#------------------------------------------------------------------------------
#$Date: 2025-04-05 06:45:22 +0300 (Sat, 05 Apr 2025) $
#$Revision: 299018 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/06/36/7063617.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7063617
loop_
_publ_author_name
'Sen, Charanjeet'
'Singh, Rohit'
'Devi, Swaita'
Niharika,
'Singhaal, Richa'
'Sahoo, Subash Chandra'
'Sheikh, Haq Nawaz'
_publ_section_title
;
 Design and synthesis of 2D coordination polymers from isophthalic and
 adipic acids: exploring Tb-based luminescent sensors for Cr3+, Fe3+ and
 p-NA
;
_journal_issue                   6
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              2350
_journal_page_last               2364
_journal_paper_doi               10.1039/D4NJ05061D
_journal_volume                  49
_journal_year                    2025
_chemical_compound_source        synthesized
_chemical_formula_moiety         'C11 H12 Dy O8'
_chemical_formula_sum            'C11 H12 Dy O8'
_chemical_formula_weight         434.710
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_audit_creation_date             2024-07-04
_audit_creation_method
;
Olex2 1.5
(compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748)
;
_audit_update_record
;
2024-11-22 deposited with the CCDC.	2025-01-08 downloaded from the CCDC.
;
_cell_angle_alpha                93.118(2)
_cell_angle_beta                 108.138(2)
_cell_angle_gamma                108.871(3)
_cell_formula_units_Z            2
_cell_length_a                   6.8112(2)
_cell_length_b                   10.0395(3)
_cell_length_c                   10.5052(3)
_cell_measurement_reflns_used    6821
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.2670
_cell_measurement_theta_min      3.3610
_cell_volume                     636.29(4)
_computing_cell_refinement       'CrysAlisPro 1.171.39.31d (Rigaku OD, 2017)'
_computing_data_collection       'CrysAlisPro 1.171.39.31d (Rigaku OD, 2017)'
_computing_data_reduction        'CrysAlisPro 1.171.39.31d (Rigaku OD, 2017)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'olex2.refine 1.5 (Bourhis et al., 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_type            HyPix3000
_diffrn_measured_fraction_theta_full 0.9978
_diffrn_measured_fraction_theta_max 0.9310
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -49.00 -12.00   0.50    2.00    --   -9.95 113.00   4.00   74
  2  ω     -3.00  46.00   0.50    2.00    --   10.22-113.00 -87.00   98
  3  ω    -21.00  53.00   0.50    2.00    --   -9.95  38.00 -60.00  148
  4  ω    -22.00  48.00   0.50    2.00    --   -9.95  38.00  30.00  140
  5  ω    -58.00 -26.00   0.50    2.00    --   -9.95 125.00  30.00   64
  6  ω    -52.00 -26.00   0.50    2.00    --   -9.95 125.00 -30.00   52
  7  ω    -37.00  -4.00   0.50    2.00    --   10.22 126.00-166.85   66
  8  ω     11.00  53.00   0.50    2.00    --   10.22-125.00-180.00   84
  9  ω    -11.00  29.00   0.50    2.00    --   10.22 -99.00-150.00   80
 10  ω      7.00  59.00   0.50    2.00    --   10.22-125.00   0.00  104
 11  ω    -41.00  -8.00   0.50    2.00    --   10.22 131.00 -53.26   66
 12  ω     29.00  74.00   0.50    2.00    --   10.22  38.00 120.00   90
 13  ω    -57.00  -9.00   0.50    2.00    --   10.22 -19.00  30.00   96
 14  ω    -57.00  18.00   0.50    2.00    --   10.22 -19.00 120.00  150
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type
'SuperNova, Single source at offset/far, HyPix3000'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0718
_diffrn_reflns_av_unetI/netI     0.0628
_diffrn_reflns_Laue_measured_fraction_full 0.9978
_diffrn_reflns_Laue_measured_fraction_max 0.9310
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            7762
_diffrn_reflns_point_group_measured_fraction_full 0.9978
