.2158 0.0471 0.020 Uiso 1 1 calc R
C13 C 0.7948(5) -0.2396(5) -0.0292(5) 0.0201(12) Uani 1 1 d .
H13 H 0.7964 -0.3094 0.0017 0.024 Uiso 1 1 calc R
C14 C 0.8859(5) -0.1938(5) -0.1004(5) 0.0229(12) Uani 1 1 d .
H14 H 0.9489 -0.2325 -0.1188 0.027 Uiso 1 1 calc R
C15 C 0.8835(5) -0.0917(5) -0.1437(5) 0.0207(12) Uani 1 1 d .
H15 H 0.9457 -0.0598 -0.1920 0.025 Uiso 1 1 calc R
C16 C 0.7907(5) -0.0336(5) -0.1178(4) 0.0154(11) Uani 1 1 d .
C17 C 0.7938(5) 0.0771(5) -0.1613(5) 0.0180(11) Uani 1 1 d .
C18 C 0.8179(5) 0.2148(5) -0.2884(5) 0.0199(12) Uani 1 1 d .
C19 C 0.9810(5) 0.3114(5) -0.2635(5) 0.0279(13) Uani 1 1 d .
H19A H 1.0341 0.3269 -0.1812 0.042 Uiso 1 1 calc R
H19B H 0.9942 0.4005 -0.2705 0.042 Uiso 1 1 calc R
H19C H 1.0193 0.2689 -0.3227 0.042 Uiso 1 1 calc R
C20 C 0.7322(5) 0.1839(5) -0.4160(5) 0.0277(13) Uani 1 1 d .
H20A H 0.7814 0.1567 -0.4738 0.042 Uiso 1 1 calc R
H20B H 0.7265 0.2670 -0.4222 0.042 Uiso 1 1 calc R
H20C H 0.6330 0.1080 -0.4350 0.042 Uiso 1 1 calc R
C21 C 0.7530(5) 0.2602(5) -0.1878(5) 0.0202(12) Uani 1 1 d .
C22 C 0.8196(6) 0.4167(5) -0.1221(5) 0.0307(14) Uani 1 1 d .
H22A H 0.7830 0.4337 -0.0516 0.046 Uiso 1 1 calc R
H22B H 0.7919 0.4593 -0.1778 0.046 Uiso 1 1 calc R
H22C H 0.9266 0.4574 -0.0948 0.046 Uiso 1 1 calc R
C23 C 0.5861(5) 0.1966(5) -0.2276(5) 0.0265(13) Uani 1 1 d .
H23A H 0.5433 0.0971 -0.2730 0.040 Uiso 1 1 calc R
H23B H 0.5569 0.2420 -0.2797 0.040 Uiso 1 1 calc R
H23C H 0.5510 0.2100 -0.1558 0.040 Uiso 1 1 calc R
N1 N 0.7869(4) 0.1907(4) -0.1027(4) 0.0190(9) Uani 1 1 d .
N2 N 0.8063(4) 0.0821(4) -0.2739(4) 0.0194(10) Uani 1 1 d .
O1 O 0.7231(3) 0.0334(3) 0.2336(3) 0.0166(7) Uani 1 1 d .
O2 O 0.8847(3) 0.3139(3) 0.2736(3) 0.0228(8) Uani 1 1 d .
O3 O 0.5586(3) 0.1951(3) 0.2976(3) 0.0227(8) Uani 1 1 d .
O4 O 0.6351(3) 0.3532(3) 0.1428(3) 0.0220(8) Uani 1 1 d .
O5 O 0.5946(3) -0.0390(3) -0.0305(3) 0.0148(7) Uani 1 1 d .
O6 O 0.7952(4) 0.2343(3) 0.0118(3) 0.0209(8) Uani 1 1 d .
O7 O 0.8199(4) -0.0053(4) -0.3551(3) 0.0275(9) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O1 Dy1 O4 150.51(12) . .
O1 Dy1 O3 82.83(12) . .
O4 Dy1 O3 76.51(12) . .
O1 Dy1 O6 113.73(12) . .
O4 Dy1 O6 79.31(12) . .
O3 Dy1 O6 152.43(12) . .
O1 Dy1 O2 74.31(11) . .
O4 Dy1 O2 83.85(12) . .
O3 Dy1 O2 87.38(12) . .
O6 Dy1 O2 77.00(12) . .
