#------------------------------------------------------------------------------
#$Date: 2016-03-26 02:37:28 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180148 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/45/7104528.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7104528
loop_
_publ_author_name
'Li, Jingqiu'
'Koh, Lip Lin'
'Hor, T S Andy'
_publ_section_title
;
 One-pot oxidation and protonation of a bridging sulfide and rare
 crystallographic evidence of a coordinated [SO] complex in
 [Pt2(micro-S2O2H)(PPh3)4]+.
;
_journal_issue                   23
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              3416
_journal_page_last               3418
_journal_paper_doi               10.1039/b902625h
_journal_volume                  34
_journal_year                    2009
_chemical_formula_moiety         'C73 H61 O2 P4 Pt2 S2. C1 F3 S1 O3'
_chemical_formula_sum            'C73 H61 F3 O5 P4 Pt2 S3'
_chemical_formula_weight         1685.46
_chemical_name_systematic
;
?
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 107.4620(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   18.2167(8)
_cell_length_b                   10.3392(4)
_cell_length_c                   18.3226(8)
_cell_measurement_reflns_used    5398
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      2.33
_cell_volume                     3292.0(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0229
_diffrn_reflns_av_sigmaI/netI    0.0272
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            22812
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         1.88
_exptl_absorpt_coefficient_mu    4.498
_exptl_absorpt_correction_T_max  0.4982
_exptl_absorpt_correction_T_min  0.1449
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            GOLD
_exptl_crystal_density_diffrn    1.700
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    .
_exptl_crystal_description       rHOMBUS
_exptl_crystal_F_000             1660
_exptl_crystal_size_max          0.70
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.18
_refine_diff_density_max         1.448
_refine_diff_density_min         -0.664
_refine_diff_density_rms         0.098
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.046
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     426
_refine_ls_number_reflns         7555
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.046
_refine_ls_R_factor_all          0.0285
_refine_ls_R_factor_gt           0.0248
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0347P)²+1.9460P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0619
_refine_ls_wR_factor_ref         0.0637
_reflns_number_gt                6847
_reflns_number_total             7555
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b902625h.txt
_cod_data_source_block           7424
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P2/n
_cod_database_code               7104528
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.325512(6) 0.162047(10) 0.719630(5) 0.02380(4) Uani 1 1 d . . .
S1 S 0.19777(4) 0.08347(8) 0.66909(4) 0.03288(16) Uani 1 1 d . . .
O1 O 0.20699(19) -0.0744(3) 0.6862(2) 0.0736(9) Uani 1 1 d . . .
H1O H 0.2500 -0.153(4) 0.7500 0.028(12) Uiso 1 2 d S . .
P1 P 0.32502(4) 0.22163(7) 0.59769(4) 0.02617(15) Uani 1 1 d . . .
P2 P 0.44953(4) 0.22505(7) 0.78117(4) 0.02641(15) Uani 1 1 d . . .
C1U C 0.46141(18) 0.4001(3) 0.78060(16) 0.0316(6) Uani 1 1 d . . .
C2U C 0.5333(2) 0.4581(3) 0.8118(2) 0.0441(8) Uani 1 1 d . . .
H2U H 0.5774 0.4071 0.8323 0.053 Uiso 1 1 calc R . .
C3U C 0.5388(3) 0.5923(4) 0.8122(3) 0.0600(11) Uani 1 1 d . . .
H3U H 0.5873 0.6321 0.8307 0.072 Uiso 1 1 calc R . .
C4U C 0.4737(3) 0.6670(3) 0.7858(3) 0.0616(13) Uani 1 1 d . . .
H4U H 0.4779 0.7576 0.7881 0.074 Uiso 1 1 calc R . .
C5U C 0.4028(3) 0.6110(4) 0.7561(2) 0.0548(10) Uani 1 1 d . . .
H5U H 0.3588 0.6630 0.7375 0.066 Uiso 1 1 calc R . .
C6U C 0.3962(2) 0.4761(3) 0.75375(18) 0.0383(7) Uani 1 1 d . . .
H6U H 0.3476 0.4371 0.7340 0.046 Uiso 1 1 calc R . .
C1V C 0.48926(17) 0.1919(3) 0.88352(16) 0.0303(6) Uani 1 1 d . . .
C2V C 0.54616(18) 0.1011(3) 0.91243(17) 0.0356(7) Uani 1 1 d . . .