_diffrn_reflns_point_group_measured_fraction_max 0.9310
_diffrn_reflns_theta_full        25.2417
_diffrn_reflns_theta_max         27.41
_diffrn_reflns_theta_min         3.25
_exptl_absorpt_coefficient_mu    5.907
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.35570
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.31d (Rigaku Oxford Diffraction, 2017)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.269
_exptl_crystal_description       block
_exptl_crystal_F_000             416.372
_exptl_crystal_size_max          0.02
_exptl_crystal_size_mid          0.015
_exptl_crystal_size_min          0.008
_refine_diff_density_max         3.4602
_refine_diff_density_min         -4.3380
_refine_diff_density_rms         0.3142
_refine_ls_d_res_high            0.7719
_refine_ls_d_res_low             6.2610
_refine_ls_goodness_of_fit_ref   1.0301
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    21
_refine_ls_number_parameters     186
_refine_ls_number_reflns         2700
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.0301
_refine_ls_R_factor_all          0.0505
_refine_ls_R_factor_gt           0.0493
_refine_ls_shift/su_max          0.0009
_refine_ls_shift/su_mean         0.0001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1026P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1339
_refine_ls_wR_factor_ref         0.1355
_reflns_Friedel_coverage         0.0
_reflns_limit_h_max              8
_reflns_limit_h_min              -8
_reflns_limit_k_max              12
_reflns_limit_k_min              -12
_reflns_limit_l_max              13
_reflns_limit_l_min              0
_reflns_number_gt                2584
_reflns_number_total             2700
_reflns_threshold_expression     I>=2u(I)
_cod_data_source_file            d4nj05061d2.cif
_cod_data_source_block           gjp-i9
_cod_depositor_comments
'Adding full bibliography for 7063611--7063619.cif.'
_cod_database_code               7063617
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All O(H,H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(O4) = Uanis(O9)
3. Others
 Fixed Sof: O4(0.7) O9(0.3)
4.a Rotating group:
 O8(H8a,H8b), O7(H7a,H7b)
4.b Secondary CH2 refined with riding coordinates:
 C10(H10a,H10b), C11(H11a,H11b)
4.c Aromatic/amide H refined with riding coordinates:
 C3(H3), C7(H7), C5(H5), C6(H6)
;
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_occupancy
_atom_site_disorder_group
Dy1 Dy 0.75763(4) 0.08473(3) 0.92101(3) 0.01613(16) Uani 1.000000 . . .
O5 O 0.3687(8) 0.0266(5) 0.8837(5) 0.0212(10) Uani 1.000000 . . .
O6 O 0.0368(8) 0.0003(5) 0.8775(5) 0.0230(11) Uani 1.000000 . . .
O2 O 0.4102(8) 0.1769(5) 0.1529(5) 0.0220(10) Uani 1.000000 . . .
O1 O 0.4139(9) 0.0432(5) 0.3098(5) 0.0257(11) Uani 1.000000 . . .
O3 O 0.7345(11) 0.2484(6) 0.7865(6) 0.0385(15) Uani 1.000000 . . .
C9 C 0.1855(10) 0.0380(7) 0.8250(6) 0.0151(13) Uani 1.000000 . . .
O8 O 1.1101(9) 0.2730(6) 0.9969(8) 0.0510(19) Uani 1.000000 . . .
H8a H 1.195(6) 0.274(6) 1.086(3) 0.076(3) Uiso 1.000000 GR . .
H8b H 1.1039(9) 0.3649(8) 0.997(8) 0.076(3) Uiso 1.000000 GR . .
O7 O 0.7579(11) 0.2616(7) 1.0746(8) 0.057(2) Uani 1.000000 . . .
H7a H 0.659(11) 0.2284(14) 1.128(6) 0.085(3) Uiso 1.000000 GR . .
H7b H 0.708(14) 0.337(5) 1.0328(13) 0.085(3) Uiso 1.000000 GR . .
C1 C 0.4620(12) 0.1629(8) 0.2790(8) 0.0207(15) Uani 1.000000 . . .
C2 C 0.5805(11) 0.2932(8) 0.3851(7) 0.0204(14) Uani 1.000000 . . .
C3 C 0.6400(15) 0.2762(9) 0.5199(9) 0.0228(17) Uani 1.000000 . . .
H3 H 0.6023(15) 0.1851(9) 0.5421(9) 0.027(2) Uiso 1.000000 R . .
C10 C 0.1408(14) 0.0911(9) 0.6900(8) 0.0243(16) Uani 1.000000 . . .
H10a H 0.0499(14) 0.1488(9) 0.6870(8) 0.029(2) Uiso 1.000000 R . .
H10b H 0.2803(14) 0.1520(9) 0.6847(8) 0.029(2) Uiso 1.000000 R . .