O1 Dy1 O5 112.35(11) . 2_655
O4 Dy1 O5 85.01(11) . 2_655
O3 Dy1 O5 80.71(12) . 2_655
O6 Dy1 O5 110.25(12) . 2_655
O2 Dy1 O5 165.30(11) . 2_655
O1 Dy1 O5 79.96(12) . .
O4 Dy1 O5 129.49(12) . .
O3 Dy1 O5 133.73(11) . .
O6 Dy1 O5 72.84(11) . .
O2 Dy1 O5 127.56(11) . .
O5 Dy1 O5 67.12(12) 2_655 .
O1 Dy1 Dy1 97.03(9) . 2_655
O4 Dy1 Dy1 109.32(9) . 2_655
O3 Dy1 Dy1 108.64(9) . 2_655
O6 Dy1 Dy1 91.68(9) . 2_655
O2 Dy1 Dy1 160.98(9) . 2_655
O5 Dy1 Dy1 33.69(8) 2_655 2_655
O5 Dy1 Dy1 33.43(7) . 2_655
C2 C1 H1A 109.5 . .
C2 C1 H1B 109.5 . .
H1A C1 H1B 109.5 . .
C2 C1 H1C 109.5 . .
H1A C1 H1C 109.5 . .
H1B C1 H1C 109.5 . .
O1 C2 C3 124.4(4) . .
O1 C2 C1 116.3(4) . .
C3 C2 C1 119.2(4) . .
C2 C3 C4 124.5(5) . .
C2 C3 H3 117.7 . .
C4 C3 H3 117.7 . .
O2 C4 C3 124.8(4) . .
O2 C4 C5 116.9(4) . .
C3 C4 C5 118.3(5) . .
C4 C5 H5A 109.5 . .
C4 C5 H5B 109.5 . .
H5A C5 H5B 109.5 . .
C4 C5 H5C 109.5 . .
H5A C5 H5C 109.5 . .
H5B C5 H5C 109.5 . .
C7 C6 H6A 109.5 . .
C7 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C7 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
O3 C7 C8 124.8(5) . .
O3 C7 C6 117.8(5) . .
C8 C7 C6 117.4(5) . .
C9 C8 C7 125.6(5) . .
C9 C8 H8 117.2 . .
C7 C8 H8 117.2 . .
O4 C9 C8 125.9(5) . .
O4 C9 C10 116.2(5) . .
C8 C9 C10 117.9(5) . .
C9 C10 H10A 109.5 . .
C9 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C9 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
O5 C11 C12 120.1(4) . .
O5 C11 C16 122.0(4) . .
C12 C11 C16 117.9(4) . .
C13 C12 C11 121.2(4) . .
C13 C12 H12 119.4 . .
C11 C12 H12 119.4 . .
C12 C13 C14 120.8(4) . .
C12 C13 H13 119.6 . .
C14 C13 H13 119.6 . .
C15 C14 C13 119.0(5) . .
C15 C14 H14 120.5 . .
C13 C14 H14 120.5 . .
C14 C15 C16 121.3(5) . .
C14 C15 H15 119.3 . .
C16 C15 H15 119.3 . .
C15 C16 C11 119.8(4) . .
C15 C16 C17 120.1(4) . .
C11 C16 C17 120.1(4) . .
N1 C17 N2 107.4(4) . .
N1 C17 C16 128.1(5) . .
N2 C17 C16 124.5(5) . .
N2 C18 C20 109.2(4) . .
N2 C18 C19 106.5(4) . .
C20 C18 C19 111.4(4) . .
N2 C18 C21 100.2(4) . .
C20 C18 C21 115.0(4) . .
C19 C18 C21 113.5(4) . .
C18 C19 H19A 109.5 . .
C18 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
C18 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
C18 C20 H20A 109.5 . .
C18 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C18 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
N1 C21 C23 105.4(4) . .
N1 C21 C22 110.8(4) . .
C23 C21 C22 109.3(4) . .
N1 C21 C18 100.2(4) . .
C23 C21 C18 114.1(4) . .
C22 C21 C18 116.1(4) . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C21 C23 H23A 109.5 . .
C21 C23 H23B 109.5 . .
H23A C23 H23B 109.5 . .
C21 C23 H23C 109.5 . .
H23A C23 H23C 109.5 . .
H23B C23 H23C 109.5 . .
O6 N1 C17 126.3(4) . .
O6 N1 C21 121.6(4) . .
C17 N1 C21 111.9(4) . .
O7 N2 C17 126.6(4) . .
O7 N2 C18 121.3(4) . .
C17 N2 C18 111.9(4) . .
C2 O1 Dy1 137.3(3) . .