H2V H 0.5634 0.0489 0.8789 0.043 Uiso 1 1 calc R . .
C3V C 0.5781(2) 0.0867(4) 0.99129(19) 0.0438(8) Uani 1 1 d . . .
H3V H 0.6175 0.0259 1.0107 0.053 Uiso 1 1 calc R . .
C4V C 0.5523(2) 0.1611(3) 1.0407(2) 0.0454(9) Uani 1 1 d . . .
H4V H 0.5737 0.1510 1.0939 0.054 Uiso 1 1 calc R . .
C5V C 0.4953(2) 0.2501(4) 1.01204(19) 0.0493(9) Uani 1 1 d . . .
H5V H 0.4774 0.3008 1.0457 0.059 Uiso 1 1 calc R . .
C6V C 0.4639(2) 0.2659(4) 0.93389(18) 0.0432(8) Uani 1 1 d . . .
H6V H 0.4250 0.3277 0.9149 0.052 Uiso 1 1 calc R . .
C1W C 0.51635(17) 0.1415(3) 0.74014(17) 0.0299(6) Uani 1 1 d . . .
C2W C 0.4996(2) 0.0118(3) 0.72152(19) 0.0383(7) Uani 1 1 d . . .
H2W H 0.4549 -0.0251 0.7282 0.046 Uiso 1 1 calc R . .
C3W C 0.5478(2) -0.0632(4) 0.6933(2) 0.0473(8) Uani 1 1 d . . .
H3W H 0.5360 -0.1504 0.6806 0.057 Uiso 1 1 calc R . .
C4W C 0.6138(2) -0.0080(4) 0.6842(2) 0.0525(10) Uani 1 1 d . . .
H4W H 0.6472 -0.0583 0.6655 0.063 Uiso 1 1 calc R . .
C5W C 0.6304(2) 0.1191(4) 0.7020(2) 0.0449(8) Uani 1 1 d . . .
H5W H 0.6751 0.1556 0.6949 0.054 Uiso 1 1 calc R . .
C6W C 0.58261(19) 0.1952(3) 0.73047(19) 0.0374(7) Uani 1 1 d . . .
H6W H 0.5949 0.2823 0.7431 0.045 Uiso 1 1 calc R . .
C1X C 0.28716(17) 0.0886(3) 0.53142(17) 0.0310(6) Uani 1 1 d . . .
C2X C 0.2470(2) 0.1078(4) 0.45511(18) 0.0420(8) Uani 1 1 d . . .
H2X H 0.2326 0.1919 0.4369 0.050 Uiso 1 1 calc R . .
C3X C 0.2278(2) 0.0033(4) 0.4054(2) 0.0490(9) Uani 1 1 d . . .
H3X H 0.2010 0.0169 0.3535 0.059 Uiso 1 1 calc R . .
C4X C 0.2475(2) -0.1182(4) 0.4316(2) 0.0494(9) Uani 1 1 d . . .
H4X H 0.2345 -0.1885 0.3976 0.059 Uiso 1 1 calc R . .
C5X C 0.2864(2) -0.1400(3) 0.5073(2) 0.0451(8) Uani 1 1 d . . .
H5X H 0.2995 -0.2248 0.5249 0.054 Uiso 1 1 calc R . .
C6X C 0.30627(19) -0.0367(3) 0.55804(19) 0.0380(7) Uani 1 1 d . . .
H6X H 0.3324 -0.0515 0.6100 0.046 Uiso 1 1 calc R . .
C1Y C 0.26541(17) 0.3632(3) 0.56247(17) 0.0285(6) Uani 1 1 d . . .
C2Y C 0.26674(18) 0.4234(3) 0.49475(17) 0.0347(7) Uani 1 1 d . . .
H2Y H 0.2989 0.3910 0.4674 0.042 Uiso 1 1 calc R . .
C3Y C 0.2214(2) 0.5297(3) 0.46762(19) 0.0414(8) Uani 1 1 d . . .
H3Y H 0.2218 0.5688 0.4214 0.050 Uiso 1 1 calc R . .
C4Y C 0.1750(2) 0.5791(3) 0.5085(2) 0.0432(8) Uani 1 1 d . . .
H4Y H 0.1438 0.6515 0.4899 0.052 Uiso 1 1 calc R . .