C11 C 0.0250(15) -0.0286(9) 0.5670(8) 0.0290(18) Uani 1.000000 . . .
H11a H -0.1123(15) -0.0915(9) 0.5734(8) 0.035(2) Uiso 1.000000 R . .
H11b H 0.1182(15) -0.0842(9) 0.5675(8) 0.035(2) Uiso 1.000000 R . .
C4 C 0.7566(13) 0.3957(8) 0.6222(8) 0.0251(16) Uani 1.000000 . . .
C7 C 0.6387(14) 0.4300(9) 0.3534(9) 0.0280(17) Uani 1.000000 . . .
H7 H 0.6004(14) 0.4418(9) 0.2628(9) 0.034(2) Uiso 1.000000 R . .
O4 O 0.9975(19) 0.4641(10) 0.8543(10) 0.053(3) Uani 0.700000 . P 1
C8 C 0.8239(19) 0.3714(10) 0.7659(9) 0.042(2) Uani 1.000000 . . .
C5 C 0.8110(14) 0.5329(9) 0.5863(9) 0.0310(18) Uani 1.000000 . . .
H5 H 0.8878(14) 0.6132(9) 0.6541(9) 0.037(2) Uiso 1.000000 R . .
C6 C 0.7532(14) 0.5487(9) 0.4554(9) 0.0328(19) Uani 1.000000 . . .
H6 H 0.7901(14) 0.6397(9) 0.4331(9) 0.039(2) Uiso 1.000000 R . .
O9 O 0.862(5) 0.474(3) 0.857(3) 0.053(3) Uani 0.300000 . P 2
loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
_atom_type_scat_dispersion_source
C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870
51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
Dy -0.09334 4.42895 26.50700 17.63830 14.55960 2.96577 2.18020 0.20217 12.18990
111.87400 4.29728 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236
57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390
32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)'
'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O6 Dy1 O5 145.44(16) 1_655 . ?
O6 Dy1 O5 114.79(16) 2_657 . ?
O6 Dy1 O5 112.12(15) 1_655 2_657 ?
O6 Dy1 O5 49.85(14) 2_657 2_657 ?
O2 Dy1 O5 75.06(16) 2_656 . ?
O2 Dy1 O5 72.51(16) 2_656 2_657 ?
O2 Dy1 O6 78.53(16) 2_656 2_657 ?
O2 Dy1 O6 71.76(16) 2_656 1_655 ?
O1 Dy1 O5 77.86(17) 2_656 . ?
O1 Dy1 O5 120.47(17) 2_656 2_657 ?
O1 Dy1 O6 125.91(17) 2_656 2_657 ?
O1 Dy1 O6 74.70(17) 2_656 1_655 ?
O1 Dy1 O2 53.06(17) 2_656 2_656 ?
O3 Dy1 O5 143.8(2) . 2_657 ?
O3 Dy1 O5 87.9(2) . . ?
O3 Dy1 O6 103.7(2) . 1_655 ?
O3 Dy1 O6 151.63(19) . 2_657 ?
O3 Dy1 O2 125.9(2) . 2_656 ?
O3 Dy1 O1 73.4(2) . 2_656 ?
C9 Dy1 O5 90.23(17) 2_657 . ?
C9 Dy1 O5 24.95(16) 2_657 2_657 ?
C9 Dy1 O6 90.05(17) 2_657 1_655 ?
C9 Dy1 O6 24.90(16) 2_657 2_657 ?
C9 Dy1 O2 74.41(17) 2_657 2_656 ?
C9 Dy1 O1 127.47(18) 2_657 2_656 ?
C9 Dy1 O3 158.0(2) 2_657 . ?
O8 Dy1 O5 144.4(2) . . ?
O8 Dy1 O5 114.8(2) . 2_657 ?
O8 Dy1 O6 69.6(2) . 1_655 ?
O8 Dy1 O6 79.1(2) . 2_657 ?
O8 Dy1 O2 140.38(19) . 2_656 ?
O8 Dy1 O1 122.0(2) . 2_656 ?
O8 Dy1 O3 72.6(2) . . ?
O8 Dy1 C9 97.0(2) . 2_657 ?
O7 Dy1 O5 69.5(2) . 2_657 ?
O7 Dy1 O5 77.0(2) . . ?
O7 Dy1 O6 136.4(2) . 1_655 ?