C4 O2 Dy1 134.6(3) . .
C7 O3 Dy1 133.6(3) . .
C9 O4 Dy1 133.7(3) . .
C11 O5 Dy1 125.8(3) . 2_655
C11 O5 Dy1 120.8(3) . .
Dy1 O5 Dy1 112.88(12) 2_655 .
N1 O6 Dy1 136.7(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O1 2.260(3) .
Dy1 O4 2.278(3) .
Dy1 O3 2.306(3) .
Dy1 O6 2.320(3) .
Dy1 O2 2.323(3) .
Dy1 O5 2.342(3) 2_655
Dy1 O5 2.358(3) .
Dy1 Dy1 3.9169(12) 2_655
C1 C2 1.506(6) .
C1 H1A 0.9800 .
C1 H1B 0.9800 .
C1 H1C 0.9800 .
C2 O1 1.269(5) .
C2 C3 1.387(6) .
C3 C4 1.397(6) .
C3 H3 0.9500 .
C4 O2 1.273(5) .
C4 C5 1.509(6) .
C5 H5A 0.9800 .
C5 H5B 0.9800 .
C5 H5C 0.9800 .
C6 C7 1.521(7) .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 O3 1.268(6) .
C7 C8 1.396(7) .
C8 C9 1.394(7) .
C8 H8 0.9500 .
C9 O4 1.264(6) .
C9 C10 1.513(6) .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 O5 1.353(5) .
C11 C12 1.404(6) .
C11 C16 1.413(6) .
C12 C13 1.383(6) .
C12 H12 0.9500 .
C13 C14 1.393(7) .
C13 H13 0.9500 .
C14 C15 1.376(6) .
C14 H14 0.9500 .
C15 C16 1.405(6) .
C15 H15 0.9500 .
C16 C17 1.451(6) .
C17 N1 1.331(6) .
C17 N2 1.373(6) .
C18 N2 1.503(6) .
C18 C20 1.510(7) .
C18 C19 1.530(6) .
C18 C21 1.541(7) .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 N1 1.504(6) .
C21 C23 1.528(6) .
C21 C22 1.530(6) .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 H23A 0.9800 .
C23 H23B 0.9800 .
C23 H23C 0.9800 .
N1 O6 1.299(5) .
N2 O7 1.266(5) .
O5 Dy1 2.342(3) 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
O1 C2 C3 C4 1.7(9) . .
C1 C2 C3 C4 179.4(5) . .
C2 C3 C4 O2 -1.1(9) . .
C2 C3 C4 C5 -179.1(5) . .
O3 C7 C8 C9 1.2(9) . .
C6 C7 C8 C9 179.2(5) . .
C7 C8 C9 O4 -1.4(9) . .
C7 C8 C9 C10 175.8(5) . .
O5 C11 C12 C13 174.6(4) . .
C16 C11 C12 C13 -3.4(7) . .
C11 C12 C13 C14 1.3(7) . .
C12 C13 C14 C15 0.6(8) . .
C13 C14 C15 C16 -0.2(8) . .
C14 C15 C16 C11 -1.9(8) . .
C14 C15 C16 C17 178.0(5) . .
O5 C11 C16 C15 -174.3(4) . .
C12 C11 C16 C15 3.7(7) . .
O5 C11 C16 C17 5.8(7) . .
C12 C11 C16 C17 -176.3(4) . .
C15 C16 C17 N1 -139.3(5) . .
C11 C16 C17 N1 40.7(7) . .
C15 C16 C17 N2 40.0(7) . .
C11 C16 C17 N2 -140.1(5) . .
N2 C18 C21 N1 26.3(4) . .
C20 C18 C21 N1 143.2(4) . .
C19 C18 C21 N1 -86.9(4) . .
N2 C18 C21 C23 -85.8(4) . .
C20 C18 C21 C23 31.1(6) . .
C19 C18 C21 C23 161.0(4) . .
N2 C18 C21 C22 145.6(4) . .
C20 C18 C21 C22 -97.5(5) . .
C19 C18 C21 C22 32.4(6) . .
N2 C17 N1 O6 -169.7(4) . .
C16 C17 N1 O6 9.7(8) . .
N2 C17 N1 C21 15.9(5) . .
C16 C17 N1 C21 -164.8(4) . .
C23 C21 N1 O6 -83.8(5) . .
C22 C21 N1 O6 34.3(6) . .
C18 C21 N1 O6 157.5(4) . .
C23 C21 N1 C17 90.9(5) . .
C22 C21 N1 C17 -150.9(4) . .