C5Y C 0.17435(19) 0.5231(3) 0.5761(2) 0.0399(7) Uani 1 1 d . . .
H5Y H 0.1436 0.5583 0.6042 0.048 Uiso 1 1 calc R . .
C6Y C 0.21903(17) 0.4141(3) 0.60323(17) 0.0332(6) Uani 1 1 d . . .
H6Y H 0.2178 0.3750 0.6492 0.040 Uiso 1 1 calc R . .
C1Z C 0.41348(17) 0.2620(3) 0.57563(16) 0.0297(6) Uani 1 1 d . . .
C2Z C 0.4502(2) 0.1743(3) 0.5404(2) 0.0375(7) Uani 1 1 d . . .
H2Z H 0.4287 0.0919 0.5265 0.045 Uiso 1 1 calc R . .
C3Z C 0.5176(2) 0.2076(4) 0.5260(2) 0.0490(9) Uani 1 1 d . . .
H3Z H 0.5415 0.1480 0.5016 0.059 Uiso 1 1 calc R . .
C4Z C 0.5506(2) 0.3269(4) 0.5468(2) 0.0483(9) Uani 1 1 d . . .
H4Z H 0.5972 0.3480 0.5376 0.058 Uiso 1 1 calc R . .
C5Z C 0.5151(2) 0.4156(3) 0.5812(2) 0.0429(8) Uani 1 1 d . . .
H5Z H 0.5375 0.4974 0.5952 0.051 Uiso 1 1 calc R . .
C6Z C 0.44654(18) 0.3845(3) 0.59511(17) 0.0347(7) Uani 1 1 d . . .
H6Z H 0.4221 0.4459 0.6177 0.042 Uiso 1 1 calc R . .
O2S O 0.3235(4) 0.4732(13) 0.3352(5) 0.117(3) Uani 0.50 1 d P . .
S2 S 0.26197(19) 0.5111(2) 0.26715(11) 0.0575(7) Uani 0.50 1 d P . .
O1S O 0.2066(3) 0.5670(4) 0.2881(2) 0.1030(14) Uani 1 1 d . . .
F1 F 0.2158(3) 0.2848(3) 0.2873(2) 0.1154(12) Uani 1 1 d . . .
C1S C 0.2271(6) 0.3533(9) 0.2302(5) 0.064(2) Uani 0.50 1 d P . .
F2 F 0.1659(5) 0.3585(8) 0.1704(5) 0.113(3) Uani 0.50 1 d P . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Pt1 P1 96.70(3) . . ?
P2 Pt1 S1 94.54(3) . 2_556 ?
P1 Pt1 S1 168.66(3) . 2_556 ?
P2 Pt1 S1 173.36(3) . . ?
P1 Pt1 S1 89.72(3) . . ?
S1 Pt1 S1 79.00(3) 2_556 . ?
O1 S1 Pt1 102.17(12) . 2_556 ?
O1 S1 Pt1 103.34(12) . . ?
Pt1 S1 Pt1 87.37(2) 2_556 . ?
H1O O1 S1 134.9(13) . . ?
C1Y P1 C1Z 102.12(14) . . ?
C1Y P1 C1X 107.66(14) . . ?
C1Z P1 C1X 101.97(14) . . ?
C1Y P1 Pt1 112.65(10) . . ?
C1Z P1 Pt1 121.81(9) . . ?
C1X P1 Pt1 109.42(10) . . ?
C1U P2 C1W 111.85(14) . . ?
C1U P2 C1V 100.43(14) . . ?
C1W P2 C1V 103.03(14) . . ?
C1U P2 Pt1 112.33(10) . . ?
C1W P2 Pt1 110.02(10) . . ?
C1V P2 Pt1 118.60(10) . . ?
C6U C1U C2U 120.0(3) . . ?
C6U C1U P2 118.3(2) . . ?
C2U C1U P2 121.5(3) . . ?
C3U C2U C1U 119.2(4) . . ?
C4U C3U C2U 120.3(4) . . ?
C5U C4U C3U 120.8(3) . . ?
C4U C5U C6U 119.7(4) . . ?
C1U C6U C5U 119.8(3) . . ?
C2V C1V C6V 118.9(3) . . ?
C2V C1V P2 122.8(2) . . ?
C6V C1V P2 118.2(2) . . ?