O7 Dy1 O6 87.4(2) . 2_657 ?
O7 Dy1 O2 139.55(19) . 2_656 ?
O7 Dy1 O1 144.6(3) . 2_656 ?
O7 Dy1 O3 81.2(3) . . ?
O7 Dy1 C9 77.1(2) . 2_657 ?
O7 Dy1 O8 70.9(2) . . ?
C1 Dy1 O5 74.74(19) 2_656 . ?
C1 Dy1 O5 97.25(19) 2_656 2_657 ?
C1 Dy1 O6 71.38(19) 2_656 1_655 ?
C1 Dy1 O6 103.2(2) 2_656 2_657 ?
C1 Dy1 O2 27.3(2) 2_656 2_656 ?
C1 Dy1 O1 25.8(2) 2_656 2_656 ?
C1 Dy1 O3 98.9(2) 2_656 . ?
C1 Dy1 C9 101.7(2) 2_656 2_657 ?
C1 Dy1 O8 136.4(2) 2_656 . ?
C1 Dy1 O7 151.7(2) 2_656 . ?
C9 O5 Dy1 151.6(4) . . ?
C9 O5 Dy1 92.7(4) . 2_657 ?
C9 O6 Dy1 98.3(4) . 2_657 ?
C9 O6 Dy1 139.2(4) . 1_455 ?
C1 O2 Dy1 91.4(4) . 2_656 ?
C1 O1 Dy1 95.5(5) . 2_656 ?
C8 O3 Dy1 147.0(6) . . ?
O5 C9 Dy1 62.3(3) . 2_657 ?
O6 C9 Dy1 56.8(3) . 2_657 ?
O6 C9 O5 119.1(6) . . ?
C10 C9 Dy1 175.7(5) . 2_657 ?
C10 C9 O5 120.3(6) . . ?
C10 C9 O6 120.6(6) . . ?
H8a O8 Dy1 112.5 . . ?
H8b O8 Dy1 114.4 . . ?
H8b O8 H8a 104.8 . . ?
H7a O7 Dy1 115.9 . . ?
H7b O7 Dy1 114.9 . . ?
H7b O7 H7a 102.2 . . ?
O2 C1 Dy1 61.3(4) . 2_656 ?
O1 C1 Dy1 58.7(4) . 2_656 ?
O1 C1 O2 120.0(7) . . ?
C2 C1 Dy1 179.3(5) . 2_656 ?
C2 C1 O2 118.9(7) . . ?
C2 C1 O1 121.0(7) . . ?
C3 C2 C1 118.2(7) . . ?
C7 C2 C1 122.3(7) . . ?
C7 C2 C3 119.5(7) . . ?
H3 C3 C2 120.1(5) . . ?
C4 C3 C2 119.8(7) . . ?
C4 C3 H3 120.1(5) . . ?
H10a C10 C9 108.9(4) . . ?
H10b C10 C9 108.9(4) . . ?
H10b C10 H10a 107.7 . . ?
C11 C10 C9 113.5(6) . . ?
C11 C10 H10a 108.9(5) . . ?
C11 C10 H10b 108.9(5) . . ?
C11 C11 C10 112.1(9) 2_556 . ?
H11a C11 C10 109.2(5) . . ?
H11b C11 C10 109.2(5) . . ?
H11b C11 H11a 107.9 . . ?
C8 C4 C3 117.8(7) . . ?
C5 C4 C3 119.2(8) . . ?
C5 C4 C8 123.1(7) . . ?
H7 C7 C2 119.7(5) . . ?
C6 C7 C2 120.6(8) . . ?
C6 C7 H7 119.7(5) . . ?
C4 C8 O3 116.8(8) . . ?
O4 C8 O3 122.7(9) . . ?
O4 C8 C4 118.8(9) . . ?
O9 C8 O3 116.2(14) . . ?
O9 C8 C4 116.7(14) . . ?
O9 C8 O4 44.5(13) . . ?
H5 C5 C4 119.6(5) . . ?
C6 C5 C4 120.7(8) . . ?
C6 C5 H5 119.6(5) . . ?
C5 C6 C7 120.2(8) . . ?
H6 C6 C7 119.9(5) . . ?
H6 C6 C5 119.9(5) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O5 2.631(5) 2_657 ?
Dy1 O5 2.417(5) . ?
Dy1 O6 2.509(5) 2_657 ?