C18 C21 N1 C17 -27.7(5) . .
N1 C17 N2 O7 177.9(4) . .
C16 C17 N2 O7 -1.5(8) . .
N1 C17 N2 C18 3.8(5) . .
C16 C17 N2 C18 -175.6(4) . .
C20 C18 N2 O7 44.1(6) . .
C19 C18 N2 O7 -76.3(6) . .
C21 C18 N2 O7 165.2(4) . .
C20 C18 N2 C17 -141.4(4) . .
C19 C18 N2 C17 98.2(5) . .
C21 C18 N2 C17 -20.3(5) . .
C3 C2 O1 Dy1 -0.3(8) . .
C1 C2 O1 Dy1 -178.0(3) . .
O4 Dy1 O1 C2 -44.7(6) . .
O3 Dy1 O1 C2 -90.3(5) . .
O6 Dy1 O1 C2 66.8(5) . .
O2 Dy1 O1 C2 -1.0(4) . .
O5 Dy1 O1 C2 -167.1(4) 2_655 .
O5 Dy1 O1 C2 132.9(5) . .
Dy1 Dy1 O1 C2 161.7(4) 2_655 .
C3 C4 O2 Dy1 -0.9(8) . .
C5 C4 O2 Dy1 177.1(3) . .
O1 Dy1 O2 C4 1.6(5) . .
O4 Dy1 O2 C4 161.5(5) . .
O3 Dy1 O2 C4 84.8(5) . .
O6 Dy1 O2 C4 -118.0(5) . .
O5 Dy1 O2 C4 120.6(5) 2_655 .
O5 Dy1 O2 C4 -62.1(5) . .
Dy1 Dy1 O2 C4 -63.3(6) 2_655 .
C8 C7 O3 Dy1 0.3(8) . .
C6 C7 O3 Dy1 -177.7(3) . .
O1 Dy1 O3 C7 157.8(4) . .
O4 Dy1 O3 C7 -1.0(4) . .
O6 Dy1 O3 C7 28.4(6) . .
O2 Dy1 O3 C7 83.3(4) . .
O5 Dy1 O3 C7 -88.0(4) 2_655 .
O5 Dy1 O3 C7 -133.5(4) . .
Dy1 Dy1 O3 C7 -107.1(4) 2_655 .
C8 C9 O4 Dy1 0.2(8) . .
C10 C9 O4 Dy1 -177.1(3) . .
O1 Dy1 O4 C9 -46.0(5) . .
O3 Dy1 O4 C9 0.7(4) . .
O6 Dy1 O4 C9 -165.9(4) . .
O2 Dy1 O4 C9 -88.0(4) . .
O5 Dy1 O4 C9 82.4(4) 2_655 .
O5 Dy1 O4 C9 137.1(4) . .
Dy1 Dy1 O4 C9 106.1(4) 2_655 .
C12 C11 O5 Dy1 -78.3(5) . 2_655
C16 C11 O5 Dy1 99.6(4) . 2_655
C12 C11 O5 Dy1 92.9(4) . .
C16 C11 O5 Dy1 -89.2(5) . .
O1 Dy1 O5 C11 -52.7(3) . .
O4 Dy1 O5 C11 125.8(3) . .
O3 Dy1 O5 C11 -122.5(3) . .
O6 Dy1 O5 C11 66.2(3) . .
O2 Dy1 O5 C11 8.5(4) . .
O5 Dy1 O5 C11 -172.3(4) 2_655 .
Dy1 Dy1 O5 C11 -172.3(4) 2_655 .
O1 Dy1 O5 Dy1 119.59(14) . 2_655
O4 Dy1 O5 Dy1 -61.96(18) . 2_655
O3 Dy1 O5 Dy1 49.8(2) . 2_655
O6 Dy1 O5 Dy1 -121.57(15) . 2_655
O2 Dy1 O5 Dy1 -179.26(11) . 2_655
O5 Dy1 O5 Dy1 0.0 2_655 2_655
C17 N1 O6 Dy1 -66.0(6) . .
C21 N1 O6 Dy1 107.9(4) . .
O1 Dy1 O6 N1 94.1(4) . .
O4 Dy1 O6 N1 -113.7(4) . .
O3 Dy1 O6 N1 -142.7(4) . .
O2 Dy1 O6 N1 160.2(4) . .
O5 Dy1 O6 N1 -33.1(4) 2_655 .
O5 Dy1 O6 N1 23.7(4) . .
Dy1 Dy1 O6 N1 -4.4(4) 2_655 .