C1V C2V C3V 120.1(3) . . ?
C4V C3V C2V 120.3(3) . . ?
C5V C4V C3V 119.5(3) . . ?
C4V C5V C6V 120.5(3) . . ?
C1V C6V C5V 120.6(3) . . ?
C6W C1W C2W 119.3(3) . . ?
C6W C1W P2 125.1(3) . . ?
C2W C1W P2 115.5(2) . . ?
C3W C2W C1W 120.9(3) . . ?
C2W C3W C4W 119.0(4) . . ?
C5W C4W C3W 120.4(3) . . ?
C4W C5W C6W 121.1(3) . . ?
C5W C6W C1W 119.3(3) . . ?
C2X C1X C6X 119.2(3) . . ?
C2X C1X P1 122.9(2) . . ?
C6X C1X P1 117.6(2) . . ?
C1X C2X C3X 120.2(3) . . ?
C4X C3X C2X 120.1(3) . . ?
C3X C4X C5X 120.7(3) . . ?
C4X C5X C6X 120.1(4) . . ?
C5X C6X C1X 119.5(3) . . ?
C6Y C1Y C2Y 119.0(3) . . ?
C6Y C1Y P1 120.5(2) . . ?
C2Y C1Y P1 120.4(2) . . ?
C3Y C2Y C1Y 120.6(3) . . ?
C2Y C3Y C4Y 119.8(3) . . ?
C5Y C4Y C3Y 120.4(3) . . ?
C4Y C5Y C6Y 120.2(3) . . ?
C1Y C6Y C5Y 120.0(3) . . ?
C2Z C1Z C6Z 118.5(3) . . ?
C2Z C1Z P1 122.1(2) . . ?
C6Z C1Z P1 119.4(2) . . ?
C3Z C2Z C1Z 120.4(3) . . ?
C4Z C3Z C2Z 120.7(3) . . ?
C3Z C4Z C5Z 119.9(3) . . ?
C4Z C5Z C6Z 120.1(3) . . ?
C5Z C6Z C1Z 120.3(3) . . ?
F2 O2S S2 107.0(7) 2 . ?
F2 O2S C1S 47.4(5) 2 2 ?
S2 O2S C1S 60.0(4) . 2 ?
F2 O2S S2 101.7(6) 2 2 ?
S2 O2S S2 5.61(18) . 2 ?
C1S O2S S2 55.1(4) 2 2 ?
S2 S2 O1S 86.1(6) 2 . ?
S2 S2 O1S 67.0(6) 2 2 ?
O1S S2 O1S 122.3(4) . 2 ?
S2 S2 O2S 161.7(6) 2 . ?
O1S S2 O2S 109.2(4) . . ?
O1S S2 O2S 110.2(5) 2 . ?
S2 S2 C1S 94.0(3) 2 2 ?
O1S S2 C1S 121.7(5) . 2 ?
O1S S2 C1S 110.6(5) 2 2 ?
O2S S2 C1S 69.7(6) . 2 ?
S2 S2 C1S 65.1(3) 2 . ?
O1S S2 C1S 106.9(4) . . ?
O1S S2 C1S 105.7(4) 2 . ?
O2S S2 C1S 99.9(6) . . ?
C1S S2 C1S 30.7(6) 2 . ?
S2 S2 O2S 12.7(4) 2 2 ?
O1S S2 O2S 85.0(4) . 2 ?
O1S S2 O2S 77.8(3) 2 2 ?
O2S S2 O2S 153.4(8) . 2 ?
C1S S2 O2S 83.8(5) 2 2 ?
C1S S2 O2S 53.8(4) . 2 ?
S2 S2 F2 129.9(3) 2 2 ?
O1S S2 F2 124.5(3) . 2 ?
O1S S2 F2 111.3(4) 2 2 ?
O2S S2 F2 32.6(4) . 2 ?
C1S S2 F2 37.4(4) 2 2 ?
C1S S2 F2 68.1(4) . 2 ?
O2S S2 F2 120.9(5) 2 2 ?
S2 O1S S2 26.96(18) . 2 ?
C1S F1 C1S 40.1(7) . 2 ?
C1S C1S F2 174.6(16) 2 . ?
C1S C1S F1 72.6(10) 2 . ?
F2 C1S F1 112.8(8) . . ?