Dy1 O6 2.466(5) 1_655 ?
Dy1 O2 2.468(5) 2_656 ?
Dy1 O1 2.413(5) 2_656 ?
Dy1 O3 2.237(6) . ?
Dy1 C9 2.968(6) 2_657 ?
Dy1 O8 2.384(5) . ?
Dy1 O7 2.332(6) . ?
Dy1 C1 2.811(8) 2_656 ?
O5 C9 1.253(8) . ?
O6 C9 1.263(8) . ?
O2 C1 1.289(9) . ?
O1 C1 1.229(9) . ?
O3 C8 1.251(11) . ?
C9 C10 1.519(10) . ?
O8 H8a 0.9310 . ?
O8 H8b 0.9371 . ?
O7 H7a 0.9962 . ?
O7 H7b 0.9929 . ?
C1 C2 1.484(11) . ?
C2 C3 1.383(11) . ?
C2 C7 1.391(11) . ?
C3 H3 0.9300 . ?
C3 C4 1.392(11) . ?
C10 H10a 0.9700 . ?
C10 H10b 0.9700 . ?
C10 C11 1.523(12) . ?
C11 C11 1.531(16) 2_556 ?
C11 H11a 0.9700 . ?
C11 H11b 0.9700 . ?
C4 C8 1.493(12) . ?
C4 C5 1.411(11) . ?
C7 H7 0.9300 . ?
C7 C6 1.384(12) . ?
O4 C8 1.280(13) . ?
C8 O9 1.27(3) . ?
C5 H5 0.9300 . ?
C5 C6 1.341(12) . ?
C6 H6 0.9300 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O5 C9 Dy1 -164.0(11) . . . 2_657 ?
Dy1 O5 C9 O6 -162.4(9) . . . . ?
Dy1 O5 C9 O6 1.6(4) 2_657 . . . ?
Dy1 O5 C9 C10 19.9(10) . . . . ?
Dy1 O5 C9 C10 -176.1(4) 2_657 . . . ?
Dy1 O6 C9 Dy1 139.1(8) 1_455 . . 2_657 ?
Dy1 O6 C9 O5 137.4(6) 1_455 . . . ?
Dy1 O6 C9 O5 -1.7(4) 2_657 . . . ?
Dy1 O6 C9 C10 176.0(4) 2_657 . . . ?
Dy1 O6 C9 C10 -44.9(7) 1_455 . . . ?
Dy1 O2 C1 O1 -0.6(4) 2_656 . . . ?
Dy1 O2 C1 C2 179.2(3) 2_656 . . . ?
Dy1 O1 C1 O2 0.6(4) 2_656 . . . ?
Dy1 O1 C1 C2 -179.2(3) 2_656 . . . ?
Dy1 O3 C8 C4 155.6(13) . . . . ?
Dy1 O3 C8 O4 -9.3(14) . . . . ?
Dy1 O3 C8 O9 -60.4(19) . . . . ?
Dy1 C9 O5 Dy1 -164.0(6) 2_657 . . . ?
Dy1 C9 O6 Dy1 139.1(4) 2_657 . . 1_455 ?
O5 C9 C10 C11 94.5(7) . . . . ?
O6 C9 C10 C11 -83.2(7) . . . . ?
O2 C1 C2 C3 -178.3(7) . . . . ?
O2 C1 C2 C7 -0.3(9) . . . . ?
O1 C1 C2 C3 1.5(9) . . . . ?
O1 C1 C2 C7 179.5(8) . . . . ?
O3 C8 C4 C3 -13.8(12) . . . . ?
O3 C8 C4 C5 168.0(9) . . . . ?
C9 C10 C11 C11 177.9(9) . . . 2_556 ?
C1 C2 C3 C4 178.3(7) . . . . ?
C1 C2 C7 C6 -178.7(8) . . . . ?
C2 C3 C4 C8 -177.9(9) . . . . ?
C2 C3 C4 C5 0.4(11) . . . . ?
C2 C7 C6 C5 0.6(10) . . . . ?
C3 C4 C8 O4 151.7(10) . . . . ?
C3 C4 C8 O9 -157.7(17) . . . . ?
C3 C4 C5 C6 -0.5(9) . . . . ?
C10 C11 C11 C10 180.0(10) . . 2_556 2_556 ?
C4 C5 C6 C7 0.0(10) . . . . ?