C1S C1S F1 67.3(10) 2 2 ?
F2 C1S F1 109.8(9) . 2 ?
F1 C1S F1 102.5(7) . 2 ?
C1S C1S S2 84.5(3) 2 2 ?
F2 C1S S2 92.9(6) . 2 ?
F1 C1S S2 123.5(7) . 2 ?
F1 C1S S2 115.1(7) 2 2 ?
C1S C1S O2S 133.7(6) 2 2 ?
F2 C1S O2S 42.9(5) . 2 ?
F1 C1S O2S 136.9(8) . 2 ?
F1 C1S O2S 118.5(7) 2 2 ?
S2 C1S O2S 50.3(5) 2 2 ?
C1S C1S S2 64.8(3) 2 . ?
F2 C1S S2 113.1(7) . . ?
F1 C1S S2 107.8(6) . . ?
F1 C1S S2 110.3(6) 2 . ?
S2 C1S S2 20.99(17) 2 . ?
O2S C1S S2 71.1(5) 2 . ?
O2S F2 C1S 89.6(7) 2 . ?
O2S F2 S2 40.4(4) 2 2 ?
C1S F2 S2 49.7(5) . 2 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 P2 2.2959(7) . ?
Pt1 P1 2.3150(7) . ?
Pt1 S1 2.3488(7) 2_556 ?
Pt1 S1 2.3748(7) . ?
S1 O1 1.661(3) . ?
S1 Pt1 2.3487(7) 2_556 ?
O1 H1O 1.45(2) . ?
P1 C1Y 1.822(3) . ?
P1 C1Z 1.824(3) . ?
P1 C1X 1.827(3) . ?
P2 C1U 1.823(3) . ?
P2 C1W 1.828(3) . ?
P2 C1V 1.829(3) . ?
C1U C6U 1.385(4) . ?
C1U C2U 1.397(5) . ?
C2U C3U 1.390(5) . ?
C3U C4U 1.376(7) . ?
C4U C5U 1.370(7) . ?
C5U C6U 1.400(5) . ?
C1V C2V 1.381(4) . ?
C1V C6V 1.381(5) . ?
C2V C3V 1.394(4) . ?
C3V C4V 1.375(5) . ?
C4V C5V 1.368(5) . ?
C5V C6V 1.383(4) . ?
C1W C6W 1.388(4) . ?
C1W C2W 1.394(4) . ?
C2W C3W 1.383(5) . ?
C3W C4W 1.385(6) . ?
C4W C5W 1.367(6) . ?
C5W C6W 1.386(5) . ?
C1X C2X 1.384(4) . ?
C1X C6X 1.392(4) . ?
C2X C3X 1.389(5) . ?
C3X C4X 1.355(6) . ?
C4X C5X 1.374(6) . ?
C5X C6X 1.390(5) . ?
C1Y C6Y 1.388(4) . ?
C1Y C2Y 1.395(4) . ?
C2Y C3Y 1.376(4) . ?
C3Y C4Y 1.384(5) . ?
C4Y C5Y 1.370(5) . ?
C5Y C6Y 1.391(4) . ?
C1Z C2Z 1.394(4) . ?
C1Z C6Z 1.402(5) . ?
C2Z C3Z 1.377(5) . ?
C3Z C4Z 1.375(5) . ?
C4Z C5Z 1.378(5) . ?
C5Z C6Z 1.386(4) . ?
O2S F2 1.210(11) 2 ?
O2S S2 1.458(9) . ?
O2S C1S 1.777(12) 2 ?
O2S S2 2.084(9) 2 ?
S2 S2 0.649(4) 2 ?
S2 O1S 1.317(5) . ?
S2 O1S 1.427(4) 2 ?
S2 C1S 1.642(9) 2 ?
S2 C1S 1.807(9) . ?
S2 O2S 2.084(9) 2 ?
S2 F2 2.150(7) 2 ?
O1S S2 1.427(4) 2 ?
F1 C1S 1.329(10) . ?
F1 C1S 1.375(11) 2 ?
C1S C1S 0.928(18) 2 ?
C1S F2 1.308(11) . ?
C1S F1 1.375(11) 2 ?
C1S S2 1.642(9) 2 ?
C1S O2S 1.777(12) 2 ?
F2 O2S 1.210(11) 2 ?
F2 S2 2.150(7) 2 ?
